790 results about "Heat setting" patented technology

The invention relates to the technical field of polyester fibers, in particular to a high-strength wear-resistant polyester fiber and a preparation method thereof. The invention aims to solve the problem that the mechanical strength and wear resistance of the existing polyester fiber are difficult to consider at the same time. The preparation method comprises the following steps: carrying out esterification and polycondensation on terephthalic acid, ethylene glycol, hydroxyl-terminated polydimethylsiloxane and isophthalic acid to obtain modified PET; the preparation method comprises the following steps: respectively carrying out oxidation treatment on graphene and a multi-walled carbon nanotube, and then adding polyether amine for grafting; carrying out melt blending with PET slices to obtain nano master batches; carrying out melt blending on the chopped glass fibers and the PET slices to prepare micron master batches; and mixing the modified PET, the nano master batch and the micron master batch, carrying out ultrasonic dispersion, adding an auxiliary agent, and carrying out melt spinning, three-section stretching and three-section heat setting treatment to obtain the high-strength wear-resistant polyester fiber. Through the synergistic effect of the components and the process, the prepared fiber has excellent mechanical properties and wear resistance, and has wide application prospects in the fields of clothing, home textiles, industry and the like.

The invention relates to the technical field of capacitor films. The invention discloses a preparation process of a multilayer polypropylene capacitance film, which comprises the following steps: S1, raw material preparation: preparing basic resin, a nano ceramic filler, a nucleating agent and an antioxidant into multilayer raw materials respectively; s2, fusing multiple layers of raw materials by an independent screw extruder, and compounding by a co-extrusion die head to form a film blank; and S3, carrying out air ring gradient cooling on the film blank. And S4, longitudinally and transversely stretching the film blank. And S5, performing heat setting in a segmented heating furnace, and performing corona treatment to improve surface energy. And S6, segmentally curing the moisture-proof coating by using an infrared oven. The multilayer heterostructure is adopted, the comprehensive performance of the capacitor film is improved through material matching, the dielectric constant, the breakdown strength and the moisture resistance are enhanced, and the problem of considering the dielectric property and the mechanical property is solved. The innovative process guarantees stable performance, is compatible with an existing production line, can realize large-scale production, meets the requirements of fields such as new energy and the like, and provides a feasible scheme for localization of high-performance capacitor films.

The invention relates to the technical field of microfiber material preparation, in particular to a preparation method of an insulating flame-retardant automotive interior microfiber material, which comprises the following steps: spinning sea-island fibers by taking PA6 as an island component and LDPE as a sea component and matching with master batches; performing opening, carding, lapping, pre-needling by a pre-needling machine and needling by a needling machine on the sea-island fibers to prepare non-woven fabric; carrying out heat setting on the non-woven fabric; preparing insulating flame-retardant polyurethane slurry, infiltrating the heat-set non-woven fabric to enable the non-woven fabric to be fully impregnated, and then feeding the non-woven fabric into an aqueous solution of dimethylformamide to be subjected to water bath curing, so as to prepare a semi-finished synthetic leather product; extracting sea components in the sea-island fibers from the synthetic leather semi-finished product by adopting a stripping process; and drying the reduced superfine fiber synthetic leather base cloth, immersing the base cloth into a softening agent aqueous solution, and then carrying out drying and leather rubbing treatment to obtain the insulating flame-retardant superfine fiber leather. The product provided by the invention is used for external protection of an intelligent auxiliary driving steering wheel sensing layer, and the resistance of the microfiber material reaches 1.2 megohm or above.

The invention relates to the field of fiber production, and particularly discloses a zinc oxide antibacterial ES fiber and a preparation method thereof. The zinc oxide antibacterial ES fiber comprises a core layer and a surface layer, and the surface layer comprises the following raw materials in parts by weight: 80-100 parts of polyethylene, 2-5 parts of a nano-zinc oxide composite material, 1-2 parts of a dispersing agent and 2-3 parts of a compatilizer; the nano-zinc oxide composite material is prepared from hydroxyapatite nanowires, a polyethylene glycol solution and coated nano-zinc oxide in a mass ratio of 1: (8-10): (1.5-2); the preparation method comprises the following steps: melting the material of the core layer to obtain a melt; mixing polyethylene, the nano-zinc oxide composite material, a dispersing agent and a compatilizer, and melting to obtain a polyethylene melt; and mixing the melt and the polyethylene melt, spinning, bundling, stretching, carrying out heat setting, curling and cutting off to obtain a finished product, the fiber has the advantages of being good in antibacterial property, high in mechanical strength, good in spinning stability and good in air permeability.

The invention provides a superfine denier profiled polyester staple fiber and a preparation method thereof.The preparation method includes the steps of raw material pretreatment, melt spinning, nascent filament treatment, heat setting and curling, oiling and cutting off and the like, polyester chips have high intrinsic viscosity and melting point, and under the action of six-zone temperature control, a high-hole-density spinneret plate and a high draft multiple, the polyester chips are subjected to melt spinning, so that the polyester chips are prepared into the superfine denier profiled polyester staple fiber. The superfine, special-shaped and hollow polyester staple fibers are prepared. The obtained polyester staple fiber has good breaking strength, rebound resilience and a low-defect structure, the bulkiness, flexibility and structural consistency of the fiber are remarkably improved, the environment and process limitation of a traditional sea-island fiber alkali stripping method is broken through, and the polyester staple fiber is suitable for the fields of high-end filling, plush imitation, non-woven materials and the like.

The invention discloses a high-strength wear-resistant yarn and a manufacturing method thereof, and belongs to the field of spinning, the manufacturing process sequentially comprises the steps of opening, carding, drawing, roving and spinning, the raw materials used for opening comprise 70 wt% of aramid fiber and 30 wt% of cotton; in the spinning procedure, single yarns are twisted firstly, then two single yarns are plied to obtain plied yarns, the twist degree of the single yarns is 900-950 twists / m, the two single yarns have the same twist direction, and the single yarns and the plied yarns have opposite twist directions; and carrying out heat setting treatment on the plied yarn to obtain the high-strength wear-resistant yarn. Aramid fibers and cotton fibers in a specific proportion are selected as spinning raw materials, single yarns with specific twist are made and then reversely twisted to form plied yarns, finally, internal stress of the yarns is eliminated through heat setting treatment, the twist is stabilized, creep deformation in use is reduced, and the prepared yarns can be used in the industrial field, daily supplies, outdoor equipment and other products needing high wear resistance and have wide application prospects. The fabric is comfortable and soft, and the durability is improved.

The invention relates to the technical field of shoemaking equipment, in particular to a cold and hot setting machine for shoe processing and a setting technology.The cold and hot setting machine for shoe processing comprises a machine body, a hot mold assembly, a shoe mold assembly and a cold mold assembly, the hot mold assembly is arranged on one side of the machine body and used for conducting heat setting on toe cap fabric, and the cold mold assembly is arranged on the other side of the machine body; the shoe mold assembly and the cold mold assembly are both arranged on the machine body, the cold mold assembly is opposite to the shoe mold assembly in the vertical direction, and the cold mold assembly is used for conducting cold setting on the shoe head fabric obtained after heat setting. The middle flexible pressing pads are arranged, materials at the thick positions of the turnup parts are promoted to be dispersed to all positions of one circle of the turnup parts through intermittent rotation of the two middle flexible pressing pads, so that the thickness consistency of all positions of one circle of the toe cap fabric is improved, and in the subsequent cooling and shaping process of the toe cap fabric, the thickness uniformity of the toe cap fabric is improved. The cooling speeds of all parts of the toe cap fabric in one circle are basically consistent, so that the cooling and shaping effects of the shoe mold assembly on the toe cap fabric are better.

The invention discloses a high transparency and high toughness polyamide fiber preparation method, which comprises: S10: carrying out melt blending on polyamide and an ethylene-alpha-olefin copolymer elastomer, and extruding under the high shear action to obtain a modified melt; s20, the modified melt is extruded through a spinneret plate to form nascent filaments, the nascent filaments are fed into a cooling area to be rapidly cooled, and nascent fibers are obtained; the retention time of the nascent filaments in the cooling area is 0.1-0.3 second, nitrogen is adopted as a cooling medium in the cooling area, and the temperature of the nitrogen is 10-14 DEG C; s30, carrying out hot stretching treatment on the nascent fiber to obtain a stretched fiber; and S40, carrying out heat setting treatment on the stretched fiber to obtain the polyamide fiber. The polyamide fiber prepared by the method has good toughness and relatively high transparency.

The invention discloses a continuous twisting preparation method and system for spiral fiber artificial muscle. The preparation method comprises the following steps: keeping first tension, continuously releasing original fibers at a first pay-off rate, performing twisting treatment, and collecting at a first take-up rate to obtain spiral twisted fibers; the second tension is kept, the spiral twisted fibers are continuously released at a second pay-off rate, the spiral twisted fibers are collected at a second take-up rate after being subjected to annealing treatment, the spiral fiber artificial muscle is obtained, and the second pay-off rate is smaller than the second take-up rate. According to the continuous twisting preparation method provided by the invention, real-time monitoring and automatic adjustment of tension in the fiber preparation process are realized, so that constant tension during continuous fiber preparation is ensured, and meanwhile, the annealing tension is directly associated with the spring index of the artificial muscle fiber through the continuous annealing heat setting device; an industrialization solution is provided for diversified application of the artificial muscle, continuous preparation is achieved, and the preparation efficiency is remarkably improved.

The invention relates to the technical field of aramid fibers, in particular to a high-strength modified meta-aramid fiber and a preparation method thereof. The meta-position aramid fiber overcomes the problem that the meta-position aramid fiber is poor in mechanical property and ultraviolet resistance. The preparation method comprises the following steps: taking MPD and DDS as diamine solids to react with IPC in a polymerization solvent to generate PMIA; the preparation method comprises the following steps: carrying out surface activation treatment on BNNS to prepare f-BNNS; the preparation method comprises the following steps: carrying out surface grafting and activating treatment on TiO2 to prepare ultraviolet-resistant nano TiO2; pMIA, the composite nano suspension and DDSM are mixed in NMP and defoamed to prepare a modified polymer spinning solution, and the high-strength modified meta-aramid fiber with good mechanical properties and ultraviolet resistance is obtained through dry spraying-wet spinning, gradient cleaning, three-stage hot stretching, heat setting, hot drying and rolling.

The invention relates to an all-cotton four-way stretch fabric and a preparation method thereof, and belongs to the technical field of textile dyeing and finishing. The preparation method comprises the following steps: performing singeing, enzyme desizing, liquid ammonia finishing, loose alkali shrinkage and overfeeding soft heat setting on gray fabric to obtain the all-cotton four-way stretch fabric. The warp-wise and weft-wise shrinkage rates of the prepared four-way stretch fabric are-3.0%-0%, the warp-wise elastic elongation rate is 12%-15%, the weft-wise elastic elongation rate is 12%-18%, and the elastic residual elongation rate is smaller than or equal to 8%; obvious warp and weft elasticity can be achieved without elastic fibers, the problems that elastic fabrics such as spandex core-spun yarn fabrics are complex to manufacture, unstable in fabric size and the like are solved, the warp and weft elasticity is obvious, the size stability is good, the hand feeling is soft, and the price is low; the preparation method is simple, does not need equipment transformation, is easy to operate and does not damage fiber strength.

The invention relates to a bi-component fiber and a preparation method thereof, polyester melt and polyamide melt are extruded from a spinneret plate side by side, cross air blowing cooling is performed to obtain nascent fiber, and then the nascent fiber is sequentially subjected to heat pipe heating, oiling, pre-interlacing, three-roller drafting heat setting and winding to obtain the bi-component fiber. The heat pipe is used for heating nascent fibers, and the temperature of the heat pipe is 90-100 DEG C; the three rollers comprise a first hot roller, a second hot roller and a third hot roller; the temperature of the first hot roller is 70-90 DEG C, the temperature of the second hot roller is 110-130 DEG C, and the temperature of the third hot roller is 140-160 DEG C; the filament number of the prepared bi-component fiber is 2.6-3.5 dtex, the breaking strength is larger than or equal to 3.23 cN / dtex, the elongation at break is 27.45-38.31%, the number of broken ends is smaller than or equal to 2.3 times / (48 bits. 24 hours), and the broken filament rate is stably controlled to be 0.30% or below. According to the preparation method, generation of internal stress is greatly reduced; the mechanical property of the bi-component fiber is improved, and the number of broken ends and the broken filament rate of the fiber are obviously reduced.

The present invention provides a waterproof breathable membrane, a preparation method therefor, and a composite fabric comprising same. The preparation method for a waterproof breathable membrane comprises: performing first mixing of a polyolefin raw material and a solvent to obtain a premixed gel; performing second mixing of an elastomer and a solvent, and then performing third mixing with the premixed gel to obtain a mixed gel; performing melt extrusion on the mixed gel to obtain an initial gel membrane, followed by performing initial stretching on a biaxial stretching machine, and then extracting by using an extracting agent to obtain an initial microporous membrane; and performing expanded stretching on the initial microporous membrane, and performing heat setting and rapid high-temperature treatment in sequence. The waterproof breathable membrane is prepared by the described preparation method. The composite fabric is composed of an inner layer fabric, an outer layer fabric, and the waterproof breathable membrane provided by the present invention which is compounded between the inner layer fabric and the outer layer fabric. The preparation method provided by the present invention facilitates industrial promotion and use, and the obtained product possesses excellent waterproof and breathable properties, as well as higher tensile strength and elongation at break.

The invention relates to the field of flame-retardant textile fabrics, and provides a comfortable flame-retardant aramid fabric and a preparation method thereof. The composite filler with the average length of 3.0-8.0 mu m and the diameter of 0.4-1.0 mu m is prepared by adopting the design of multielement blended composite fibers of hydroxyapatite / magnesium hydroxide composite filler, meta-aramid polymer, para-aramid polymer, polybenzimidazole and the like through a hydro-thermal synthesis process of performing silanization surface activation and accurately controlling the molar ratio of calcium to phosphorus to be 1.60-1.67. The preparation method comprises the following steps: preparing the composite filler with the average length of 3.0-8.0 mu m and the diameter of 0.4-1.0 mu m; then industrial production processes such as graded shearing dispersion, continuous wet spinning, multi-stage stretching heat setting and after-finishing are performed, so that synergistic improvement of flame retardant performance and comfort performance is achieved, and the technical problems that a traditional aramid fiber fabric is poor in flame retardant effect, poor in comfort, unstable in processing performance and the like are solved; the fabric has wide application value in high-end application fields such as fire protection clothing, industrial protection textiles and military protection equipment.

The invention discloses a modified ultra-high molecular weight polyethylene fiber as well as a preparation method and application thereof. The modified ultra-high molecular weight polyethylene fiber is prepared from 100 parts by mass of ultra-high molecular weight polyethylene resin, 3-10 parts by mass of modified nano composite ceramic particles, 2-8 parts by mass of modified aramid fiber, 1-5 parts by mass of modified carbon nanotubes and 1-3 parts by mass of an auxiliary agent through the processes of a two-stage blending method, dry-wet spinning, gradient hot stretching, pulse heat setting and the like. The tensile strength of the prepared modified ultra-high molecular weight polyethylene fiber is greater than 4.5 GPa, the elongation at break is kept at 5.0-5.5%, the cutting resistance is as high as 310N, the puncture resistance is as high as 465N, and the modified ultra-high molecular weight polyethylene fiber can be applied to protective products.

The invention relates to the technical field of fiber materials, in particular to a polydopamine modified polypropylene antistatic fiber and a preparation method thereof. The antistatic polypropylene fiber overcomes the problems of poor antistatic effect and mechanical property of the polypropylene fiber. The preparation method comprises the following steps: carrying out step-by-step mixing, melt extrusion, spinning, drafting and heat setting on raw materials such as polypropylene slices, polydopamine modified polypropylene, carbon nanotubes, modified titanium dioxide, modified graphene and the like to obtain the antistatic fiber. The polydopamine modified polypropylene is obtained by modifying polypropylene with dopamine hydrochloride; the modified titanium dioxide is obtained by modifying nano titanium dioxide by using 3-aminopropyltriethoxysilane; the modified graphene is obtained by sulfonating graphene oxide and adding octadecylamine for modification. All the materials and the process cooperate with each other, an antistatic system is constructed on the surface and in the fiber, and meanwhile the mechanical property is improved. The fiber prepared by the method is excellent in antistatic effect and mechanical property, and has a good application prospect.

The invention relates to the technical field of polymer functional material processing, and particularly discloses a polyethylene waterproof breathable film using PTFE micro powder as an opening agent and a preparation method of the polyethylene waterproof breathable film. The waterproof breathable film is prepared from the following components in parts by weight: 50-70 parts of linear low-density polyethylene, 10-40 parts of PTFE (Polytetrafluoroethylene) micro powder, 3-8 parts of a modified compatilizer and an auxiliary agent. The preparation method comprises the following steps: S1, activating PTFE micro-powder by a silane coupling agent and coating the PTFE micro-powder with polyethylene wax to obtain modified micro-powder; s2, uniformly mixing all the components; s3, carrying out melt extrusion at 180-210 DEG C through a double-screw extruder, and carrying out tape casting to form a cast sheet; s4, the casting piece is heated to 90-115 DEG C for two-way stretching, and micropores are formed through interface stripping between the PTFE particles and the base body; and S5, carrying out heat setting at 120-130 DEG C, cooling, and rolling to form the film. Through the synergistic effect of the self-made compatilizer and the pretreatment process, the interface anchoring force is enhanced, the problems of powder falling and water leakage of highly-filled PTFE are solved, and meanwhile, high moisture permeability, high hydrostatic pressure resistance and high mechanical property are taken into account.

The invention discloses a preparation method of a composite current collector base film based on flame-retardant and aging-resistant modified PP and a composite current collector, the method comprises the following steps: 1) preparation of a modified PP master batch: mixing 100 parts by weight of PP resin, 0.5-1.8 parts by weight of a lubricant and 10-25 parts by weight of a flame-retardant and aging-resistant composite filler, and stirring at 100-135 DEG C for 0.5-2 h to obtain the modified PP master batch; (2) carrying out melt extrusion, tape casting and sheet casting to obtain an intermediate sheet; 3) biaxial stretching; and 4) carrying out heat setting, rolling and slitting to obtain the composite current collector base film. The invention provides the PP base film with excellent flame-retardant and aging-resistant performance and good mechanical strength; furthermore, based on the PP base film, the composite current collector is obtained after copper layers are formed on the two surfaces of the PP base film by adopting a conventional water electroplating process, and the copper layers and the PP base film in the composite current collector have high bonding strength, so that the service life of the composite current collector can be effectively prolonged.

The invention discloses a moisture-absorbing breathable polyamide fiber fabric and a preparation method thereof, and relates to the technical field of polyamide fiber fabrics. The method comprises the following steps: preparing a nano silicon dioxide composite template agent, and blending the nano silicon dioxide composite template agent with chinlon slices to prepare modified master batches; after special-shaped hollow spinning and weaving, a pore-foaming agent is dissolved out through hot water treatment, and a porous structure is constructed in the fiber; then carrying out plasma activation on the fabric, and grafting monomers such as acrylic acid, acrylamide and stearyl methacrylate on the surface and in pores of the fiber by adopting a radiation grafting method to form a hydrophilic-hydrophobic dual-channel structure; then, pre-crosslinked composite particles prepared from chitosan, beta-cyclodextrin and the like are loaded in micropores of the fabric through a vacuum-positive pressure circulation process; and finally, treating by using a finishing liquid containing blocked isocyanate, and carrying out heat setting. The prepared fabric has high moisture absorption rate, large moisture absorption capacity and excellent wet air permeability, is washable and anti-yellowing, and is suitable for high-performance sports and outdoor clothes.

The present invention provides an automotive wiring harness tape and a preparation method thereof. The wiring harness tape consists of a shielding layer and a rubber coating layer. The shielding layer is prepared from materials such as polyester fiber, nylon fiber, glass fiber, carbon fiber and conductive composite fiber, and has excellent electromagnetic shielding capabilities. The rubber coating layer is formed by mixing an antioxidant, a light stabilizer and silicone rubber, which effectively reduces the VOC release of the tape while ensuring good aging resistance and mechanical properties. The preparation method includes the steps of fiber mixing, heat setting treatment, rubber coating layer preparation and cutting. By precisely controlling the proportion of each component and process parameters, the continuity and stability of the tape are ensured. The automotive wiring harness tape of the present invention not only has excellent electromagnetic shielding performance, but also has good low fogging and mechanical properties, and is suitable for complex automotive electromagnetic environments.

The invention relates to the technical field of phase change materials, in particular to a polyamide elastomer composite fiber and a preparation method and application thereof. The preparation method of the polyamide elastomer composite fiber provided by the invention comprises the following steps: (1) taking a polyamide elastomer as a shell material and a solid-liquid phase change material as a core material, and carrying out coaxial melt spinning and curing to obtain a composite fiber precursor; and (2) sequentially carrying out surface crosslinking, drafting and heat setting on the composite fiber precursor to obtain the polyamide elastomer composite fiber. The polyamide elastomer composite fiber obtained by the preparation method has relatively high phase change enthalpy, relatively high energy storage density and relatively high tensile property, and can be used in temperature-adjusting textiles.

The invention relates to the technical field of polymer functional film materials, in particular to a double-layer structure polyester film with high barrier property and a preparation method thereof. The invention discloses a double-layer structure polyester film with high barrier property and a preparation method thereof, and the preparation method comprises the following steps: forming a single-layer gradient melt sheet in situ in a die head through temperature difference-pressure difference cooperative driving; the upper nano barrier layer is oriented and the lower crystal network is enhanced through synchronous two-way stretching; triggering secondary cross-linking through heat setting to permanently lock the gradient structure; and finally, carrying out online surface activation. According to the invention, an integrated single-layer structure is used for replacing the traditional physical lamination, so that the interlayer stripping risk is fundamentally avoided, and the prepared film has ultrahigh barrier property, high strength, excellent interface adhesion and damage self-repairing function, and is suitable for high-end aluminum laminated films, capacitor films and carbon-nitrogen substrate films.

The invention discloses a preparation method of a high-performance electric-breakdown-resistant capacitor base film, which comprises the following steps: S1, preparing modified polypropylene master batch: mixing polypropylene, a cycloolefin copolymer, a barium titanate-carbon nanotube modified composite filler and an antioxidant, and carrying out melt blending, extrusion and granulation to obtain the modified polypropylene master batch; s2, carrying out melt extrusion on the modified polypropylene master batch, cooling and casting; s3, carrying out two-way stretching and heat setting on the obtained casting piece to obtain a polypropylene film; and S4, performing plasma treatment on the surface of the polypropylene film to obtain the high-performance electric-breakdown-resistant capacitor base film. The high-performance electric-breakdown-resistant capacitor base film prepared by the method has excellent electric breakdown resistance, mechanical strength, flame retardance and heat resistance, has a long-acting flame retardant effect, is excellent in comprehensive performance and has a wide market application prospect.

The invention relates to the technical field of sewing thread preparation process optimization, in particular to a preparation process optimization method and system based on polytetrafluoroethylene sewing threads, and the method comprises the steps: obtaining a polytetrafluoroethylene resin particle set, obtaining a clean resin particle set, the use amount of magnetic nano filler, the use amount of a lubricant and the use amount of an antioxidant; performing stretching operation on the formed sewing threads, monitoring the formed sewing threads in real time, obtaining a stretching ratio and initial stretching sewing threads, calculating the crystallinity of the initial stretching sewing threads, performing heat setting on the optimal stretching sewing threads, obtaining optimal sewing threads, and summarizing the optimal sewing threads and optimal stretching parameters; an optimal sewing thread set and an optimal stretching parameter set are obtained, a stretching parameter database is constructed on the basis of the optimal stretching parameter set, and preparation process optimization based on the polytetrafluoroethylene sewing thread is completed on the basis of the optimal sewing thread set and the stretching parameter database. The quality and the performance of the polytetrafluoroethylene sewing thread can be improved.

The invention belongs to the technical field of preparation of flexible electronic materials, and particularly relates to a preparation method of a flexible synaptic fabric with a pressure sensing function, which comprises the following steps: firstly, preparing raw materials of the flexible synaptic fabric, including a flexible substrate material, a conductive material, a pressure sensitive polymer, a nanocellulose enhancer and a binder; then preparing conductive fibers loaded with silver nanowires and graphene through two-step dipping, and then sequentially dipping and coating a pressure sensitive polymer and a nanocellulose composite binder; a double-face protruding peak type structure is woven through a warp knitting machine, and finally the flexible synaptic fabric with the pressure sensing function is prepared through heat setting and surface modification treatment. The problems that a flexible pressure sensing fabric structure in the prior art is narrow in pressure sensing range and insufficient in sensitivity response interval can be solved.

The present disclosure provides a cross-linking enhanced meta-aramid and a preparation method therefor. In the method, an isocyanate is used as a cross-linking agent, treatment is performed for a period of time at a certain temperature after a catalyst is added, and then water washing, drying, and heat setting are performed to prepare a high-strength meta-aramid. With the present disclosure, a cross-linked meta-aramid is prepared and has an improved binding force between fibers and has excellent mechanical properties and high temperature resistance.

The invention discloses a cold-drawing heat-setting high-elasticity cowhells belt composite material, and relates to the technical field of composite materials. The invention relates to a cold-drawing heat-setting high-elasticity cowhells belt composite material. The composite material is prepared from the following raw materials in parts by weight: 12 to 18 parts of nano calcium carbonate, 0.1 to 0.4 part of silane coupling agent KH-550, 30 to 40 parts of modified thermoplastic polyurethane, 18 to 22 parts of ethylene-vinyl acetate copolymer, 5 to 8 parts of natural rubber, 3 to 5 parts of diisononyl phthalate, 0.3 to 0.5 part of compound antioxidant, 0.2 to 0.4 part of ultraviolet light absorber UV-9, 6 to 8 parts of aramid short fiber and 0.2 to 0.5 part of zinc stearate. 10 to 15 parts of modified polyethylene terephthalate fiber, 0.2 to 0.3 part of graphene and 0.5 to 1.5 parts of organic silicon treatment liquid. According to the cold-drawing heat-setting high-elasticity cowhells belt composite material, a matrix is reinforced through modified thermoplastic polyurethane and modified polyethylene terephthalate fibers, and the strength is improved through aramid short fibers subjected to plasma pretreatment. Molecular orientation is optimized by a cold drawing and heat setting process, weather resistance is enhanced by an organic silicon coating, and good overall elasticity, high strength and excellent wear resistance and weather resistance are achieved.

The present invention discloses a method for preparing a thick biaxially oriented liquid crystal polymer film, which is characterized by: adding LCP resin to a drying tank, drying it, and then putting it into a melt extrusion device for melt extrusion; the molten LCP resin is extruded through a T-die, and the formed LCP sheet flows onto a steel belt below, and the temperature of the steel belt is controlled by a hot air plate below; the LCP sheet runs on the steel belt, and then a circulating needle-punched belt is brought into contact with both sides of the LCP, and the LCP sheet is extended in the horizontal direction by the uniform movement of the needle-punched belt, and then peeled off from the steel belt after natural cooling; the LCP film is subjected to high-temperature heat setting and then cooled to obtain a thick biaxially oriented liquid crystal polymer film. The liquid crystal polymer film prepared by the present invention has the characteristics of high mechanical strength, uniform longitudinal and transverse tensile strength, and relatively thick thickness, and can be widely used in the fields of rigid high-frequency and high-speed copper-clad laminates, high-temperature resistant sheets, wireless charging insulation sheets, flame-retardant sheets, chip carriers, etc.

The invention relates to the technical field of high polymer materials and synthetic fibers, and particularly discloses a high-wear-resistance polyamide fiber and a preparation method thereof. The fiber is prepared by taking polycaprolactam as a matrix, compounding spherical nano silicon carbide and molybdenum disulfide nanosheets as wear-resistant components, taking a maleic anhydride grafted hydrogenated styrene-ethylene-butadiene-styrene block copolymer as an interface compatilizer, and taking hyperbranched polyamide-amine as a dispersing agent. The polyester fiber is prepared through the processes of master batch preparation, melt spinning, multi-stage hot drafting and relaxation heat setting. Through the synergistic effect of all the components and the optimization process, the wear resistance of the fiber is remarkably improved, and meanwhile, the common problems of toughness reduction and fatigue resistance deterioration in high-wear-resistance modification are effectively solved. The polyamide fiber is tough and durable, is specially used for manufacturing high-safety-requirement products such as mountaineering ropes, rescue ropes and industrial lifting belts, and can reduce the fracture risk in repeated use and guarantee the use safety.

The invention belongs to the technical field of preparation of composite fibers, and particularly relates to a preparation method of a heterocycle-containing polyamide composite fiber, which comprises the following steps: under the protection of inert gas, mixing a heterocycle-containing diamine monomer and terephthaloyl chloride in a polar solvent in proportion to prepare heterocycle-containing polyamide; mixing the amino modified cellulose nanomaterial, a tannic acid modified metal oxide and a Schiff base oligomer to form a composite dispersion liquid, adding heterocycle-containing polyamide, a lithium salt and a cross-linking agent into the composite dispersion liquid, dissolving and defoaming to obtain a spinning solution, and extruding the spinning solution into a coagulating bath through wet spinning; and carrying out multi-step washing, drying and heat setting treatment to obtain the heterocycle-containing polyamide composite fiber.