Patents
Literature
Patsnap Eureka AI that helps you search prior art, draft patents, and assess FTO risks, powered by patent and scientific literature data.

1486 results about "Methylene" patented technology

Methylene (systematically named methylidene and dihydridocarbon; also called carbene) is an organic compound with the chemical formula CH₂ (also written [CH₂]). It is a colourless gas that fluoresces in the mid-infrared range, and only persists in dilution, or as an adduct.

Electrolyte and battery

An electrolyte and a battery. The electrolyte comprises a first lithium salt, a second lithium salt and a first additive, the first lithium salt at least comprising lithium bis(fluorosulfonyl)imide, the second lithium salt being one or two selected from lithium difluoro(oxalato)borate and lithium difluoro(bisoxalato) phosphate, and the first additive being methylene methanedisulfonate. On the basis of the electrolyte comprising the first lithium salt and the second lithium salt, the first additive, i.e. methylene methanedisulfonate (MMDS), is further added in the electrolyte; the second lithium salt helps to improve the cycling stability and high-temperature storage performance of batteries, and the first additive helps to improve the oxidation resistance of the second lithium salt under high voltages, so as to further modify the composition and structure of SEI films, thus reducing the impedance of SEI films, improving the stability of SEI films, and improving the cycling performance and high-temperature storage performance of batteries.
Owner:GUANGZHOU TINCI MATERIALS TECH +1

Light conversion adhesive film composition

The invention provides a light conversion film composition. The light conversion film composition comprises the following components in percentage by weight: matrix resin, a light conversion agent and an auxiliary agent, the light conversion agent is a benzotriazole compound, and the auxiliary agent is an organic solvent. The structural general formula of the benzotriazole compound is as follows: # imgabs0 # R1 and R2 are respectively and independently selected from any one or more of H, C1-C20 alkyl and C1-C20 alkyl with at least one methylene substituted by a polyether chain segment, and R3 is independently a chain segment containing a carbon-carbon unsaturated double bond.
Owner:TAIZHOU HAIYOUWEI APPLIED MATERIALS CO LTD +1

Photosensitive resin composition containing anthracene methyl modified melamine photosensitizer, photosensitive dry film and application thereof

The invention provides a photosensitive resin composition containing an anthracene methyl modified melamine photosensitizer, a photosensitive dry film and application of the photosensitive dry film, the photosensitizer adopts a melamine skeleton to connect three anthracene 9-methyl structures, and through a rigid structure of the melamine skeleton and a methylene bridging (-CH2-An) design of an anthracene group, the photosensitive resin composition has the remarkable advantages that the methylene bridging structure can be used for preparing a photosensitizer, and the photosensitizer can be used as a photosensitizer for photosensitization of the anthracene methyl modified melamine photosensitizer. The breakage of carbon-oxygen bonds on alkoxy caused by p-pi conjugation is avoided, so that the migration of small molecular fragments after initiation is reduced, permeable crystallization to a polyethylene protective film is effectively inhibited, and the risk of short circuit of a line is remarkably reduced; the light quantum yield can be greatly improved by introducing a plurality of light sensing units; the melamine skeleton is used, so that the adhesive force of the initiation system on the metal foil surface can be effectively improved; in addition, the photosensitizer also shows excellent solubility and formula compatibility, and can be widely applied to the photocuring fields of dry films, paints, coatings, printing inks, molding materials and the like.
Owner:HUNAN INITIAL NEW MATERIALS CO LTD

Polyimide, polyimide film and preparation method and application thereof

The invention relates to the technical field of dielectric materials, and discloses polyimide, a polyimide film and a preparation method and application thereof, the polyimide is obtained by a polymerization reaction of a dianhydride monomer and a diamine monomer, the diamine monomer comprises a methylene bridging group and a phenyl group with a substituent group, and the methylene bridging group is a phenyl group with a substituent group. The substituent group at least comprises one methyl group. The molecular twisted conformation lock structure provided by the invention not only can improve the tolerance of polyimide, but also can doubly inhibit intrachain and inter-chain charge migration of the dielectric film, so that the dielectric film still has extremely high energy storage density and energy storage efficiency at a service temperature close to a glass-transition temperature.
Owner:CENT SOUTH UNIV

Polycyclic substituted methylene acetone compound and anti-saccharification application thereof

The invention discloses application of a compound shown as a formula I or salt or deuterated substance thereof in preparation of an anti-saccharification agent, in which ring A is a benzene ring or a five-membered ring containing O or S; the ring A may be substituted by m Ra, m being 0, 1, 2, 3 or 4; ra is hydroxyl, methyl, methoxyl, nitro or dimethylamino, and the deuterated substance is a partial deuterated substance and / or a perdeuterated substance. In the experiment of inhibiting generation of AGEs, compared with an Amino guanidine AG (Amino guanidine, AG), the anti-saccharification effect is obvious: under the low concentration, the anti-saccharification inhibition rate (the final administration concentration is 33 mu M) of the aromatic methylene acetone active small molecule compound protected by the invention is between 10% and 58%, and is far higher than the anti-saccharification inhibition rate (8.4%) of the Amino guanidine AG under the same final administration concentration (33 mu M), and the anti-saccharification inhibition rate (8.4%) of the Amino guanidine AG is far higher than the anti-saccharification inhibition rate (8.4%) of the Amino guanidine AG under the same final administration concentration (33 mu M) of the Amino guanidine AG. And the anti-saccharification inhibition rate of the radix codonopsis AG approaches to the final administration concentration (1mM) and is 57%. # imgabs0 #
Owner:AURORA CUTIS MEDICAL TECHNOLOGY (SHANGHAI) CO LTD

Sunscreen mousse composition for children and preparation method of sunscreen mousse composition

PendingCN119112692AReduce the risk of potential irritationPotential stimulus risk reducedCosmetic preparationsToilet preparationsXylyleneSunscreen agents
The invention discloses a children sunscreen mousse composition and a preparation method thereof.The children sunscreen mousse composition comprises agent materials and a propellant, the agent materials comprise an A-phase substance, a B-phase substance, a C-phase substance, a D-phase substance and an E-phase substance, the A-phase substance comprises a first solvent, a chelating agent, a thickening agent, p-hydroxyacetophenone and a humectant, and the thickening agent comprises xanthan gum; the B-phase substance comprises grease, a first sun-screening agent, a sun-screening synergist, an emulsifier, an antioxidant and a film-forming agent; the emulsifying agent is prepared from potassium cetyl phosphate and polyglycerol-10 laurate; the C-phase substance comprises a second solvent and a second sun-screening agent, and the second sun-screening agent comprises at least one of p-xylylene dichorsulfonic acid and methylene bis-benzotriazolyl tetramethyl butyl phenol; the D-phase substance comprises a preservative, a skin protecting agent and a filling agent; and the E-phase substance comprises a pH regulator and a third solvent. The sunscreen mousse composition for children has better mildness, sunscreen effect and stability, and also can provide a soft and dense mousse texture.
Owner:ZHONGSHAN TIANTU FINE CHEM CO LTD

Photosensitive resin composition containing anthracene methyl quaternary ammonium salt photosensitizer and application thereof

The invention provides a photosensitive resin composition containing an anthracene methyl quaternary ammonium salt photosensitizer and application of the photosensitive resin composition, a structural main body anthracene ring of the photosensitizer is introduced into methylene substituted by a quaternary ammonium group at a position 10 and / or a position 9, and an acid radical or halogen is adopted as an equilibrium anion; compared with a commercially available anthracene photosensitizer, the photosensitizer has excellent fat solubility and good water solubility through introduction of the quaternary ammonium salt on the premise that the photobleaching property is retained, great potential is brought to formula design of the photosensitive composition, and development waste in a later development process can be greatly reduced; the method can be widely applied to the photo-curing fields of dry films, paints, coatings, printing ink, forming materials and the like.
Owner:HUNAN INITIAL NEW MATERIALS CO LTD

Environment-friendly titanium alloy etching solution and preparation method and etching method thereof

The invention discloses an environment-friendly titanium alloy etching solution as well as a preparation method and an etching method thereof, and relates to the technical field of printed circuit board production. The environment-friendly titanium alloy etching solution comprises the following components in percentage by mass: 10-30% of ammonium fluoride, 5-15% of an oxidant, 0.1-1% of a wetting agent, 0.3-1.5% of a stabilizer, 2-10% of an accelerator and 0.5-3% of a lateral erosion inhibitor. The stabilizer is selected from at least one of Tween 20, Tween 40 and Tween 85; and the accelerator is selected from at least one of sodium methylene dinaphthalene sulfonate, sodium dibutyl naphthalene sulfonate and dodecyl benzoate. The environment-friendly titanium alloy etching solution disclosed by the invention can selectively and quickly etch titanium alloy without corroding a copper surface and other metals, so that etching factors are effectively increased, and the problem of lateral erosion of a fine circuit is solved. Meanwhile, ammonium fluoride is used as a main agent of the etching liquid instead of hydrofluoric acid, so that the environmental pollution can be effectively reduced.
Owner:SHENZHEN BANMING SCI & TECH CO LTD

Super-strong mute building drainage pipe and preparation method thereof

ActiveCN120173323AHalloysiteMeth-
The invention discloses a super-strong mute building drainage pipe and a preparation method thereof, and relates to the technical field of high polymer materials. Comprising the following raw materials in parts by mass: 100 parts of high-density polyethylene, 5-7 parts of a cold-resistant toughening agent, 8-12 parts of a synergist, 8-10 parts of a sound insulation filler and 0.3-0.5 part of an antioxidant. By introducing the synergist prepared from the components such as polyamine polyether methylene phosphonic acid, zinc nitrate hexahydrate, magnesium nitrate hexahydrate and the like, the sound insulation, flame retardance and smoke suppression capabilities of the drainage pipe can be effectively improved; by introducing the sound insulation filler prepared from the modified halloysite nanotubes, hydroxyl-terminated polydimethylsiloxane, aziridine cross-linking agent and the like, the sound insulation, flame retardance and smoke suppression capabilities of the drain pipe are further improved. Therefore, the drainage pipe prepared by the invention has a wider application prospect.
Owner:SHANGHAI YITONG TECH CO LTD

Integrated structure pickleball paddle and preparation process thereof

PendingUS20250295967A1Synthetic resin layered productsDomestic articlesEpoxyMethylenebis(chloroaniline)
An integrated structure pickleball paddle and a preparation process thereof are provided, where the pickleball paddle includes a paddle body, an edge banding, and a handle, where the edge banding and the paddle body are fused into an integrated structure by hot pressing, where the material of the edge banding is a modified TPU composite material, where the modified TPU composite material includes the following raw materials in parts by mass: 90-100 parts of modified TPU, 9-14 parts of polyvinyl fluoride, 20-30 parts of epoxy resin, 10-20 parts of ABS resin, 5-10 parts of modified nano-silicon dioxide, 0.3-0.6 parts of antioxidant, 0.2-0.5 parts of fluidity aid, 4-9 parts of 4,4′-methylene-bis(2-chloroaniline), and 3-7 parts of silicone oil. The edge banding and the paddle body are hot pressed and fused into an integrated structure, the edge banding will not fall off, and the comprehensive performance of the edge banding is better.
Owner:DONGGUAN XINSHUO COMPOSITE MATERIAL TECH CO LTD

Sunscreen composition, application and sunscreen product

The invention belongs to the field of daily chemicals, and discloses a preparation method of a sunscreen composition, which comprises the following steps: step 1, mixing and dispersing sodium stearoyl glutamate, a part of a thickener, a part of an alcohol solvent and a part of water; step 2, adding a sun-screening agent into the mixture obtained in the step 1; 3, grinding the mixture obtained in the step 2; 4, emulsifying and homogenizing the residual thickening agent, the residual alcohol solvent, the residual water and the mixture obtained in the step 3; the sun-screening agent contains methylene bis (benzotriazolyl) tetramethyl butyl phenol; the weight ratio of the sodium stearoyl glutamate to the methylene bis-benzotriazolyl tetramethyl butyl phenol is (2-7): (45-55). According to the sunscreen composition disclosed by the invention, wide experimental verification shows that the sodium stearoyl glutamate and the methylene bis-benzotriazolyl tetramethyl butyl phenol have obvious sunscreen synergy. Meanwhile, the invention also discloses the composition and application thereof.
Owner:广州华淼生物科技研究院有限公司

Aggregation-induced delayed fluorescence (AIDF) type organic scintillator material and preparation method thereof, and preparation method and application of flexible organic scintillation film

The invention belongs to the technical field of organic radiation luminescence and radiation imaging, and discloses an aggregation-induced delayed fluorescence (AIDF) type organic scintillator material and a preparation method thereof, and a preparation method and application of a flexible organic scintillation film. The molecular structure of the material comprises carbonyl, methylene, sulfuryl and other connecting units, phthalonitrile is used as an acceptor unit, carbazole is used as a donor unit, an aggregation-induced excitation state is formed through space charge transfer among molecules, efficient AIDF luminescence and large Stokes shift characteristics are realized, the self-absorption phenomenon is effectively avoided, and the luminescent efficiency is improved. The X-ray fluorescence probe is suitable for a luminescence process under an X-ray excitation condition, the sensitivity of X-ray detection is remarkably improved, and the lowest detection limit can reach 276nGy.s <-1 > and is far superior to the 5.5 mu Gy.s <-1 > standard required by medical diagnosis. Besides, the flexible scintillator film prepared based on the material system radiates and emits light within the waveband range of 450-750 nm and is perfectly matched with the response area of a silicon-based detector, X-ray imaging with the high signal-to-noise ratio is achieved, and the imaging resolution is as high as 20.01 lp.mm <-1 >.
Owner:NANJING VOCATIONAL UNIV OF IND TECH

Tires for vehicle wheels

The present invention relates to a tire for vehicle wheels which comprises at least one structural component comprising at least one reinforcing element constituted by an elongate element coated with, or embedded in, a vulcanised elastomeric compound obtained by vulcanising an elastomeric composition comprising per 100 phr of diene elastomeric polymer: (i) a predispersion of a diene elastomeric polymer and lignin, in an amount to provide the elastomeric composition with 100 to 10 phr of diene elastomeric polymer and a quantity of lignin equal to or greater than 20 phr, (ii) from 0 to 90 phr of a diene elastomeric polymer, (iii) at least 30 phr of a carbon black reinforcing filler, (iv) optionally, a reinforcing resin comprising at least 0.5 phr of a methylene acceptor compound associated with at least 0.2 phr of a methylene donor compound, (v) from 0.1 to 10 phr of carbon nanotubes, and (vi) from 0.1 to 12 phr of at least one vulcanising agent, wherein at least 50 phr of said diene elastomeric polymer is constituted by natural or synthetic isoprene rubber.
Owner:PIRELLI TYRE SPA

Low penetration sunscreen compositions

PendingUS20240407991A1Cosmetic preparationsToilet preparationsBenzoic acidEthylhexyl triazone
The present invention provides a sunscreen composition comprising: (a) diethylamino hydroxybenzoyl hexyl benzoate; (b) bis-ethylhexyloxyphenol methoxyphenyl triazine; (c) ethylhexyl triazone; and (d) methylene bis-benzotriazolyl tetramethylbutylphenol; wherein the sunscreen composition is substantially free of UV absorbers having a molecular mass of 380 Daltons or less.
Owner:KENVUE BRANDS LLC

Cholesteric liquid crystal elastomer-based circular polarization room temperature phosphorescence dynamic regulation and control method

The invention provides a cholesteric liquid crystal elastomer-based circular polarization room-temperature phosphorescence dynamic regulation and control method, which belongs to the technical field of optical materials, and comprises the following steps: 1, dissolving a liquid crystal monomer, a chiral agent, a cross-linking agent, a chain extender, a photoinitiator, a catalyst and a room-temperature phosphorescence polymer in a solvent dichloromethane to obtain a liquid crystal polymer solution; evaporating the solvent to obtain a red cholesteric liquid crystal elastomer room-temperature phosphorescent oligomer; 2, carrying out ultraviolet light polymerization on the cholesteric liquid crystal elastomer room temperature phosphorescent oligomer at room temperature to obtain a CLCE-RTP film; and step 3, regulating and controlling the circular polarization phosphorescence asymmetry factor by controlling the tensile deformation degree of the CLCE-RTP thin film. According to the invention, P1, P2 or P3 is doped with the cholesteric liquid crystal elastomer, so that the dynamic reversible regulation of the circular polarization room temperature phosphorescence asymmetry factor between 0.8 and 0.15 is realized.
Owner:NANJING UNIV OF POSTS & TELECOMM

A method for recycling cefuroxime sodium mother liquor

ActiveCN118994198Bavoid economySolve efficient recyclingOrganic chemistryDistillationMethylene DichlorideOrganosolv
The invention relates to the technical field of cefuroxime sodium medicines, and in particular provides a method for recycling a cefuroxime sodium mother liquor. On the basis of the prior art, a mother liquor nanofiltration impurity removal step and an organic solvent permeation steam recovery step are added, and cefuroxime acid and organic solvents acetone, ethyl acetate and dichloromethane in the cefuroxime sodium mother liquor can be effectively recycled and utilized, which not only solves the heavy environmental burden for production enterprises, but also brings potential considerable economic benefits to the production enterprises, and has great economic value and social value.
Owner:SHANDONG SALUBRIS PHARMA

Preparation method for extracting isopentenyl flavone compound from epimedium sagittatum and application of isopentenyl flavone compound

The preparation method comprises the following steps: crushing epimedium sagittatum to prepare paste, suspending with water, extracting with petroleum ether, dichloromethane, ethyl acetate and n-butyl alcohol respectively to obtain extractum of each part, carrying out gradient elution separation by using silica gel column chromatography, and concentrating to obtain the isopentenyl flavone compound extracted from epimedium sagittatum, thereby obtaining the isopentenyl flavone compound extracted from epimedium sagittatum. Combining the similar parts according to a thin layer chromatography (TLC) color development result to obtain a plurality of polar segments; carrying out chromatography and gradient elution on the target polar section to obtain a plurality of components, and then combining the similar components through thin-layer chromatography (TLC) dot plate absorption to obtain a plurality of sub-components; a target component is eluted and purified, fractions with different retention times are collected and dried, and two compounds are respectively obtained, have a remarkable inhibition effect on the cell viability of human breast cancer cells MCF-7, have anti-breast cancer activity, can be applied to preparation of drugs for treating breast cancer, and have huge social and economic benefits.
Owner:HENAN UNIV OF CHINESE MEDICINE

Photosensitive resin composition, cured resin film, and image display element

Provided is a photosensitive resin composition having excellent low-temperature curability and capable of providing a cured resin film having sufficient solvent resistance or sufficient hardness. Also, provided are a color filter having excellent solvent resistance or excellent hardness, and an image display element having same. A photosensitive resin composition according to the present invention contains a copolymer (A), a reactive diluent (B), a photopolymerization initiator (C), and a solvent (D). The copolymer (A) contains a structural unit (a), a structural unit (b), and a structural unit (c). The structural unit (a) has at least one selected from among an active methylene group having an alkoxycarbonyl group attached thereto, and an active methine group having an alkoxycarbonyl group attached thereto. The structural unit (c) has an acid group.
Owner:RESONAC CORP

Scale and corrosion inhibitor for seawater circulating cooling water

The invention relates to the field of water treatment, and discloses a scale and corrosion inhibitor for seawater circulating cooling water, which is prepared from phosphonic acid grafted maleic anhydride-acrylic acid copolymer, hydroxyethylidene diphosphonic acid, amino trimethylene phosphonic acid, N, N-dimethylformamide, N, N-dimethylformamide, N, N-dimethylformamide, N, N-dimethylformamide, N, N- The anti-corrosion coating is prepared from the following raw materials: N, N-diethylaminomethyl-benzotriazole, gamma-aminopropyltriethoxysilane, zinc salt and a polyoxyethylene-polyoxypropylene block copolymer. The core of the invention is that all the raw material components form the thermo-sensitive polyelectrolyte compound through a self-assembly process. The compound is stably dispersed at low temperature by utilizing the cloud point effect of the block copolymer, and is subjected to phase change and preferential deposition on a high-temperature heat exchange surface, so that targeted and efficient delivery of various active components is realized. According to the invention, the problems of incompatibility of components and poor stability of a traditional compound agent are solved, the product has excellent storage stability, and efficient and synergistic corrosion and scaling control can be realized under high-temperature and high-salinity working conditions.
Owner:JIANGSU KELIEN WATER PURIFYING TECH CO LTD

Composition for forming gel polymer electrolyte, gel polymer electrolyte, and lithium secondary battery comprising gel polymer electrolyte

The present invention provides a composition for forming a gel polymer electrolyte which includes a lithium salt; an organic solvent; and a crosslinking compound represented by Formula 1. wherein in Formula 1, L1, L2, L3, and L4 are each independently selected from a direct bond or an alkylene group having 1 to 3 carbon atoms, L5 and L6 are each independently an alkylene group having 1 to 20 carbon atoms in which at least one methylene group is optionally substituted with an ether group and at least one hydrogen is substituted with fluorine, and R1 and R2 are each independently selected from hydrogen, an alkyl group having 1 to 3 carbon atoms, or a halogen.
Owner:LG ENERGY SOLUTION LTD +1

An N-hydroxyamino-N'-acetyl indigo carmine and its fermentation method and application

This application relates to the field of microbial fermentation technology, and specifically discloses an N-hydroxyamino-N'-acetylguanine blue, its fermentation method and application. The chemical name of the N-hydroxyamino-N'-acetylguanine blue is N-(5'-hydroxyamino-2,6,2',6'-tetraoxo-1,6,1',6'-tetrahydro-2H,2'H-[3,3'] bipyridylmethylene)-acetamide, and the molecular formula is C 12 H 10 O6N4; compared with N-acetylguanine blue, the absorption of N-hydroxyamino-N'-acetylguanine blue is deeper in color at UV611, and at the same time, the formation of hydrogen bonds with amino groups on the fiber can enhance the dyeing property of the dye on the fiber and improve the wash fastness.
Owner:VERTEXYN (NANJING) BIOWORKS CO LTD

Low-temperature washing-free short-process pretreatment process

The invention belongs to the technical field of textile pretreatment processes, and particularly discloses a low-temperature washing-free short-process pretreatment process which comprises the following steps: (1) padding a fabric in a working solution, and stirring for 10-12 hours at 20-25 DEG C. The working solution comprises the following raw materials: a scouring agent, an alkali-resistant penetrant OEP-70, hydrogen peroxide, sodium silicate, ethylenediamine tetra (methylene phosphonic acid) pentasodium salt, caustic soda and water; (2) adding a water-free washing agent into the fabric subjected to padding treatment, and heating for 10-15 minutes at the temperature of 98-100 DEG C; (3) carrying out deoxidization treatment on the treated fabric; (4) immersing the treated fabric into the complex liquid, and stirring for 20-25 minutes at the temperature of 40-45 DEG C; the composite liquid is prepared from sodium dodecyl sulfate, modified chitosan, carboxymethyl cellulose, modified plant ash, polyethylene glycol and water. The fabric treated by the method is low in water consumption and high in dyeing efficiency and dye uptake, and the quality of the fabric is improved.
Owner:HANGZHOU XIAOSHAN SILK & CHEM FIBRE PRINTING & DYEING CO

Organic silicon marine antifouling and anticorrosive coating with high adhesive force as well as preparation method and application of organic silicon marine antifouling and anticorrosive coating

The invention discloses an organosilicone marine antifouling and anticorrosive coating with high adhesive force as well as a preparation method and application thereof. The organosilicone marine antifouling and anticorrosive coating is obtained by photocuring a composite coating material coated on the surface of a base material, the composite coating material is prepared from dopamine acrylamide, hexahedral polysilsesquioxane modified by sulfydryl, sulfydryl polydimethylsiloxane, N-(2, 4, 6-trichlorophenyl) maleimide, a photoinitiator and methylbenzene. The process provided by the invention is simple in synthesis condition, clean and environment-friendly, the ultraviolet light-initiated cross-linking reaction is rapid and good in effect, and the prepared antifouling and anticorrosive coating has good base material adhesion, excellent mechanical properties and antifouling and anticorrosive properties, and is suitable for industrial production. The requirements on antifouling property, base material adhesion and mechanical strength of the organic silicon coating in marine application can be greatly met, and the preparation method has a wide application prospect in the field of marine antifouling and anticorrosive coatings.
Owner:TIANJIN UNIV

4, 4, 4apos; -bis (omega-alkenyl thioether) diphenyl sulfide monomer, photopolymer type holographic recording medium, preparation method of photopolymer type holographic recording medium, grating and optical device

The invention discloses a 4, 4 '-bis (omega-alkenyl thioether) diphenyl sulfide monomer and a preparation method, the structural general formula of the 4, 4'-bis (omega-alkenyl thioether) diphenyl sulfide monomer is shown in the specification, n represents the number of methylene and is a positive integer, n = 1-10, the refractive index of a polymer obtained after the monomer and 4 '4-dimercapto diphenyl sulfide are polymerized is larger than 1.65 and smaller than 1.8, diffraction efficiency is remarkably improved, the preparation method is easy to operate, and the preparation method is suitable for industrial production. The invention further provides a photopolymer type holographic recording medium containing the monomer and a preparation method of the photopolymer type holographic recording medium, the sensitivity of the holographic recording medium is larger than 100 cm / mJ, the diffraction efficiency of a recording grating is larger than 95%, the refractive index modulation degree is larger than 0.1, the shrinkage rate is lower than 1%, and the preparation method is simple, controllable and suitable for industrial production. The invention also provides a volume holographic grating containing the holographic recording medium, a holographic optical element and an optical device.
Owner:ZHUHAI MOJIE TECH CO LTD

Method for extracting scandium from titanium white waste acid by utilizing diphosphonic acid extraction agent

The invention belongs to the technical field of extraction of scandium and diphosphonic acid extraction agents from titanium dioxide waste acid, and particularly relates to a method for extracting scandium from titanium dioxide waste acid by using a diphosphonic acid extraction agent. A scandium extraction extracting agent commonly used in titanium white waste acid generally has the problems of relatively poor selectivity, easiness in emulsification, difficulty in reverse extraction and the like. According to the method, P, P '-[(imine) bis (methylene) bis [P-alpha-hydroxyalkylphosphinic acid] is adopted as an extracting agent, trace scandium is extracted from the high-acidity titanium white waste acid, and the single extraction rate reaches 99.9%. The extraction agent is simple in synthesis method, good in stability and high in extraction capacity, and has good extraction performance on trace scandium in high-acidity and multi-impurity titanium white waste acid. The extraction agent is free of emulsification during extraction, fast in phase splitting and high in production efficiency, and compared with common phosphorus (phosphine) extraction agents, the extraction agent does not need saponification and belongs to an environment-friendly extraction agent.
Owner:UNIV OF JINAN

Preparation method of ethyl 2-n-butyl acetoacetate

The invention relates to the technical field of organic synthetic chemistry, in particular to a preparation method of ethyl 2-n-butyl acetoacetate, which comprises the following specific steps: S1, preparation of a composite solid base catalyst, S2, synthesis of ethyl 2-n-butyl acetoacetate, S3, post-treatment of a reaction solution, and S4, separation and purification of a product. The preparation method has the following beneficial effects that the magnesium-aluminum composite oxide is used as a carrier, and the composite solid base catalyst loaded with potassium and lanthanum has relatively high catalytic activity and selectivity; the magnesium-aluminum composite oxide carrier has a relatively large specific surface area and rich alkaline sites, so that a good catalytic environment is provided for the reaction; as a main active component, potassium ions can effectively activate alpha-active methylene of ethyl acetoacetate and promote formation of negative ion intermediates; the introduction of lanthanum ions can adjust the electronic structure of the catalyst, enhance the stability of the active center and inhibit the occurrence of side reactions.
Owner:SIPING FINE CHEM CO LTD

Conductive elastomer and preparation method and application thereof

The invention discloses a preparation method of a conductive elastomer. The preparation method comprises the following steps: (1) mixing N-hydroxyethyl acrylamide, glycerol and choline chloride, heating and stirring to obtain a clear and transparent solution A; (2) adding furfuryl methacrylate and N, N '-(4, 4'-methylene diphenyl) bismaleimide into the solution A prepared in the step (1), heating and stirring to obtain a clear and transparent solution B; (3) adding a photoinitiator into the solution B prepared in the step (2), and stirring in a dark place to obtain a clear and transparent solution C; and (4) pouring the solution C prepared in the step (3) into a mold, and performing in-situ polymerization under ultraviolet irradiation to obtain the conductive elastomer. The conductive elastomer has excellent mechanical strength and toughness.
Owner:华工丽颜(广东)新材料科技有限公司 +1

Rigid spiro compound as well as preparation method and application thereof

The invention relates to a rigid spiro compound and a preparation method and application thereof.The preparation method comprises the steps that 6-methylene-androstane-4-ene-3, 17-diketone (V) is dissolved in a mixed solution of dichloromethane and trifluoroacetic acid, reaction and reduced pressure distillation are conducted at the temperature of 20-25 DEG C, then extraction washing and distillation are conducted, a rigid spiro compound crude product can be obtained, and the rigid spiro compound is obtained. The crude product can be subjected to column chromatography separation and purification to obtain a refined rigid spiro compound (I). By adopting the preparation method, the friction and wear properties of the base oil are remarkably improved, and the base oil has lower friction coefficient and wear scar diameter, and has good application prospect as an antifriction and wear-resistant additive.
Owner:SHAOXING UNIVERSITY

Preparation method of modified master batch degradable material and application of modified master batch degradable material in packaging meal box

The invention relates to the technical field of high polymer materials, and discloses a preparation method of a modified master batch degradable material and application of the modified master batch degradable material in a packaging lunch box, and the modified master batch degradable material comprises the following components by mass: 75.0-93.8 parts of poly (butylene succinate); 5.0 to 20.0 parts of aliphatic series-aromatic copolyester; 1.0 to 4.0 parts of 1, 1 '-methylenebis-4, 1-phenylene-bismaleimide, and 1.0 to 4.0 parts of 1, 1'-methylenebis-4, 1-phenylene-bismaleimide; 0.5 to 2.0 parts of talcum powder; the method comprises the following steps: mixing dried poly (butylene succinate), aliphatic-aromatic copolyester, bismaleimide and talcum powder, performing reactive extrusion and melt mixing through a twin-screw extruder, and then cooling, pelletizing and drying the extrudate. Through specific components and a reactive extrusion process, a dynamic cross-linked network is formed by utilizing a Diels-Alder reaction, and the modified master batch degradable material of which the comprehensive mechanical property and the heat resistance are remarkably improved is prepared.
Owner:SHENZHEN SAIZHUO PLASTIC IND CO LTD

High-strength anti-ultraviolet regenerated PET fiber and preparation method thereof

The invention provides a high-strength anti-ultraviolet regenerated PET fiber and a preparation method thereof. The preparation method comprises the following steps: in a nitrogen atmosphere, dissolving 2, 2 '-methylenebis [6-(benzotriazolyl)-tetramethylbutylphenol] and hexamethylene diisocyanate in N-methyl pyrrolidone, adding a catalyst for reaction, then heating to remove residual monomers, cooling, dropwise adding into ice methanol to separate out a product, washing, and carrying out vacuum drying to obtain an anti-ultraviolet auxiliary agent; the preparation method comprises the following steps: dissolving an anti-ultraviolet aid and hexamethylenediamine in an aprotic solvent, adding a catalyst, carrying out condensation reaction in a nitrogen atmosphere, and carrying out centrifugal washing and vacuum drying to obtain the anti-ultraviolet composite chain extender, the preparation method comprises the following steps: mixing an anti-ultraviolet composite chain extender with recycled PET fragments, adding an antioxidant, a hydrolysis-resistant solution and a lubricant, and carrying out blending spinning through a double-screw extruder to obtain the high-strength anti-ultraviolet regenerated PET fiber. According to the invention, through anti-ultraviolet-chain extension chemical bonding, the bottleneck that the strength and the function of the regenerated PET fiber are difficult to synergistically improve is broken through.
Owner:ZHEJIANG ALICE DYEING & FINISHING CO LTD