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125 results about "Chloride salt" patented technology

Chloride (salts) Chlorides, sulfates, salinity, and dissolved minerals are all forms of “salts” that can harm fish and plant life at high concentrations. For example, the salt applied to roads, parking lots, and sidewalks during our icy winters contains chloride, a water pollutant.

Method for extracting lithium, rubidium and cesium and preparing lithium, rubidium and cesium salt through strengthened roasting of lepidolite

The invention provides a method for extracting lithium, rubidium and cesium through strengthened roasting of lepidolite and preparing lithium, rubidium and cesium salt, and belongs to the technical field of lithium, rubidium and cesium extraction.The method comprises the steps that lepidolite, a carbon / sulfur additive and chlorine salt are subjected to ball milling, roasting and grinding, and roasted sand is obtained; through thermodynamic analysis on the lepidolite, after the carbon / sulfur additive is introduced, the Gibbs free energy of the reaction of the lepidolite and the additive is reduced, the reaction trend is improved, and in the roasting process, ions such as sodium, potassium and calcium in chlorine salt and the carbon / sulfur additive are replaced in a similar isomorphic manner, so that lithium, rubidium and cesium are leached more easily; in the process of intensifying roasting by introducing the carbon / sulfur additive, the use amount of the chlorine salt additive is reduced by 10-25%, potassium-sodium mixed salt and calcium oxalate are recycled, the recycling rate is greater than 50%, and the leaching residue amount is reduced by 30-40%; and the carbon / sulfur additive can directionally promote the reaction of the calcium salt additive and the lepidolite and convert the calcium salt additive into dicalcium silicate, so that the leaching residues obtained in the subsequent leaching process are easier to recycle.
Owner:CENT SOUTH UNIV

Marine work concrete resistant to chlorine salt erosion and preparation method thereof

PendingCN121554239AAluminateAluminite
The invention discloses marine concrete resistant to chlorine salt erosion and a preparation method thereof, and belongs to the technical field of building materials. The marine concrete is prepared from the following components in parts by mass: 280 to 350 parts of cementing material, 1100 to 1200 parts of aggregate, 150 to 180 parts of mixing water and 2.5 to 4.0 parts of high-efficiency water reducing agent, and the cementing material is prepared from 210 to 270 parts of ordinary Portland cement, 50 to 70 parts of superfine slag powder and 10 to 20 parts of modifier on the basis of the cementing material; on the basis of the modifier, the modifier is prepared from 30 to 45 parts of hexacalcium aluminoferrite, 25 to 35 parts of metaettringite, 20 to 35 parts of tobermorite, 3 to 6 parts of nano attapulgite and 2 to 4 parts of a nano composite material. The components can accelerate the early hydration of cement and the volcanic ash reaction process in the concrete hardening process, so that the concrete can form a compact microstructure in the curing period and cooperate with the curing effect of a hydration product on chloride ions, thereby remarkably improving the chloride ion penetration resistance of the concrete, prolonging the service life of the structure and improving the concrete quality. The method is suitable for port engineering, maritime work structures and buildings in salinized soil areas.
Owner:WANJIANG INST OF TECH +1

Chlorine-doped nickel oxide, preparation method and application thereof, and photoelectric device

The invention provides chlorine-doped nickel oxide, a preparation method and application thereof and a photoelectric device, and relates to the field of photoelectric materials.The preparation method of the chlorine-doped nickel oxide comprises the following steps that S10, an aqueous solution of nickel salt and chlorine salt is obtained, an alkaline solution is dropwise added, centrifugation is conducted, and a coprecipitate is obtained; s20, washing, drying and roasting the coprecipitate to obtain chlorine-doped nickel oxide; wherein the molar ratio of the nickel salt to the chlorine salt is (10-20): (1-4). In the technical scheme provided by the invention, the nickel salt and the chlorine salt are co-precipitated to generate a co-precipitate of nickel hydroxide and chloride, and then the co-precipitate is washed, dried and roasted to prepare the chlorine-doped nickel oxide, so that the hole mobility of the chlorine-doped nickel oxide is improved; the alkaline solution is dropwise added for coprecipitation, so that the particle size of the coprecipitate can be reduced, and the nanoscale chlorine-doped nickel oxide is prepared, so that the dispersity of the chlorine-doped nickel oxide in a mobile phase is improved, and the chlorine-doped nickel oxide can be applied to preparation of a hole transport film and improvement of the uniformity of the hole transport film.
Owner:旗滨新能源发展(深圳)有限责任公司

Building material base material produced by utilizing household garbage incineration waste and preparation process of building material base material

The invention discloses a building material base material produced by utilizing household garbage incineration waste and a preparation process of the building material base material. The base material is prepared from the following components in percentage by weight: 30 to 50 percent of fly ash, 20 to 40 percent of bottom slag, 10 to 20 percent of Portland cement, 3 to 10 percent of Fe-N-C-coated Cu-NPs modifier and 5 to 15 percent of water. Fly ash is subjected to water washing and 600-800 DEG C heat treatment to remove chlorine salt and organic matter, and bottom slag is subjected to screening and magnetic separation to control the particle size and the iron content. Fe-N-C-coated Cu-NPs is prepared through high-temperature pyrolysis and a wet chemical method, and dioxin decomposition and heavy metal solidification are catalyzed. The preparation process comprises the steps of pretreatment, mixing, vibration molding (5-10 MPa) and wet curing (20-35 DEG C, 80-95% humidity and 7-21 days). The compressive strength of the base material reaches 11.8-14.0 MPa, the dioxin content is lower than 0.1 ng-TEQ / kg, the heavy metal curing rate is 96.5-98.5%, the porosity is 10.5-12%, solid waste resource utilization is achieved, and environmental protection and economic benefits are achieved.
Owner:CHANGSHU PUFA SECOND THERMOELECTRIC ENERGY CO LTD

Vanadium-based MXene and etching preparation method thereof

The invention provides vanadium-based MXene and an etching preparation method thereof, and the etching preparation method comprises the following steps: step 1, placing MAX powder, chlorate and alkali in a container, wherein the chlorate is placed between the MAX powder and the alkali; 2, the container is heated and subjected to heat preservation for a certain time; 3, after reacting for a certain time, stopping heating and cooling to obtain an etching mixture; and 4, the etching mixture is subjected to washing treatment and drying treatment, and the vanadium-based MXene can be obtained. According to the etching preparation method, the problem of over-etching can be avoided, and meanwhile, the preparation method is better in selectivity; no fluorine participates, so that the safety is relatively high; the etching preparation time is short, reaction equipment is simple, and the cost is low.
Owner:SICHUAN UNIV +1

High-entropy metal sulfide nano material and preparation method thereof

The invention discloses a high-entropy metal sulfide nano material and a preparation method thereof, and relates to the field of high-entropy materials.Transition metal chlorate and sodium chloride are placed in a first reaction boat in the upstream area of a reaction container; placing the zinc sulfide nano-template in a second reaction boat in a downstream area of the reaction container; heating the reaction container to 500-525 DEG C at a first heating rate, keeping the temperature for 20-40 minutes, and transporting metal chloride gas volatilized by the eutectic effect of the precursor to a second reaction boat in a downstream area along with the dynamic airflow, so that the zinc sulfide nano-template reacts with the metal chloride gas; and cooling to room temperature at a second cooling rate, and collecting a solid product in the second reaction boat to obtain the high-entropy metal sulfide nano material. According to the method, the complex microstructure of the precursor template can be copied, and topological conversion is realized; and the chemical morphology, the components, the crystal structure and the like of the high-entropy nano material can be regulated and controlled.
Owner:LANZHOU JIAOTONG UNIV

Use of oxoacid reducing element in molten chloride salts for nuclear fission reactor (MSR)

The present invention relates to the use of at least one oxoacid reducing element, and optionally a salt of the oxoacid reducing element, in a molten chloride fuel salt for a molten-salt nuclear fission reactor (MSR). The present invention also relates to a process of nuclear fission within a molten-salt nuclear fission reactor (MSR), said process being characterized in that it is carried out within the MSR reactor, placed in which is an oxoacid reducing element, and optionally a salt of the oxoacid reducing element. The present invention further relates to a molten-salt nuclear fission reactor (MSR) comprising a molten chloride fuel salt, and a mixture comprising the aluminum metal, and its oxidized form, as an oxoacid reducing element, and optionally a salt of the oxoacid reducing element.
Owner:ALEXANDRE & GAVRILOFF

Ice-blocking concrete material, application, and ice-blocking construction method for foundation pit sidewalls

The present invention relates to the technical field of ice prevention for foundation pits, and in particular, to an ice-preventing concrete material, its application, and a method for constructing ice prevention for the side walls of foundation pits. The ice-preventing concrete material includes concrete and ice-preventing particles, and the ice-preventing particles are obtained by mixing silicate cement, chloride salts, ammonium salts, lignin, and water; the chloride salt is one of calcium chloride, magnesium chloride, potassium chloride, ferric chloride, and aluminum chloride, and the ammonium salt is one of urea, ammonium nitrate, and triethanolammonium. The present invention prevents the formation of ice hanging on the side walls of foundation pits through the slow dissolution and penetration principle of ammonium salts and chloride salts, thereby avoiding safety accidents caused by ice hanging falling; the concrete and ice-preventing particles can be mixed evenly, so that they can be effectively applied or sprayed on the side walls of foundation pits, and the preparation is simple, the degree of structural corrosion is small, the pollution to the soil is small, and it has the characteristics of economy, safety, and environmental protection.
Owner:BEIJING RAIL TRANSIT CONSTR MANAGEMENT

A precision grinding process for machining the motor shaft of a swimming pool water pump

This invention discloses a precision grinding process for machining the shaft of a swimming pool pump motor, relating to the field of shaft precision grinding technology. The process includes: Step 1: Establishing an incident window using a coherent jet nozzle, allowing the jet to penetrate the air gap into the grinding zone, first wetting and then introducing the load, and recording the incident window, jet posture, and dressing rhythm as working condition metadata; Step 2: After precision grinding, according to the material type, magnetic noise is used for ferromagnetic steel and X-ray diffraction is used for austenitic steel to obtain thermal damage and residual stress, and combining this with cleanliness to generate a surface integrity label and bind it to the working condition metadata; Step 3: Performing deionized ultrasonic cleaning and rinsing according to the label to remove chloride salts and free iron, rebuilding the passivation film according to specifications using chemical passivation, controlled drying, and clean sealing; Step 4: Under the premise of qualified chemical condition, performing isotropic ultra-finishing and low-plasticity rolling on the sealed working zone to form surface compressive stress and maintain geometric tolerances, quickly indicating inspection and writing back the label.
Owner:ANHUI SUNLIMA DRIVE TECH CO LTD

A post-treatment method for improving the purity of K / NaMgF3 particles

The present invention provides a post-treatment method for improving the purity of K / NaMgF3 particles, particularly relating to the field of chemistry. The method comprises the following specific steps: (1) placing K / NaMgF3 particles in an aqueous solution and stirring and dissolving them thoroughly; (2) adding a fluoride salt and a buffer to the solution treated in step (1) and stirring thoroughly; (3) adding a magnesium salt and a chloride salt to the solution treated in step (2) and stirring thoroughly; and (4) pouring out the residual solution treated in step (3) and drying the residual solid in step (4). The K / NaMgF3 of the present invention remains unchanged and does not introduce new impurities. The method can remove MgF2 impurities while neither destroying the structure of K / NaMgF3 nor introducing new impurities. The steps are closely related, and no intermediate rinsing or treatment is required. The process is simple, and while ensuring efficient impurity removal, energy conservation and environmental protection are also taken into account. The method is applicable to various K / NaMgF3 preparation methods, does not use toxic and hazardous substances, and has low waste liquid treatment costs.
Owner:INST OF METAL RESEARCH - CHINESE ACAD OF SCI

Comprehensive utilization and treatment method and equipment system for ammonia-soda process ammonia wastewater

A comprehensive utilization and treatment method and equipment system for ammonia distillation wastewater from the ammonia-soda process includes an evaporation and concentration chamber, a heat pump system, a cooling chamber, a freezing separation chamber, a heat exchanger, an evaporation and crystallization chamber, and a cooling crystallization chamber. Combined with solar radiation, the wastewater undergoes a multi-stage heat exchange cycle through evaporation, cooling and freezing separation, gas-liquid separation, evaporation and crystallization, and cooling crystallization. This process effectively and continuously separates sodium chloride and calcium chloride salts while recovering fresh water. The sodium chloride recovery rate is 75%, the calcium chloride recovery rate is 75%, and the fresh water recovery rate is 55%. This reduces the input cost of raw salt and the amount of mixed solids landfilled in the alkali production process, lowering operating costs. The wastewater can be directly used as lime slurry or, after treatment, as raw water for molten salt, conserving water resources. Through the comprehensive utilization of the wastewater, evaporation efficiency is increased, land area previously occupied by solar pond evaporation of the wastewater is reduced, and the comprehensive utilization of waste resources is maximized.
Owner:SHANGHAI INST FOR DESIGN & RES ON ENVIRONMENTAL ENG

Coal bed gas produced water resource utilization process

The invention belongs to the technical field of safety and environmental protection, and provides a coalbed methane produced water resource utilization process which comprises the following steps: obtaining coalbed methane produced water containing various chloride salts, and pretreating the coalbed methane produced water containing various chloride salts to remove impurities; the method comprises the following steps: conveying coal bed gas produced water from which impurities are removed and which contains various salts such as chlorides and the like to a multi-effect evaporation assembly, and sequentially carrying out five-effect countercurrent evaporation, three-effect countercurrent evaporation and single-effect vacuum evaporation treatment, so as to obtain NaCl solids, KCl solids and salt slurry containing CaCl2; and feeding the salt slurry containing CaCl2 into a spray drying device, and drying to obtain a CaCl2 solid. NaCl solids, KCl solids and CaCl2 solids are obtained through five-effect countercurrent evaporation, three-effect countercurrent evaporation, single-effect vacuum evaporation and drying treatment, salt products meet the requirements of industrial salt, and coal bed gas produced water is utilized to a large extent.
Owner:CHINA PETROLEUM ENG & CONSTR +2

A testing device and method for high performance concrete resistant to chlorides freeze-thaw action

The application relates to the technical field of concrete testing, and discloses a high-performance concrete testing method for resisting the action of chloride salt freeze-thaw, which comprises a workbench, a plurality of detection stations are arranged on the workbench, a plurality of sensing control lifting frames are arranged on the two sides of the workbench, a plurality of detection cover plates are arranged on the top of the sensing control lifting frames, the detection cover plates correspond to the positions of the detection stations, in the application, the concrete test sample is placed on the detection station, when the conveying belt conveys the sample to the specified position, the sensing control lifting frame senses the position of the detection station, drives the detection cover plate to move downwards until the cover plate covers the detection station, at this moment, the detection probe is located in the detection station, the internal concrete sample is proportionally detected, and the detection data is uploaded to the transmitter after the detection is completed, so that the purpose of accurately detecting the concrete is achieved.
Owner:DALIAN JIAOTONG UNIVERSITY

Experimental device

The utility model discloses an experimental device, which comprises a test piece box, a plurality of test cavities, a plurality of connecting rods, a plurality of connecting rods and a plurality of connecting rods, the salt solution box is provided with a salt storage box, a salt conveying pipe and a plurality of mixed liquid boxes, and the salt conveying pipe is used for conveying chlorate and sulfate to each mixed liquid box; a plurality of water pumps are arranged, and each test cavity is communicated with the corresponding mixed liquid box through the corresponding water pump; the temperature control device comprises a compression condenser and a heater, the compression condenser is used for refrigerating the test piece, and the heater is used for heating the test piece; and the control system is used for controlling the operation of each component. By arranging the multiple independent test cavities, the multiple independent mixed liquid boxes and the temperature control device, the test device has multiple test function modes, in addition, under different function modes, different temperature parameters can be controlled through the temperature control device, the actual road environment can be better simulated, and the accuracy of test results can be ensured to a great extent.
Owner:XINJIANG TRANSPORTATION PLANNING SURVEYING & DESIGN INST +2

A process for preparing chlorides by reducing chlorination of rare metal oxides

ActiveCN118359225BTungsten halidesNiobium compoundsChloride saltWater chlorination
This invention discloses a process for preparing chlorides by reducing chlorination with rare metal oxides, comprising the following steps: S1, in an inert atmosphere, a mixture containing rare metal oxide powder, a reducing agent, and a chloride salt is subjected to a reduction reaction at a predetermined temperature 1; S2, the temperature is lowered to a predetermined temperature 2, oxygen is introduced, and the concentration of oxygen in the mixed gas is adjusted to carry out a chlorination reaction, and the chlorinated product is condensed and collected. This invention eliminates the need for gaseous chlorinating agents such as chlorine or hydrogen chloride, avoiding the leakage risks of liquid chlorine and compressed hydrogen chloride during storage and transportation; the raw materials can be directly rare metal oxides, with a wide range of sources, good process adaptability, and significantly reduced production costs.
Owner:HUNAN YIJIA NEW MATERIALS CO LTD

Preparation method of chlorine salt conversion film with high corrosion resistance

The invention provides a preparation method of a chlorine salt conversion film with high corrosion resistance, which comprises the following steps: dissolving manganese chloride and calcium chloride in water, then adding ammonium dihydrogen phosphate, sodium nitrate and EDTA (Ethylene Diamine Tetraacetic Acid), and carrying out conversion treatment to obtain a conversion film solution containing free Mn < 2 + > and Ca < 2 + > and Mn < 2 + > and Ca < 2 + > complexed by EDTA; placing the conversion film solution in a water bath kettle with the temperature of 50-60 DEG C for heating and heat preservation; the magnesium alloy is put into a conversion film solution, monohydrogen phosphate of Mn < 2 + > preferentially nucleates and grows to form a high-thickness film layer, then monohydrogen phosphate of Mn < 2 + > and Ca < 2 + > complexed by EDTA preferentially performs targeted nucleation at the defect position of the film layer, and a conversion film with high thickness and density is formed on the surface of the magnesium alloy. According to the preparation method of the chlorine salt high-corrosion-resistance conversion film, the preparation cost is low, and the prepared film layer is thick and uniform.
Owner:NORTHEASTERN UNIV CHINA

A method for synthesizing sodalite from 4A zeolite and simultaneously solidifying radioactive waste salt in situ.

This invention provides a method for synthesizing sodalite from 4A zeolite and simultaneously solidifying radioactive waste salts in situ, belonging to the field of radioactive waste salt solidification treatment technology in the dry reprocessing of spent fuel. The invention involves mixing 4A zeolite powder, radioactive waste salts, alkali metal chloride salts, and a dispersant at a specific liquid-to-solid ratio, followed by heating and drying to obtain a solidification precursor. The precursor is then ground, sieved, and sintered at temperatures not exceeding 900°C to obtain a solidified sodalite body. The method provided by this invention features low energy consumption, simple operation, low 4A zeolite usage, high radioactive waste salt coating rate, and high radioactive element fixation. The synthesized solidified sodalite body exhibits strong thermal stability and high mechanical hardness, with a normalized leaching rate of less than 5 x 10⁻⁶ after soaking in water at 90°C for 28 days. ‑ 4 g / (cm 2 ·d) The sodalite solidified body of the present invention can be geologically stored for a long time, effectively reducing the risk of migration, diffusion and leakage of radioactive materials.
Owner:WUHAN UNIV

Hydrophobic modification method of recycled aggregate polluted by chlorine salt and preparation method of chlorine-sealing rib-protecting recycled concrete applying hydrophobic modification method

The invention relates to the technical field of building materials, and discloses a hydrophobic modification method of chlorine salt polluted recycled aggregate and a preparation method of chlorine-sealing rib-protecting recycled concrete applying the hydrophobic modification method. The hydrophobic modification method of the chlorine salt-polluted recycled aggregate comprises the following steps: dipping the chlorine salt-polluted recycled aggregate in a silane emulsion diluent, taking out the chlorine salt-polluted recycled aggregate, and airing the chlorine salt-polluted recycled aggregate to complete hydrophobic modification of the chlorine salt-polluted recycled aggregate. Compared with unmodified recycled aggregate, the chlorine salt polluted recycled aggregate modified by the method provided by the invention has the advantages that the hydrophobic capacity is better, and the dissolution amount of water-soluble chloride ions is lower. The invention further discloses a preparation method of the chlorine-sealing rib-protecting recycled concrete, the chlorine-sealing rib-protecting recycled concrete comprises the following components: 300-500 parts of cement, 600-700 parts of sand, 1000-1100 parts of hydrophobic modified recycled aggregate and 1-3 parts of a water reducing agent, and the water-cement ratio is controlled to be 0.35-0.55. The method has the advantages that the durability of the recycled concrete member prepared from the chlorine salt polluted recycled aggregate is enhanced, and the utilization rate of the chlorine salt polluted recycled aggregate is increased.
Owner:FUZHOU UNIV

Calcium or magnesium chloride salt-based composition

ActiveUS12419908B1Powder deliverySpray deliveryCough suppressionLarynx
Hydration of a larynx and / or vicinity with a composition comprising a salt formulation (e.g., CaCl2, MgCl2, KCl and / or NaCl) can achieve prophylactic and / or therapeutic effects (e.g., cough suppression, improving voice quality, increasing pulse oxygen saturation and / or increasing mucosal vaccination effectiveness). The composition is administered as dry particles (e.g., aerosol) or as a liquid (e.g., solution, aerosol). The liquid can have a pH of 7.0 up to around 10.0, or preferably around 7.5 up to around 9.5, or more preferably around 8.0 up to around 9.0, or even more preferably 8.0 to 8.5 or most preferably around 8.0. The droplets can have a mass median aerodynamic diameter from approximately 8 μm to approximately 15 μm or from approximately 15 μm to approximately 500 μm. A therapeutic dose (e.g., 0.5 mg to 4.0 mg mass of salt) is administered in response to an indication. Such can employ an osmolitically active composition.
Owner:SENSORY CLOUD LLC

Movable assembly type construction sand purification device and system

The application discloses a movable assembled construction sand purification device and system, and belongs to the field of construction sand purification. The sand cleaning equipment is integrated into movable modules according to different functions, and the modules are combined according to process requirements. When used, the modules can be combined, and part of the modules can be reused. Various functional devices are respectively integrated and installed in a box, the box can be transported to a use site by a transport tool, and can be used after unloading and hoisting. Different combination modes can be adopted according to different properties of sand, such as machine-made sand, sea sand or river sand, to form a purification system. The purification system can effectively remove the edges and corners of machine-made sand, needle-shaped sand and weathered layers on the surface of sand particles, effectively remove the chloride salt (chloride ion content can reach 0.000% to 0.002%) and other harmful substances of sea sand, reduce the sea sand into the state of river sand before entering the sea, and can be safely used like river sand, so that the reinforcement corrosion and the deterioration of concrete are avoided.
Owner:XIAMEN ZHONGSHA TECH CO LTD

Method and system for wastewater treatment using in-situ cleaning of electrodes

A system for wastewater treatment employing in-situ cleaning of electrodes, comprising: at least one reactor for treating wastewater, said wastewater comprising chloride salts (sodium chloride, potassium chloride, calcium chloride, etc.) with a chloride concentration between 500 mg / L to 5,000 mg / L; and a controller for controlling the current supplied to the reactor by controlling the electrode active area and / or current density, such that the total amount of aqueous free chlorine produced during the wastewater treatment requires the addition of a certain amount of sodium bisulfite determined experimentally to produce a treated wastewater with a concentration of hydrochloric acid between 500 mg / L and 5,000 mg / L and a pH less than or equal to 4. After the addition of sodium bisulfite in the treated wastewater, the wastewater is recirculated back into the reactor. This ensures in-situ cleaning of the electrodes within the electrochemical reactor without the need for any additional equipment.
Owner:AXINE WATER TECH

An apparatus and method for preparing Ti3O5 powder materials

This application discloses an apparatus and method for preparing Ti3O5 powder materials. Belonging to the field of oxide functional powder material preparation technology, the method utilizes TiO2 powder as raw material, sodium chloride-potassium chloride-calcium chloride as electrolyte, zinc and / or tin as cathode, and a graphite rod as anode. A sandwich-type electrolysis system of "zinc-tin-TiO2 powder-chloride salt" is constructed through density differences to directly electrolyze TiO2 powder to prepare Ti3O5 powder materials. This apparatus and method significantly shorten the traditional Ti3O5 powder material preparation process, and the zinc-tin cathode and electrolyte can be reused, greatly reducing costs. The electrolysis process involves few side reactions, is environmentally friendly, and emits no harmful substances, resulting in high-purity Ti3O5 powder materials.
Owner:JIANGXI SILICON-BASED SCIENCE & TECHNOLOGY RESEARCH CO LTD +1

Method for preparing rare earth hydroxide from alkali metal hydroxide and recycling rare earth hydroxide

The invention discloses a method for preparing rare earth hydroxide from alkali metal hydroxide and recycling the rare earth hydroxide, which comprises the following steps: (1) mixing an alkali metal hydroxide solution and a rare earth chloride salt solution and reacting, after the reaction is finished, carrying out solid-liquid separation to obtain a precipitate and a mother solution, and washing the precipitate to obtain the rare earth hydroxide and a washing solution; (2) carrying out impurity removal and concentration on the mother liquor, and then electrolyzing to obtain an alkali metal hydroxide solution, Cl2 and H2; returning the obtained alkali metal hydroxide solution to the step (1), and recycling the alkali metal hydroxide solution as a precipitant; and (3) the Cl2 and H2 in the step (2) react to obtain hydrochloric acid, the hydrochloric acid is used for reverse extraction of the loaded organic phase to obtain a rare earth chloride salt solution, and the step (1) is returned. According to the method, the rare earth hydroxide can be obtained, and comprehensive recycling of the alkaline precipitant, the wastewater and the regenerated acid is realized.
Owner:BAOTOU RESEARCH INSTITUTE OF RARE EARTHS

A corrosion test method suitable for adapting the corrosion strength of a passenger car to the domestic environment

This invention discloses a corrosion testing method adapted to the corrosion intensity of domestic passenger vehicles in the field of automotive material corrosion evaluation technology. The method involves washing, wiping, drying, scratching, masking, and weighing the passenger vehicle sample before placing it in a cyclic corrosion test chamber. A composite corrosion solution is then prepared using deionized water, sodium chloride, calcium chloride dihydrate, magnesium chloride hexahydrate, anhydrous sodium sulfate, sodium nitrate, ammonium chloride, sodium bicarbonate, and iron-manganese-sulfur-nitrate-silicon complex corrosion-promoting microspheres. Subsequently, the sample undergoes a series of cyclic treatments including salt spray deposition, wet heat penetration, hot air drying, and room temperature rehumidification. The corrosion performance of the corroded sample is then tested. This invention can simulate the chloride salt, wet heat, and alternating wet-dry corrosion environments experienced by domestic passenger vehicles in service, improving the adaptability and discriminative power of corrosion intensity evaluation.
Owner:CARI AUTOMOBILE INSPECTION CENT (HULUN BUIR) CO LTD +1

Cement slurry for reinforcing and leaking stoppage in drilled hole and preparation method of cement slurry

The invention discloses cement slurry for reinforcing and leaking stoppage in a drilled hole and a preparation method of the cement slurry, and relates to the technical field of geological drilling engineering.The cement slurry is prepared from, by weight, 60-70 parts of sulphoaluminate cement, 20-30 parts of Portland cement, 3.5-5.5 parts of a composite early strength agent, 2-4 parts of an anti-freezing and anti-leakage agent and 0.3-0.5 part of a polycarboxylate superplasticizer. 0.1 to 0.2 part of polyacrylamide, and 18 to 22 parts of water; the composite early strength agent is a mixture of chlorine salt and calcium formate; the anti-freezing and anti-leakage agent is a mixture of glycerol and nano silica fume. The cement slurry has a very good leakage-proof plugging effect, solves the problem of slurry loss during leakage, is controllable in solidification time, low in maintenance energy consumption, free of external heating and complex heat preservation, controllable in heat release, and capable of avoiding local overheating cracking, avoiding the risk of slurry freezing in a low-temperature environment, and ensuring normal hydration.
Owner:SICHUAN HUAFENG DRILLING ENG CO LTD

Household garbage incineration fly ash mechanical separation resource utilization method

The invention discloses a mechanical separation and resource utilization method for household garbage incineration fly ash. The method comprises the following steps: firstly washing and separating the household garbage incineration fly ash, then pickling and separating, and respectively collecting a soluble salt-containing first liquid phase obtained by washing and separating, a lead-containing second liquid phase obtained by pickling and separating and dioxin-enriched solid-phase fly ash; mixing the second liquid phase with the first liquid phase to enable the pH value of the mixed solution to be 8-9, then adding sulfide to enable the sulfide to completely react with Pb < 2 + > in the mixed solution to generate PbS precipitate, and separating to obtain lead concentrate and a third liquid phase containing chlorine salt; calcium chloride, potassium chloride and sodium chloride are efficiently recycled from the third liquid phase based on nanofiltration and flotation separation, the content of the potassium chloride and the sodium chloride obtained through centrifugation reaches up to 99%, the potassium chloride and the sodium chloride can be used as industrial-grade products, and the overall resource utilization degree of the household garbage incineration fly ash can be improved.
Owner:SOUTH CHINA INST OF ENVIRONMENTAL SCI MEP

A method for preparing a hollow fiber composite membrane containing a cavity structure

This invention relates to a method for preparing membrane materials, specifically a method for preparing hollow fiber composite membranes containing void structures. Addressing the characteristics of hollow fiber carriers, this invention employs an organic phase solution flowing into the carrier for interfacial polymerization. To address the issue of chloride ion loss in the later stages of polymerization, chloride salts such as lithium chloride or sodium chloride are added to the organic phase solution. These chloride salts replenish the chloride ions lost during silver chloride synthesis and act as phase transfer agents to promote the interfacial polymerization reaction between the two phases, ensuring the compactness of the polyamide.
Owner:TAIZHOU HEYI NEW MATERIAL TECH CO LTD

Particulate food preservative composition

A particulate food preservative composition is disclosed, which comprises at least 60 wt. % of preservation granules having a diameter in the range of 150-1800 um, wherein the preservation granules are compacted agglomerates of: (a) particles containing at least 90 wt. % of the chloride salt and (b) particles containing at least 70 wt. % of the alkali metal salt of organic acid, said preservation granules comprising (i) at least 20 wt. % of chloride salt selected from sodium chloride, potassium chloride, magnesium chloride and combinations thereof; and (ii) at least 20 wt. % of an alkali metal salt of an organic acid selected from acetic acid, lactic acid, propionic acid and combinations thereof; the combination of the chloride salt and the alkali metal salt of an organic acid constituting at least 80 wt. % of the dry matter that is contained in the preservation granules. Methods of making the compositions is also disclosed.
Owner:PURAC BIOCHEM BV

Foundation bottom plate protection system and method in strong corrosion geological environment

A kind of foundation bottom plate protection system and method in strong corrosion geological environment, system includes foundation bottom plate, deep well cylinder, main pipeline, branch pipeline, pumping device, the foundation bottom plate is fixed on foundation by anti-floating anchor rod, the main pipeline is arranged in the foundation, the main pipeline both sides are evenly distributed with several branch pipelines, the branch pipeline top end is evenly distributed with water-permeable hole, one end of the main pipeline is closed, the other end is connected with deep well cylinder, the deep well cylinder is embedded in the soil of the structure to be built side, the top end of deep well cylinder is exposed to ground, the pumping device is connected with deep well cylinder, the deep well cylinder is equipped with the treatment mechanism for corrosive groundwater;Method includes forward treatment mode and reverse treatment mode.The application can improve the corrosion and waterproof effect by improving the foundation bottom plate structure, fundamentally avoid the erosion of building structure by high chloride salt and sulfate in geology.
Owner:CHINA STATE CONSTR ZHONGXIN CONSTR ENG CO LTD

Removal of sulfate from seawater

A method and system of providing seawater into a subterranean formation, including adding chloride salt having a metal cation to the seawater (having sulfate), precipitating sulfate salt (of the metal cation and sulfate), removing the sulfate salt as precipitated to give treated seawater having less sulfate than the seawater, and injecting the treated seawater into the subterranean formation.
Owner:SAUDI ARABIAN OIL CO