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3242 results about "Ethylenediamine" patented technology

Ethylenediamine (abbreviated as en when a ligand) is the organic compound with the formula C₂H₄(NH₂)₂. This colorless liquid with an ammonia-like odor is a strongly basic amine. It is a widely used building block in chemical synthesis, with approximately 500,000 tonnes produced in 1998. Ethylenediamine readily reacts with moisture in humid air to produce a corrosive, toxic and irritating mist, to which even short exposures can cause serious damage to health (see safety). Ethylenediamine is the first member of the so-called polyethylene amines.

Hot pepper and determining method for 96 pesticide residues in product of hot pepper

The invention discloses hot pepper and a determining method for 96 pesticide residues in a product of the hot pepper. The determining method comprises the following steps: homogenously extracting residual pesticide in a sample with 1% acetic acid-acetonitrile solution, purifying the extracting solution with a Florisil solid phase extraction column, dispersing and purifying the extracting solution with ethylenediamine-N-propyl silane (PSA) and octadecyl silane bonded phase (C18) substrate, detecting 69 pesticide residuals in the purified concentrated liquid of the Florisil column by GC-MS (gaschromatographic mass spectrometry), detecting 27 pesticide residuals in the substrate dispersed purified liquid by liquid chromatography-tandem mass spectrometry (LC-MS / MS), using the black substrate solution dilution standard to construct the updated calibration curves, adopting an internal standard method to quantify when using GC / MS to detect the residuals, and adopting an external standard method to quantify when using LC-MS / MS to detect the residuals. The average recovery rate of the method is 70.7-118.6%; the average relative standard deviation (RSD) is 3.2-11.4%; the detection limit is 0.13-28.2 ug / kg. The determining method has the advantages of simplicity and convenience in operation, high speed, accuracy, high sensitivity and good repeatability.

Method for synthesizing carboxyl butadiene-styrene latex used for cement group water-proofing material

This invention relates to a synthesis method for carboxylated styrene-butadiene latex used in the cement-based waterproof coating. The preparation method involves 30 to 50 shares of butadiene or isoprene isoprene, 30 to 55 shares of styrene, 0.1 to 5 shares of methyl acrylate , 1 to 5 shares of itaconic acid, 1 to 8 shares of n-butyl acrylate butyl acrylate, 1.2 to 2.8 hares of emulsifier, 0.3 to 1.2 hares of initiator potassium supersulphate, 0.2 to 0.8 shares of molecular weight regulator, 0.01 to 0.5 shares of pH buffer sodium bicarbonate, 0.01 to 5 shares of electrolyte, 0.01 or 5 shares of chelating agent ethylenediamine tetraacetic acid or endrate disodium and 100 to 150 shares of soft water for polymerization. The electrolyte is the combination of potassium phosphate and disodium hydrogen phosphate, with the ratio of 3 to 2: 1; in the polymerization reaction, monomer and a variety of agents are added with intermission. And reaction temperature control adopts the two-step laddered control. When the conversion rate reaches 99.0 percent, the mixture experiences the vacuum degassing treatment. The latex produced by the present invention is of good compatibility with the additives as the paint during the paint preparation. The prepared paint is of excellent fluidity, water retention and machinery stability under the high-cut condition. The improved mortar has the advantages of good permeability, high bond strength and so on.

Polyamide and amine hybridized nanosilicon dioxide hyperbranched polymer and preparation method thereof

The invention discloses a polyamide and amine hybridized nanosilicon dioxide hyperbranched polymer and a preparation method thereof. The preparation method of the polymer comprises the following steps of firstly, modifying the surface of nanosilicon dioxide by using a coupling agent; then, carrying out Michael addition reaction and amidation reaction on the modified nanosilicon dioxide by using ethylenediamine and methyl acrylate; finally, carrying out functional modification by using allyl glycidyl ether to obtain a functional polyamide and amine hybridized nanosilicon dioxide monomer, and initiating polymerization reaction on the functional polyamide and amine hybridized nanosilicon dioxide monomer, acrylamide, acrylic acid and a heat-resistant and salt-tolerant monomer by using a redox initiator or azobis(isobutylamidine) initiator. The hyperbranched polymer has a network structure with a polyamide and amine hybridized nanosilicon dioxide unit as a center, has excellent shear resistance, strong thickening property, heat resistance and salt tolerance, and is wide in adaptability and capable of being used as an oil displacement agent for increasing the recovery rate of raw oil in an oil field environment with a high mineralization degree and a wide temperature range; the preparation method of the polyamide and amine hybridized nanosilicon dioxide hyperbranched polymer is reliable in principle, simple and convenient to operate and wide in application prospect.

Hyper-branched polycarboxylate high-efficiency water reducing agent and preparation method thereof

The invention relates to a hyper-branched polycarboxylate high-efficiency water reducing agent and a preparation method thereof. The water reducing agent is prepared by polymerizing one of tert-butyl acrylate and methyl tert-butyl acrylate with sodium methyl-acryl sulfonate and allyl polyethenoxy ether to form a copolymer main chain, and then performing condensation polymerization on one of acrylic acid and methacrylic acid with ethylene diamine to form a hyper-branched polyamide structure which is grafted to two ends of the main chain. The preparation method comprises the following steps: (1) preparing the sodium methyl-acryl sulfonate into solution with DMF, and heating the solution in a nitrogen atmosphere; (2) dissolving the other two monomers and an initiating agent into the DMF to prepare mixed solution, and dripping the mixed solution into the step (1) to react for 1 to 20 hours; (3) adding a condensating agent CDI after the reaction and performing condensation reaction by using N-methyl morpholine as an organic base, the ethylene diamine and the acrylic acid as the monomers and the DMF as a solvent; and (4) performing vacuum distillation to remove the residual monomers and the solvent, and refluxing for 2 to 5 hours by using methylene chloride solution of trifluoroacetic acid to obtain the water reducing agent. The hyper-branched polycarboxylate water reducing agent has the advantages of low admixture, high water reducing rate, small slump loss, good compatibility with cement, no corrosivity to steel bars, strong frost resistance and the like.
Owner:厦门路桥翔通建材科技有限公司 +1

Preparation method of nitrogen-doped graphene-loaded metal monatomic catalysts

Disclosed is a preparation method of nitrogen-doped graphene-loaded metal single atom catalysts. As a compounding agent, ethylenediamine tetraacetic acid disodium salt is subjected to an ion exchange reaction with metal ions in liquid phases to form a stable compound, the compound is fully and evenly mixed with alkali metal salt after drying by distillation, and the nitrogen-doped graphene-loaded metal single atom catalysts are obtained through simultaneous pyrolysis conversion. The prepared catalysts have the appearance characteristics of two-dimensional microstructures which are super-thin and large in area, the thickness is 0.5-2 nm, the number of graphene layers is 1-8, the metal load is within 0.01-10 wt%, and the catalysts can be applied to the field of catalysis synthesis of energy, catalysis, medicine and biology. The method can be widely applied to the synthesis of various metal single atom catalysts, obtained metal single atoms can all be firmly riveted on the surface of graphene, the load amount is high, and the thermal stability is good. The method has the advantages of being simple and safe in operation process, low in cost, controllable to prepare, large in synthesis amount, suitable for industrialized production and large-scale application and the like.
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