216 results about "Butanone" patented technology

The invention discloses a colorful acid and alkali resistant laser printing ink and a preparation method thereof. The printing ink is composed of the following components in parts by weight: 0 to 30 parts of butanone, 10 to 30 parts of isopropanol, 2 to 6 parts of curing agent, 10 to 15 parts of pigment, and 10 to 30 parts of glycidyl ether epoxy resin. The glycidyl ether epoxy resin is adopted to produce the printing ink, aliphatic polyamine is further chosen as the curing agent, the acid and alkali resistant performance of the printing ink is strengthened through optimizing the formula, thus the shortage that the colorful laser printing ink is lost when being mixed with acid and alkali is overcome, moreover, the color of the laser printing product is more abundant, and the patterns are more clear.

The invention discloses an insulating tape for a new energy battery and a preparation method of the insulating tape, and relates to the technical field of new energy battery assemblies. The insulating tape for the new energy battery is prepared by coating pretreated glass fiber cloth with a coating, the coating is prepared from the following raw materials in parts by weight: 15 to 20 parts of modified polyimide resin, 2 to 4 parts of epoxy resin E-51, 71 to 77 parts of an ethanol / butanone mixed solvent, 3 to 5 parts of modified nano silicon dioxide, 0.2 to 0.4 part of a silane coupling agent KH-550, 0.1 to 0.3 part of polydimethylsiloxane, 0.1 to 0.2 part of paraffin-based mineral oil and 0.3 to 0.5 part of triethylene tetramine. The glass fiber cloth pretreatment material comprises deionized water and a 5%-8% sodium hydroxide solution. The insulating adhesive tape for the new energy battery contains the modified polyimide resin, so that the high temperature resistance and electrolyte resistance of the adhesive tape can be enhanced, the insulativity is improved, and the modified nano silicon dioxide is good in dispersity. The preparation process is fine, the glass fiber cloth is fully pretreated, the preparation process is standard, and the use requirements of new energy batteries can be met.

The invention provides a high-hydrophobicity anti-pollution flashover coating and a preparation method thereof, and relates to the field of coatings. The silicone rubber composition is prepared from the following raw materials in parts by weight: 80 to 100 parts of hydroxyl-terminated polydimethylsiloxane; 5 to 15 parts of modified nano silicon dioxide; 10 to 30 parts of a composite self-repairing microcapsule; 10 to 25 parts of a flame retardant; 3-8 parts of a cross-linking agent; 0.5-2 parts of a catalyst; 1-5 parts of an accelerant; 40 to 100 parts of a solvent; the modified nano silicon dioxide is fumed silica subjected to surface treatment by a fluorine-containing silane coupling agent and a platinum catalyst; the capsule wall of the composite self-repairing microcapsule is a polylactic acid-glycolic acid copolymer, and the capsule core of the composite self-repairing microcapsule is a mixed solution of a hydroxyl-terminated polydimethylsiloxane oligomer and methyltris (methylethylketoximino) silane. The coating has excellent hydrophobicity, weather resistance and targeted repair function.

The invention discloses an optical paste film and a preparation method thereof, and relates to the technical field of optical functional materials. The optical slurry film is prepared by taking a polyethylene glycol terephthalate film as a base material and coating an optical slurry coating, the optical slurry coating is prepared from the following raw materials in parts by weight: 12 to 16 parts of nano silicon dioxide, 22 to 28 parts of acetone and butanone mixed solvent, 7 to 9 parts of modified titanium dioxide, 4 to 6 parts of nano zirconium oxide, 30 to 35 parts of modified epoxy resin, 18 to 22 parts of butyl acrylate, 4 to 6 parts of dioctyl sebacate, 2.5 to 3.5 parts of silane coupling agent KH-570, 1 to 1.5 parts of organic silicon flatting agent and 0.6 to 1 part of organic silicon defoaming agent. 1.2-1.8 parts of an antioxidant 1010, 3-4 parts of a photoinitiator 184 and 6-8 parts of bis (4-tert-butylphenyl) iodine hexafluorophosphate; the polyethylene glycol terephthalate film pretreatment material comprises absolute ethyl alcohol and deionized water. The raw materials are scientifically proportioned, the titanium dioxide and the epoxy resin are clearly modified, the preparation process is complete, and the finished product is high in light transmittance, good in weather resistance, adaptive to the requirements of the optical field and high in practicability.

The invention relates to the technical field of bolts, and provides a bolt special for stainless steel mechanical equipment and a preparation method thereof. A bolt special for stainless steel mechanical equipment comprises a bolt body and a surface coating, and the surface coating is prepared from, by weight, 100 parts of epoxy resin E-44, 50-55 parts of a curing agent, 1.5-2 parts of a curing accelerator, 20-25 parts of flaky iron oxide, 10-12 parts of modified boron nitride, 2-3 parts of an ultraviolet light absorber, 3-5 parts of silicon dioxide, 1-1.5 parts of a dispersing agent, 25-35 parts of butanone and 10-12 parts of xylene. According to the bolt special for the stainless steel mechanical equipment, the corrosion resistance of the stainless steel bolt in a high-concentration acid-base solution and high-temperature and high-pressure seawater is improved.

An antifungal composition including a first essential oil, and a second essential oil, where the composition is configured to reduce disease onset, pathogen spread, or a combination thereof. Further, an antifungal compound including one or more aroma compounds selected from 4-(4-hydroxyphenyl)-2-butanone, furaneol, ethyl methylphenylglycidate, ethyl hexanoate, ethyl butanoate, beta-ionone, alpha-ionone, (R)-(+)-limonene, (S)-(-)-limonene, cis-3-Hexen-1-ol, nerol, linalool, 2-heptanone, alpha-terpineol, beta-damascenone, β-caryophyllene, ethyl 2-methylbutanoate, β-myrcene, gamma-octalactone, alpha-humulene, nerolidol, (E,E)-2,4-decadienal, (E,E)-α-farnesene, vanillin, phenylethyl acetate, citral, 3-methylbutan-1-ol, or a combination thereof.

The invention relates to the technical field of high polymer materials, and particularly discloses a flame-retardant heat-conducting silica gel insulating coating and a preparation method thereof. The invention discloses a flame-retardant heat-conducting silica gel insulating coating. Comprising the following components: polydimethylsiloxane, aluminum hydroxide, modified nano aluminum oxide, a phosphorus-nitrogen flame retardant, silicon dioxide, methyltris (methylethylketoxime) silane, vinyltris (methylethylketoxime) silane, dibutyltin dilaurate, a diluent, amino propyl triethoxy silane, propyl trimethoxy silane and ethyl aminopropyl trimethoxy silane. And the polydimethylsiloxane is formed by compounding polydimethylsiloxane with the viscosity of 1,500 cp and polydimethylsiloxane with the viscosity of 20,000 cp. According to the invention, by finely blending the proportion of various functional components, especially the optimal combination of polydimethylsiloxane, modified nano aluminum oxide, the flame retardant and the filler, the flame retardance and thermal conductivity of the coating are effectively improved, and meanwhile, good insulativity and mechanical properties are ensured.

The preparation method comprises the following steps: S1, hydrophilic-hydrophobic bi-component modification reaction: dissolving a styrene-maleic anhydride copolymer, hydrophilic polyethylene glycol monomethyl ether and hydrophobic long-chain alkyl alcohol in butanone according to a ratio, adding a catalyst, stirring, reacting, filtering, washing, and drying to obtain the dispersing agent for the lithium battery diaphragm based on the modified benzyl resin micelle. Performing ester exchange reaction on anhydride bonds of the styrene-maleic anhydride copolymer and polyether hydroxyl and alkyl alcohol hydroxyl respectively to obtain a modified intermediate; s2, neutralization reaction: dropwise adding organic alkali into the modified intermediate, and adjusting the pH value to obtain a modified SMA solution containing carboxylate groups; s3, preparing nano-micelles: dropwise adding the modified SMA solution into deionized water, and stirring to enable the modified SMA solution to be self-assembled to form the nano-micelles, so as to obtain nano-micelle dispersion liquid; and S4, dispersing agent forming: stirring the nano-micelle dispersion liquid to remove butanone so as to obtain the water-based dispersing agent.

This invention discloses a production process for sulfur dioxide-resistant electroplated aluminum and the resulting electroplated aluminum, relating to the field of electroplated aluminum. The production process for sulfur dioxide-resistant electroplated aluminum includes: coating a release coating onto a base film layer to obtain a release layer; coating an imaging coating onto the release layer to obtain a color layer; molding and aluminum plating the color layer to obtain an aluminum-plated layer; and coating the aluminum-plated layer with an adhesive to obtain electroplated aluminum. The imaging coating comprises the following raw materials in parts by weight: 80-100 parts of modified monomeric acrylic polymer, 7-10 parts of isocyanate curing agent, 3-6 parts of highly branched semi-crosslinked polyurethane prepolymer, 0.8-1.5 parts of dispersant, 0.2-0.5 parts of defoamer, 35-50 parts of methyl ethyl ketone (MEK), and 35-50 parts of pentamidine ketone (PHK). The highly branched semi-crosslinked polyurethane prepolymer has a molecular weight of 110,000-120,000 and a softening point temperature of 220-240°C. This application provides electroplated aluminum resistant to sulfur dioxide corrosion.

The application belongs to the technical field of medicine synthesis, and particularly relates to a preparation method of methoxychlorpromazine monohydrochloride monohydrate. The method comprises the following steps: step 1, methoxychlorpromazine base is dissolved in a polar solvent, and hydrochloric acid is added to obtain a mixed solution; step 2, a poor solvent of methoxychlorpromazine monohydrochloride monohydrate is added to the mixed solution, crystallization is carried out, and separation is performed, and methoxychlorpromazine monohydrochloride monohydrate is obtained; the poor solvent is selected from one or a mixture of two or more of isopropyl alcohol, n-butyl alcohol, acetone, butanone, ethyl acetate, butyl acetate, dichloromethane, trichloromethane, toluene, methyl tert-butyl ether, isopropyl ether and diethyl ether. The method has the advantages of simple process, good repeatability, easy operation, high yield, product purity of more than 99.8%, complete compliance with the requirements of European Pharmacopoeia 9.0 and US Pharmacopoeia USP43, and suitability for industrial production.

The invention provides yellow glue resistant to corrosion of a plasticizer and a preparation method of the yellow glue. The yellow glue is prepared from a polyurethane prepolymer, a chloroprene rubber sheet, methyl methacrylate, benzoyl peroxide, an anti-aging agent, butanone, cyclohexane, dimethyl carbonate and tackifying resin. The polyurethane prepolymer is prepared from the following components in parts by weight: 10 to 14 parts of 1, 4-butanediol adipic acid polyester polyol, 4 to 8 parts of polycaprolactone polyol, 1 to 3 parts of diphenylmethane diisocyanate, 0.05 to 0.15 part of 1, 6-hexanediol, 1 to 2 parts of hydroxyethyl methacrylate, 0.01 to 0.03 part of organic bismuth catalyst and 75 to 80 parts of butanone. The polyurethane prepolymer with specific crystallization performance is synthesized through cooperation of polycaprolactone polyol and polyester polyol, and the yellow glue is endowed with excellent plasticizer corrosion resistance and low-temperature activation capacity. Active groups in the polyurethane prepolymer are subjected to graft copolymerization with the chloroprene rubber adhesive and MMA, and a plasticizer-resistant polyurethane chain segment is introduced into a molecular chain of the chloroprene rubber adhesive, so that a hard segment-soft segment alternating block structure is formed, and corrosion resistance and viscoelasticity are both considered.

The application discloses a kind of efficient natamycin purification methods, comprising the following steps: taking two kinds of dichloromethane, chloroform, acetone, butanone, methanol, ethanol, petroleum ether, n-hexane are mixed to obtain mixed solution, adjust the pH of mixed solution to 6.0-7.0, then natamycin crude product is added to mixed solution and stirred into slurry;Slurry is extracted to obtain that natamycin wet product, and the natamycin wet product after extraction is washed with organic solvent;Natamycin wet product after washing is dried, and natamycin purification product is obtained.Compared with prior art, the present application optimizes the existing natamycin purification process, simplifies the natamycin purification method, reduces the production cost, improves the production efficiency, the product purity can reach more than 98%, and the product yield can reach more than 95%.The application has the advantages of less equipment investment, easy operation, less environmental pollution, simple operation, and is suitable for product industrial production.

The specification describes a process for the upgrading of ketones, comprising the step of reacting a ketone and hydrogen together in the presence of a catalyst system comprising either a condensation catalyst and a separate hydrogenation catalyst, or a condensation catalyst on which a transition metal is supported. The condensation catalyst is a mixed oxide material comprising aluminium, calcium and optionally magnesium, and has a Ca:(Mg+Al) weight ratio of 0.25 ≤ Ca:(Mg+Al) ≤ 2.5 and a Mg:Al weight ratio of 0 ≤ Mg:Al ≤ 3.0. The process is particularly suitable for the upgrading C3, C4 or C5 ketones such as acetone or butanone.

The invention discloses aquadag for an alkaline battery and application of the aquadag. The aquadag comprises the following raw materials in percentage by weight: 12-16% of graphite powder, 5-8% of conductive carbon black, 1-2% of graphene, 15-18% of epoxy resin, 30-50% of butanone and 10-20% of cyclohexanone. The preparation method of the aquadag comprises the following steps: (1) uniformly stirring butanone and cyclohexanone to obtain a composite solvent; (2) adding solid epoxy resin into the composite solvent, and stirring at 800-1000 rpm to completely dissolve the solid epoxy resin; (3) slowly adding graphite powder and conductive carbon black graphene into the composite solvent, and dispersing at a high speed of 1100-1200 rpm for 45-50 min to obtain a mixture; and (4) carrying out ball milling on the mixture, sieving with a 200-mesh sieve, and discharging to obtain the aquadag. The graphene is doped into the aquadag, so that the technical effect of improving the comprehensive performance of the battery is achieved.

The invention discloses a preparation method of liquid aliphatic secondary amine, which comprises the following steps: 1, carrying out reductive alkylation reaction on aliphatic secondary amine, 3, 3-dimethyl-2-butanone and hydrogen under the action of a platinum-carbon catalyst and a sulfur-containing organic matter; and 2, filtering the reaction mixture, and carrying out vacuum distillation to obtain the target product. According to the method, hydrogen is used as a reducing agent, the process is green and environment-friendly, side reactions are few, and the purity of the prepared aliphatic secondary amine can reach 98% or above. The preparation method comprises the following steps: dissolving trace dimethyl sulfoxide in an ethanol solution to form a dimethyl sulfoxide-ethanol dispersion mixed solution, adding the dimethyl sulfoxide-ethanol dispersion mixed solution into a high-pressure hydrogenation reaction kettle, fully mixing the dimethyl sulfoxide-ethanol dispersion mixed solution with an obtained imine mixture, and adding a platinum-carbon catalyst. The preparation method of the liquid aliphatic secondary amine, which is disclosed by the invention, has the advantages of high catalyst selectivity and strong activity, and is suitable for producing the liquid aliphatic secondary amine.

The invention relates to an electrochemical selective oxidation method of butanone, which is carried out in an electrolysis system and specifically comprises the following steps: (1) an anode chamber of the electrolysis system comprises an anode electrolyte and an anode electrode, and the surface of the anode electrode comprises an anode catalyst; and (2) mixed gas of O2 and butanone is introduced into a cathode chamber of the electrolysis system, two-electron redox reaction is carried out on the surface of a cathode catalyst of a cathode electrode to reduce O2 into H2O2, the generated H2O2 and butanone react on the interface of the cathode catalyst, a target organic compound is selectively generated, and the cathode catalyst comprises a carbon-based material. The invention aims to solve the three core problems of poor selectivity, serious pollution and low safety in the traditional butanone oxidation process, and compared with the traditional strong oxidation process, the method adopts an electrochemical synthesis path, takes electrons as a cleaning reagent, realizes high-precision selective control on the butanone oxidation path, can directionally generate a high-value product, and has the advantages of high product yield and high product quality. And the problems of complex product and difficult separation in the traditional process are fundamentally avoided.

This invention discloses a method for preparing epoxy binder-coated modified magnetic powder, comprising 90-95 wt% modified magnetic powder and 5-10 wt% epoxy binder. The epoxy binder is diluted uniformly with methyl ethyl ketone (MEK) as a diluent, and the volume ratio of MEK to epoxy binder is 10-20. After uniform mixing, the modified magnetic powder is added, and mixing continues while maintaining a stirring temperature of 50-60℃ for 2-4 hours. The mixture is then sieved through a 300-500 mesh nylon sieve to obtain epoxy binder-coated modified magnetic powder. This invention utilizes a two-step coupling agent to modify the magnetic powder, enabling the modified magnetic powder and porous chitosan fine powder to form a good bond and fix within the porous structure, resulting in magnetic powder with low agglomeration, good dispersibility, and good insulation effect, thus meeting the purpose of inductor production and use. The product obtained by this invention has high resistivity and low loss.

The application discloses a kind of biological base alcohol type beauty glue and preparation method thereof, it is related to adhesive technical field.The raw material composition of the beauty glue includes biological base polysiloxane, nano zinc oxide, biological base composite mildew inhibitor, hydrophobic fumed silica, titanium acid tetraisopropyl ester, methyl tributyl ketone oxime base silane, nano calcium carbonate, epoxy soybean oil, tea polyphenol;The biological base polysiloxane: raw material includes biological base 1,3-propylene glycol, hydroxyl end-capped polydimethylsiloxane, silane coupling agent;The biological base composite mildew inhibitor: raw material includes lecithin, epsilon-polylysine, tea tree oil, vitamin E.The preparation method of beauty glue includes preparing biological base polysiloxane, preparing biological base composite mildew inhibitor, basic filler dispersion, and preparing beauty glue finished product step.The biological base alcohol type beauty glue prepared in the application has good mildew-proof effect and excellent mechanical properties.

The present application relates to a kind of bio-based surface treatment agent and its preparation method, belong to the technical field of treating agent.The raw material of bio-based surface treatment agent provided by the present application includes polyol PE-6056, isocyanate XFLO100, catalyst, CHDI, anti-sedimentation auxiliary agent, solvent, the solvent includes butanone, tetrahydrofuran, acetone, dimethylformamide, cyclohexanone, the bio-based surface treatment agent prepared has good initial adhesion, peeling strength when using, hydrolysis resistance and ageing resistance, with good application prospect.

The invention discloses a synthesis method of a silicon-substituted benzo-bicyclo [3.1. 1] heptane compound, which comprises the following steps: under the action of a copper catalyst, alkali and a silicon reagent, putting o-alkynyl phenyl cyclobutanone in a solvent for reaction, and carrying out post-treatment to obtain the silicon-substituted benzo-bicyclo [3.1. 1] heptane compound, the silicon source is (dimethylphenylsilyl) boronic acid pinacol ester. The silicon-substituted benzo-bicyclo [3.1. 1] heptane compound is prepared by combining a cheap metal copper catalyst with a silicon reagent. The reaction system is good in selectivity and mild in condition, the highest yield can reach 68%, and the method has wide application prospects.

The invention provides a damp-heat aging resistant three-layer waterproof adhesive tape as well as a preparation method and application thereof, and belongs to the technical field of waterproof adhesive tapes. The waterproof screen cloth comprises a screen cloth layer and a waterproof layer which are bonded through a bonding adhesive, the waterproof layer is coated with the TPU hot melt adhesive layer; the laminating glue comprises the following components in parts by weight: 95-105 parts of PU glue, 4-6 parts of precipitated silica, 8-12 parts of an isocyanate curing agent and 60-70 parts of butanone; the TPU hot melt adhesive layer is prepared from the following components in parts by weight: 45 to 60 parts of polyester polyol, 10 to 20 parts of polyether polyol, 20 to 25 parts of diphenylmethane diisocyanate (MDI), 5 to 10 parts of chain extender and the like. The adhesive tape solves the problems that the existing adhesive tape is poor in damp-heat aging resistance and the adhesive strength is easy to decrease by improving the formula of the laminating adhesive of the mesh cloth layer and the waterproof layer and the formula of the TPU hot melt adhesive layer, and has excellent damp-heat aging resistance, stable waterproofness and lasting adhesive strength.

This invention discloses a bicyclic [2.1.1]hexene compound and its preparation and application. The invention uses bicyclic [1.1.0]butanone and phosphate ester as starting materials, and potassium tert-butoxide tetrahydrofuran solution as base. The reaction is carried out under reflux at 80°C to obtain the bicyclic [2.1.1]hexene compound. The prepared compound has certain transpeptidase inhibitory activity and can effectively inhibit the infection and spread of Staphylococcus aureus.

The invention discloses a low-VOC (volatile organic compound) environment-friendly foaming PVC (polyvinyl chloride) profile and a preparation method, and relates to the technical field of building plastic profiles, the profile faces door and window joints in contact with silicone sealants (acetic acid type and oxime type) and polyurethane foaming agents, the profile adopts a three-layer structure: a surface layer is a sol-gel silica anti-infiltration layer; the near surface is a reaction-adsorption transition layer and contains beta-cyclodextrin grafted aminated silicon dioxide, zinc ion exchange zeolite and epoxy polyhedral oligomeric silsesquioxane; the foam core is a low-source foaming system and is matched with low-migration plasticizing lubrication; external acetic acid, oxime and tertiary amine are subjected to peak clipping and in-situ fixation in a epidermis-foam core transition zone through side feeding directional enrichment and plasma coating; under the conditions of ISO 16000-9 and VDA278, delta TVOC is less than or equal to 30 mu g / m, acetic acid, diacetylmonoxime and tertiary amine are reduced by more than or equal to 80%, more than or equal to 75% and more than or equal to 70%, and the adhesion and atomization performance is kept.

The invention discloses a method for purifying methyl isobutyrylacetate, which comprises the following steps of: introducing a concentrated material obtained at the front end into the middle part of a continuous rectifying tower T1 for rectifying to obtain light components at the top of the tower, and removing dichloromethane, methanol and 3-methyl-2-butanone; a tower kettle substrate of the continuous rectifying tower T1 enters the middle part of a continuous rectifying tower T2 to be rectified, and diethyl methyl ester with the purity of 90% is obtained at the tower top; a tower kettle substrate of the continuous rectifying tower T2 enters the middle part of a continuous rectifying tower T3 to be rectified, and an isobutyryl methyl acetate product is produced at the tower top; the method has the advantages that the methyl isobutyrylacetate is purified by adopting a continuous rectification method, and rectification parameters are optimized, so that the yield of the methyl isobutyrylacetate can reach 85% or above under the condition that the purity of the methyl isobutyrylacetate is not lower than 99%; and the continuous rectification is continuous feeding and continuous extraction, the retention time is short, and the energy consumption is low.

The application discloses a method for improving the separation yield of pseudo-isomethyl ionone, which comprises the following steps: condensation reaction of butanone and citral in a solvent under the action of an alkaline catalyst; after neutralization of the reaction solution, part of the solvent and unreacted raw materials are removed through a first desolventizing tower; the material in the first desolventizing tower is mixed with water and then enters a second desolventizing tower; and the liquid in the second desolventizing tower enters an oil-water separation tank to obtain a crude pseudo-isomethyl ionone product and waste brine. The method adopts double-tower continuous separation to remove the reaction solvent of pseudo-isomethyl ionone, and water is added between the two towers, so that water washing and salt removal are realized during the separation, and the separation yield of the crude product is greater than 99%. The method is simple in operation and is an economical separation method of pseudo-isomethyl ionone.

The application discloses a use method and application of a vegetable bud inhibition agent, and belongs to the technical field of plant body or local preservation and plant growth regulator. The application uses furan sulfide compounds as a bud inhibition agent to perform fumigation treatment on rhizome vegetables, so that the bud inhibition effect of the rhizome vegetables can be effectively delayed. The product has good bud inhibition effect, and the bud inhibition effect is comparable to that of 3-decene-2-butanone and menthol essential oil which are commercially used. The method has low bud inhibition cost, and can be used as a green alternative technology of traditional fumigation agents such as chloranil. The furan sulfide compounds as active ingredients are commonly used as food essence and spices, belong to food additives, and are widely applied in the food industry, are safe to use, simple to operate and low in cost.

This invention belongs to the field of soluble dietary fiber, specifically relating to a method for preparing soluble dietary fiber through solid-state fermentation of wheat bran. The invention uses wheat bran, *Zygosporum tobira*, auxiliary carbon source, nitrogen source, and inorganic salts for solid-state fermentation, ultrasonic extraction, centrifugation, low-temperature settling, filtration, and drying to obtain soluble dietary fiber. This invention is based on the nucleophilic addition between a thiol group (R-SH) and an amino group (R-NH2). In the reaction, the sulfur atom of the thiol group attacks the nitrogen atom of the amino group, forming a C-S bond and nitrogen (N2) molecules, while simultaneously releasing hydrogen ions (H+). + Because 3-mercapto-2-butanone gas contains ketone groups, the soluble dietary fiber containing butanone groups produced after reacting with amino groups has a unique aroma. This aroma can improve the taste of dietary fiber, making it easier to eat and more palatable.

The invention relates to a preparation method of tetramethylpyrazine, which is characterized in that 3-hydroxy-2-butanone and ammonium acetate are used as raw materials, a potassium hydrogen persulfate compound (Oxone) is used as an oxidizing agent, and 2, 3, 5, 6-tetramethylpyrazine is prepared through reaction. The preparation method has the beneficial effects that the reaction is rapid, the condition is mild, an organic solvent is not needed, and industrial popularization is easy; the color of a reaction system solution in the reaction process is light, and the reaction solution can be used mechanically, so that the green, environment-friendly and safe production and purification processes of the product are realized; the prepared product can be directly obtained in a filtering mode, and the product is high in purity, good in appearance, high in yield and suitable for one-pot production.

The invention relates to the technical field of butanone-water azeotropic system separation, in particular to a method for separating butanone from a butanone-water azeotropic system. According to the method for separating butanone from the butanone and water azeotropic system, a device is used for separation, and the device comprises an extractive distillation tower, an extraction agent recovery tower and a water-extraction agent separation tower. According to the method, p-xylene is taken as an extraction agent, butanone in a butanone and water azeotropic system is extracted by an extractive distillation tower, and a butanone-p-xylene mixture and a water-p-xylene mixture are obtained. The butanone-p-xylene soluble mixture is rectified and separated into butanone and p-xylene through an extractant recovery tower. And rectifying and separating the water-p-xylene solution mixture into water and p-xylene through a water-extractant separation tower. The extracting agent disclosed by the invention has the advantages of low intersolubility with water and high selectivity to butanone, is low in extracting agent residue and stable in separation effect, and has a good application prospect in separation of a butanone-water azeotropic system.

The present disclosure provides a ketoreductase mutant having activity on both (R)-(-)-1,3-butanediol and (S)-(-)-1,3-butanediol, and a computational design method for obtaining the mutant. The ketoreductase mutant disclosed in the present application can catalyze the reaction of racemic 1,3-butanediol to synthesize 4-hydroxy-2-butanone, which has good industrial application value.