622 results about "Acetaldehyde" patented technology

The invention discloses a medicinal and edible anti-alcoholism composition and a preparation method thereof, and relates to the crossing field of biotechnology and food and medicine, the composition comprises the following components: dried orange peel powder, vitamin C, glutathione, phellinus igniarius extract, polygonatum sibiricum extract, oriental wormwood extract, isatis root extract, schisandra chinensis extract, ginseng powder, lucid ganoderma extract and licorice extract. Silymarin, puerarin, white tomato powder, watermelon powder, fucoidin, tomato powder, mung bean powder, celery powder, turmeric powder, hawthorn fruit powder, honey powder, corn peptide, soybean peptide powder, xanthan gum and stevioside are added. The composition provided by the invention has the effect of increasing the content of ethanol dehydrogenase and acetaldehyde dehydrogenase in blood after drinking, and has the capability of promoting alcohol metabolism.

The invention discloses an aldehyde reductase mutant and application thereof in synthesis of a dexmethylphenidate hydrochloride intermediate, and belongs to the field of molecular biology and enzyme engineering. The aldehyde reductase mutant, polynucleotide for coding the mutant, and the recombinant expression vector can express the aldehyde reductase mutant and are used for constructing a recombinant cell or a recombinant strain for expressing the aldehyde reductase mutant. The provided aldehyde reductase mutant can catalyze 2-phenyl-2-((R)-piperidine-2)-acetaldehyde into (R)-2-phenyl-2-((R)-piperidine-2)-1-ethanol, especially improves the stereoselectivity of (R)-2-phenyl-2-((R)-piperidine-2)-1-ethanol, solves the problems of strict conditions, complex reaction and high cost in the existing synthesis method, and has a wide application prospect in the field of synthesis of (R)-2-phenyl-2-((R)-piperidine-2)-1-ethanol. Wide application prospects are realized.

The invention relates to a plant lactobacillus with effects of dispelling effects of alcohol, protecting the liver and restoring consciousness and application of the plant lactobacillus. The plant lactobacillus is a plant lactobacillus BGI-J9 strain, and the preservation number of the plant lactobacillus is CCTCC NO: M 20242630. The invention further discloses a preparation method of the plant lactobacillus with the effects of dispelling effects of alcohol, protecting the liver and restoring consciousness and application of the plant lactobacillus with the effects of dispelling effects of alcohol, protecting the liver and restoring consciousness. The strain has excellent tolerance to gastric acid, intestinal juice and cholate in a gastrointestinal tract system, can survive in the gastrointestinal tract, and provides a basis for continuously playing a probiotic effect; the compound has excellent inhibition capability on common intestinal pathogens; free radicals can be removed, and oxidative damage to the body is reduced; good alcohol metabolism enzyme synthesis capability and alcohol metabolism promoting potential are realized; the strain also has an excellent improvement effect on alcohol-damaged mice, specifically, the metabolism of ethanol and acetaldehyde in a body is accelerated, the occurrence time of drunkenness is obviously delayed, and the sobering time is shortened; intestinal injury and systemic inflammation caused by alcohol are improved; liver oxidative stress caused by alcohol is improved, and the occurrence and development process of alcoholic fatty liver is delayed; and cognitive function impairment caused by alcohol is improved.

The invention discloses application of a supported heterogeneous catalyst of oxide and copper-manganese spinel in preparation of acetaldehyde by anaerobic dehydrogenation of ethanol, and belongs to the technical field of heterogeneous catalysis for preparation of acetaldehyde and hydrogen by anaerobic dehydrogenation of ethanol. The reaction is carried out in a fixed bed reactor, under the conditions that the reaction atmosphere is nitrogen, the reaction temperature is 280 DEG C and the mass space velocity is 66.1 h <-1 >, the ethanol conversion rate is 72.5%, the acetaldehyde selectivity is 95.0%, and the space time yield of acetaldehyde based on the copper-manganese composite oxide is 43.5 h <-1 >, so that high-selectivity preparation of acetaldehyde and hydrogen under relatively mild conditions is realized; the system has the remarkable advantages of simple catalyst preparation, high catalytic activity under the condition of high mass airspeed, high space-time yield of acetaldehyde, high atom utilization rate of the system, good stability and the like. The CuMnTi-1 catalyst can be stabilized for more than 70 hours, the CuMnTi-1 improves the utilization rate of copper and manganese, improves the catalytic performance, reduces the demand quantity of copper-manganese spinel in the reaction, and reduces the overall cost of catalyst preparation.

The invention discloses yoghurt oil with fruity flavor and a preparation method of the yoghurt oil, and belongs to the technical field of yoghurt oil processing. The Lactococcus lactis SITRS-0011 provided by the invention can be independently used as a leavening agent, when the Lactococcus lactis SITRS-0011 is used for fermenting yoghurt oil, the titration acidity can reach 83.21 DEG T, the yoghurt oil contains 2, 3-butanedione (1180 [mu] g / kg), acetoin (2092 [mu] g / kg), lactones (623 [mu] g / kg), 3-methylbutyraldehyde (117 [mu] g / kg), phenethyl alcohol (1863 [mu] g / kg), phenylacetaldehyde (336 [mu] g / kg) and other substances, and the Lactococcus lactis SITRS-0011 is rich in milk flavor, has flower fragrance and nut flavor, is unique in flavor, and can be used for preparing the and the overall sensory score is high.

To provide a food quality preservative enabling further reduction of acetaldehyde concentration in a food packaging body.SOLUTION: A food quality preservative is used, the preservative comprising at least an ethanol vapor-releasing body, an oxygen absorber, and an aminooxyalkyl group-containing polysiloxane having a structural unit represented by the following general formula (1). [In the formula, R independently represents an alkyl group having 1 to 4 carbon atoms, an alkoxy group having 1 to 4 carbon atoms, or a hydroxyl group. The alkyl group may have an amino group (-NH2) at any position. Q independently represents a divalent organic group having 1 to 20 carbon atoms. n represents a real number of 0 to 100].SELECTED DRAWING: None

The invention discloses a high-ammonia-nitrogen wastewater treatment process, and belongs to the technical field of pyridine wastewater treatment, and the high-ammonia-nitrogen wastewater treatment process comprises the following steps: preparing hydrotalcite: weighing cobalt nitrate, magnesium nitrate and aluminum nitrate, adding distilled water, and stirring to obtain a salt solution; weighing sodium hydroxide and anhydrous sodium carbonate, adding distilled water, and stirring to obtain alkali liquor; pumping the salt solution and the alkali solution into a round-bottom flask, and heating and dispersing the round-bottom flask on an oil bath pan; putting the ground sample into a ceramic crucible, calcining in a muffle furnace, weighing a silver-ammonia solution and acetaldehyde, and pouring into a round-bottom flask; the pyridine wastewater is weighed, the hydrotalcite is added, stirring adsorption is performed for 20 min, the hydrogen peroxide is added, suction filtration is performed after the reaction, and the hydrotalcite is filtered and separated out for recycling. The problem that existing wastewater treatment is difficult is solved. The method has the advantages of high catalytic activity, easiness in recovery and reutilization of hydrotalcite, no need of adding any auxiliary chemical reagent, mild reaction conditions, low cost and convenience in operation, and can meet the requirements of industrial production.

The present application provides a kind of for the preparation of C 3+ The application discloses a catalyst for olefin, a preparation method and application, the catalyst is supported by a molecular sieve, and the molecular sieve is MFI molecular sieve or SBA-16 molecular sieve, and the catalyst is loaded with multi-metal, and the multi-metal includes metal tungsten, transition metal and alkali metal. The catalyst is used for providing Lewis acid sites by introducing metal tungsten into MFI molecular sieve or SBA-16 molecular sieve by one-step process, and further selectively introducing transition metal and alkali metal. By selectively coupling hydrogenation-dehydrogenation sites, C-C coupling sites and alkali metal sites in the same multifunctional catalyst, the synergies between the molecular sieve carrier and the multi-metal are realized. The catalyst realizes high-efficiency ethanol-to-C 3+ Olefins conversion in ethanol, with acetaldehyde as the reaction intermediate, and has the advantages of high C 5+ Olefins selectivity.

The invention discloses a copper-based catalyst for preparing acetaldehyde through ethanol dehydrogenation as well as a preparation method and application of the copper-based catalyst. The preparation method comprises the following steps: S1, carrying out alkalization treatment on protic mordenite in a strong alkali solution to increase the number of surface hydroxyl groups of the protic mordenite; and S2, adding the mordenite obtained in the step S1 into a copper salt solution to load copper ions, and then sequentially carrying out low-temperature drying shaping and medium-temperature activation stages to obtain the copper-based catalyst with networked Cu-OH-Si-O bonds on the surface. Through the synergistic effect of alkali liquor regulation and control and staged oxygen roasting, the dispersity and stability of a Cu active center in the catalyst are improved, the acetaldehyde selectivity of the reaction of preparing acetaldehyde through ethanol dehydrogenation is also improved, and side reactions are inhibited. Carrying out heat treatment regeneration on the inactivated copper-based catalyst in an oxygen-containing atmosphere; and after regeneration, the networked Cu-OH-Si-O bond on the surface of the copper-based catalyst is reconstructed.

A Levodopa-selective sensor is provided. A continuous levodopa monitor is also provided. The levodopa sensor includes a sensor area having a working electrode with a levodopa-selective chemistry configured for at least partial implantation in a host. The sensor also includes at least one membrane adjacent the levodopa-selective chemistry. The at least one membrane includes an enzyme domain that at least one enzyme selected from a tyrosinase; a mutated tyrosinase with specificity towards I-3,4-dihydroxyphenylalanine; a dihydroxyphenylalanine 4,5-dioxygenase; a mutated dihydroxyphenylalanine 4,5-dioxygenase with specificity towards I-3,4-dihydroxyphenylalanine; and combinations thereof; a synthase enzyme with specificity towards I-3,4-dihydroxyphenylalanine; a mutated synthase enzyme with specificity towards I-3,4-dihydroxyphenylalanine; a 3,4-dihydroxyphenyl-acetaldehyde synthase; a mutated 3,4- dihydroxyphenyl-acetaldehyde synthase with specificity towards I-3,4-dihydroxyphenylalanine; a dioxygenase enzyme with specificity towards I-3,4-dihydroxyphenylalanine; and a mutated dioxygenase enzyme with specificity towards I-3,4-dihydroxyphenylalanine.

The invention provides a device for preparing pentaerythritol through continuous condensation reaction and a reaction method thereof. The device comprises an enhanced reaction tower and a plug flow reactor which are connected in sequence, wherein a strengthening unit is arranged at the bottom in the strengthening reaction tower, an acetaldehyde feeding hole is formed in the lower part of the strengthening reaction tower, and the acetaldehyde feeding hole is formed in the lower part of the strengthening unit; an alkali liquor feeding hole, a formaldehyde feeding hole and a circulating feeding hole are sequentially formed in the upper part of the enhanced reaction tower from top to bottom; a discharge hole is formed in the bottom of the enhanced reaction tower; a spray layer is arranged at the top in the enhanced reaction tower, the spray layer is connected with the alkali liquor feed port, a liquid level sensor is arranged below the spray layer, and the liquid level sensor is arranged at a position 0.2-2 m below the spray layer; preferably, the liquid level sensor is arranged at the position 0.8 m below the spraying layer. According to the device disclosed by the invention, reactants are continuously fed, and products are continuously produced, so that the reaction rate is obviously accelerated.

The invention discloses a genetically engineered probiotic composition for expressing ADH (adenosine dihydrogenase) and ALDH (aldehyde dehydrogenase) and application of the genetically engineered probiotic composition in hangover alleviating and liver protection. The genetically engineered probiotic composition (such as EcN.1917-ADH and EcN.1917-ALDH) is constructed by introducing genes of alcohol dehydrogenase (ADH, NCBI (National Center for Biotechnology Information) Gene ID: 855349) and acetaldehyde dehydrogenase (ALDH, NCBI Gene ID: 855206) of saccharomyces cerevisiae into probiotics (such as escherichia coli). The engineering bacterium shows remarkable ethanol, acetaldehyde and endurance capacity in an in-vitro experiment, and the ethanol degradation rate is remarkably higher than that of a wild type strain; a mouse drunkenness model verifies that drunkenness and death caused by drinking can be reduced through pretreatment, drunkenness tolerance time is remarkably prolonged, and movement coordination disorder caused by alcohol can be improved. The strain can effectively promote alcohol metabolism and relieve alcoholic liver injury, and a new candidate strain is provided for development of a hangover-alleviating and liver-protecting viable bacterial preparation.

The invention discloses a carbamoyl-substituted diarylethene derivative as well as a preparation method and application thereof, and the preparation method comprises the following steps: reacting R-substituted 3-bromo-2-hydroxybenzaldehyde with an arylmethyl triphenylphosphonium bromide compound or an aryl acetic acid compound to obtain an intermediate A; then the intermediate A and cuprous cyanide are subjected to a heating reaction in N, N-dimethylformamide and nitrogen atmosphere, and an intermediate B is obtained; and finally, heating the intermediate B, acetaldoxime and indium trichloride in toluene for reaction to obtain the carbamoyl-substituted diarylethene derivative. The carbamoyl-substituted diarylethene derivative disclosed by the invention has a remarkable effect in an in-vitro anti-tumor activity test, particularly has excellent anti-proliferation ability to human BRCA mutant tumor cells, and can be used for preparing medicines for treating PARP-1 activity abnormity related diseases. The synthesis route is simple, the cost is low, and large-scale implementation is facilitated.

A method for preparing glycine by using threonine relates to a fermentation process in which threonine is decomposed into glycine and acetaldehyde by aldolase. Glycine and acetyl coenzyme A can be produced in a fermentation process, in which acetaldehyde is reduced into acetyl coenzyme A or an acetyl coenzyme A derivative by acetylating acetaldehyde dehydrogenase; or threonine is dehydrogenated by threonine dehydrogenase to obtain 2-amino-3-ketobutyric acid, which is then ligated by 2-amino-3-ketobutyrate CoAligase to obtain acetyl coenzyme A. Coenzyme A can be converted into an acetyl coenzyme A derivative under different fermentation conditions.

A Levodopa-selective sensor is provided. A continuous levodopa monitor is also provided. The levodopa sensor includes a sensor area having a working electrode with a levodopa-selective chemistry configured for at least partial implantation in a host. The sensor also includes at least one membrane adjacent the levodopa-selective chemistry. The at least one membrane includes an enzyme domain that at least one enzyme selected from a tyrosinase; a mutated tyrosinase with specificity towards 1-3,4-dihydroxyphenylalanine; a dihydroxyphenylalanine 4,5-dioxygenase; a mutated dihydroxyphenylalanine 4,5-dioxygenase with specificity towards 1-3,4-dihydroxyphenylalanine; and combinations thereof; a synthase enzyme with specificity towards 1-3,4-dihydroxyphenylalanine; a mutated synthase enzyme with specificity towards 1-3,4-dihydroxyphenylalanine; a 3,4-dihydroxyphenyl-acetaldehyde synthase; a mutated 3,4-dihydroxyphenyl-acetaldehyde synthase with specificity towards 1-3,4-dihydroxyphenylalanine; a dioxygenase enzyme with specificity towards 1-3,4-dihydroxyphenylalanine; and a mutated dioxygenase enzyme with specificity towards 1-3,4-dihydroxyphenylalanine.

The present invention discloses a pyruvate decarboxylase mutant with improved catalytic efficiency and its application. The present invention constructs a pyruvate decarboxylase mutant derived from Candida tropicalis for catalytic production of 4-hydroxyphenylacetaldehyde. The catalytic half-life (5.7 h) and TTN (24,600) of the mutant of the present invention are increased by 2.85 times and 2.07 times respectively compared with the control, and the mutant exhibits high decarboxylation activity. When the obtained mutant of the present invention uses 4-hydroxyphenylpyruvic acid as a substrate and reacts for 12 h at 25 °C and pH 6.5, the yield of 4-hydroxyphenylacetaldehyde can reach 5.08 g / L, and the molar conversion rate of the substrate reaches 67.28%. By adopting the method of the present invention, the production capacity of the unit catalyst and the reaction efficiency of the catalyst are improved, and the industrialization process of producing 4-hydroxyphenylacetaldehyde by the enzyme conversion method is accelerated.

The invention belongs to the field of chemical detection, and particularly relates to a method for detecting ethylene oxide, 2-chloroethanol and acetaldehyde in a frozen beverage by solid-phase microextraction gas chromatography-mass spectrometry. The invention relates to a method for detecting ethylene oxide, 2-chloroethanol and acetaldehyde in a frozen beverage by solid-phase microextraction gas chromatography-mass spectrometry, which comprises the following steps: S.1) taking a frozen beverage sample to be detected, homogenizing and uniformly mixing; s.2) weighing a certain amount of sample, and adding sodium chloride and hydrochloric acid; s.3) determining the sample by adopting a solid-phase microextraction gas chromatography-mass spectrometry method; and S.4) quantitatively analyzing the contents of ethylene oxide, 2-chloroethanol and acetaldehyde in the frozen drink sample to be detected by adopting an external standard method. According to the method disclosed by the invention, the derivatization reaction and the solid-phase microextraction process are combined into one, and the difficulties of complicated pretreatment, long time consumption, low accuracy, unstable result, high detection limit and the like in the traditional analysis technology are overcome. Meanwhile, the precision of a detection result is high, the influence of a complex matrix is removed, and the reproducibility is good.

Disclosed herein is a method for converting ethanol to 1,3-butadiene, wherein the method utilizes H2 produced during a first step of the method for subsequent conversions involved in the method. In particular aspects, H2 produced from converting ethanol to acetaldehyde is used to promote the conversion of the acetaldehyde to 1,3-butadiene. The H2 promotes enhanced catalyst stability, as well as enhanced selectivity and yields of the 1,3-butadiene product. In particular aspects, the method comprises two steps to produce the 1,3-butadiene from the ethanol and H2 produced from a first step facilitates enhanced selectivities and yields for the second step.

A Levodopa-selective sensor is provided. A continuous levodopa monitor is also provided. The levodopa sensor includes a sensor area having a working electrode with a levodopa-selective chemistry configured for at least partial implantation in a host. The sensor also includes at least one membrane adjacent the levodopa-selective chemistry. The at least one membrane includes an enzyme domain that at least one enzyme selected from a tyrosinase; a mutated tyrosinase with specificity towards I-3,4-dihydroxyphenylalanine; a dihydroxyphenylalanine 4,5-dioxygenase; a mutated dihydroxyphenylalanine 4,5-dioxygenase with specificity towards I-3,4-dihydroxyphenylalanine; and combinations thereof; a synthase enzyme with specificity towards I-3,4-dihydroxyphenylalanine; a mutated synthase enzyme with specificity towards I-3,4-dihydroxyphenylalanine; a 3,4-dihydroxyphenyl-acetaldehyde synthase; a mutated 3,4- dihydroxyphenyl-acetaldehyde synthase with specificity towards I-3,4-dihydroxyphenylalanine; a dioxygenase enzyme with specificity towards I-3,4-dihydroxyphenylalanine; and a mutated dioxygenase enzyme with specificity towards I-3,4-dihydroxyphenylalanine.

The invention relates to genetic engineering combined lactobacillus salivarius and application of the genetic engineering combined lactobacillus salivarius. The strain is classified and named as combined lactobacillus salivarius CTMT2, and the preservation number of the strain is CCTCC (China Center for Type Culture Collection) M 2025547. After an NIAAA model is injected into the stomach of an alcoholic liver mouse, the acetaldehyde level of the liver of the mouse is obviously reduced, and the alcoholic fatty liver symptom of the mouse is obviously relieved; after long-term intragastric administration of a high-glucose and high-fat modeling mouse, the acetaldehyde level in excrement of the mouse can be obviously reduced, the progress of liver fibrosis is improved, and good application prospects are achieved.

This application discloses an acetaldehyde recovery device and method in the production of 1,3-butanediol, belonging to the field of fine chemicals. The device includes: a feed pump, a preheater, a distillation column, a falling film reboiler, a bottom circulating pump, a bottom cooler, a top primary condenser, a reflux ratio distributor, a top secondary condenser, a top product tank, a top transfer tank, a bottom product tank, a bottom transfer tank, a vacuum condenser, a vacuum pump inlet separator, a high vacuum unit, and a vacuum pump outlet separator. The horizontal condenser is directly installed at the top of the distillation column, giving it advantages such as simple structure, convenient operation, low pipeline loss, and high vacuum. A method for acetaldehyde recovery in the production of 1,3-butanediol using this device is also disclosed. Compared to existing technologies, this invention uses falling film evaporation combined with vacuum deep cooling, which avoids the thermal decomposition of 3-hydroxybutyraldehyde and achieves low-temperature, high-efficiency acetaldehyde recovery. It is suitable for continuous production.

The application provides a system and method for integrated acetaldehyde distillation and recovery, which comprises a vertically arranged main tower, the main tower is sequentially divided into a distillation section, a catalytic reaction section, a stripping section and a stripping section from top to bottom, the top of the distillation section is provided with a self-adaptive distributor and a tower top pressure controller, the catalytic reaction section comprises catalytic filler plates and a transverse liquid redistributor, and the catalytic filler plates are loaded with catalysts. The four sections of stripping, stripping, catalytic reaction and distillation are integrated in the vertical main tower, the intermediate cooling and conveying equipment are cancelled, and the investment and energy consumption are significantly reduced. The catalytic reaction section adopts the corrugated filler loaded with catalysts and cooperates with the transverse liquid redistributor, so that the liquid forms thin layer flow, the reaction residence time is effectively prolonged, and the hydrolysis decomposition rate of 2-methyl-1,3-dioxolane (MD) and the acetaldehyde recovery rate are improved.

The invention relates to a method for preparing anhydrous acetaldoxime by a system for co-producing diacetylmonoxime and acetaldoxime, and relates to the technical field of acetaldoxime. The method comprises the following steps: adding diacetylmonoxime, acetaldehyde and a modified TS-1 molecular sieve into a reactor, and reacting to generate crude acetaldehyde oxime; feeding the crude acetaldehyde oxime into an acetaldehyde removal tower for rectification separation; rectifying and separating acetaldehyde tower bottoms to obtain butanone; adding an extracting agent into the tower top acetaldoxime solution, and feeding into a distillation kettle for extraction; the extracted acetaldehyde oxime is fed into an acetaldehyde oxime finished product tower to be further rectified and purified; the preparation method comprises the following steps: reacting a TS-1 molecular sieve, anhydrous toluene and 3-mercaptopropyltrimethoxysilane to obtain a sulfhydrylated TS-1 molecular sieve; the preparation method comprises the following steps: taking a sulfhydrylated TS-1 molecular sieve, tetrahydrofuran, diethyl vinylphosphonate, mercaptododeborane disodium salt and Darocur1173 as photoinitiators, and reacting under the irradiation of 365nm ultraviolet light to obtain the modified TS-1 molecular sieve. The acetaldehyde oxime prepared by the method has higher content and yield.

The invention discloses a brewing process for improving the grain steaming efficiency by boiling grains at constant high temperature, and belongs to the technical field of white spirit brewing. The process comprises the steps of sorghum cleaning, constant-temperature grain cooking, spreading for cooling, adding yeast, fermenting in a barrel and distilling, and the core is that constant-temperature hot water of 60 + / -1 DEG C is adopted, three-stage cooking is matched with two-time deep turning under the micro-pressure environment of 0.02-0.05 MPa according to the water-grain ratio of (2.3-2.7): 1, the core penetration rate of cooked grains is larger than or equal to 95%, and the pretreatment time is shortened to 30 minutes; by combining three-stage temperature-controlled fermentation, acetaldehyde is reduced to 0.48 g / L, fusel oil is reduced to 1.12 g / L, the flavor and efficiency of the raw wine are improved, and the dual effects of energy conservation and quality improvement are achieved.

The invention relates to polyfurandicarboxylic acid glycol ester resin as well as a preparation method and application thereof, and belongs to the technical field of organic high-molecular compounds. The preparation method of the polyethylene furandicarboxylate resin provided by the invention comprises the following steps: S1, mixing 2, 5-furandicarboxylic acid, ethylene glycol, a catalyst and an inhibitor, and carrying out esterification reaction to obtain an ester; and S2, carrying out low-pressure condensation polymerization on the ester obtained in the step S1 to obtain the polyethylene furandicarboxylate resin, the inhibitor is ethylene carbonate; according to the GB / T14571.2-2018 standard, based on the chromatographic purity of the ethylene glycol, the chromatographic peak area of the inhibitor in the mixture of the ethylene glycol and the inhibitor is 0.05%-0.6% of the sum of the chromatographic peak area of the inhibitor and the chromatographic peak area of the ethylene glycol. The preparation method can effectively reduce the content of acetaldehyde in the polyethylene furandicarboxylate resin.

The utility model relates to the technical field of wine processing, in particular to a wine aging electric heating extractor which is characterized in that when the wine aging electric heating extractor is used, wine liquid is put into an aging tank, an electric heating net plate is started, the electric heating net plate heats the wine liquid in the aging tank, and a stirring assembly is started, so that the stirring assembly uniformly stirs the wine liquid in the aging tank; according to the wine brewing device, wine liquid is rapidly heated, meanwhile, the ventilation assembly is started, so that oxygen in external air makes contact with the wine liquid, alcohol substances are promoted to be oxidized, air is exhausted through the exhaust pipe after rising in the wine liquid, and in the exhausting process, hydrogen sulfide, acetaldehyde and other components are accelerated to be moved out of the wine liquid; comprising an aging tank, an electric heating net plate, an exhaust pipe and an electromagnetic valve, the outer side wall of the aging tank is sleeved with the electric heating net plate, the exhaust pipe is arranged at the top end of the aging tank, the electromagnetic valve is installed on the exhaust pipe, the aging tank further comprises a stirring assembly, a ventilation assembly and a liquid drainage assembly, the stirring assembly and the ventilation assembly are arranged in the aging tank, and the liquid drainage assembly is arranged at the bottom end of the aging tank.

The invention relates to a bis (2, 2-methylene disulfide) episulfide compound with an ultrahigh refractive index and a preparation method thereof, and belongs to the technical field of optical materials, and the preparation method comprises the following preparation steps: taking chloroacetaldehyde dimethyl acetal, a solvent, disulfur dichloride and an acidifying agent, and carrying out a sulfuration substitution reaction to prepare 2-chloro-1, 2-dithiol; the preparation method comprises the following steps: carrying out nucleophilic substitution reaction on methoxycarbonyl sulfonyl chloride, a low-boiling-point solvent and 2-chloro-1, 2-ethanedithiol, and dropwise adding a bicarbonate saturated aqueous solution to carry out cyclization reaction so as to prepare a methoxycarbonyl disulfide-episulfide compound; and adding dimercaptomercaptan, and reacting to obtain a product. The process route provided by the invention solves the problems of tedious step-by-step reaction, more byproducts and high cost in the prior art.

The invention discloses Leishan fish sauce sour essence as well as a preparation method and application thereof. The leishan fish sauce acid essence is prepared from ethyl acetate, absolute ethyl alcohol, ethyl isovalerate, ethyl hexanoate, isoamyl alcohol, furfuryl alcohol, ethyl lactate, ethyl caprylate, acetic acid, diethyl succinate, methyl salicylate, ethyl benzoate, ethyl laurate, hexanoic acid, phenethyl alcohol, 4-methyl guaiacol, ethyl myristate, ethyl palmitate, ethyl oleate, capsicum oleoresin, ethyl phenylacetate and ginger oil. And lactic acid, glycerol triacetate, ocimene, ethyl isovalerate, ethyl butyrate, anethole and phenylacetaldehyde. The Leishan fish sauce sour essence disclosed by the invention is soft and harmonious in overall fragrance, natural and vivid, still has stable flavor characteristics at high temperature, can make up the problem of flavor deficiency in sour soup products, realizes accurate reproduction and controllable release of composite fragrance, improves the standardization level of products, and effectively improves the preference degree of consumers.

Dichloroacetonitrile is an important raw material required for the production of florfenicol, a new Class II veterinary drug in China, and has a promising market prospect. The present invention discloses a method for preparing dichloroacetonitrile, comprising the following steps: using dichloroacetaldehyde as a raw material, in the presence of different nitrogen sources and a copper catalyst, and using air as an oxidant to generate dichloroacetonitrile. The reaction liquid is filtered, extracted, and distilled to obtain a colorless liquid with a purity greater than 99%. Compared with the traditional method of preparing dichloroacetonitrile using phosphorus pentoxide, the present invention has a simple reaction, mild conditions, simple post-processing, and is more environmentally friendly, providing a new approach to the production of dichloroacetonitrile.