The invention discloses an
antimony electrolyte impurity removal adsorbent as well as a preparation method and application thereof, and relates to the technical field of
antimony electrolyte purification. The adsorbent is specially used for solving the problem that lead and
bismuth ions similar to
antimony in potential in the antimony
electrolyte are difficult to deeply remove. The preparation method comprises the following steps: mixing
sulfuric acid, deionized water,
antimony oxide powder and
hydrogen peroxide according to a
specific mass ratio (1: (0.8-1.5): (0.5-1.5)), and controlling the liquid-
solid ratio to be 8-15 mL / g to form a synthetic initial solution; then reacting for 0.5-4 hours under the condition of stirring at the temperature of 60-90 DEG C and the speed of 200-600 r / min; and finally, carrying out
solid-liquid separation and
drying at 55-110 DEG C for 1-12 hours. When the adsorbent is applied, the adsorbent is added into electrolyte according to the proportion of 500-5000 times of the total
mass of lead and
bismuth, reaction is performed for 1-6 hours under the conditions of 30-90 DEG C and 200-550 r / min, and deep purification can be realized after standing,
settling and separating. The method is short in technological process, mild in condition, easy to operate,
environmentally friendly and high in lead and
bismuth removal rate, purified liquid can return to an
electrolysis system, the saturated adsorbent can be regenerated and reused, and good
economic benefits and application prospects are achieved.