39644results about "Process efficiency improvement" patented technology

Processes for extracting lithium from a clay mineral and compositions thereof are described. The extraction process includes providing a clay mineral comprising lithium, mixing a cation source with the clay mineral, performing a high-energy mill of the clay mineral, and performing a liquid leach to obtain a lithium rich leach solution.

The present invention belongs to the technical field of machining and punching, and in particular relates to a surface pressurized punching device for anode plate machining. The surface pressurized punching device comprises a workbench of a table structure, a machine unit mounted on one side of the workbench, and a rack welded to the table top of the workbench, wherein an operation platform is fastened to the table top of the workbench and inside the rack by means of bolts, and clamping plates which are oppositely arranged are slidably mounted on two sides of the surface of the operation platform; and a hydraulic cylinder is mounted at the center of the surface of the rack, and an output shaft of the hydraulic cylinder running into the rack is fixedly connected to a drill rod by means of a coupler. By means of providing a reaming assembly, an electric motor B is controlled by an external power supply to operate while the hydraulic cylinder drives the drill rod to move, such that the electric motor B drives, by means of a gear A and a chain, a gear B to rotate synchronously while the electric motor B moves with the drill rod by means of an outer frame, thereby driving the drill rod to rotate. Thus, the surface of the drill rod can rotationally grind and finish holes in an anode plate while the drill rod performs drilling, thereby reducing burrs.

The invention discloses a 8.8-grade large-specification cold heading steel wire rod with excellent hardenability and a production method thereof, and belongs to the technical field of steel products. The steel wire rod is prepared from the following chemical components in percentage by mass: 0.35 percent to 0.39 percent of C, less than or equal to 0.10 percent of Si, 0.60 percent to 0.85 percent of Mn, 0.20 percent to 0.40 percent of Cr, 0.15 percent to 0.25 percent of Mo, 0.05 percent to 0.10 percent of Ni, 0.020 percent to 0.040 percent of Al, 0.0040 percent to 0.0080 percent of Ca, 0.0010 percent to 0.0030 percent of Ce, less than or equal to 0.0050 percent of N and the balance of Fe and inevitable impurities. The process route comprises the steps of molten iron pretreatment, converter smelting, LF refining, continuous casting, continuous rolling, billet cleaning, heating, rolling and controlled cooling. The produced # imgabs0 cold heading steel wire rod is good in cold heading performance, the hardness of the cross section of the wire rod is larger than 45 HRC after quenching, and the cold heading steel wire rod can be used for producing 8.8-grade high-strength bolts, nuts, screws and other hexagonal flange standard parts.

The invention provides lithium and aluminum hydroxyfluoride extraction equipment and a low-grade cathode carbon block recovery process, and relates to the technical field of metal recycling, the lithium and aluminum hydroxyfluoride extraction equipment comprises a bracket, a tank body, a mounting plate, a driving mechanism, a reciprocating mechanism, a water washing liquid discharging mechanism and an acid leaching liquid discharging mechanism; the tank body is installed in the support, a top plate is installed at the top end of the tank body through bolts, and a supporting frame is installed on the upper surface of the top plate through bolts. According to the scheme, a layer of pickle liquor is covered and injected after water washing liquid enters, so that the two extracting solutions can be added in a laminated manner, and the water washing liquid and the pickle liquor are quantitatively added in the laminated adding process, so that layered mixing is realized in the adding process of the device, and the efficiency of the device is improved. According to the device, the subsequent stirring time can be shortened, electric power is saved, meanwhile, it is guaranteed that two kinds of liquid are mixed more sufficiently and stably, and meanwhile the internal alkaline balance can be guaranteed through a stacked adding mode.

The invention relates to a high-strength complex-phase hot-rolled wire rod for a 2100MPa-grade stranded wire and a manufacturing method of the high-strength complex-phase hot-rolled wire rod, after a C-Si-Mn-Cr-Mo high-carbon component system is rolled and spun into a wire rod, the wire rod is subjected to online molten salt strong quenching isothermal treatment, so that the wire rod is firstly subjected to front-section molten salt treatment and is cooled at a cooling speed of greater than or equal to 33 DEG C / s, and enters a bainite phase region from an austenite state; the method comprises the following steps: firstly, carrying out first-stage molten salt treatment to promote transformation of austenite into bainite, then carrying out later-stage molten salt treatment to form a structure mainly comprising bainite, carrying out isothermal tempering on the structure, reserving part of untransformed retained austenite, and finally, carrying out roller way slow cooling to promote transformation of the untransformed retained austenite into martensite, and carrying out tempering, the microstructure of the hot-rolled wire rod comprises a complex-phase structure composed of tempered bainite and tempered martensite, the tensile strength of the hot-rolled wire rod can reach 1435-1485 MPa, the percentage reduction of area of the hot-rolled wire rod is 31%-36%, off-line heat treatment of follow-up machining is avoided, and the risk of wire breakage is reduced.

The invention discloses a method for manufacturing 7072 alloy high-performance air conditioner foil in a low-carbon, efficient and short-process mode, and relates to the technical field of aluminum foil machining. S2, continuous casting and rolling; s3, cold foil rolling; s4, finished product annealing; and S5, checking and packaging. Through component adjustment, iron and silicon alloy elements are controlled at the lower limit of the national standard, generation of coarse aluminum-iron-silicon phases is reduced, and low ductility caused by coarse grains after finished product annealing is avoided; in the cold foil rolling process, indexes of a working roll and rolling oil are adjusted, process parameters are optimized, the blank is directly rolled into a finished product, the direct rolling process is beneficial to improving the mechanical property of the finished product, and punching production of downstream customers is facilitated; and after triple continuous rolling is finished, subsequent cold foil rolling continuous rolling is rapidly arranged, deformation heat generated by triple continuous rolling and rolling of each pass is fully utilized, and large-machining-rate rolling of each pass is achieved.

The invention discloses a copper extraction effect analysis method and system, and the method comprises the steps: carrying out the continuous scanning of the surface of a copper sample through an optical sensor, and obtaining the chromaticity change time sequence data in a refining process; and carrying out segmentation processing on the data by utilizing a preset threshold value, and extracting dynamic change trend characteristics and key point locations. And in combination with conductivity and hardness value data recorded by a real-time monitoring system, a polynomial regression model is constructed, and correlation between copper purity and physical characteristics is established. And through historical data calibration and mean filtering optimization, the mapping relation between chromaticity change and copper purity is determined. And finally, according to the optimized chromaticity characteristic value and the calibrated correlation model, calculating the quantitative score of the real-time refining effect, and judging the grading basis of the copper purity. According to the method, the real-time evaluation of the copper purity and the dynamic optimization of the refining process are realized, and the refining efficiency and the product quality are improved.

The invention relates to a hot-rolled wire rod for a 2260MPa-grade stranded wire and a manufacturing method of the hot-rolled wire rod, after the high-carbon component design of C-Si-Mn-Cr-Mo-Nb-Al is adopted for rolling and spinning to form the wire rod, online molten salt isothermal toughening treatment is carried out, so that the wire rod is firstly subjected to front-section molten salt treatment and is rapidly cooled, and enters a sorbite phase region from an austenite state to form a structure taking a sorbite structure as a main structure; and then carrying out rear-section molten salt treatment, reducing the circulation volume of molten salt, promoting the unconverted retained austenite to be continuously converted into sorbite, carrying out isothermal tempering, promoting fusing of a part of sorbite lamellar layers, and finally carrying out slow cooling through a roller way, so as to prepare the hot-rolled wire rod of which the microscopic structure comprises a mixed structure consisting of tempered sorbite, ferrite and fused sorbite, the tensile strength can reach 1534-1584 MPa, the percentage reduction of area can reach 33%-38%, and the alloy can be used in the application fields of manufacturing 2260 MPa grade stranded wires and the like without additional heat treatment procedures.

The invention belongs to the technical field of non-oriented electrical steel manufacturing, and relates to a method for producing non-oriented silicon steel based on thin-strip cast rolling. The low-silicon and aluminum-free component design is adopted, the hot-rolled thin substrate is directly obtained through thin strip cast rolling, casting blank continuous casting and casting blank heating are omitted, the hot rolling reduction is greatly reduced, it is avoided that unfavorable textures of alpha and gamma components in the finished non-oriented silicon steel are remarkably improved, and the high magnetic induction of the finished product is guaranteed; after acid pickling and cold rolling, grain growth is promoted by means of high-temperature cover annealing, and low iron loss of a finished product is guaranteed; the high-magnetic-induction low-iron-loss non-oriented silicon steel with the thickness specification of 0.50 mm is obtained, the grain size of a finished product is 80-100 microns, the iron loss P1.5 / 50 is smaller than or equal to 4.0 W / kg, and the magnetic induction B5000 is larger than or equal to 1.76 T.

The invention belongs to the field of metal materials, and particularly relates to a high-strength hot-rolled pickled steel plate for an automobile chassis and a production method thereof. The steel plate is mainly suitable for manufacturing automobile chassis structural parts. The steel comprises the following chemical components: C, Si, Mn, Al, V, Ni, Cu, Cr, Pt and Y, P is limited to be less than or equal to 0.015%, S is limited to be less than or equal to 0.005%, N is limited to be less than or equal to 0.006%, and the balance is Fe and inevitable impurities. The yield strength of the steel plate ranges from 498 MPa to 552 MPa, the tensile strength ranges from 608 MPa to 643 MPa, the transverse elongation A ranges from 33% to 38%, the steel plate is qualified after transverse cold bending by 180 degrees D = a, the surface quality is good, oxide scale stripes and chromatic aberration defects are avoided, the surface roughness Ra ranges from 1.10 micrometers to 1.35 micrometers, and the steel plate has excellent corrosion resistance.

The invention discloses a high aspect ratio micropore pulse abrupt change current copper filling method and system, and belongs to the technical field of printed circuit board manufacturing, and the method comprises the steps: obtaining micropore structure parameters, and generating a gradient pulse abrupt change current waveform; monitoring a deposition thickness parameter of the orifice of the micropore in real time, and when the deposition thickness parameter exceeds a preset thickness threshold value, activating the reverse peak clipping pulse group; generating a resonant composite sound field in the electroplating bath; detecting the concentration distribution of the additive in the micropores in real time, and generating a dynamic adjusting instruction according to the concentration distribution of the additive; the independent injection rate of the accelerator and the inhibitor is controlled according to the dynamic adjusting instruction; and based on the gradient pulse abrupt change current waveform, the resonant type composite sound field and the dynamic adjusting instruction, the copper filling process is executed till the target deposition parameters are achieved. According to the method, a multi-field coupling mechanism of gradient pulse dynamic peak clipping, composite sound field synergistic mass transfer and additive concentration real-time regulation and control is adopted, and defect-free high-reliability copper filling can be achieved.

The invention discloses a thermomechanical treatment method for an Al-Mg-Si alloy rolled plate, and relates to the technical field of aluminum alloys, and the thermomechanical treatment method comprises the following working procedures of fusion casting, head and tail cutting, surface milling, homogenizing heat treatment, temperature-controlled rolling, solid solution quenching and pre-aging treatment, and after a cast ingot obtained by fusion casting of an aluminum alloy raw material is subjected to head and tail cutting and surface milling, the Al-Mg-Si alloy rolled plate is obtained; and after homogenization heat treatment is conducted, temperature control rolling is directly conducted through waste heat, quenching and pre-aging treatment are conducted after temperature control rolling is completed, and the alloy rolled plate is obtained. According to the method, the purposes of saving energy, simplifying the process flow and improving the production efficiency are achieved, the microstructure of a cast ingot can be regulated and controlled, crystal grains are refined, wrong distribution is improved, the strength of a rolled plate is further improved, the problem that mechanical properties are unstable is solved, and the generation of a rib line is avoided.

The present application relates to the field of wastewater treatment, and provides a treatment system and method for electroless nickel-plating waste liquid. The treatment system comprises a decomplexing pretreatment system; an oxidation-decomplexing system comprising a redox reactor and a decomplexing reactor which are connected in sequence, wherein an oxidizing agent in the redox reactor is oxygen, and an oxidizing agent in the decomplexing reactor is hydrogen peroxide; a chemical precipitation system comprising a neutralization reaction tank and a sedimentation tank which are connected in sequence, wherein the sedimentation tank is equipped with a filter system; and an evaporation crystallization system comprising an evaporation device, a crystallization device, and a separation device which are arranged in sequence. In the treatment system and method for electroless nickel-plating waste liquid, a two-stage oxidation method is employed to achieve oxidation and decomplexing of the waste liquid; in addition, combining chemical precipitation treatment and evaporation crystallization treatment not only reduces the waste liquid treatment cost but also avoids the introduction of other impurities, and allows for the separation of nickel salts and phosphate salts, so that the operation is easy and convenient, the treatment cost is low, the nickel removal rate is high, and resource utilization of nickel is facilitated.

The invention discloses a rapid method for determining the grade of target elements in concentrate based on mineral dissociation degree, and the grade of the target elements in the concentrate under a certain fineness condition is calculated according to the dissociation degree of target minerals in a raw ore sample under the certain fineness condition and the content of the target elements in the target minerals in the raw ore sample. By means of the method, the grade of the target element in the concentrate under the specified fineness condition can be calculated more quickly and more effectively, the beneficiation effect under the fineness condition can be predicted in advance when beneficiation operation is not conducted, and powerful data support is provided for formulation of the beneficiation technological process.

The invention relates to the technical field of metal smelting, and provides an electrolytic refining device which comprises an anode assembly, a cathode assembly and an electrolytic bath, the cathode assembly comprises a cathode structure, the cathode structure comprises an ultrasonic transducer and a cathode head, the cathode head is connected with the ultrasonic transducer, and the ultrasonic transducer converts ultrasonic electric signals into mechanical vibration; the electrolytic bath is used for containing electrolyte, and at least part of the anode assembly and at least part of the cathode head are arranged in the electrolytic bath. The ultrasonic transducer drives the cathode head to vibrate, so that dendritic crystals gathered on the surface of the cathode head fall off, dendritic crystal accumulation on the surface of the cathode head is reduced, the surface of the cathode head keeps active, the service life of the cathode structure is prolonged, the electrolytic refining reaction rate and stability are improved, the electrolytic refining reaction can be continuously and uniformly carried out, and energy consumption in the electrolytic process is reduced. The maintenance cost and the production downtime are reduced, and the current efficiency and the collection rate of target metal are improved.

The invention discloses a wide and thick steel plate for a 600MPa-grade high-performance marine riser and a production method of the wide and thick steel plate, according to the component design of the wide and thick steel plate, CEIIW is controlled to be 0.35%-0.41%, CEPcm is controlled to be 0.14%-0.18%, and beneficial influences on strengthening, phase change, microstructure, steel plate performance and post-welding performance are achieved; on the basis of component design, production methods of low-temperature heating, rough rolling multi-stage thickness section high-temperature gradient deformation and low-temperature rolling, intermediate temperature-waiting blank rapid cooling after rough rolling is finished, finish rolling low-temperature deformation, multi-stage water cooling and the like are adopted to obtain polygonal ferrite and batten bainite; the steel further comprises a small amount of granular bainite microstructures and dispersed fine precipitates, and the average height of deformed austenite does not exceed 15 microns; the problem of matching of comprehensive technical characteristics such as high strength, high toughness, high fatigue performance, corrosion resistance, strain resistance and good welding performance of the wide and thick steel plate for the high-performance marine oil and gas exploitation vertical pipe is solved.

The invention relates to the technical field of aluminum foil processing, in particular to a method for producing high-stability 3102 alloy air-conditioning foil in a short process, which comprises the following steps of: smelting, continuously casting and continuously rolling an aluminum alloy raw material to obtain a strip, directly trimming the strip, rolling the strip on a cold rolling unit, preparing a cold-rolled coil with the thickness of 0.15-0.2 mm after three-pass rolling, rolling the cold-rolled coil by an aluminum foil rolling mill, and rolling the cold-rolled coil by an aluminum foil rolling mill to obtain the high-stability 3102 alloy air-conditioning foil. The tensile strength of the aluminum foil finished product is 135-139 Mpa, the ductility is larger than or equal to 19%, and the cupping is larger than or equal to 5.9 mm. The aluminum foil finished product is suitable in tensile strength, small in fluctuation range, higher in ductility and cupping value, capable of better meeting the use requirements of air conditioner foil, capable of guaranteeing the product quality and meanwhile capable of improving the product quality. According to the method, the production process is greatly shortened, the production cost is reduced, and the production efficiency is improved.

The invention discloses a method for detecting the tensile property of a titanium alloy wire, and relates to the technical field of material detection.The method comprises the following steps that S1, sample preparation and microstructure pre-detection are conducted; s2, carrying out pre-stretching stress distribution equalization treatment; s3, determining an area where local plastic deformation possibly occurs in the sample; s4, performing dynamic tensile load increment control; s5, displacement field analysis is introduced, and data correction is carried out; s6, microcrack monitoring is carried out; s7, fracture mechanism analysis and fracture morphology characterization are carried out; and S8, constructing a dynamic damage evolution model. According to the method, by effectively simulating complex load conditions of the titanium alloy wire in actual use, test errors caused by constant-rate loading in a traditional method are avoided. In combination with dynamic correction of stress-strain data and a micro-crack monitoring technology, key behaviors of yield, plastic deformation, crack propagation and the like of the material under different loading conditions can be captured in real time, so that the tensile property of the material is accurately evaluated.

The invention discloses a 340MPa grade P-containing hot-dip galvanized iron alloy high-strength IF steel, the chemical composition of which is as follows by weight: C: ≤0.003%, Si: ≤0.03%, Mn: 0.35-0.65%, P: 0.03-0.075%, S≤0.010%, Als: 0.020-0.045%, Nb: 0.008-0.015%, Ti: 0.02-0.03%, B: 0.0004-0.0010%, N≤0.0035%, and the remainder is Fe and unavoidable impurities; The elements also meet the following restrictions: calculated according to the corresponding weight percentage of each element, 10C+3N+2S≤Ti+2Nb≤12C+3N+2S, 60B≤P≤80B; the present invention adds P element to IF steel, and through composition and process optimization control, obtains a P-containing hot-dip galvanized iron alloy high-strength IF steel with a yield strength of 180-320 MPa, a tensile strength of 340-440 MPa, an elongation of 35-46%, a value (average plastic strain ratio) ≥1.8, high surface quality, high formability, and good cold brittleness.

The invention discloses an external field reinforced molybdenum concentrate impurity removal method, and belongs to the technical field of molybdenum concentrate impurity removal. The method comprises the following steps: (1) microwave enhanced chloridizing roasting: uniformly mixing the molybdenum concentrate and calcium chloride, and carrying out microwave heating roasting in an inert atmosphere protection environment to obtain a roasted product; (2) ultrasonic enhanced acid leaching: adding the roasted material obtained in the step (1) into a hydrochloric acid solution, leaching under an ultrasonic condition, and then sequentially carrying out suction filtration, washing and drying to obtain an acid leached material; and (3) ultrasonic enhanced alkaline leaching is conducted, specifically, the acid leaching material obtained in the step (2) is added into a sodium hydroxide solution, leaching is conducted under the ultrasonic condition, then suction filtration, washing and drying are conducted in sequence, and iron and silicon removal of the molybdenum concentrate is completed. By means of the method, the iron and silicon removal effect of the molybdenum concentrate can be effectively improved, and the iron and silicon removal rate can reach 97% or above.

The invention discloses a method for testing corrosion resistance of high-precision stainless steel. The method comprises the following steps: acquiring multi-dimensional microscopic characteristic data of a sample surface and determining a microscopic sensitive area; applying multi-field coupling dynamic excitation to the sensitive area to determine a critical condition for triggering corrosion; triggering initial corrosion according to a critical condition and performing adaptive tracking on an expansion process to obtain spatio-temporal data; monitoring the environmental parameter change of the microcell based on the spatio-temporal data, and analyzing the corresponding relationship between the surface topography change and the environmental parameter change to determine a key condition for forming a feedback amplification effect; and according to the key conditions, executing an accelerated test of multi-level oscillation enhancement, and carrying out stage decomposition treatment to obtain a corrosion resistance prediction result. According to the technical scheme, a dynamic feedback mechanism between the surface microstructure and the corrosion behavior can be accurately disclosed, the problem of evaluation deviation caused by neglecting microstructure evolution in a traditional method is solved, and accurate prediction of the long-term corrosion resistance of the high-precision stainless steel in a complex service environment is achieved.

The present invention relates to the technical field of steel plate production, and particularly to a thick steel plate for high-strength storage tanks with a low ductile-brittle transition temperature and a preparation method thereof. The chemical components in the steel are as follows: C: 0.22% - 0.26%, Si: 0.13% - 0.144%, Mn: 0.73% - 0.92%, P≤0.015%, S≤0.01%, Cr: 0.03% - 0.049%, V: 0.01% - 0.019%, Nd: 0.00016% - 0.00047%, and the balance is Fe and impurities. Microalloying is used to ensure the excellent internal structure and service performance of the steel plate; the purity of the molten steel is improved by optimizing the smelting process; the internal structure of the steel plate is optimized and the plate shape is improved by adopting a four-stage slab heating process and a three-stage controlled rolling process; the simulated post-weld heat treatment process is used to improve the strength-ductility matching and adjust the microstructure of the material, ensuring the low-temperature service performance of the steel plate in the full thickness direction.

The heavy multidirectional die-casting equipment comprises a machine body, the machine body comprises a base, a stand column, a fixed cross beam and a movable cross beam, the stand column is installed on the base, the fixed cross beam is installed at the top of the stand column, and a vertical die-casting mechanism is installed at the bottom of the fixed cross beam; the telescopic end of the vertical die-casting mechanism is connected with a movable cross beam installed on the stand column. The die-casting die is installed on the die changing mechanism, and the die changing mechanism is installed on the base. Horizontal die-casting mechanisms are installed on the two sides of the base, an injection system is installed below the base, and core-pulling mechanisms are arranged on the front side and the rear side of the die-casting die respectively. According to the heavy multi-directional die-casting equipment and method for the vehicle body integrated casting, the vertical die-casting mechanism and the horizontal die-casting mechanism are used in cooperation, a vehicle body chassis and a side wall can be integrally formed in a die-casting mode, the heavy multi-directional die-casting equipment and method are suitable for production of large vehicle body structural parts such as a rear bottom plate and a front cabin frame, and the production efficiency is greatly improved.

The invention relates to the field of steelmaking. More specifically, the invention relates to a process for controlling nitrogen increase in electric furnace smelting. The invention provides a method for producing low-nitrogen steel from electric furnace full waste steel. The method specifically comprises the steps that waste steel is loaded into an electric furnace, CO2 gas is injected into the electric furnace before and after loading, air is exhausted, and micro-positive pressure in the electric furnace is kept. The method comprises the following steps: after an electric furnace forms a molten pool, injecting limestone powder at the top of the furnace with the injection amount of 60-80kg / t and the injection carrier gas of CO2 gas, after the electric furnace forms the molten pool, injecting oxygen and carbon powder by adopting a carbon-oxygen lance to make foamed slag, injecting CO2 gas into the molten pool to decarburize, produce two times of CO gas and intensify denitrification, and during tapping of the electric furnace, protecting steel flow from ending with air by adopting CO2 gas, and feeding into the next process for smelting after tapping of the electric furnace. Application proves that when the method is used for smelting low-nitrogen steel, nitrogen in the electric furnace can be controlled not to be increased, N is smaller than or equal to 0.003% after tapping of the electric furnace, the smelting rate of the low-nitrogen steel grade is increased, and low-carbon emission production of special varieties is achieved.

The invention belongs to the technical field of metallurgical continuous casting, and particularly relates to a method for removing tundish inclusions based on cooperation of an external electric field and physics. The invention discloses a method for removing tundish inclusions based on cooperation of an external electric field and physics, and mainly aims at solving the problems that as the inclusions in tundish molten steel enter a subsequent continuous casting link, a submersed nozzle is clogged and blocked, and the quality of a casting blank is deteriorated. The key point is that an external electric field and physics synergistic effect is used; a bottom blowing device is arranged to provide power for floating of inclusions; an original baffle weir structure of the tundish is improved, and the probability of catching inclusions is increased; and an external electric field is cooperatively used, so that the inclusions are promoted to float towards the tundish covering agent and be attached to the blocking weir. By means of the method for cooperatively removing the tundish inclusions based on the external electric field and physics, the tundish molten steel inclusions can be obviously removed, the service performance of a subsequent water gap is optimized, the casting blank quality is improved, and the improvement of the high-quality steel smelting level in China is assisted.

This invention discloses a process for controlling the shape of A514GrQ extra-thick plates for offshore platforms. It uses 800-1000mm thick steel ingots, and after removing and cleaning the ingot risers, ensures uniform thickness of the ingot body, laying the foundation for obtaining steel plates with excellent flatness. The heating process is optimized to ensure uniform heating of the ingot head, middle, and tail, facilitating uniform deformation during rolling. Homogenized rolling is employed to reduce cooling water usage, limit the reduction per pass, and control the final rolling temperature, avoiding uneven internal stress and shape rebound in the steel plate. The final product is a 180-210mm thick steel plate with a maximum flatness ≤8mm and a lateral flatness ≤4mm within a length of 10000mm and a width of 2400mm, significantly reducing subsequent leveling tasks.

The invention discloses a high-recovery-ratio and high-uniformity TC4 titanium alloy cast ingot preparation method which comprises the following steps: selecting titanium alloy plate-shaped materials to process material frames, and arranging a plurality of material frames in a material box of an EB furnace; the recycled titanium alloy material is classified and sampled to analyze chemical components. Pressing sponge titanium, the intermediate alloy and aluminum shots into an electrode pressing block; the electrode pressing block is arranged in the middle of the material frame, the recycled material stacks are stacked in the material frame in a staggered mode, and gaps are filled. Performing primary smelting through an electron beam cooling bed to obtain a primary cast ingot; and VAR smelting is conducted, specifically, the primary cast ingot is loaded into a VAR furnace to be subjected to secondary smelting. According to the preparation method of the TC4 titanium alloy cast ingot with the high recovery ratio and the high uniformity, an EB + VAR smelting process is adopted, the addition proportion of the recovered materials is high, and the alloy cast ingot with uniform components is prepared.

The invention provides a mineral leaching property analysis method, which belongs to the field of process mineralogy, and comprises the following steps: crushing and enriching a sample to be detected, and selecting single mineral particles to obtain target mineral particles; the preparation method comprises the following steps: coating a sample preparation grinding tool with epoxy resin glue, adding target mineral particles, and carrying out curing and grinding treatment to obtain a primary sample; cutting the primary sample, placing the grinding surface downwards and the three wear-resistant alloys at the bottom of a sample preparation grinding tool, injecting epoxy resin glue, curing to form a composite sample, accurately grinding, polishing, performing carbon spraying treatment, performing first automatic mineralogical analysis, measuring the area of a target mineral, cleaning, and performing leaching treatment to obtain a treated sample; and after solidification, accurate grinding and polishing and carbon spraying treatment, secondary automatic mineralogical analysis is carried out, the area of the residual target mineral is measured, and the leaching index of the target mineral is calculated. Reliable technical support is provided for mineral processing technology optimization and resource evaluation, and the method is particularly suitable for development of efficient leaching technologies of precious metal, rare earth and the like.

According to the high-strength ship plate with the excellent firework performance and the manufacturing method, a low-carbon chemical component system is adopted, V-N, Ti and other refined grain elements are added, formation of a ferritic structure in steel is promoted, RE elements are added, and the purity of the steel is improved; the manufacturing method comprises the steps of smelting, continuous casting, reheating, rolling, accelerated cooling and stacking slow cooling, the rolling process adopts two-stage controlled rolling, the first-stage rolling adopts a high-temperature fast rolling and high-pressure reduction process, and the second-stage rolling adopts a fast rolling process with high finish rolling temperature; the steel plate produced by using the method has excellent comprehensive mechanical properties and fire performance, the yield strength is greater than 485MPa, and the tensile strength is 560-620MPa; the yield strength of the steel plate after fire work is larger than 475 MPa, the tensile strength is 551-610 MPa, the percentage elongation after fracture is larger than or equal to 25.5%, and the impact absorption energy at the temperature of-80 DEG C is larger than 200 J.

The invention relates to a crown ether covalent organic framework material as well as a preparation method and application thereof. The preparation method comprises the following steps: dissolving a crown ether monomer and an amino monomer in an o-dichlorobenzene solvent, adding a catalyst acetic acid aqueous solution, and uniformly dispersing to form a reaction solution; the method comprises the following steps: freezing a reaction solution through a liquid nitrogen bath, vacuumizing, filling nitrogen, carrying out a heating reaction, and carrying out post-treatment operations such as washing and drying on a reaction product, so as to obtain the crown ether covalent organic framework material BADT-DB18C6-COF. The crown ether covalent organic framework material is formed by condensation of a crown ether aldehyde monomer and an amino monomer, the crown ether monomer is 4, 4 ', 4' ', 4 '''-(6, 7, 9, 10, 17, 18, 20, 21-octahydrodibenzo [B, K] [1, 4, 7, 10, 13, 16] hexaoxacyclo octadecene-2, 3, 13, 14-tetrayl) tetrabenzaldehyde, and the crown ether monomer is 4, 4 ', 4' ', 4'''-(6, 7, 9, 10, 17, 18, 20, 21-octahydrodibenzo [B, K] [1, 4, 7, 10, 13, 16] hexaoxacyclo octadecene-2, 3, 13, 14-tetrayl) tetrabenzaldehyde. The amino monomer is 4 ', 5'-bis (4-aminophenyl)-[1, 1 ': 2', 1 ''-terphenyl]-4, 4''-diamine. The crown ether covalent organic framework material BADT-DB18C6-COF prepared by the invention is mainly used as an adsorbent, is used for adsorbing and recovering uranium, thorium and americium ions from a solution, shows good adsorption capacity on radionuclides U-238, Th-232 and Am-243, and is particularly suitable for the field of spent fuel post-treatment in the nuclear industry.