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13031results about How to "No pollution in the process" patented technology

Method for preparing diethyl oxalate by coupling CO

The invention discloses a method for preparing diethyl oxalate by CO coupling reaction. By applying a gas phase method, CO is coordinated with ethyl nitrite and is catalyzed by bimetallic supported catalyzer to couplingly generate crude diethyl oxalate, the reaction is a self-sealing circulation process, the CO gas mixed with the ethyl nitrite coming from a regeneration reactor is preheated and then enters into a coupling reactor, after the reaction, the gas is separated by condensation, so that the colorless and transparent condensed diethyl oxalate liquid is produced, and the uncondensed gas containing NO enters into the regeneration reactor to react with ethanol and oxygen in order to generate ethyl nitrite which is again circulated back to the coupling reactor for continuous use. The invention is carried out on the basis of previous laboratory research and under the background of industrial production and fulfils the continuous run examination of the bench scale test and pilot magnification under the condition of industrial operation, the temperature of the coupling reaction is low, and the concentration of products is increased. The method has the advantages of more energy saving, no pollution and high benefit. The total conversion rate of the CO generated by reaction is one hundred percent, and the selectivity of diethyl oxalate is over ninety six percent.
Owner:TIANJIN UNIV

Method for recovering and preparing lithium iron phosphate from waste lithium iron phosphate battery

The invention discloses a method for recovering and preparing lithium iron phosphate from waste lithium iron phosphate batteries. The method comprises: 1) dismantling the recovered waste lithium iron phosphate batteries, stripping battery cases, immersing the batteries, separating the electrode plates from the powder material of positive and negative terminals through a method of alternation of ultrasonic and mechanical stirring, taking out the electrode plates and diaphragms, and obtaining mixed liquor; 2) performing a preliminary ball milling to the mixed liquor, and drying the uniformly mixed slurry obtained by the preliminary ball milling; 3) calcining the dried material in oxidizing atmosphere to obtain a recovered material, adding iron source, phosphorous source and optionally new lithium iron phosphate, then adding carbon source, high energy ball milling the obtained material, drying the material to obtain a pre-burning material of the recovered material; 4) microwave sintering or solid state sintering the pre-burning material of the recovered material in protective atmosphere to obtain the product of lithium iron phosphate. The preparation method has the advantages of environmental protection, no pollution, simpleness and practicality, high production utilization rate, simple
Owner:ZHEJIANG UNIV

Method for soft soil foundation treatment through microorganism grouting sand drain

InactiveCN104631430AImprove vertical load carrying capacityPermeability changeOrganic fertilisersSoil conditioning compositionsSoil scienceSalt solution
Disclosed is a method for soft soil foundation treatment through microorganism grouting sand drain. The method comprises the steps that a, a pile hole 1 is formed in a soft soil foundation to be treated, and sand is poured into the pile hole 1 to form a sand pile; b, a urease-producing microorganism solution 9 and a nutritive salt solution 10 are sequentially and evenly injected into the sand pile through a grouting tube 6, sand cementation is achieved through the microorganism induction calcium carbonate crystal technology, the concentration of the urease-producing microorganism solution 9 and the concentration of the nutritive salt solution 10 are controlled, sand in the pile body forms a specific cementation mode, and the good water permeable characteristic is ensured; c, after the microorganism grouting solidification sand pile is formed, a flexible water permeable sand cushion 4 is laid on the top of the foundation jointly formed by the sand oil and pile space soil 2, prepressing loads 5 are exerted on the top of the flexible water permeable sand cushion 4, pore water in the pile space soil 2 is made to be drained along a drainage channel formed by the sand pile and the sand cushion, the pile space soil is solidified, and the composite foundation with the high bearing capacity is formed jointly through the soft soil obtained after drainage and solidification are carried out on the microorganism grouting sand pile and the flexible water permeable sand cushion covering the soft soil.
Owner:NANJING FORESTRY UNIV

Normal-temperature synthesis method for polycarboxylic acid water-reducing agent

The invention discloses a normal-temperature synthesis method for a polycarboxylic acid water-reducing agent, and belongs to the field of cement concrete water-reducing agents. The water-reducing agent is prepared by the following steps of: copolymerizing polyoxyethylene ether monomer or polyoxyethylene ester monomer a containing unsaturated double bonds, unsaturated monocarboxylic acid and derivative monomer thereof b, unsaturated dicarboxylic acid c and unsaturated sulfonic acid or salt monomer thereof d in aqueous solution under the action of an oxidation reduction initiator, and finally neutralizing the solution by using alkali solution to obtain the water-reducing agent. The reaction can be performed at room temperature by adopting an oxidation reduction initiating system, and the appropriate reaction temperature is between 5 and 30 DEG C; and the synthesis process does not need heating, so energy is saved, and high-temperature side reaction is effectively controlled. The prepared polycarboxylic acid high-performance water-reducing agent has the characteristics of high water-reducing rate and good collapse protecting performance. The water-reducing agent has wide application range, and the method has low production process requirement and is suitable for industrialized large-scale production.
Owner:BEIJING UNIV OF TECH

Electrothermal film and manufacturing method thereof

The invention relates to an electrothermal film and a manufacturing method thereof, belonging to the technical field of semiconductor heating. The electrothermal film is mainly prepared by adopting stannic chloride, titanium tetrachloride, stannic chloride, titanium trichloride, ferric chloride, antimony trichloride, calcium chloride, potassium chloride, cadmium chloride, stannic dioxide, stannictetroxide, hydrofluoric acid, boric acid, ethanol, isopropyl alcohol and inorganic water. By adopting the above formula, the mixture is mixed, stirred and heated to prepare into electrothermal film treating fluid, a semi-finished product of the electrothermal film is obtained by spraying the electrothermal film treating fluid at negative pressure on the electrothermal film carrier, and then silveroxide slurry is coated on the semi-finished product of the electrothermal film for baking to form a finished product of the electrothermal film. The electrothermal film has reasonable proportion andsimple manufacturing process, can be manufactured into various electrothermal film heating devices, has a working temperature capable of being up to 500 DEG C, and has wider application range. The electrothermal film of the invention also has the function of far infrared radiation, can play a role of physical therapy and health care to human body, and can help improve the quality and output of agricultural products.
Owner:GUANGDONG HALLSMART INTELLIGENCE TECH CORP LTD

Tiny satellite formation flying control method based on atmospheric drag and control device

The invention provides a control method and a control device used for micro-satellite cluster flying based on atmosphere resistance, and relates to the technical field of micro-aircraft and astronautics measuring and controlling. The signal output terminal of a GPS receiver is connected with the signal input terminal of a track determining device; the signal output terminals of a solar battery array and a three-axis magnetometer are connected with the input terminal of an attitude fusion filter; the output terminal of the three-axis magnetometer is connected with the input terminal of a pure magnetic measuring attitude fusion filter; the signal output terminal of the attitude fusion filter is connected with the second input terminal of a satellite line; the first output terminal of the satellite chain is connected with the input terminal of a cluster formation control law; the second output terminal of the satellite chain is connected with the input terminal of the satellite attitude control law; the formation and attitude of the satellite cluster flying are controlled by controlling a pneumatic plate. The method and the device achieve the objects of long service life of the aircraft, low power dissipation, low cost and no pollution on the basis of atmosphere resistance.
Owner:NANJING UNIV OF AERONAUTICS & ASTRONAUTICS

Preparation method of star polycarboxylic acid high-performance water reducing agent

ActiveCN102887979AExtended Dionon Design-Structure-PropertyExpanding the theoretical connotation of the design-structure-performance of moleculesWater reducerPollution
The invention relates to a preparation method of a star polycarboxylic acid high-performance water reducing agent. Polybasic alcohol and (methyl) acrylic acid used as main raw materials for esterification are esterified and polymerized to prepare the star polycarboxylic acid high-performance water reducing agent material: the (methyl) acrylic acid and polybasic alcohol used as reactants are esterified under the action of a catalyst to firstly prepare a star polymerizable active terminal, and free-radical polymerization reaction is carried out with unsaturated polyethenoxy ether, molecular weight regulator and unsaturated carboxylic acid monomer under the action of an initiator to prepare the star polycarboxylic acid high-performance water reducing agent. The invention is easy to control, and has the advantages of high polymerization degree, low cost and no pollution; the esterification reaction is carried out form an active core, and the free-radical polymerization is carried out to generate the chain arm, thereby implementing the polycarboxylic acid high-performance water reducing agent in a star molecular structure; and under the condition of common doping amount and low doping amount, the star polycarboxylic acid high-performance water reducing agent has better cement paste flowability and holding capacity than the traditional linear and comb polycarboxylic acid water reducing agents, and has favorable cement adaptability and concrete application performance.
Owner:GUIZHOU DR SHI TECH

Application of tungsten-based catalyst in lignin catalytic hydrogenation for producing aromatic compound

The invention relates to hydrocracking of lignin, and specifically relates to a method for applying a tungsten-based catalyst to catalyze lignin hydrocracking for producing an aromatic compound. The catalyst comprises a main active component of non-zero-valent tungsten, and a second metal component of a small amount of one or more transition metals selected from zero-valent nickel, cobalt, ruthenium, iridium, palladium, platinum, iron, and copper. According to the method, raw materials such as lignin, biomass hydrolysis residue, lignosulfonate, and alkaline lignin are subject to catalytic hydrogenation under a hydrothermal condition with a temperature of 120 to 450 DEG C and a hydrogen pressure of 1 to 20MPa; the raw materials are cracked into C6-C9 phenolic compounds with high selectivity. A maximal phenol yield reaches 55.6%. Compared to existing technologies, according to the invention, renewable natural biomasses are adopted as raw materials, such that the raw materials are cheap, and have wide sources; inorganic acid and alkali are not required, such the production of a large amount of alkaline solution in traditional lignin catalysis is avoided; the tungsten-based catalyst is cheap; the reaction process is green, and has atom economical characteristics.
Owner:DALIAN INST OF CHEM PHYSICS CHINESE ACAD OF SCI

Chinese medicine residue organic fertilizer and production method thereof

The invention provides a Chinese medicine residue organic fertilizer. Wastes after extraction of Chinese traditional medicines can be fully utilized, utilization of waste materials is realized, and a bactericidal and insect disease preventing organic fertilizer full of nutritional ingredients is also provided for agricultural production. The Chinese medicine residue organic fertilizer is prepared by fermenting Chinese medicine residue, excrement of animals, solid waste, bacillus subtilis and EM. The Chinese medicine residue organic fertilizer has the advantages that the Chinese medicine residue, excrement of animals and solid waste are mixed, biological fermentation bacteria are added for carrying out rapid fermentation, organic fertilizer is processed, waste materials are changed into things of value, harm is turned into good, the problem of treatment of abandoned herb residue produced by a Chinese medicine factory is solved, and waste treatment cost is also greatly reduced, so that a win-win situation of environmental protection and economic development is realized. By adopting the organic fertilizer made from the Chinese medicine residue, soil can be effectively improved, crop pest also can be effectively prevented, and quality, yield and safety of crops are improved.
Owner:INST OF S&T INFORMATION SHANDONG ACADEMY OFAGRI SCI

Environment-friendly type hyperconcentration biological enzyme liquid laundry detergent and preparation method thereof

The invention relates to a detergent for daily use, and specifically relates to an environment-friendly type hyperconcentration biological enzyme liquid laundry detergent and a preparation method thereof. The prepared product in the invention is mobile liquid with low viscosity, contains no phosphates, fluorescent brightening agents or alkylphenol polyoxyethylene, and has no pollution to environment. The production process for the product is simple; preparation and mass production of the product are easy; the product can be widely used for washing of various fabrics and clothing and is both applicable to hand wash and machine wash. The environment-friendly type hyperconcentration biological enzyme liquid laundry detergent comprises, by weight, 0.5 to 50 parts of fatty alcohol polyoxyethylene ether sodium sulfate-70, 0.5 to 50 parts of fatty alcohol polyoxyethylene ether-9, 0.5 to 30 parts of sodium alkylbenzene sulfonate-60, 0.2 to 15 parts of triethanolamine, 0.1 to 10 parts of sodium citrate, 0 to 5 parts of citric acid, 0 to 5 parts of aliphatic acid, 0.02 to 8 parts of biological enzyme, 0.1 to 20 parts of an enzyme stabilizer, 0.5 to 30 parts of a solvent, 0 to 15 parts of a hydrotropic agent, 0 to 5 parts of a bactericide, 0.001 to 5 parts of an antiseptic, 0 to 3 parts of essence and 1.0 to 40 parts of softened water.
Owner:上海开米科技有限公司
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