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66368results about How to "No pollution in the process" patented technology

Method for preparing humic acid and salt thereof by oxidation and degradation of brown coal

The invention discloses a method for producing humic acid and salt thereof through the oxidative degradation of young lignite. The method comprises the following steps: carrying out the oxidation reaction of the lignite containing the humic acid and aqueous hydrogen peroxide solution; after the reaction, obtaining water soluble fulvic acid through centrifugal separation, supernatant filtration, concentration and drying; adding alkali into the fulvic acid to prepare a fulvic acid salt product; carrying out the alkaline extraction and centrifugal separation of the residue deposit of the production of the fulvic acid, adding acid into the supernatant till the pH value is 1 to 2, carrying out a reaction at an increased temperature or room temperature, carrying out centrifugal separation after the reaction is finished, and obtaining purified ulmic acid after precipitation and drying; and directly concentrating and drying the supernatant in the previous step to obtain the humate. The method can improve the yield of the fulvic acid and total humic acid in the young lignite, and simultaneously increase the active group in the humic acid. The method can be used for producing fulvic acid, fulvic acid salt, ulmic acid and ulmic acid salt products. In particular, the method puts an end to the environmental pollution caused by the nitric acid which is taken as an oxidation degradation agent. In addition, the method has a short technological line, low cost, simple requirements on equipment, and moderate conditions. The method which can be applied to the industrialized production has good application prospect.
Owner:KUNMING UNIV OF SCI & TECH +4

Method for preparing diethyl oxalate by coupling CO

The invention discloses a method for preparing diethyl oxalate by CO coupling reaction. By applying a gas phase method, CO is coordinated with ethyl nitrite and is catalyzed by bimetallic supported catalyzer to couplingly generate crude diethyl oxalate, the reaction is a self-sealing circulation process, the CO gas mixed with the ethyl nitrite coming from a regeneration reactor is preheated and then enters into a coupling reactor, after the reaction, the gas is separated by condensation, so that the colorless and transparent condensed diethyl oxalate liquid is produced, and the uncondensed gas containing NO enters into the regeneration reactor to react with ethanol and oxygen in order to generate ethyl nitrite which is again circulated back to the coupling reactor for continuous use. The invention is carried out on the basis of previous laboratory research and under the background of industrial production and fulfils the continuous run examination of the bench scale test and pilot magnification under the condition of industrial operation, the temperature of the coupling reaction is low, and the concentration of products is increased. The method has the advantages of more energy saving, no pollution and high benefit. The total conversion rate of the CO generated by reaction is one hundred percent, and the selectivity of diethyl oxalate is over ninety six percent.
Owner:TIANJIN UNIV

Multi-element composite nano-material, preparation method thereof and application thereof

The invention provides a multi-element composite nano-material for a super capacitor, and a preparation method of the nano-material. The nano-material comprises a carbon material, metal oxide and conducting polymer, and components of the nano-material can be two or more than two materials. By the aid of the characteristics such as fine electrical conductivity, long cycle life and high specific surface area of the carbon material, high pseudo-capacitance of the metal oxide and low internal resistance, low cost and high operating voltage of the conducting polymer, different types of electrode materials generate synergistic effects, advantages are mutually combined, shortcomings are mutually weakened, the energy storage characteristics of an electric double-layer capacitor and a pseudo-capacitor are simultaneously made full use of, a composite electrode material with high power density, fine circulating stability and higher energy density is prepared, and the multi-element composite nano-material is excellent in comprehensive performance when used for an electrode of the super capacitor, has the advantages of simple preparation process, short cycle, low cost and the like, and is suitable for large-scale industrial production.
Owner:中科(马鞍山)新材料科创园有限公司

Kitchen waste pretreatment device

ActiveCN103464449ADeodorization up to standardWith automatic sortingSolid waste disposalControl systemOil water
The invention discloses a kitchen waste pretreatment device. The kitchen waste pretreatment device comprises a closed shell and a control system. The kitchen waste pretreatment device is characterized in that the upper end of the shell is provided with a feeding funnel and a feeding motor; the shell is internally provided with an automatic sorting device, a biological fermentation drying device, an oil-water separation device, an ionization deodorization device and a gas condensation device; the feeding funnel is communicated with a kitchen waste charge hole of the automatic sorting device through a discharge hole; the automatic sorting device is communicated with a charge hole of the biological fermentation drying device through a kitchen waste outlet; the automatic sorting device is communicated with the oil-water separation device through a liquid outlet; the biological fermentation drying device is communicated with the gas condensation device through a gas exhaust opening; the gas condensation device is communicated with the ionization deodorization device, so that the effects of automatic sorting, rapid fermentation treatment speed, uniform fermentation, rapid heating speed, capability of oxygenating in fermentation, standard gas deodorization and environment protection and no pollution are achieved.
Owner:SHANDONG MINGLIU KITCHEN WASTE TREATMENT EQUIP CO LTD

Method for recovering and preparing lithium iron phosphate from waste lithium iron phosphate battery

The invention discloses a method for recovering and preparing lithium iron phosphate from waste lithium iron phosphate batteries. The method comprises: 1) dismantling the recovered waste lithium iron phosphate batteries, stripping battery cases, immersing the batteries, separating the electrode plates from the powder material of positive and negative terminals through a method of alternation of ultrasonic and mechanical stirring, taking out the electrode plates and diaphragms, and obtaining mixed liquor; 2) performing a preliminary ball milling to the mixed liquor, and drying the uniformly mixed slurry obtained by the preliminary ball milling; 3) calcining the dried material in oxidizing atmosphere to obtain a recovered material, adding iron source, phosphorous source and optionally new lithium iron phosphate, then adding carbon source, high energy ball milling the obtained material, drying the material to obtain a pre-burning material of the recovered material; 4) microwave sintering or solid state sintering the pre-burning material of the recovered material in protective atmosphere to obtain the product of lithium iron phosphate. The preparation method has the advantages of environmental protection, no pollution, simpleness and practicality, high production utilization rate, simple
Owner:ZHEJIANG UNIV

Ultraviolet light cured transfer printing film and preparation method and application thereof

The invention belongs to the field of decorative materials, and particularly relates to an ultraviolet light cured transfer printing film and a preparation method and application thereof. The preparation method comprises the following steps of: uniformly coating or printing a mold release agent on a base load film, and performing infrared curing; uniformly coating or printing an ultraviolet light cured printing ink with a patterning function on a mold release agent layer, and performing curing through ultraviolet irradiation; or uniformly coating or printing an ultraviolet cured protective layer coating with anti-scratching and wear-resistant functions on the mold release agent layer first, then uniformly coating or printing the ultraviolet light cured printing ink with the patterning function on the mold release agent layer after the curing through the ultraviolet irradiation, and performing the curing through the ultraviolet irradiation; and uniformly coating or printing an ultraviolet light cured bottom color coating on an ultraviolet light cured printing ink decorative pattern layer, and performing the curing through the ultraviolet irradiation to obtain the ultraviolet light cured transfer printing film which can be used for producing an ultraviolet light cured transfer printing film decorative board. The ultraviolet light cured transfer printing film has high material strength, and has the advantages of high weathering resistance, high environmental protection, rich colors and patterns, full lacquer film, high hardness, scratch resistance, easy cleaning, noninflammability and the like.
Owner:ZHUHAI DONGCHENG UV MATERIALS

Biochar mixing type protected horticultural vegetable field soil heavy metal passivant and preparation method thereof

The invention relates to a soil improvement technology and an environment protection technology and particularly discloses a biochar mixing type protected horticultural vegetable field soil heavy metal passivant and a preparation method thereof. The soil heavy metal passivant comprises the following components in percentage by weight: 50 to 60 percent of biochar, 5 to 10 percent of medical stone powder, 5 to 10 percent of diatomite powder, 10 to 20 percent of lignite and 10 to 20 percent of coal ash. The preparation method for the soil heavy metal passivant comprises the following steps of: mixing the medical stone powder which is screened by an 80-mesh sieve, the diatomite powder which is screened by an 80-mesh sieve, the lignite, and the coal ash which is screened by an 80-mesh sieve, uniformly stirring, mixing with biochar which is screened by a 20-mesh sieve, fully stirring, and mixing uniformly to prepare the soil heavy metal passivant. The soil heavy metal passivant is easy to prepare; and the effects of passivating the protected horticultural vegetable field soil heavy metal, and reducing the content of recyclable heavy metal of plant in soil can be achieved under the synergistic effects of all components.
Owner:SHENYANG INST OF APPL ECOLOGY CHINESE ACAD OF SCI

Laser fusing and coating process of wear resistant and anticorrosion alloy coatings at surface of slide plate of railroad turnout

A laser cladding process of an exterior wear-resisting anti-corrosive alloy coating of a slide chair of a railway switch comprises processes as follows: firstly, the surface of the slide chair is pre-heated, which means the surface of the slide chair is degreased and de-rusted under room temperature; and the surface is cleaned up by alcohol; then alloy powder is prefabricated, which means iron-base, nickel-base or cobalt base alloy powders that are ready for cladding are preplaced on the processed surface of the slide chair, and a scraping straightedge provided with a rail is used for adjusting the pretreated metal powder so that the alloy powder can be distributed on the surface of the slide chair evenly and has proper thickness to meet the thick requirement of the coating after cladding; and finally, the slide chair is hardened by the laser cladding; the laser of CO2 gas is adopted; a numerical control machine is used as a working table and the surface of the slide chair is hardened by the laser cladding. The laser cladding process has the characteristics of no pollution, high production rate, low energy consumption, the little finishing allowance of cladding coating and low combined cost.
Owner:SHENYANG DALU LASER COMPLETE EQUIP

Method for soft soil foundation treatment through microorganism grouting sand drain

Disclosed is a method for soft soil foundation treatment through microorganism grouting sand drain. The method comprises the steps that a, a pile hole 1 is formed in a soft soil foundation to be treated, and sand is poured into the pile hole 1 to form a sand pile; b, a urease-producing microorganism solution 9 and a nutritive salt solution 10 are sequentially and evenly injected into the sand pile through a grouting tube 6, sand cementation is achieved through the microorganism induction calcium carbonate crystal technology, the concentration of the urease-producing microorganism solution 9 and the concentration of the nutritive salt solution 10 are controlled, sand in the pile body forms a specific cementation mode, and the good water permeable characteristic is ensured; c, after the microorganism grouting solidification sand pile is formed, a flexible water permeable sand cushion 4 is laid on the top of the foundation jointly formed by the sand oil and pile space soil 2, prepressing loads 5 are exerted on the top of the flexible water permeable sand cushion 4, pore water in the pile space soil 2 is made to be drained along a drainage channel formed by the sand pile and the sand cushion, the pile space soil is solidified, and the composite foundation with the high bearing capacity is formed jointly through the soft soil obtained after drainage and solidification are carried out on the microorganism grouting sand pile and the flexible water permeable sand cushion covering the soft soil.
Owner:NANJING FORESTRY UNIV
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