1150 results about "Acetamide" patented technology

The invention belongs to the field of photocatalytic materials, and particularly relates to a high-entropy sulfide and a preparation method and application thereof. The high-entropy sulfide is granular, the molecular general formula is (MnaFebCocCudZe) xS, x is equal to 1, and the atomic ratio of Mn to Fe to Co to Cu to Zn is a: b: c: d: e of (1-2): (1-2): (1-2): (1-2): (1-2): (1-2): (1-2). The preparation method comprises the following steps: S1, dissolving metal salt in a mixed solvent of isopropanol and glycerol according to the atomic ratio of metal elements, and carrying out solvothermal reaction to obtain a precursor; and S2, dispersing the precursor in ethanol, adding thioacetamide as a sulfur source, and carrying out solvothermal reaction to obtain the high-entropy sulfide. The high-entropy sulfide disclosed by the invention is used as a photocatalytic material and shows excellent photocatalytic performance.

The invention discloses a photocatalytic preparation method of a deuterated acetamide compound, and belongs to the technical field of synthesis of deuterated acetamide compounds. According to the technical scheme, the method is characterized in that a dichloroacetamide compound is used as a raw material, D2O is used as a deuterium source, and the dideuterated acetamide compound is synthesized through reaction under the room-temperature nitrogen illumination condition; according to the method, dichloroacetamide compounds are taken as raw materials, D2O is taken as a deuterium source, deuterated dichloroacetamide compounds are synthesized through room-temperature reaction, and monodeuterated or trideuterated acetamide compounds are respectively obtained through photocatalytic reaction according to different solvents (H2O or D2O) added into a system. The preparation method provided by the invention has the advantages of simple and safe operation, mild reaction conditions, no transition metal participation, cheap and easily available deuterium source, high deuteration rate, controllable number and the like.

The invention discloses a fluralamide moxidectin drop and a preparation method thereof, and relates to the technical field of veterinary drugs. The drop is prepared from the following components in parts by weight: 26 to 26.5 parts of fluralan, 1.32 parts of moxidectin, 0.10 part of butylated hydroxytoluene, 29.5 to 30.5 parts of dimethylacetamide, 19.5 to 20 parts of tetrahydrofuran polyethylene glycol ether, 13 to 13.5 parts of diethyl toluamide, 8.5 to 9.3 parts of acetone and 1.0 to 1.5 parts of ethanol. The invention has the effects of improving the stability, permeability and lasting effect of the medicine.

The invention relates to the technical field of layered composite fabrics, in particular to a bio-based antibacterial fiber fabric and a preparation method thereof. The preparation method comprises the following steps: carrying out a reaction on diisocyanate, polyether polyol, bio-based polyester polyol and hexamidine dihydroxyethyl sulfonate in N, N-dimethylacetamide, so as to obtain a polyurethane prepolymer solution; 2-(4-aminophenyl)-5-aminobenzimidazole and amino-modified nano-zinc oxide are sequentially added into the polyurethane prepolymer solution for a reaction, a prepared polyurethane spinning solution is subjected to dry spinning to prepare polyurethane fibers, and then the polyurethane fibers are sequentially spun into yarn and fabric; the bio-based nylon is subjected to melt spinning to obtain bio-based nylon fibers, and the bio-based nylon fibers are sequentially spun into yarns and fabrics; the bio-based antibacterial fiber fabric is prepared by taking a polyurethane fabric as an inner-layer fabric and taking a bio-based chinlon fabric as an outer-layer fabric, and the fabric is good in antibacterial performance and moisture absorption performance.

The invention provides a method for promoting acquisition of clean fuel by light / sound concerted catalytic degradation of waste plastics and upgrading and conversion thereof, which comprises the following steps: uniformly mixing g-C3N4, cadmium acetate and thioacetamide according to a predetermined proportion, pouring into a reaction kettle, placing in a high-temperature oven for a predetermined time, centrifuging, cleaning and drying to obtain a catalyst, the method comprises the following steps: loading a catalyst on the surface of aerogel, hydrogel or non-woven fabric to obtain an MTSJA-loaded catalyst, treating waste plastic with NaOH, adding the MTSJA-loaded catalyst, stirring under irradiation of a xenon lamp, starting ultrasound for reaction, and carrying out light / sound synergistic catalytic degradation on the waste plastic. According to the method, energy consumption is not needed, toxic and harmful gas is not generated, the purposes of energy conservation and environmental protection can be achieved, meanwhile, carbon dioxide in water can be catalytically reduced to generate clean energy such as methane in the process of degrading the waste plastic, and further obtaining of the energy is promoted.

The invention discloses a method for synthesizing a Mn0. 43Cd0. 57S / Cu2MoS4 photocatalyst by adopting a solvothermal method, and belongs to the technical field of catalysts. The preparation method comprises the following steps: preparing copper molybdenum sulfide by using cuprous oxide as a template, synthesizing copper molybdenum sulfide with high purity and good crystallinity by combining a solvothermal method, preparing manganese cadmium sulfide by using manganese acetate, cadmium acetate, sodium hydroxide and thioacetamide as raw materials, adding copper molybdenum sulfide before a hydrothermal reaction, successfully modifying the manganese cadmium sulfide by constructing a heterojunction, and preparing the copper molybdenum sulfide modified manganese cadmium sulfide. The Mn0. 43Cd0. 57S / Cu2MoS4 photocatalyst is synthesized, and the photocatalytic hydrogen production rate of the cadmium manganese sulfide is improved. Moreover, the hydrogen production rate of the Mn0. 43Cd0. 57S / Cu2MoS4 photocatalyst prepared by the invention can reach 8233 mu mol / (g.h), which is 2.08 times of the hydrogen production rate of pure cadmium manganese sulfide, and 1.24 times of the hydrogen production rate of cadmium manganese sulfide loaded with 1% platinum.

The present disclosure relates to pharmaceutically acceptable salts, cocrystals, and crystalline forms thereof, of a compound which is N—((S)-1-(3-(4-chloro-3-(methylsulfonamido)-1-(2,2,2-trifluoroethyl)-1H-indazol-7-yl)-6-(3-methyl-3-(methylsulfonyl)but-1-yn-1-yl)pyridin-2-yl)-2-(3,5-difluorophenyl)ethyl)-2- ((3bS,4aR)-5,5-difluoro-3-(trifluoromethyl)-3b,4,4a,5-tetrahydro-TH-cyclopropa[3,4]cyclopenta[1,2-c]pyrazol-1-yl)acetamide, which is useful in the treatment of a Retroviridae viral infection including an infection caused by the HIV virus.

The present invention relates to the field of the preparation of polyurethane elastic fibers, and relates to a preparation method for a bio-based polyurethane elastic fiber, comprising: preparing polyether polyol from sucrose, glycerol, dimethylamine and propylene oxide; adding a solvent, i.e., N,N-dimethylacetamide, and polyether polyol and polyisocyanate into a reaction tank, and adding p-Toluenesulfonyl semicarbazide and aluminum methylenebis(2,4-di-tert-butylphenoxy) phosphate to prepare a spinning solution; and subjecting the spinning solution to spinning and oil application by means of dry spinning technology to obtain the bio-based polyurethane elastic fiber. The present invention ensures that the properties of polyurethane elastic fibers do not deteriorate or are partially enhanced, while the cost and performance advantages are achieved.

The invention provides a method for preparing high-purity hafnium tetrachloride by wet extraction and separation, which comprises the following steps: stirring and leaching hafnium alloy waste serving as a raw material by using HNO3 and HF mixed acid, then adding thioacetamide, adjusting the pH value to 4-5, stirring and filtering; compounding tributyl phosphate, trioctylphosphine oxide and sulfonated kerosene to obtain a composite extracting agent, and stirring and mixing to form a homogeneous organic phase; in a hydrochloric acid medium, controlling the volume ratio of an organic phase to a water phase to be (2.5-3.5): 1, carrying out three-stage counter-current extraction, and standing for phase splitting; the extracted organic phase passes through an adsorption column filled with iminodiacetic acid modified silica gel; and carrying out reverse extraction by using a hydrochloric acid solution, and then carrying out reduced pressure evaporation concentration, cooling crystallization and dehydration to obtain hafnium tetrachloride. According to the method, the zirconium and hafnium separation efficiency in the hafnium tetrachloride preparation process is improved, and the problem that the content of zirconium and hafnium impurities in the product is too high is solved.

The invention relates to a nitrogen-containing heterocyclic compound as well as a preparation method and application thereof, belongs to the technical field of heterocyclic compound synthesis, and solves the problems of low reaction efficiency and high energy consumption caused by the fact that an existing method for synthesizing an indole maleimide derivative needs to be carried out step by step. The preparation method comprises the following steps: step 1, adding indoleacetamide and a nucleophilic reagent into a mixed solution, and reacting; 2, performing post-treatment to obtain a nitrogen-containing heterocyclic compound; the mixed solution comprises alkali, an additive and an organic solvent; the alkali comprises one of triethylamine (Et3N), N, N-diisopropylethylamine, pyridine and 1, 8-diazabicyclo [5.4. 0] undec-7-ene, and the alkali comprises one of 1, 8-diazabicyclo [5.4. 0] undec-7-ene.

The application discloses a preparation method of a hydrophilic oil-water separation anti-pollution membrane and the anti-pollution membrane and application thereof, and prepares MNRs material; the MNRs material is dispersed in dimethylacetamide, is uniformly stirred, polyvinylpyrrolidone is added, and stirring is continued, and a first mixture is obtained through ultrasonic treatment; the first mixture is mixed with polyvinylidene fluoride to obtain a second mixture, and the second mixture is stirred; the treated second mixture is dip-coated on a carrier, the dip-coated carrier is treated in deionized water to obtain an ultrafiltration membrane; the ultrafiltration membrane is soaked in a tea polyphenol solution with a Tris-HCl buffer solution, and is shaken to obtain the hydrophilic oil-water separation anti-pollution membrane. The hydrophilic oil-water separation anti-pollution membrane has excellent separation efficiency and flux recovery rate for four different oil-water mixtures of kerosene, gasoline, edible oil and n-hexane. The preparation process of the oil-water separation membrane is simple, the cost is low, and the reaction condition is mild; when the oil-water separation membrane is applied to organic wastewater separation, the oil-water separation membrane has the advantages of high efficiency, good removal performance and good recycling performance.

This application relates to the field of microbial fermentation technology, and specifically discloses an N-hydroxyamino-N'-acetylguanine blue, its fermentation method and application. The chemical name of the N-hydroxyamino-N'-acetylguanine blue is N-(5'-hydroxyamino-2,6,2',6'-tetraoxo-1,6,1',6'-tetrahydro-2H,2'H-[3,3'] bipyridylmethylene)-acetamide, and the molecular formula is C 12 H 10 O6N4; compared with N-acetylguanine blue, the absorption of N-hydroxyamino-N'-acetylguanine blue is deeper in color at UV611, and at the same time, the formation of hydrogen bonds with amino groups on the fiber can enhance the dyeing property of the dye on the fiber and improve the wash fastness.

The invention is applicable to the field of preparation of modified polyimide materials, and provides a transparent polyimide film material with corona resistance and a preparation method thereof, the transparent polyimide film material comprises the following raw materials: nano SiO2 particle-N, N-dimethylacetamide dispersion liquid, a diamine monomer, a benzoxazine monomer and a dianhydride monomer; wherein the N, N-dimethylacetamide dispersion liquid contains nano silicon dioxide (the particle size is about 10-20 nm, and the mass fraction is 30 wt% + / -5 wt%). The transparent polyimide film with corona resistance is prepared by uniformly dispersing nano silicon dioxide particles and benzoxazine in a polyimide matrix by adopting an in-situ polymerization method, the film realizes excellent corona resistance of a material, and meanwhile, the preparation method has the advantages of simple process, energy conservation, environmental protection, high efficiency and the like.

The invention relates to the technical field of battery materials, and discloses a composite solid electrolyte diaphragm as well as a preparation method and application thereof. The composite solid electrolyte diaphragm comprises a base membrane and a solid electrolyte coating arranged on at least one surface of the base membrane, the solid electrolyte coating comprises an electrolyte I and an electrolyte II; the electrolyte I is lithium titanium aluminum phosphate and lithium lanthanum zirconium tantalum oxide; and the electrolyte II is a compound of lithium bis (oxalate) borate and acetamide in a molar ratio of 1: (6.5-7.5). The composite solid electrolyte diaphragm provided by the invention can realize relatively high ionic conductivity, and when the composite solid electrolyte diaphragm is used in a lithium ion battery, the battery can have relatively low internal resistance.

The invention discloses a preparation method of a rare earth ion doped antibacterial modified hydroxyapatite whisker material, and relates to the technical field of medical biomaterials.The preparation method comprises the steps that acetamide is dissolved in deionized water, and a solution A is obtained; dissolving calcium salt, cerium salt and ammonium salt in a certain proportion in the solution A to obtain a solution B; stirring the solution B at room temperature, performing ultrasonic dispersion, and adjusting the pH value to be acidic to obtain a solution C; and putting the solution C into a high-pressure reaction kettle, heating and reacting, aging, cleaning, carrying out suction filtration, and drying to obtain the cerium-doped hydroxyapatite whisker material. The preparation process is simple, the product is stable, and the prepared modified hydroxyapatite whisker has an obvious antibacterial effect on escherichia coli and staphylococcus aureus and can be applied to the field of bone repair antibacterial materials.

The invention discloses a preparation method of a vanadium battery electrolyte oxidation corrosion resistant composite membrane, which comprises the following steps: S1, uniformly dispersing graphene oxide nanosheets on the surface of an SPEEK (sulfonated polyether ether ketone) matrix by using sulfonated polyether ether ketone as a substrate to obtain an SPEEK / GO (graphene oxide) substrate; s2, treating the SPEEK / GO substrate in oxygen plasma treatment equipment, and ultrasonically cleaning the SPEEK / GO substrate with isopropanol for 10-20 minutes; s3, dissolving polybenzimidazole in N, N-dimethylacetamide (the concentration is 3-5wt%), and magnetically stirring until the polybenzimidazole is completely dissolved; the preparation method comprises the following steps: adding TiO2 nanoparticles (the particle size is 20-25nm, and the TiO2 nanoparticles are pretreated by a silane coupling agent KH-570) according to the mass ratio of 15-20%, ultrasonically dispersing and carrying out ice bath to obtain PBI-TiO2 dispersion liquid; s4, the SPEEK / GO substrate treated in the step S1 is vertically immersed in PBI-TiO2 dispersion liquid, the final coating thickness is 1.5 + / -0.2 [mu] m, and a pretreated film is obtained; and S5, carrying out hot pressing on the pretreated membrane by using a hot press, and then carrying out gradient cooling to room temperature to obtain the final composite membrane. The vanadium battery is better in vanadium resistance and corrosion resistance and suitable for high-power-density vanadium batteries.

The invention belongs to the technical field of near-infrared organic dye synthesis, and particularly discloses a cyanine dye with J aggregation characteristic, J aggregation nanoparticles, and preparation methods and applications of the cyanine dye and the J aggregation nanoparticles. The cyanine dye is 1-ethyl-2-(2-(2-(-3-(2-(1-ethyl-3, 3-dimethyl-1, 3-dihydro-2H-benzo [g] indole-2-subunit) ethylidene)-2-(2, 2, 2-trifluoro-N-(2-methylbenzyl) acetamide) cyclopent-1-ene-1-yl) vinyl)-3, 3-dimethyl-3H-benzo [g] indoleiodised salt, and the structural formula of the cyanine dye is shown in the description. The preparation method is simple, the J aggregation nanoparticles can be prepared by utilizing the unique property of J aggregation, the J aggregation nanoparticles have high light stability and have strong fluorescence emission in a near-infrared second region, and the material prepared by the invention can be used as a contrast agent and is applied to the field of near-infrared second region fluorescence imaging.

The invention discloses a preparation method of a spiro [4.5] trienone compound containing difluoro gamma-lactam, which comprises the following steps: reacting an N-(4-methoxyphenyl)-N-methyl-3-phenylpropanamide compound and an N-allyl-2, 2-difluoro-2-bromo-N-aryl acetamide compound in an argon atmosphere under the action of a photocatalyst and alkali to obtain the spiro [4.5] trienone compound containing difluoro gamma-lactam. And reacting under the irradiation of 467 nm blue light to obtain the spiro [4.5] trienone compound containing difluoro gamma-lactam. The reaction operation is simple and convenient, the product specificity is high, the substrate application range is wide, and the price is low. The invention provides a simple and efficient preparation method of the spiro [4.5] trienone compound containing difluoro gamma-lactam for the first time.

The application relates to a preparation method of a hollow fiber membrane composite thermal insulation material, which comprises the following steps: adding 18-22% of polyurethane, 4-8% of polyethylene glycol 2000 and 72-76% of N,N-dimethylacetamide into a spinning reaction kettle to mix, stir and defoam to prepare homogeneous casting solution; based on a non-solvent induced phase separation method, the homogeneous casting solution is coated on the surface of a polyester braided tube through a spinneret by adopting a concentric circle composite spinning technology, is gathered on a spinning wheel after a coagulation bath to form a reinforced polyurethane hollow fiber membrane assembly which is arranged in parallel and obliquely crosses and is mutually bonded, and the fiber membrane assembly is hot-pressed to prepare the hollow fiber membrane composite thermal insulation material under the conditions of a temperature of 60-150 DEG C and a pressure of 120-470 MPa. Since the coating layer and the braided tube are both through porous structures, the prepared composite material has good air permeability.

The invention relates to the field of composite ultrafiltration membranes, in particular to a GO / PVDF composite ultrafiltration membrane for MBR and a preparation method of the GO / PVDF composite ultrafiltration membrane. The GO / PVDF composite ultrafiltration membrane is prepared by adopting 18% of polyvinylidene fluoride as a membrane base material, 6% of polyvinylpyrrolidone as a pore-foaming agent, 0-2% of graphene oxide as a modifier and the balance of N, N-dimethylacetamide as a solvent through an impregnation phase inversion method. The GO with low mass fraction is added into the section of the membrane to form a large and thick finger-shaped pore structure, the filtration resistance of membrane pores is reduced, the filtration flux, hydrophilicity, permeability and interception performance of the membrane are improved, the method is simple to operate, the prepared finished product is excellent in performance, and the research and application expansion of a membrane modification technology are promoted.

The invention discloses a preparation method of a polyimide-boron nitride nanosheet heat-conducting composite film. The preparation method comprises the following steps: firstly, dispersing boron nitride nanosheets into N, N-dimethylacetamide containing poly (diallyldimethylammonium chloride) to prepare slurry; meanwhile, 4, 4 '-diaminodiphenyl ether reacts with pyromellitic dianhydride to prepare a polyamide acid solution. And mixing the two materials, forming a layered structure through vertical and horizontal temperature gradients by adopting a bidirectional freezing casting technology, and freezing by liquid nitrogen to obtain the aerogel in oriented arrangement. And performing hot pressing and step-by-step thermal imidization treatment to obtain the heat-conducting composite film. According to the method, the highly-oriented arrangement of boron nitride nanosheets is constructed through bidirectional freezing casting, and the composite film has excellent heat-conducting property and keeps good mechanical strength and flexibility in combination with the surface modification effect. The process is simple and controllable, and is suitable for the fields of flexible electronics, 5G heat dissipation, battery thermal management and the like.

The invention discloses a high-self-cleaning weather-resistant GRTV insulating coating for electrical equipment, which comprises the following components: a film-forming agent consisting of solvent-type fluororesin, hydroxyl-terminated polysiloxane, acrylic resin and polyether polyol, a reinforcing agent consisting of at least two of MQ silicon resin, silicon dioxide, silicon nitride and fluororesin micro powder, a filling agent consisting of aluminum oxide, a curing agent consisting of a curing agent and a solvent, the curing agent is composed of two or three components of tetraethoxysilane, methyltriacetamide silane, dimethyl diacetamide silane or dibutyltin oxide, and trichloroethylene or butyl acetate is used as an organic solvent; the anti-pollution flashover coating is good in adhesive force, excellent in electrical insulation performance, good in hydrophobicity, high in anti-pollution flashover capacity, excellent in mildew resistance, algae resistance and anti-burst scattering characteristic, good in self-cleaning performance and capable of better exerting the anti-pollution flashover efficiency under the conditions of high salinity, high humidity and heavy pollution, and the insulation strength is not affected by environment temperature and moisture.

The invention relates to the technical field of benzamide, in particular to a preparation process of 4-hydroxythiobenzamide, which comprises the following steps: S1, preparing raw materials: preparing the 4-hydroxythiobenzamide from the following raw materials in parts by weight: 80-100 parts of formic acid, 80-100 parts of hydrochloric acid, 20-30 parts of 4-hydroxybenzaldehyde, 8-12 parts of hydroxylamine hydrochloride, 8-12 parts of thioacetamide and 4-6 parts of sodium hydroxide. According to the preparation method, after 4-hydroxybenzaldehyde is subjected to activating treatment reaction, part of positive charges on aldehyde carbon are dispersed, oxygen atoms in an acetal structure are connected with the aldehyde carbon through covalent bonds to generate an electron withdrawing induction effect, the reaction sequence and the reaction path of the 4-hydroxybenzaldehyde can be controlled through aldehyde activation, and the reaction efficiency of the 4-hydroxybenzaldehyde is improved. Therefore, the generation of byproducts is reduced, and the purity of a reaction product obtained from 4-hydroxybenzaldehyde is improved.

The application discloses a kind of hydrolysis-resistant acetylacetamide modified polyvinyl alcohol and preparation method thereof, and the preparation method comprises the following steps: double vinyl ketone and first and alcohol amine compound are reacted to generate N-(hydroxyalkyl) acetylacetamide intermediate;Then trichloro cyanogen and N-(hydroxyalkyl) acetylacetamide intermediate are reacted to generate 3,5-bis[acetylacetamide alkoxyl] monochloro s-triazine;Finally, 3,5-bis[acetylacetamide alkoxyl] monochloro s-triazine is reacted with PVA in polar solvent to generate AAM-PVA.The AAM-PVA prepared in the application can be used as a protective colloid for polyvinyl acetate emulsion polymerization, and the prepared emulsion adhesive has obvious improvement in water resistance, tensile strength and stability;The raw materials of the application are cheap and easy to obtain, the preparation process is simple, the reaction conditions are mild, and there is no waste water and waste gas emission.

The present invention belongs to the technical field of fabric color fixing agents and provides a novel acidic color fixing agent free of bisphenol S and a preparation method thereof; the acidic color fixing agent is composed of the following components in parts by weight: 15-25 parts of water, 10-15 parts of phenol, 15-25 parts of dimethylacetamide, 2-5 parts of sodium sulfite, 10-15 parts of acetic acid, 5-7 parts of concentrated sulfuric acid, 15-20 parts of acrylic acid, 2-5 parts of ethylene glycol dimethyl ether, and 1-3 parts of sorbitol; the preparation method comprises the following steps: mixing a formula amount of phenol, dimethylacetamide, acrylic acid, acetic acid, and sodium sulfite, heating, adding concentrated sulfuric acid to react, cooling, adding a formula amount of water, and adding a formula amount of ethylene glycol dimethyl ether and sorbitol to obtain the product. Compared with the prior art, the present invention does not contain bisphenol S, has a good color fixing effect, can effectively improve various fastnesses such as water fastness, perspiration fastness, and seawater resistance, has little effect on the color change of the fabric after treatment, and has good tolerance to hardness ions.

The invention relates to an electroreduction method for synthesizing acetamide by coupling carbon dioxide and nitrate through electrocatalysis. The electroreduction method specifically comprises the steps that cobalt salt, copper salt, a nitrogen source and carbon source carbon black are mixed, heated and calcined, and a carbon nitride loaded copper-cobalt diatomic catalyst is prepared; loading the obtained carbon nitride loaded copper-cobalt diatomic catalyst on the surface of carbon paper to prepare a gas diffusion electrode of a three-chamber flow cell electrolytic tank; the obtained gas diffusion electrode is applied to a three-chamber flow cell electrolytic tank to prepare acetamide through electroreduction. The copper-cobalt double-atom catalyst is used for synthesizing acetamide through electrochemical coupling of carbon dioxide and nitrate, the acetamide Faraday efficiency in a flow cell can reach 18% or above, and the yield is 81.2 mg L <-1 >. H <-1 >. Compared with the prior art, the prepared copper-cobalt diatomic catalyst has high selectivity for generation of acetamide through co-reduction coupling of carbon dioxide and nitrate radicals, and synchronous treatment of greenhouse gas carbon dioxide and nitrate wastewater and value-increasing utilization of carbon and nitrogen resources can be achieved.

The invention discloses a compound fluralana external preparation for dogs, a preparation method and application, belongs to the technical field of veterinary drugs, and solves the problems that an existing preparation is poor in skin surface permeability, a solvent is easy to volatilize, and use experience and drug effect exertion are influenced. The preparation is prepared from the following raw materials: fluralana, moxidectin, ethyl butylacetamidopropionate and N, N-dimethylformamide. The preparation method comprises the following steps: adding N, N-dimethylacetamide, acetone, an auxiliary adjuvant, a transdermal penetration enhancer, an antioxidant and a surface film-forming agent; according to the invention, the combination of the fluralab and the moxidectin can play a synergistic effect and expand an anti-parasitic spectrum so as to achieve an internal and external driving effect; both the fluralab and the moxidectin belong to high-fat-soluble substances, parasites can be quickly repelled and killed by adding novel adjuvant natural parasite expelling ingredients, and meanwhile, the skin permeability can be improved by adding the efficient transdermal penetration enhancer, and the risk that medicine residues are licked by pets is reduced.

Silicone hydrogel contact lens formulations are described herein. The formulation has a silicone component and a silicone-free component. The silicone component comprises two or three compounds represented by a formula 1, a formula 2 or a formula 3. The silicone-free component includes a methacrylate component and an N-vinyl amide component. The methacrylate component is prepared from hydroxybutyl methacrylate (HOB) and isobornyl methacrylate (IBM). And the N-vinyl amide component is prepared from N-vinyl N-methyl acetamide. When compounds of Formula 1 and compounds of Formula 2 are present in the formulation in specific ratios relative to each other, specific amounts of HOB and IBM are provided to achieve specific ratio results in desired silicone hydrogel contact lenses. Silicone hydrogel contact lenses are also described.

The invention discloses a method for rapidly synthesizing MOFs (Metal-Organic Frameworks) derived sulfide CoS / Co-MOF (Metal-Organic Frameworks). The synthesis method comprises the following steps that a Co-MOF precursor is obtained through a solvothermal method, then the Co-MOF precursor is mixed with thioacetamide, absolute ethyl alcohol and dimethylacetamide, and the MOFs derivative sulfide CoS / Co-MOF composite material is obtained through the solvothermal method. Compared with a traditional pyrolysis method, the method is easy and convenient to operate and mild in condition, the reaction time is greatly shortened, and in addition, a series of electrochemical tests (LSV, CV, EIS and CP) prove that the CoS / Co-MOF composite material shows excellent OER performance and is an excellent OER catalyst.

The invention relates to the technical field of electrolytes, in particular to a wide-temperature-range high-voltage lithium ion battery electrolyte containing an amide solvent and a preparation method of the wide-temperature-range high-voltage lithium ion battery electrolyte. The fluorinated amide solvent comprises a main solvent and a cosolvent, the main solvent comprises one or more of perfluoro-2-methyl pyrrolidone, perfluoro-N-methyl pyrrolidone, perfluoro-epsilon-caprolactam, N, N-difluoroethyl formamide and trifluoroacetamide, and the cosolvent comprises one or more of perfluoro-2-methyl pyrrolidone, perfluoro-N-methyl pyrrolidone, perfluoro-epsilon-caprolactam, N, N-difluoroethyl formamide and trifluoroacetamide. The lithium salt comprises one or more of lithium bis (fluorosulfonyl) imide, lithium bis (trifluoromethanesulfonyl) imide, lithium bis (oxalato) borate, lithium difluoro (oxalato) borate and lithium tetrafluoroborate; the functional additives comprise a high-voltage additive, a temperature-adaptive additive and a flame retardant. The obtained electrolyte can maintain good electrochemical performance in a wide temperature range, has high voltage stability, improves the energy density and safety of the lithium ion battery, and prolongs the cycle life of the lithium ion battery.