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41 results about "Acesulfame potassium" patented technology

Acesulfame potassium (/ˌeɪsiːˈsʌlfeɪm/ AY-see-SUL-faym), also known as acesulfame K (K is the symbol for potassium) or Ace K, is a calorie-free sugar substitute (artificial sweetener) often marketed under the trade names Sunett and Sweet One. In the European Union, it is known under the E number (additive code) E950. It was discovered accidentally in 1967 by German chemist Karl Clauss at Hoechst AG (now Nutrinova). In chemical structure, acesulfame potassium is the potassium salt of 6-methyl-1,2,3-oxathiazine-4(3H)-one 2,2-dioxide. It is a white crystalline powder with molecular formula C₄H₄KNO₄S and a molecular weight of 201.24 g/mol.

Process method for optimizing acesulfame potassium crystal habit

The invention discloses a process for optimizing the crystal habit of an acesulfame potassium product. The process comprises the following steps: heating and dissolving an acesulfame crude product and a solvent to prepare a supersaturated solution, firstly, sequentially carrying out activated carbon adsorption and membrane adsorption for decoloration, then cooling at a certain rate for cooling crystallization, adding a certain amount of primary seed crystal in a nucleation stage 1, adding a certain amount of secondary seed crystal in a nucleation stage 2, and after the temperature of the material is reduced to 10 DEG C, cooling and crystallizing to obtain the acesulfame potassium crystal. And centrifugally drying the material to obtain the acesulfame potassium stable crystal form product. According to the present invention, the suitable solvent and the suitable cooling rate are selected, and the seed crystal is added during the cooling crystallization process, such that the content of the metastable crystal form is significantly reduced, the content of the stable crystal form is increased, and the particle size distribution, the yield and the purity of the acesulfame potassium product are effectively improved so as to solve the caking problem of the acesulfame potassium product during the storage process.
Owner:NANTONG HONGXIN CHEM CO LTD +1

Refreshing cigarette and preparation method thereof

The invention discloses a refreshing cigarette and a preparation method thereof, and particularly relates to the technical field of refreshing products. The refreshing cigarette comprises 6% of a plant extract, 2% of a mint extract, 36% of sorbitol, 16% of xylitol, 15% of maltitol, 2% of edible perfume essence, 2% of glycerin, 3% of D-mannitol, 3% of sucralose, 2% of acesulfame potassium, 2% of phospholipid, 3% of sucrose and 8% of starch. The preparation method of the refreshing cigarette comprises the following steps: S1, selecting raw materials: selecting natural plants as the raw materials; s2, boiling and purifying: extracting effective components in the plants through a specific boiling process; s3, mixing; s4, combined machining; s5, inspecting a finished product; and S6, packaging and delivering. According to the refreshing cigarette and the preparation method thereof provided by the invention, the mint extract, the glycerol, the D-mannitol, the sucralose, the acesulfame potassium and other components act together, so that an obvious refreshing effect is provided.
Owner:NINGXIA JIUYUAN AGRICULTURAL TECHNOLOGY CO LTD

Process for preparing acesulfame-k and recycling by-products

The application discloses a preparation and by-product recycling process of acesulfame potassium, and belongs to the technical field of food additive production and processing. Amino sulfonic acid is added into N-butyl pyridine hydrogen sulfate ionic liquid and triethylamine in batches to obtain a homogeneous mixed solution; secondly, the mixed solution and diketene are introduced into a micro-channel reactor to perform a condensation reaction; and the discharge liquid is introduced into a polystyrene sulfonic acid resin loaded SO3 fixed bed reactor to perform a cyclization reaction; subsequently, the cyclization product is subjected to hydrolysis, decolorization, potassium salt crystallization and drying to obtain the acesulfame potassium product; and the crystallization mother liquor is separated through a nanofiltration membrane, and the intercepted liquid is an ionic liquid and triethylamine mixture, which is directly reused. The application inhibits the self-polymerization of diketene through the micro-channel reactor, replaces concentrated sulfuric acid with solid acid to avoid waste acid pollution, and realizes efficient recycling of by-products by combining nanofiltration membrane separation and catalytic depolymerization technology, and has the characteristics of green environmental protection and economic efficiency.
Owner:ANHUI JINHE INDUSTRIAL CO LTD

A method of extracting an intermediate ACH

PendingCN122301804AHigh extraction yieldreduce carryPotassium acesulfameSulfanilamide
This invention discloses a method for extracting the intermediate ACH, belonging to the field of fine chemicals. The method involves passing a layered acid containing acesulfame potassium (DCM) and a dichloromethane solution into a rotary extraction tower for extraction. The temperature of the layered acid entering the tower is 30-31°C. The extraction pressure and the temperature of the dichloromethane entering the tower are controlled. The extracted dichloromethane layer enters a vibrating extraction tower for back-extraction with deionized water. The back-extracted DCM is neutralized, concentrated, crystallized, and dried to obtain the finished product, potassium acesulfame potassium. Using this method, the ACH content in the extracted acid is reduced to below 0.1%, and the ACH extraction yield reaches over 98%. Because the rotary extraction tower effectively reduces the acid carryover in the DCM, it lowers the back-extraction load, ensuring the product quality of potassium acesulfame potassium. Simultaneously, it simplifies the process conditions, reduces energy consumption, and saves production costs.
Owner:NANTONG ACETIC ACID CHEM +1

Acesulfame potassium hydrolysis process and application

The invention belongs to the technical field of food additive preparation, and particularly relates to an acesulfame potassium hydrolysis process and application. The process adopts a secondary hydrolysis process, and comprises the following steps: introducing sulfonation liquid in a front section and washing acid water (2-4%) in a rear section into a first hydrolysis reactor, and accurately controlling the specific gravity of hydrolysis acid and temperature parameters (for example, the specific gravity is 1.2-1.3, and the temperature is-5 DEG C to 15 DEG C); materials in the middle of the first hydrolysis reactor continuously overflow into a second hydrolysis reactor (hydrolysis transfer kettle) containing a stirring pump and an external circulation pump, the reaction time is prolonged, mass transfer is enhanced through external circulation, and the material retention time is prolonged; and feeding the material in the second hydrolysis reactor into a hydrolysis layering tank, standing, separating an upper-layer acid phase, washing a lower-layer organic phase with water, and finally neutralizing with potassium hydroxide to obtain an acesulfame potassium crude product sugar water solution. The reaction sufficiency is improved through secondary hydrolysis, the temperature is stabilized, the ice maker load and the labor intensity are reduced, the process adaptability is enhanced, and the acesulfame potassium production stability and yield are effectively improved.
Owner:ANHUI JINHE INDUSTRIAL CO LTD

A method for simultaneously determining caffeine and various sweeteners in new tea beverages by high performance liquid chromatography

PendingCN122150470AComponent separationBiotechnologyAlitame
The application belongs to the technical field of chromatographic detection, and specifically discloses a method for simultaneously determining caffeine and various sweeteners in new tea drinks by high performance liquid chromatography. The application first prepares a sample of the new tea drink; then extracts the sample by ultrasonic wave to obtain a sample to be detected; and then detects the components to be detected in the sample to be detected by using specific high performance liquid chromatography conditions, and obtains the content of the components to be detected through post-processing; the components to be detected include caffeine, acesulfame potassium, sodium saccharin, aspartame, alitame, advantame, neotame, stevioside, rebaudioside A and rebaudioside C. The testing method disclosed by the application can simultaneously determine caffeine and various sweeteners in new tea drinks, improves the detection efficiency, reduces the detection cost, prevents and controls the food safety risk, and promotes the standardization system construction of new tea drinks.
Owner:YAAN QUALITY INSPECTION & TESTING INST (YAAN FOOD & DRUG INSPECTION INST)

Non-aspartame sweetener compositions and related method

PCT designated stage expiredWO2025136791A3ConfectioneryChewing gumSteviolmonosidePhysical chemistry
Non-aspartame sweetener compositions, systems and methods for predicting the sweetness intensity of confectionery products, and coating compositions comprising rebaudioside M are disclosed herein. A non-aspartame sweetener composition may include one or more of an unencapsulated high intensity sweetener other than a steviol glycoside, an agglomerated rebaudioside, an agglomerated high intensity sweetener other than a steviol glycoside, and a mixture of steviol glycosides. The composition may also include at least one of a first encapsulated high intensity sweetener and a second encapsulated high intensity sweetener different from the first encapsulated high intensity sweetener, wherein each of the first encapsulated high intensity sweetener and the second encapsulated high intensity sweetener is one of saccharin and its salts, acesulfame and its salts, or another high intensity sweetener other than a steviol glycoside.
Owner:WM WRIGLEY JR CO

Novel cyclization reaction device and system for acesulfame potassium production

The invention discloses a novel cyclization reaction method, device and system for acesulfame potassium production. The system comprises a premixing device, a cyclization device, a centrifugal device and a heat exchange device. The method comprises the following steps: firstly, sulfur trioxide and dichloromethane form a premixed solution, the premixed solution and DKA enter a cyclization reactor together, a cyclization reaction in the cyclization reactor is subjected to process reinforcement through a rotating packed bed, mutual contact and relative flow velocity of triethylamine salt and sulfur trioxide are improved, the reaction is promoted to proceed forwards, and ACH is finally produced through hydrolysis. The system achieves the purpose of continuous production through extremely short retention time and small reactor size, and greatly improves the DKA conversion rate (99.5%) and the AK sugar yield (87.5%).
Owner:NANTONG HONGXIN CHEM CO LTD +1

Compound-taste lemon black tea beverage formula capable of balancing sour-sweet ratio and tea astringent taste

The invention discloses a compound-taste lemon black tea beverage formula capable of balancing the sour-sweet ratio and the tea astringency. The compound-taste lemon black tea beverage formula consists of high fructose corn syrup, BS921 instant black tea powder, green spring lemon normal juice, table salt, citric acid monohydrate, malic acid, sodium citrate, potassium sorbate, sodium cyclamate, acesulfame potassium, aspartame, caramel color, sunset yellow, vitamin C, CJ9433 black tea essence, CJ9183 lemon essence and purified water. By constructing a four-dimensional balance model of a sweet gradient system, a sour buffer system, an astringent inhibition system and a color and aroma stabilizing system, the problems that existing lemon black tea is unbalanced in sour-sweet ratio, heavy in astringent taste, thin in taste and poor in stability are solved. Through the synergistic effect of the compound sweetening agent and the sour buffer salt, the product is palatable in sourness and sweetness, mellow in tea fragrance, free of bitter and astringent aftertaste, full in compound taste and good in shelf life stability.
Owner:郑财

Oral solution containing salbutamol sulfate and preparation method thereof

According to the salbutamol sulfate-containing oral solution and the preparation method thereof provided by the invention, sucralose or acesulfame potassium is taken as a flavoring agent, so that the oral solution is relatively good in dissolvability, can relieve bitter taste and obtain a relatively good taste masking effect, is relatively good in taste, improves the medication compliance of a patient, improves the stability of the oral solution and prolongs the validity period of the medicine. The oral solution containing salbutamol sulfate provided by the invention is simple in preparation method, and has good taste masking effect and stability.
Owner:NANJING HEALTHNICE MEDICAL TECH +3

Flavored beverage capable of improving sleep and preparation method thereof

The invention relates to a flavor beverage capable of improving sleep and a preparation method thereof. Every 50ml of the flavored beverage comprises the following raw materials: a functional agent, a sweetening agent, an acidulant, a stabilizing agent and a solvent, the functional agent is prepared from 100 to 150 mg of gamma-aminobutyric acid, 2.5 to 3.5 g of resistant dextrin, 8 to 12 mg of long pepper extract powder, 6 to 10 mg of ginger extract powder, 12 to 18 mg of EGCG, 0.6 to 1.0 mg of L-phenylalanine compound, 3.0 to 4.5 mg of vitamin B6 and 1.5 to 2.25 mg of vitamin B2; the sweetening agent is prepared from 2.0 to 3.0 g of high fructose corn syrup, 0.4 to 0.6 g of fructose, 2.5 to 3.5 mg of acesulfame potassium and 1.2 to 1.8 mg of aspartame; the sour agent is prepared from 25 to 35 mg of vitamin C, 20 to 30 mg of citric acid and 3 to 5 ml of natural flavor extracting solution; the stabilizing agent is prepared from 5.0 to 7.0 mg of xanthan gum and 4.0 to 6.0 mg of glycerin monostearate; the solvent is purified water, and the total volume is 50ml; wherein the purity of the gamma-aminobutyric acid is greater than or equal to 99%, the piperine content in the long pepper extract powder is greater than or equal to 5%, and the gingerol content in the ginger extract powder is greater than or equal to 1%. The flavor beverage capable of improving sleep provided by the invention can mildly help sleep, and is high in bioavailability, healthy in taste, strong in stability, free of melatonin dependence and easy in mass production.
Owner:JIANGSU DEHE BIOTECH

Electrolyte and sodium-ion battery containing the electrolyte

This invention provides an electrolyte and a sodium-ion battery. The electrolyte comprises a sodium salt, a non-aqueous organic solvent, and additives. The additives include: (a) sodium acesulfame potassium, with the structural formula shown in Formula 1; and (b) an acid anhydride compounds. The electrolyte comprises sodium acesulfame potassium and an acid anhydride compounds. Sodium acesulfame potassium can form a tough, shatter-resistant, and high-temperature resistant interfacial film during the first charge-discharge stage of the battery. However, this interfacial film contains sulfur and nitrogen elements, which easily dissolve in the electrolyte, consuming some of the active sodium to form a new interfacial film, causing gas production and a decrease in the initial coulombic efficiency of the battery. The acid anhydride compounds, due to their high film-forming potential, easily form a dense interfacial film at the negative electrode, effectively mitigating the side reactions of sodium acesulfame potassium in the electrolyte after film formation. Using this electrolyte in a sodium-ion battery can improve the initial coulombic efficiency, high-temperature storage performance, and cycle performance of the sodium-ion battery under high voltage.
Owner:ZHUHAI SMOOTHWAY ELECTRONICS MATERIALS

Sweetener and manufacturing method thereof

PCT designated stageWO2026010037A1Food coatingBiotechnologyThaumatin
A sweetener according to exemplary embodiments comprises: a core including one selected from erythritol, xylitol, sorbitol, maltitol, mannitol, inositol, lactitol, isomalt, and allulose; and a shell surrounding at least a portion of the core and including one selected from stevia, enzyme-treated stevia, steviol glycoside, mogroside, thaumatin, sucralose, aspartame, saccharin, acesulfame potassium, and neotame, wherein a content ratio of the shell to the core may be 0.002 to 0.05. The sweetener has a core-shell structure, wherein the core and the shell are each made into a single raw material without any separate additives (e.g. excipients), and thus is close to zero calories.
Owner:DR TRUE CORP

Oral components

PendingJP2026105716ASucroseActive agent
The present invention aims to provide an oral composition that has an astringent sensation while effectively suppressing discoloration over time. [Solution] An oral composition comprising (A) component: pyridoxine or a salt thereof, (B) component: fluorine-containing compound, and (C) component: an anionic surfactant, wherein the content of component (B) is such that when converted to a fluoride ion concentration it is 1000 to 4000 ppm, and the content of component (C) is such that it is 0.05 to 5% by mass, preferably further comprising (D) component: at least one selected from the group consisting of saccharin sodium, sucralose, xylitol, erythritol, maltitol, acesulfame potassium, trehalose, and mannitol, and more preferably further comprising (E) component: at least one selected from the group consisting of tocopherol acetate and tocopherol nicotinate.
Owner:LION CORP

A meloxicam benzenesulfonate orally disintegrating tablet formulation and a method of preparing the same

The application discloses a kind of meloxicam benzenesulfonic acid oral disintegration tablets and preparation method thereof, belong to pharmaceutical preparation technical field, the oral disintegration tablet includes granule / powder A, granule / powder B and auxiliary material;Wherein, the granule / powder A includes: meloxicam benzenesulfonic acid, mannitol, antioxidant, stabilizer, first binder and first disintegrating agent;The antioxidant is butylated hydroxyanisole, and the stabilizer is tartaric acid and / or magnesium metasilicate aluminum;The granule / powder B includes: filler, mannitol, second binder and second disintegrating agent;The auxiliary material includes third disintegrating agent, potassium acetylsulfanate and magnesium stearate.The application is by adjusting tartaric acid, butylated hydroxyanisole, magnesium metasilicate aluminum and the matching of filler, adjusts granulation mixing mode and changes tabletting tablet type, so that the related substance of meloxicam benzenesulfonic acid oral disintegration tablet increases significantly slower, disintegration is significantly faster, solve the technical problem existing in prior art.
Owner:JINAN LIMIN PHARMA

Material boiling tank with condensate water recovery function for acesulfame potassium production

The utility model discloses an acesulfame potassium production material boiling tank with a condensate water recovery function, which comprises a base, the center position of the top of the base is fixed at the bottom position of a matching frame, and a material boiling tank body is arranged at the top position of the matching frame in a rolling manner; the left side shaft end position of the cooking tank body is fixed at the circle center position of the rotating gear; and the outer side of the threaded rod is in threaded connection with a set of moving blocks, the bottoms of the moving blocks are slidably arranged at the top of a fixed seat, and the bottom of the fixed seat is fixed to the top of the base through bolts. According to the acesulfame potassium production material boiling tank with the condensate water recycling function, the lifting mechanism is arranged, so that the material boiling tank body is obliquely arranged at the top of the connecting frame, raw materials boiled in the base can be conveniently collected and treated, and in addition, condensate water formed by heat exchange of a heat exchange plate can be recycled and treated through an arranged condensate water tank.
Owner:SUZHOU NUTA FOOD TECH CO LTD

A low temperature process for the preparation of sugar-free, mint-flavored soda water with high retention of menthol

PendingCN122271459AMentholFood industry
This invention discloses a low-temperature preparation process for sugar-free mint-flavored soda water with high menthol retention rate, belonging to the field of food industry technology. The process includes the following steps: pre-cooling drinking water to 0-4°C to obtain cooling water; pre-cooling mint concentrate to 0-5°C to obtain cooled mint concentrate; adding the cooled mint concentrate to the cooling water under a nitrogen protective atmosphere and mixing; vacuum deoxygenating the mixture to reduce the dissolved oxygen concentration to below 1.5 mg / L; introducing carbon dioxide into the deoxygenated mixture for carbonation, controlling the temperature at 0-8°C; adding sodium bicarbonate and acesulfame potassium to obtain the mint-flavored soda water base; and performing nitrogen-displacement low-temperature filling at 0-8°C to obtain the finished product. This invention, through low-temperature operation throughout, nitrogen protection, and vacuum deoxygenation, effectively inhibits the volatilization and oxidative degradation of menthol, achieving a menthol retention rate of over 90% and significantly improving the product's shelf-life stability.
Owner:CHONGQING RUSHUI BEVERAGE CO LTD

Acesulfame potassium drying device

The utility model belongs to the technical field of drying equipment, and particularly relates to an acesulfame potassium drying device which comprises a stock bin, a vacuum drying cylinder, a vacuum pump, a condenser, a storage tank, a draught fan, a first condensate tank, a second condensate tank, a first water pump and a second water pump, the first condensate tank is connected with the first water pump in series, and the second condensate tank is connected with the second water pump in series. The condensate tank I is connected with the condensate tank II; the stock bin is connected with the vacuum drying cylinder, and the vacuum drying cylinder is communicated with the second water pump and the second condensate tank to form a closed circulating pipeline. The vacuum drying cylinder is externally connected with a vacuum pump, the vacuum pump is connected with a condensate tank I, the condensate tank I is connected to a condenser, and the condenser is internally connected with the vacuum drying cylinder; a storage tank is arranged at the bottom of the vacuum drying cylinder; and the storage tank is connected with a fan. According to the acesulfame potassium drying device, hot steam generated when acesulfame potassium is dried in the vacuum drying cylinder can be recycled, so that the purpose of saving cost is achieved, and the quality stability and consistency of products can be effectively improved.
Owner:ANHUI JINHE INDUSTRIAL CO LTD

Oral components

PendingJP2026105715ASulfanilamideMaltitol
The present invention aims to provide an oral composition in which discoloration over time caused by pyridoxine or its salts is suppressed, and bitterness is reduced. [Solution] The present invention provides an oral composition comprising (A) component: pyridoxine or a salt thereof, and (B) component: a fluorine-containing compound, wherein the content of component (A) is 0.11 to 0.95% by mass, and the content of component (B) is such that when converted to a fluoride ion concentration, it is 1000 to 20000 ppm, and preferably further comprising (C) component: at least one sweetener selected from the group consisting of saccharin sodium, sucralose, xylitol, erythritol, maltitol, acesulfame potassium, trehalose, and mannitol.
Owner:LION CORP

Composition for reducing sugar and modifying flavor as well as preparation method and application of composition

The invention provides a composition for reducing sugar and modifying flavor, which is prepared from the following components in parts by weight: 13 to 20 parts of yeast extract, 32 to 40 parts of glucosyl stevioside, 0.05 to 0.08 part of neohesperidin dihydrochalcone, 0.2 to 0.4 part of African arrowroot extract and 25 to 30 parts of sucrose flavor essence. The sweetener can replace traditional sweeteners such as white granulated sugar and high fructose corn syrup to achieve the purpose of clean sugar reduction, and can also replace traditional artificially synthesized sweeteners such as aspartame and acesulfame potassium to solve the problems that the traditional artificially synthesized sweeteners are low in sweetening speed, obvious in aftertaste and lack of mellow sweet taste, and the sweetener is suitable for industrial production. Meanwhile, the problems of insufficient flavor release and the like caused by reduction of the white granulated sugar of the product can be solved.
Owner:ANGEL YEAST CO LTD +1

Zero sugar stable foam beverage

PCT designated stageWO2026011046A1Food scienceBiotechnologyBrix
The present disclosure relates to a beverage base comprising water; a nutritive sweetener in an amount of 12 Brix or less or a non-nutritive sweetener or a combination of both; and at least one multifunctional component selected from aspartame, acesulfame potassium, sucralose, quillaia extract, class 1 caramel, emulsifying pectin, a flavoring, and any combination thereof. The viscosity of the beverage base at 21.1 °C is about 1.01-1.8 cP. When a 50 mL sample of the beverage base is subjected to a foam analyzer and air is injected into the sample at a flow rate of 400 mL / min, the beverage base holds a foam volume of about 20 mL or more for 8 minutes or longer. The present disclosure is further related to a ready to drink beverage comprising the beverage base and at least one dissolved gas.
Owner:PEPSICO INC

Crystal particle anti-caking device for acesulfame potassium preparation

The utility model relates to the technical field of acesulfame potassium preparation, in particular to a crystal particle anti-caking device for acesulfame potassium preparation, which comprises a processing frame, a material receiving frame is movably connected to the middle section in the processing frame, and a material screening frame groove is embedded in the center in the material receiving frame. An inclined material guide plate is fixedly installed at the position, located at the lower end of the material receiving frame, in the treatment frame, one end of the material guide plate extends out of a discharging groove formed in one side face of the treatment frame, first transverse grooves are formed in the positions, located in the center of the top, of the front inner wall and the rear inner wall of the treatment frame correspondingly, and inclined grooves are formed in the two ends of each first transverse groove; the two groups of chutes are in mirror symmetry relative to the central axis of the transverse groove I, and a transverse groove II is formed in one end, far away from the transverse groove I, of each of the two groups of symmetrical chutes. Therefore, the influence on the quality of the acesulfame potassium crystal due to crystal caking is reduced.
Owner:ANHUI WEIDUO FOOD INGREDIENTS CO LTD

A functional fruit tea beverage with zero sugar and zero fat and a preparation method thereof

The present application relates to the technical field of normal temperature fruit tea beverage, and specifically provides a zero-sugar and zero-fat functional fruit tea beverage and a preparation method thereof. The mass ratio of soluble soybean polysaccharide to Luo-shen oolong tea liquid in the zero-sugar and zero-fat functional fruit tea beverage is (0.5-2):(300-400). The sweetening agent in the zero-sugar and zero-fat functional fruit tea beverage is composed of erythritol, xylitol, stachyose, sucralose and acesulfame potassium. The optimal stabilizer is screened out by testing different stabilizer raw materials, and the sweetening agent combination which does not affect the stability of the product is screened out, so that the system stability problems such as precipitation, water separation and particle floating during the shelf life of the product are improved, and the product maintains high stability. The product provided by the present application has pure sweetness, does not add food essence, and the sweetness does not have the artificial feeling of lengthening.
Owner:INNER MONGOLIA MENGNIU DAIRY IND (GROUP) CO LTD

New process method for synthesizing acesulfame potassium

The invention discloses a novel process method for synthesizing acesulfame potassium, and belongs to the technical field of fine chemical organic synthesis. The process comprises the following steps: under the catalytic action of solid superacid, performing dehydration and ring closing on acetosulfamic acid triethylamine salt to generate cyclization liquid, layering and extracting the prepared cyclization liquid to obtain dichloromethane solution of acesulfamic acid, and neutralizing, concentrating, crystallizing and drying to obtain an AK product. Through the catalytic action of the solid superacid, the stability of the cyclization intermediate is improved, the quality of the product is effectively improved, the content of acesulfame potassium (AK) reaches 99.5% or above, meanwhile, the process conditions are mild, the catalyst is easy to recycle and separate, the production cost is saved, and industrial application is easy.
Owner:NANTONG HONGXIN CHEM CO LTD +1

Zero sugar stable foam beverage

PendingUS20260007153A1Food scienceBiotechnologyBrix
The present disclosure relates to a beverage base comprising water; a nutritive sweetener in an amount of 12 Brix or less or a non-nutritive sweetener or a combination of both; and at least one multifunctional component selected from aspartame, acesulfame potassium, sucralose, quillaia extract, class 1 caramel, emulsifying pectin, a flavoring, and any combination thereof. The viscosity of the beverage base at 21.1° C. is about 1.01-1.8 cP. When a 50 mL sample of the beverage base is subjected to a foam analyzer and air is injected into the sample at a flow rate of 400 mL / min, the beverage base holds a foam volume of about 20 mL or more for 8 minutes or longer. The present disclosure is further related to a ready to drink beverage comprising the beverage base and at least one dissolved gas.
Owner:PEPSICO INC

Method for simultaneously determining content of acesulfame potassium, phloretin and perillartine in food essence based on UPLC

ActiveCN117405786BComponent separationBiotechnologyAcesulfame potassium
The application discloses a method for simultaneously determining contents of advantame, phloretin and perillartine in edible essence based on UPLC, and belongs to the technical field of chemical analysis and detection, and comprises preparation of three sweetener series standard solutions, preparation of a to-be-measured sample solution, and subsequent detection and quantitative analysis by means of an ultra-high performance liquid chromatograph, and is suitable for simultaneous detection of the three sweeteners advantame, phloretin and perillartine. Compared with the prior art, different detection methods need to be adopted for detection of the three sweeteners, and the method can effectively separate and quantitatively analyze the three sweeteners with different absorption wavelengths at one time, and is rapid and convenient to operate, high in detection efficiency and easy to popularize.
Owner:BOLTON (HUBEI) BIOTECHNOLOGY CO LTD

Simple and efficient acesulfame potassium continuous flow sulfonation process and application

The invention belongs to the technical field of food additive synthesis, and particularly relates to a simple and efficient acesulfame potassium continuous flow sulfonation process and application. The process comprises the following steps: diluting an acylation intermediate with dichloromethane until the mass fraction is 18-20%, and controlling the temperature to be 15-20 DEG C; an SO3 dichloromethane solution with the SO3 mass fraction of 15% is prepared, the equivalent weight of the SO3 dichloromethane solution is 4-6 times that of the acylation intermediate, and the temperature is controlled to be 15-20 DEG C; the two materials are simultaneously pumped into a continuous flow reactor by a pump, so that the conveying is completed within the same time; after entering a continuous flow mixer, materials react at the flow speed of 6-8 m / s (SO3 dichloromethane solution) and 3-5 m / s (diluted acylation intermediate) to generate a cyclization intermediate, and the cyclization intermediate and water jointly flow into a receiving bottle through a three-way pipe. The method can be applied to food additive synthesis and acesulfame potassium industrial production, and an efficient and stable technical scheme is provided for acesulfame potassium sulfonation production.
Owner:ANHUI JINHE INDUSTRIAL CO LTD +1

Waste liquid multi-stage treatment device based on acesulfame potassium continuous neutralization process

The utility model belongs to the technical field of acesulfame potassium waste liquid treatment, and particularly relates to a waste liquid multi-stage treatment device based on an acesulfame potassium continuous neutralization process, which comprises a treatment tank I, a discharge port I and a discharge port II which are respectively arranged at the bottoms of the treatment tank I and the treatment tank II, a feeding port is arranged on the upper surface of the treatment tank II, and a filter component I is arranged in the treatment tank I; a filter component II is arranged on one side of the bottom of the treatment tank II; according to the utility model, the waste liquid is primarily filtered by the filter assembly I, impurities such as suspended matters and particulate matters are effectively removed, cleaner waste liquid is provided for subsequent neutralization treatment, the waste liquid is filtered again by the filter assembly II, and the waste of a solvent and the environmental pollution are effectively reduced through multi-stage filtration and neutralization treatment; the product quality of the acesulfame potassium continuous neutralization process is not influenced by impurities in waste liquid, and reasonable recovery and full utilization are realized.
Owner:ANHUI WEIDUO FOOD INGREDIENTS CO LTD

Ferulic acid derivative with bitterness inhibiting effect as well as preparation method and application of ferulic acid derivative

The invention discloses a ferulic acid derivative with a bitterness inhibiting effect as well as a preparation method and application of the ferulic acid derivative. The ferulic acid derivative comprises a compound A1 (3-(3-nitro-4, 5-dihydroxyphenyl) acrylic acid) and a compound A2 (3-(2-chloro-4-fluorophenyl) acrylic acid). By introducing nitro (A1) or halogen (A2), the bitterness inhibition rate of acesulfame potassium and coffee is remarkably improved, the bitterness inhibition activity is further enhanced, and no bad flavor is generated. The preparation method is simple in process, the obtained ferulic acid derivative has good economic benefits and practical benefits, and the effect of preventing or inhibiting unpleasant bitter taste can be achieved only by adding a small amount (0.1-10 mM) of the ferulic acid derivative into food.
Owner:SOUTH CHINA UNIV OF TECH