The present invention relates to a method for preparing an organic compound, in particular to a method for preparing an organic phosphate nucleator, which includes the following steps: phosphorylation reaction, hydrolyzation and salification. Since the solvent for the phosphorylation reaction adopts halogenated hydrocarbon instead of benzene series compounds, which is cheap, the cost can be reduced, and since the yield of the organic phosphate synthesized with the halogenated hydrocarbon used as the solvent is higher, the yield of the final product, the organic phosphate, is greatly increased. Moreover, since the solvent does not adopt the benzene series compounds, toxicity is low, non-burning operation is safe, environment can be protected, recycling is convenient, and the diaryl-substituted organophosphate metal salt used as nucleator prepared by the method has obvious effect in the improvement of the processing property of resin.