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2318 results about "Mixed systems" patented technology

Large-scale preparation method of transparent super-hydrophobic/super-amphiphobic coating

InactiveCN106800885AExcellent superhydrophobic/superamphiphobic propertiesHigh transparencySpecial surfacesCoatingsNanoparticle ComplexAlcohol
The invention discloses a large-scale preparation method of a transparent super-hydrophobic / super-amphiphobic coating. The method comprises the steps of ultrasonically dispersing nano particles into an alcohol-water mixed system and carrying out hydrolysis and condensation reaction on the nano particles and fluoride-free or fluorine-containing organosilane under the acid or alkali catalysis action to prepare a transparent suspension liquid of a fluoride-free or fluorine-containing organosilane polymer-nano particle compound; and applying the transparent suspension liquid of the compound on the surface of a substrate material through spraying or dip-coating to obtain the transparent super-hydrophobic / super-amphiphobic coating with good performance. Preparation of the transparent super-hydrophobic / super-amphiphobic coating of 10-100m<2> can be completed within an hour; large-scale preparation of the large-area transparent super-hydrophobic / super-amphiphobic coating is achieved for the first time; the preparation method is low in cost and simple in process; and the prepared coating has excellent super-hydrophobic or super-amphiphobic property, relatively good mechanical stability, chemical stability and environment stability, and has a wide application prospect.
Owner:LANZHOU INST OF CHEM PHYSICS CHINESE ACAD OF SCI

Method for preparing graphene-carbon nano tube hybrid composite

The invention provides a method for preparing a graphene-carbon nano tube hybrid composite and relates to a method for preparing a functional high molecular material and a device thereof. The method comprises the following steps of: carrying out the stirring and sonic oscillation treatment on graphene and carbon nano tubes to preform an entangled network structure, thoroughly mixing the entangled network structure and polymer particles, and thus obtaining an uniformly-mixed system in which the graphene-carbon nano tube network is coated on the surfaces of the polymer particles after removing the solvent; and putting the uniformly-mixed system in a mould, hot-compacting, and obtaining the graphene-carbon nano tube hybrid composite after cooling and demoulding. By mingling the graphene and the carbon nano tubes in advance to form the communicated network structure, the method realizes the advantage complementation of the graphene and carbon nano tube structures and enables the hybrid composite to have favorable electric conduction and heat conduction properties. The method can be widely used in the fields such as aviation, transportation and communication, electronic industry, civil facilities, construction, chemical industry and the like, can be produced in the industrial scale, and has the advantages of low cost and environmental friendliness.
Owner:SHENYANG JIANZHU UNIVERSITY

Nano-material-containing high-strength high-heat insulation exterior wall inorganic heat-retaining face brick

The invention belongs to the field of building materials, relates to a use of a nano-material in a building exterior wall heat-retaining system and provides a nano-material-containing high-strength high-heat insulation exterior wall inorganic heat-retaining face brick. The nano-material-containing high-strength high-heat insulation exterior wall inorganic heat-retaining face brick is characterized in that nano-particles are used so that compressive strength, tensile strength and bonding strength are improved. The nano-material-containing high-strength high-heat insulation exterior wall inorganic heat-retaining face brick is prepared by adding a nano-material having a nanoscale particle size into a mixed system of cement, an auxiliary gel material, a polymer binder, an inorganic light heat-retaining material, fibers and water, uniformly mixing, carrying out pressing molding of the mixture, carrying out organic polymer crosslinking and cement hydration drying, and carrying out waterproof layer coating. The nano-material-containing high-strength high-heat insulation exterior wall inorganic heat-retaining face brick has the advantages of excellent flame resistance, high compressive strength, high tensile strength, high bonding strength and good insulation effects.
Owner:平湖市法而特建筑保温科技有限公司

Graphene modified carbon fiber emulsion sizing agent and preparation method thereof

The invention relates to a graphene modified carbon fiber emulsion sizing agent and a preparation method thereof. The conventional solvent sizing agent is not environment-friendly. The sizing agent is a mixed system consisting of organic resin, an emulsifying agent, a lubricating agent, graphene, an organic solvent and deionized water, wherein the emulsifying agent, the lubricating agent, the graphene and the organic solvent are respectively 2 to 14 percent, 0.5 to 2 percent, 0.05 to 1 percent and 30 to 200 percent based on the mass of the organic resin; and the solid content of the mixed system is 0.1 to 5 percent. The preparation method of the sizing agent comprises the following steps of: dissolving the organic resin in the organic solvent to form organic resin solution, adding the emulsifying agent, the lubricating agent and the deionized water into the organic resin solution, and stirring until the mixed system is subjected to phase transfer; adding the deionized water until the solid content is 30 to 50 percent to obtain organic resin emulsion; and adding the graphene into the organic resin emulsion, and adding the deionized water to dilute the mixed system until the solid content is 0.1 to 5 percent so as to obtain the graphene modified sizing agent. The method is simple and reliable, and the prepared graphene modified sizing agent can well protect carbon fibers and effectively improve the interface property of the carbon fibers and matrix resin.
Owner:NINGBO INST OF MATERIALS TECH & ENG CHINESE ACADEMY OF SCI

Preparation method of catalyst for acrylic acid by oxidizing acraldehyde

The invention relates to a preparation method of a catalyst for acrylic acid by oxidizing acraldehyde, which is characterized by comprising the following steps of: dispersing water soluble metal salts containing the components of Mo, V, W, Cu and Sb into a water/organic phase mixed system at the temperature of 30-100DEG C; maintaining the weight ratio of an organic solvent to water as 5-50 percent; reacting to generate composite oxide precursor serum; separating water by a distilling process under the condition of continuously supplementing organic phases at the temperature of 20-120DEG C, wherein the water content of distillate is not greater than 10 percent; then, pelleting by a spray drying process and roasting at the temperature of 200-600DEG C to prepare catalyst active components; mixing primary roasting powder, a forming additive and a strength improver; coating the active components on the surface of an inert carrier by using an adhesive, wherein the carrying capacity occupies5-70 percent of the total quantity of the catalyst; drying a formed product for 5-48 hours at room temperature; and then, roasting the formed product for 1-15 hours at the temperature of 200-600DEG Cto obtain a spherical catalyst with the active components carried on the inert carrier.
Owner:CHINA NAT OFFSHORE OIL CORP +1

Preparation method of mesoporous-microporous composite molecular sieve

The invention discloses a preparation method of a mesoporous-microporous composite molecular sieve. The preparation method comprises the following steps of adding a microporous molecular sieve subjected to hydrothermal treatment into a mixed system of a silicon source, an acid solution and a surfactant, then carrying out crystallization, filtration and washing, and then carrying out drying and calcination to obtain the mesoporous-microporous composite molecular sieve. The preparation method fully utilizes non-framework aluminum falling from the microporous molecular sieve, avoids an aluminum source used by the conventional molecular sieve preparation technology, is conducive to improvement of a silica-alumina ratio of the mesoporous-microporous composite molecular sieve, realizes a high degree of crystallization, and improves hydrothermal stability and thermostability of the mesoporous-microporous composite molecular sieve. The mesoporous-microporous composite molecular sieve is suitable for the field of macromolecule catalysis, is conducive to improvement of a reaction conversion ratio and reaction selectivity, and is especially suitable for being used in a cracking catalyst for maximum-degree production of middle distillate from heavy oil as a raw material.
Owner:CHINA PETROLEUM & CHEM CORP +1

Preparation method of SiO2/polytetrafluoroethylene hybridized super-hydrophobic coating

The invention discloses a preparation method of a SiO2/polytetrafluoroethylene hybridized super-hydrophobic coating. The preparation method comprises the following steps: hydrolyzing a silane coupling agent in an alcohol-water solvent at appropriate temperature and pH value, allowing the solution to react with silicon sol, enabling the surface of silicon dioxide particles to be grafted with organic radicals, adding a certain volume of PTFE (Polytetrafluoroethylene) emulsion and an auxiliary in the modified silica solution to prepare a uniformly-mixed system, ageing for a certain time, performing coating treatment, and preparing the coating. The preparation method of the SiO2/polytetrafluoroethylene hybridized super-hydrophobic coating is to utilize the silane coupling agent to modify the silica solution, enable the silanol structures on the surface of the SiO2 particles to be grafted with part of hydrophobic groups, in the meantime improve the dispersibility of the particles, utilize a sol-gel method to enable the modified silica solution and the PTFE emulsion to be hybridized to form the uniformly-mixed system to prepare the super-hydrophobic coating. Therefore, the bonding force between polytetrafluoroethylene and the base material can be effectively improved, the rigidity and the abrasive resistance can be improved, the roughness of the coating surface can be constituted, and furthermore the contact angle on the surface can be increased.
Owner:LUSHAN COLLEGE OF GUANGXI UNIV OF SCI & TECH

Preparation method and application of ZnIn2S4-graphene composited photochemical catalyst

The invention discloses a preparation method and application of a ZnIn2S4-graphene composited photochemical catalyst. The preparation method comprises the following steps of: placing graphite oxide into a reducibility alcohol agent for ultrasonic dispersion; adding zinc sulfate and indium chloride into the reducibility alcohol agent, stirring and dissolving; adding thioacetamide into two systems after the two systems are mixed; transferring the mixed systems into a hydrothermal kettle for a reaction; and after the reaction is finished, carrying out vacuum filtration on the obtained product, washing, vacuumizing and grinding to obtain a nano ZnIn2S4-graphene composited photochemical catalyst. In the invention, grapheme is taken as a supporting material, and a solvothermal synthesis method is adopted to further prepare the nano ZnIn2S4-graphene composited photochemical catalyst. The catalyst prepared by using the method in the invention has the advantages of wide visible light responding range and high photocatalysis activity, can be used for transformation and use of solar energy and comprehensive ecological improvement, such as air purification, sewage disposal, hydrogen production through photodegradation, preparation of alcohol or hydrocarbon chemical fuels and the like by the photocatalysis and reduction of CO2.
Owner:HUNAN INSTITUTE OF SCIENCE AND TECHNOLOGY
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