6043 results about "Ether" patented technology

The invention provides a positive electrode, a low-temperature electrolyte, a low-temperature sodium-ion battery and a preparation method and application of the low-temperature sodium-ion battery, and belongs to the technical field of battery materials. The low-temperature sodium ion battery comprises a positive electrode, a negative electrode and a low-temperature electrolyte, wherein the positive electrode comprises a positive electrode active material, a binder, sodium salt containing fluorine and sulfur and conductive carbon; the positive electrode is improved by adding sodium salt containing fluorine and sulfur, sulfur / fluorine rich in anion derivatives can be formed on a contact interface of the positive electrode and an electrolyte to form a firm SEI film, the internal resistance of the battery is further reduced, and the coulombic efficiency of the battery during charging and discharging at normal and low temperatures is improved. The low-temperature electrolyte comprises an ester solvent and an ether additive, by adding the ether solvent, the physicochemical property of the electrolyte and the composition of an SEI film on a contact interface of an electrode and the electrolyte are optimized, the viscosity of the electrolyte at low temperature is reduced, the ionic conductivity is improved, and formation of the SEI film rich in sodium fluoride on the surface of a negative electrode can be promoted; and thus, the problem of low coulombic efficiency of battery charge-discharge cycle at low temperature is solved.

The invention belongs to the technical field of anion exchange membranes, and relates to a cross-linked polyaromatic piperidine anion exchange membrane and a preparation method thereof. The exchange membrane structure comprises a copolymer structure of the following repetitive structural units, the selected rigid main chain polyaromatic hydrocarbon can ensure the mechanical strength of the anion exchange membrane, meanwhile, the toughness of the anion exchange membrane is further enhanced by adopting a cross-linked structure, and a formed cross-linked network can reduce swelling of the anion exchange membrane, so that the anion exchange membrane is more stable in performance. The mechanical performance is improved; according to the invention, ether-free skeleton polyaromatic hydrocarbon is selected as a main chain and has the characteristic of strong alkali-resistant stability, six-membered nitrogen heterocyclic ions are adopted as functional groups, and a large steric hindrance structure can hinder nucleophilic substitution and elimination reaction, so that the alkali-resistant stability of the anion exchange membrane is improved, and the service life of the anion exchange membrane is prolonged. And in the # imgabs0 #, X is equal to 0.05 to 0.15.

The invention discloses sound-insulation and heat-insulation building mortar and a preparation method thereof, and relates to the technical field of building materials, the sound-insulation and heat-insulation building mortar comprises, by weight, 42-48 parts of a cementing material, 15-25 parts of an auxiliary material, 17-22 parts of lightweight aggregate, 30-35 parts of a functional filler, and 1-2 parts of an additive; the cementing material is a mixture of sulphoaluminate cement and Portland cement; the auxiliary material is a mixture of fly ash and quartz sand, the lightweight aggregate is a mixture of 20-40-mesh hollow vitrified microbeads and 70-90-mesh hollow vitrified microbeads, and the mass ratio of the hollow vitrified microbeads to the hollow vitrified microbeads is 1: (2-3); the functional filler is a mixture of modified waste rubber particles and modified fibers; the additive is a mixture of a polycarboxylate superplasticizer and hydroxypropyl methyl cellulose ether. The mortar disclosed by the invention is good in thermal insulation performance and excellent in mechanical property, the method disclosed by the invention is simple to operate and low in cost, and the prepared mortar is excellent in performance.

The invention relates to the technical field of filling materials, and particularly discloses an ardealite-based high-strength anti-seepage filling material and a preparation process thereof, the ardealite-based high-strength anti-seepage filling material comprises 50%-65% of pretreated ardealite, 15%-25% of Portland cement, 5%-15% of superfine slag powder, 5%-10% of electrolytic manganese residues, 5%-8% of silica fume, 3%-6% of metakaolin, 2%-4% of a composite alkali activator and 0.5%-1.2% of a polycarboxylic acid water reducer, 0.3%-0.8% of an organic silicon water repellent and 0.05%-0.1% of cellulose ether; according to the invention, through chemical reaction of Mn < 2 + > in the electrolytic manganese residue and SO4 < 2-> in the phosphogypsum, micron-sized manganite crystals (MnAl2 (SO4) 4. 22H2O) are generated to actively fill internal micro-cracks of the material, so that a filling body is endowed with a self-repairing function and the impermeability is improved, and a composite alkali activator composed of NaOH and water glass is used for synergistically activating potential gelling activity of the superfine slag powder and the silica fume, so that the self-repairing filling material is prepared. And the formation of hydration products is accelerated, and 0.3-0.5 T of pulsed magnetic field is applied in the stirring process, so that the manganite crystals are guided to orderly grow along the expected stress direction of the filling body, and the compressive strength is improved.

The invention relates to the technical field of coatings, and discloses an amino-terminated ether-containing hyperbranched polyamide modified epoxy resin coating, which comprises a component A: 100 parts of a water-borne epoxy resin emulsion, 5-20 parts of titanium dioxide, 1-2.5 parts of a dispersant, and 0.05-0.2 part of an antifoaming agent; the component B is prepared from 50 to 70 parts of amino-terminated ether-containing hyperbranched polyamide; the amino-terminated ether-containing hyperbranched polyamide contains an active amino-terminated group, so that the amino-terminated ether-containing hyperbranched polyamide is used as a curing agent and is subjected to a cross-linking curing reaction with epoxy resin, the hyperbranched polyamide has a three-dimensional branched network structure and forms a spatial cross-linked interpenetrating network system with the epoxy resin, and the hyperbranched polyamide contains a flexible ether-containing chain segment and an alkyl chain segment, so that the cross-linking property of the hyperbranched polyamide is improved. The epoxy resin coating has a good toughening effect, improves the impact resistance and impact strength of an epoxy resin coating layer and a casting body thereof, and keeps high hardness and tensile strength at the same time.

The invention belongs to the technical field of polyurethane elastomers, and particularly relates to a high-static-rigidity high-damping low-pressure-change polyurethane elastomer and a preparation method thereof. Comprising a polyol component and an isocyanate component, and the polyol component comprises polyol A, a chain extender, a stabilizer, a hydrolysis-resistant agent and a catalyst; the isocyanate component is prepared from isocyanate, polyhydric alcohol B and branched chain unit alcohol; the polyol A comprises amine ether polyol and polytetrahydrofuran ether polyol; the polyhydric alcohol B comprises bio-based hydrolysis-resistant polyhydric alcohol and polytetrahydrofuran ether polyhydric alcohol; the bio-based hydrolysis-resistant polyol is prepared by carrying out a reaction on sebacic acid, 1, 2-propylene glycol and 1, 4-butanediol; the branched-chain unit alcohol is prepared from tetrahydrofuran and isooctanol through a reaction. By introducing the bio-based hydrolysis-resistant polyhydric alcohol and branched chain monohydric alcohol, the damping effect is remarkably enhanced, and on this basis, through formula adjustment and raw material screening, the product toughness is greatly improved, the compression set is reduced, and the performance of the product in heavy haul railway application is effectively optimized.

The invention relates to the technical field of organic chemical synthesis, in particular to a preparation method of 3, 4 '-diaminodiphenyl ether.The preparation method comprises the steps that S1, under inert gas and in a first solvent, m-dinitrobenzene and p-acetamidophenol are subjected to a heating reaction under the condition of a weak base catalyst, and 3-nitro-4-acetamido diphenyl ether is prepared; s2, in a second solvent, the 3-nitro-4-acetamido diphenyl ether is subjected to a hydrogenation reduction reaction, and 3-amino-4-acetamido diphenyl ether is prepared; and S3, dissolving the 3-amino-4-acetaminodiphenyl ether in an alcohol solvent system, adding an aqueous solution of alkali, controlling the reaction temperature, carrying out a hydrolysis reaction, and after the reaction is finished, carrying out post-treatment to obtain the 3, 4 '-diaminodiphenyl ether. The preparation method provided by the invention has the advantages of easily available raw materials, low price, good selectivity and high product yield, and is more suitable for industrial production by comprehensively considering economical efficiency and safety.

The present disclosure provides a solid electrolyte composition that can suppress deterioration in ion conductivity of an ionic solid electrolyte material. The solid electrolyte composition according to the present disclosure contains a sulfur element-free ionic solid electrolyte material and an organic solvent, where the organic solvent includes at least one selected from the group consisting of a hydrocarbon and a compound having a functional group; and the functional group is at least one selected from the group consisting of an ether group, a halogen group, and a Si—O—C group.

The invention provides a modified coal gangue-based large-flow-state grouting and water plugging material and a preparation method thereof. Comprising 80-90 parts of a coal gangue sample, 1-5 parts of Portland cement, 1-5 parts of sulphoaluminate cement, 0.51-3 parts of a polycarboxylic acid water reducing agent, 1-4 parts of cellulose ether with the viscosity of 200w, 0.1-5 parts of a calcium oxide expanding agent, 0.5-5 parts of a plastic expanding agent, 0.5-1 part of redispersible latex powder, 0.5-5 parts of polyacrylamide with the molecular weight of 1000 and water, and the water-material ratio is 0.4. According to the modified coal gangue-based large-flow-state grouting and water plugging material and the preparation method thereof, the cement consumption can be remarkably reduced, the cost is reduced, the utilization rate of solid wastes (such as coal gangue) is increased, and the material has good flow-state performance and adjustable setting time; the method is suitable for deep and large shaft surrounding rock water seepage treatment in coal mining and other mine engineering.

The invention discloses a porphyrin-based covalent organic framework nano material, a preparation method and application of the porphyrin-based covalent organic framework nano material in polyurethane, and belongs to the field of functional nano materials and antibacterial materials. The porphyrinyl covalent organic framework nano material is prepared from 5, 10, 15, 20-tetra (4-aminophenyl) porphyrin and bis-(5-formyl furfuryl) ether through a Schiff base reaction, and the structural formula of the porphyrinyl covalent organic framework nano material is # imgabs0. The porphyrinyl covalent organic framework nano material prepared by the invention has relatively high photothermal conversion efficiency when being used as a photothermal agent, and has a relatively good sterilization effect under the condition of relatively low concentration. Besides, based on the porphyrin-based covalent organic framework nano material, a WPUS / Por-COF composite film is prepared, the composite film has excellent mechanical properties and excellent photothermal conversion efficiency, and has a good sterilization effect under the condition of relatively low concentration, bacteria can be inactivated within a short time, and the sterilization rate can reach 99% or above.

The invention provides a preparation method of an h-BN / PI high-temperature-resistant anticorrosive coating, and relates to the technical field of polymer composites.The preparation method of the h-BN / PI high-temperature-resistant anticorrosive coating comprises the steps that under the protection of inert atmosphere, aromatic diamine containing impurity element five-membered rings and aromatic dianhydride containing ether bonds are taken and subjected to a polymerization reaction in a polar aprotic solvent, and the h-BN / PI high-temperature-resistant anticorrosive coating is obtained. A polyamide acid solution is obtained; performing ultrasonic-assisted liquid phase stripping on the micron-sized hexagonal boron nitride to obtain single-layer hexagonal boron nitride; adding the single-layer hexagonal boron nitride into the polyamide acid solution for multiple times, and uniformly stirring to obtain a hexagonal boron nitride / polyimide composite solution; and coating the hexagonal boron nitride / polyimide composite liquid on a to-be-coated surface, and carrying out gradient heating curing to obtain the h-BN / PI high-temperature-resistant anticorrosive coating. The h-BN / PI high-temperature-resistant anticorrosive coating based on interaction of multiple hydrogen bonds has relatively good high temperature resistance, relatively good resistance mechanical property and excellent corrosion resistance.

The invention belongs to the technical field of oil and gas development, and particularly relates to an oil and gas well blocking remover and a preparation method thereof. The blocking remover comprises the following components: 5-8% of low-carbon composite organic acid, 5-7% of fluoboric acid, 6-9% of ammonium bifluoride, 4-6% of an anti-acid sludge mutual solvent, 2-4% of a corrosion inhibitor, 2-4% of polyoxypropylene polyoxyethylene propylene glycol ether, 8-12% of a permeation dispersion surfactant, 2-5% of a sulfur dissolving agent, 2-5% of a stable chlorine dioxide solution and the balance of water. The preparation method comprises the following steps: adding the low-carbon composite organic acid, the fluoboric acid and the ammonium bifluoride into water and stirring; adding an acid sludge resisting mutual solvent and a sulfur dissolving agent, and stirring; adding the corrosion inhibitor, the polyoxypropylene polyoxyethylene propylene glycol ether and the permeation dispersion surfactant, and stirring; and finally, reducing the stirring speed, adding the stable chlorine dioxide solution, and stirring to uniformly mix. The blocking remover provided by the invention is comprehensive in blocking removal function, very good in dissolving and dispersing performance on complex blocking substances, very small in corrosion damage to a shaft pipe wall and wide in applicability.

The invention provides solid-waste-based fluid-state solidified soil and a preparation method of the solid-waste-based fluid-state solidified soil. The solid waste-based flow state solidified soil comprises a filling material, a framework material and a reinforcing material, the filling material comprises the following components in parts by weight: 60-95 parts of engineering residue soil, 5-40 parts of alkaline waste residues, 5-30 parts of a cementing material, 1-10 parts of a polymer emulsion, 0.5-3 parts of silica fume, 0.1-1 part of cellulose ether, 0.1-1 part of a compound water reducing agent and 0.5-2 parts of an exciting agent. The framework material comprises waste concrete blocks and / or waste brick blocks; the reinforcing material comprises a waste safety net and / or fiber gridding cloth. The flow-state solidified soil can achieve rapid backfilling in a narrow space, is excellent in shrinkage cracking resistance and impermeability, simple in preparation method and convenient to apply and construct, effectively solves the problems that the flow-state solidified soil is large in shrinkage, prone to cracking and the like, improves the quality of a backfilling project, achieves in-situ resource utilization of construction waste, and reduces the construction cost. And the construction cost of engineering can be reduced, and the problems of land occupation, environment pollution and the like caused by solid waste stacking are reduced.

The present disclosure provides a solid electrolyte composition that can suppress deterioration in ion conductivity of an ionic solid electrolyte material. The solid electrolyte composition according to the present disclosure contains a sulfur element-free ionic solid electrolyte material and an organic solvent, where the organic solvent includes at least one selected from the group consisting of a hydrocarbon and a compound having a functional group; and the functional group is at least one selected from the group consisting of an ether group, a halogen group, and a Si—O—C group.

The invention relates to the technical field of polyurethane coatings, in particular to a hydrophobic flame-retardant polyurethane coating and a preparation method thereof. The preparation method comprises the following steps: firstly, taking 9, 10-dihydro-9-oxa-10-phosphaphenanthrene-10-oxide and methallyl alcohol as raw materials, and reacting to obtain hydroxyl grafted phosphaphenanthrene; taking 1, 1, 3, 3-tetramethyldisiloxane and methallyl alcohol as raw materials, and reacting according to a molar ratio of 1: 2 to obtain dihydroxy siloxane; then cyanuric chloride, hydroxyl grafted phosphaphenanthrene and dihydroxyl siloxane react according to the molar ratio of 1: 1: (1.5-1.8), and the dihydroxyl-terminated silicon-containing flame retardant is obtained. The preparation method comprises the following steps: mixing a dihydroxyl-terminated silicon-containing flame retardant with polytetrahydrofuran ether glycol to serve as a soft segment, and reacting with isocyanate to obtain a hydrophobic flame-retardant polyurethane emulsion; mixing the hydrophobic flame-retardant polyurethane emulsion, an anti-aging agent, an ultraviolet light absorber, a defoaming agent, kaolin, nano silicon dioxide and talcum powder to obtain the hydrophobic flame-retardant polyurethane coating.

The invention discloses an organic amine composite absorbent for carbon capture and application thereof, and belongs to the technical field of carbon dioxide capture, the organic amine composite absorbent for carbon capture is in a solution state and comprises the following components: a main agent, an auxiliary agent, an accelerant A, an accelerant B and water; wherein the mass ratio of the main agent to the auxiliary agent is 2: (1-2); the mass ratio of the auxiliary agent to the accelerant A is 2: (1-2); the mass ratio of the accelerant A to the accelerant B is 2: (1-2); the total mass concentration of the main agent, the auxiliary agent, the accelerant A and the accelerant B in the organic amine composite absorbent for carbon capture is 30-40 wt%; the main agent is selected from N-methyldiethanolamine or N, N-diethyl ethanolamine, the auxiliary agent is selected from piperazine or hydroxyethyl ethylenediamine, the accelerant A is selected from triethylene glycol monomethyl ether and / or ethylene glycol monomethyl ether, and the accelerant B is selected from ethyl butyl ether and / or isobutyl ether. The organic amine composite absorbent for carbon capture has a wide application prospect in removal of carbon dioxide in flue gas.

A method for cooling an information technology system, comprising: receiving a flow of at least a subcooled liquid phase change refrigerant; cooling the information technology system by sensible heat transfer in an evaporator, to produce at least gaseous refrigerant; and exchanging heat from the at least gaseous refrigerant from the evaporator to the subcooled liquid phase change refrigerant. The phase change refrigerant may be a hydrofluorocarbon ether having a boiling point of 30-65° C. at 1-12 bar.

The invention relates to a construction method of a multi-class lipid retention time general prediction model and a prediction system. The method comprises the following steps: by taking experimental retention time tRE of a lipid compound in a training set as a dependent variable and characteristic structure parameters of the lipid compound as an independent variable, carrying out quantitative processing on the independent variable and then carrying out regression modeling analysis, the characteristic structure parameters comprise the total carbon number c and the total carbon-carbon double bond number d of a fatty acyl chain, an ether chain, an alkenyl ether chain or / and a sphingosine skeleton, the types of skeletons contained in the lipid compound and the number of corresponding skeletons, and the types of characteristic groups and residues in the lipid compound and the number of corresponding residues; carrying out numerical quantization on parameters according to the number of skeletons, characteristic groups or residues of the corresponding types; the QSRR general prediction model of the retention time of the multi-class lipid compounds is obtained by adopting regression modeling, a more accurate MRM data acquisition window can be set for the lipid compounds, and the sensitivity, stability and coverage can be improved.

The invention belongs to the technical field of new building materials, and provides a low-alkalinity and early-strength ardealite filling and curing material and a preparation method thereof.The low-alkalinity and early-strength ardealite filling and curing material is prepared from ardealite, a curing agent and water, the curing agent comprises silica fume, limestone powder, superfine granulated blast furnace slag powder, metakaolin, calcium aluminate powder, Portland cement clinker powder, a suspension stabilizer and hydroxypropyl methyl cellulose ether. The problems of delayed coagulation, low early strength and high alkalinity of a common cement-based ardealite filling material can be solved, and the technical requirements of ardealite cemented filling are met.

The invention relates to the technical field of preparation of epoxy insulating materials, in particular to an epoxy resin material constructed by a multistage molecular chain cross-linked network and a preparation method, and the epoxy resin material realizes synergistic improvement of insulation and mechanical properties. Epoxy resin monomers with different rigid and flexible group contents and different chain lengths under the same chain structure are combined according to a certain proportion and are mixed into a homogeneous-phase resin matrix at a high temperature, and then the homogeneous-phase resin matrix and an anhydride curing agent are subjected to cross-linking curing at the high temperature to prepare the epoxy insulating material. The rigidity and flexibility of an epoxy cross-linked network are regulated and controlled by utilizing the multi-rigid group and multi-epoxy group of a short-chain resin monomer in a resin matrix and the multi-active hydroxyl and high-flexibility ether bond content of a long-chain resin monomer, and a charge barrier is constructed. Finally, the epoxy resin material with high mechanical property and high electrical insulation property is prepared, and the insulation property and the mechanical property are synergistically improved.

The invention belongs to the field of dielectric materials and dielectric energy storage, and particularly relates to a fluorene polyester and polyaryletherurea blended dielectric energy storage polymer film and a preparation method thereof. The preparation method specifically comprises the following steps: adding fluorene polyester and polyaryletherurea into a solvent, fully dissolving to obtain a mixed solution, uniformly coating a substrate with the mixed solution, and then drying; and carrying out vacuum annealing on the dried film, and then carrying out curing treatment to strip the film from the substrate to obtain the fluorene polyester and polyaryletherurea blended dielectric energy storage polymer film, thereby improving the charge-discharge efficiency and high discharge energy density of the polymer under high temperature and high field, and solving the problems of high electric leakage loss and low cost of the existing polymer film. And the charging and discharging efficiency is low.

The invention relates to a synthesis method and application of a poly (ether) sulfuryl block copolymer based on chain exchange reaction, and belongs to the technical field of high polymer materials, the synthesis method comprises the following preparation steps: S1, taking an organic solvent, adding a poly (ether) sulfuryl material into the organic solvent, heating and stirring until the poly (ether) sulfuryl material is completely dissolved to obtain a mixed system; and S2, adding an amino-containing hydrophilic polymer material with reaction activity into the mixed system prepared in the step S1, and removing the solvent after reaction to obtain the poly (ether) sulfuryl block copolymer. The preparation process is easy to operate, the production period is short, the obtained material is stable in performance, and industrial production is easy.

The invention belongs to the technical field of refrigerants, and provides a mixed refrigerant for replacing R290 and a preparation method and application thereof, the mixed refrigerant comprises a first component, a second component and a third component; the first component is trans-1, 2-difluoroethylene, the second component is 2, 3, 3, 3-tetrafluoropropene, and the third component is trifluoromethyl methyl ether; compared with R290 refrigerants in the prior art, the mixed refrigerant has the advantages that flammable and explosive components do not exist, and high-risk combustible gas clusters cannot be formed due to density layering after leakage, so that the mixed refrigerant has high safety performance, and the safety level can be not lower than A2L; the mixed refrigerant has the environment-friendly characteristic of low GWP, the GWP is smaller than or equal to 150, and the environment-friendly requirement is met; the thermophysical property and the refrigeration and / or heating cycle performance of the mixed refrigerant are similar to or better than those of R290; the mixed refrigerant can be used for directly replacing an R290 refrigerant.

The invention relates to the technical field of corrosion resistance, in particular to a corrosion-resistant and wear-resistant copper insert and a preparation method thereof.The copper insert is subjected to plating treatment in an ionic liquid electroplating mode, then the surface of a plating layer is subjected to hole sealing treatment, and a nickel-copper-composite halloysite nanotube layer is electrically deposited on the surface of the formed copper insert; the preparation method comprises the following steps: taking a halloysite nanotube as a nano loader of a corrosion inhibitor, and coating with dopamine to obtain a composite halloysite nanotube; in the hole sealing liquid, the composite halloysite nanotube is used as a filler, silane modified polyurethane is used as a base material, the silane modified polyurethane is a prepolymer synthesized by using isophorone diisocyanate and polytetramethylene ether glycol as raw materials, octylamine ring-opened 3-(2, 3-epoxypropoxy) propyltrimethoxysilane is used as a chain extender, and the silane modified polyurethane is used as the base material. And 2-(perfluorodecyl) ethanol and aminopropyltriethoxysilane are used as end-capping reagents, so as to prepare the high-temperature-resistant coating.

The invention discloses a chlorine-resistant and acid-resistant composite nanofiltration membrane and a preparation method thereof, and belongs to the technical field of membrane separation. A polyhydric alcohol or / phenol compound monomer containing no less than two hydroxyl groups is subjected to interfacial polymerization with cyanuric chloride, so that a relatively loose network structure can be formed, and selective separation of dye and salt is realized. As a hydrochloric acid (HCl) byproduct can be generated in the reaction process, an alkaline compound is added as an acid-binding agent to neutralize HCl and promote the interfacial polymerization reaction, the formed composite nanofiltration membrane structure does not contain amino groups and polyamide bonds sensitive to active chlorine, the reaction sites of the active chlorine are reduced, and the chlorine-resistant stability of the membrane is good. Meanwhile, the polymer film contains a triazine ring structure, and a formed ether bond has good chemical stability, so that the acid-resistant stability of the film is good. The prepared composite nanofiltration membrane has good nanofiltration separation performance, shows good chlorine-resistant and acid-resistant stability, and can be used for separation of dyes / salts.

The invention relates to the technical field of purification of organic chemicals, in particular to an aroma purification method of leaf alcohol. Comprising the following steps: preparing a methanesulfonic acid magnetic catalyst; esterification of leaf alcohol; and alcoholysis and fractionation of the esterification solution. According to the method, acetic acid is used for esterification of leaf alcohol, then clear water and a sodium carbonate solution are used for washing, the clear water can effectively remove some water-soluble impurities and acidic byproducts, and the sodium carbonate solution not only can neutralize residual acidic substances, but also can promote siloxane impurities in initial leaf alcohol to be hydrolyzed and then taken away by a water phase, so that the content of the siloxane impurities in the leaf alcohol is reduced; in the subsequent process of producing leaf alcohol through alcoholysis of the organic phase I, pure water and ethanol, silyl ether impurities are hydrolyzed in a high-temperature and strong-alkali environment, products are dissolved in waste liquid to be removed, olefine aldehyde impurities with the boiling point lower than that of leaf alcohol are removed through azeotropic fractionation with ethanol, in conclusion, the impurities in the finished product leaf alcohol can be effectively reduced, and the yield of the finished product leaf alcohol is increased. And the prepared finished product leaf alcohol is high in purity and pure in fragrance.

The invention relates to the technical field of dispersing agents, and particularly discloses a high-concentration water-based graphene dispersing agent. The high-concentration water-based graphene dispersing agent is prepared from the following raw materials in parts by weight: 25 to 30 parts of a modified nonionic surfactant, 8 to 12 parts of sodium lignin sulfonate, 0.4 to 0.8 part of a de-foaming agent and 90 to 100 parts of de-ionized water, the modified nonionic surfactant is prepared by the following steps: carrying out dehydration esterification reaction on 1-pyrene butyric acid and N-hydroxysuccinimide, carrying out nucleophilic substitution reaction on the obtained product and polyethylene glycol monododecyl ether to obtain modified 1-pyrene butyric acid, and finally polymerizing the modified 1-pyrene butyric acid and n-butyl acrylate. The method is easy to operate, graphene does not need to be subjected to oxidation reduction, the integrity of a graphene sheet layer can be completely kept, and the performance of the graphene can be fully exerted; the prepared graphene dispersing agent realizes efficient dispersing effect, excellent stability and environment-friendly safety characteristics, and provides solid technical support for wide application of graphene in multiple fields.

The invention relates to the technical field of electronic materials, in particular to a preparation method of low-halogen alkali-soluble photosensitive resin and solder resist ink. Comprising the following steps: adding amino resin, alcohol olefin and a catalyst A into a solvent, mixing, and carrying out an ether exchange reaction to obtain an initial etherified product; adding peroxide into the initial etherification product, and carrying out epoxidation reaction to obtain an epoxy resin intermediate; adding an olefine acid compound, a catalyst B and a polymerization inhibitor into the epoxy resin intermediate, and carrying out ring-opening esterification reaction to obtain an epoxy acrylate intermediate; and adding acid anhydride into the epoxy acrylate intermediate, and carrying out carboxylation reaction to obtain the low-halogen alkali-soluble photosensitive resin. The problem of high halogen content of the existing alkali-soluble photosensitive resin is solved, and the solder resist ink prepared from the alkali-soluble photosensitive resin has high sensitivity, high resolution, high heat resistance, high acid and alkali resistance and high electrical insulation property.

The invention provides composite anionic cellulose ether as well as a preparation method and application thereof. The composite anionic cellulose ether is prepared by etherifying alkalized cellulose through an etherifying agent A and an etherifying agent B in sequence, the etherifying agent A is selected from water-soluble halogenated alkyl sulfonic acid and / or water-soluble halogenated alkyl sulfonate; the etherifying agent B is selected from water-soluble halogenated alkyl carboxylic acid and / or water-soluble halogenated alkyl carboxylate. According to the composite anionic cellulose ether, a sulfonic acid group and a carboxylic acid group are sequentially introduced, so that the composite anionic cellulose ether has relatively high temperature resistance and salt and calcium resistance; the compound can be used as a filtrate reducer for the drilling fluid, can effectively control the filter loss of the drilling fluid, and can improve the salt pollution resistance of the drilling fluid, especially the calcium and magnesium ion pollution resistance.

The invention provides an electrolyte and a lithium battery containing the same. The electrolyte comprises a lithium salt, a solvent and an inducer, the solvent comprises one or more of siloxane compounds as shown in a formula I; the inducer is selected from one or more of C1-C5 halogenated alkanes, C1-C5 halogenated cycloalkanes, C2-C6 halogenated aliphatic ethers and C6-C12 halogenated aromatic compounds. The electrolyte provided by the invention utilizes the intermolecular interaction force between the siloxane compound and the inducer, so that the dissolution of the lithium salt in the solvent is realized, and the electrolyte has high compatibility to a lithium metal negative electrode, has a wide electrochemical window, can be well matched with a high-voltage positive electrode material and a lithium metal negative electrode material, and has a good application prospect. And the cycle life and coulombic efficiency of the battery can be improved.