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2368results about "Artificial filament heat treatment" patented technology

Figured sea-island super-fine fiber, and preparation method thereof and synthetic leather preparing process method using same

The invention relates to a figured sea-island super-fine fiber, and a preparation method and a synthetic leather preparing process method using the same, which belong to the technical field of leather and leather manufacture methods. The figured sea-island super-fine fiber is characterized in that the weight percentage ratio of island components of the fiber to sea components of the fiber is 50 percent to 80 percent/50 percent to 20 percent, wherein the island components are polyamide (PA) 6 or polyethylene terephthalate (PET), and the sea components are polyolefins or phospholamban (PLB) or polyvinyl alcohol (PVOH). The preparation method comprises the steps of slice drying and melting, composite spinning, oiling and falling into a barrel, drafting curling and drying cutting. The synthetic leather preparing method comprises the following steps that: 1. the components are sequentially prepared into a single-layer fiber net, a composite layer fiber net, needle-punched non-woven cloth and needle-punched non-weaving cloth; 2.soakage and coagulation are sequentially carried out on the non-weaving cloth, the non-weaving cloth is washed, so that a synthetic leather impregnated substrate is formed, repeated soaking squeezing, azeotropic distillation and drying are sequentially carried out, so the synthetic leather is obtained. The synthetic leather produced by the invention has the advantages of excellent mechanical performance, excellent dyeing performance, excellent dyefastness, better production controllability, economy and environment protection. Compared with natural leather and products of the natural leather, the synthetic leather has the advantages that use performance such as durability, weatherability, antibacterium mothproofing, dyefastness and the like of products is much superior to that of the natural leather and the products of the natural leather.
Owner:烟台万华超纤股份有限公司

Method for preparing polyacrylonitrile carbon fiber protofilament by dry and wet methods

The invention discloses a method for preparing polyacrylonitrile carbon fiber protofilament by dry and wet methods. The method comprises the steps of polymerization, demonomerization and defoaming, filtration, coagulation, washing and drafting, oiling densification, steam drafting, heat setting and drying. Three-level coagulating baths at the temperature of between 10 DEG C below zero and 70 DEG C and with dimethyl sulfoxide with concentration of 10 to 60 mass percent are adopted in the coagulation step, and the first coagulating bath contains aqueous ammonia accounting for 0.05 to 1 percent of the mass of the first coagulating bath; and a spinning head is subjected to 1.5 to 5 times positive drafting in the first coagulating bath, and the drafting is 0 in the second and third coagulatingbathes. According to the method for preparing the polyacrylonitrile carbon fiber protofilament, the spinning process is stable, the broken filament is little, the spinning speed is high, the spinningis stable, the prepared protofilament has few defects, the density is not less than 1.180g/cm<3>, and the tensile strength is not less than 7cN/dtex. The protofilament can be prepared into a high-performance carbon fiber with tensile strength of more than 4.9GPa and elastic modulus of between 260 and 280GPa by high-temperature carbonization.
Owner:KINGFA SCI & TECH CO LTD +1

Preparation method of functional polyester fiber

The invention relates to a preparation method of a functional polyester fiber. The preparation method comprises the following steps: performing esterification by stages, wherein dihydric alcohols, polyhydric alcohols and functional inorganic powder are mixed according to a certain mole ratio, in the first esterification stage, acid is slightly excess to ensure that monomers with low capability of participating in esterification reaction in the polyhydric alcohols fully react and are grafted into polyester molecular chains, and in the second esterification stage, the dihydric alcohols are replenished to control the terminal carboxyl group of copolyester. The preparation method has the advantages that polyhydric functional groups can improve the apparent viscosity of a system and play a role in wrapping the introduced functional inorganic powder (such as far infrared ceramic inorganic powder, titanium dioxide powder and zinc oxide antibacterial powder), thus improving the dispersion uniformity of particles; settlement is unlikely to happen in the polymerization process and then functional polyester is prepared through condensation polymerization; the functional polyester fiber is finally prepared by carrying out melt spinning on the prepared polyester, has good moisture absorption property and flexibility and can be widely used for preparing far-infrared moisture absorbing and sweat releasing antistatic and antibacterial fabrics next to the skin.
Owner:JIANGSU HENGZE COMPOSITE MATERIALS TECH

Process for producing polyester industrial fiber for processing safe air bag of automobile

The invention relates to a process for producing a polyester industrial long fiber for processing a safe air bag of an automobile, which sequentially comprises the following steps: A. processing a polyester slice with high viscosity: enabling the viscosity of the polyester slice to reach 1.0-1.1dl/g; B. melting and spinning: transmitting the polyester slice after solid phase polymerization to a spinning screw rod extruder, melting in a spinning screw rod, entering a spinning assembly by a metering pump and extruding from a fiber spray plate with a diameter of 190 mm to 220 mm to spin fusant, , then heating by a slow cooling heater, carrying out cooling for molding by a side-molding blowing device and then entering a spinning passage; C. stretching and winding: oiling the surface of a fiber and carrying out second-grade high-speed stretching with the total stretching multiple being 5.0 to 5.8, carrying out high-temperature loosing thermoforming at 230 DEG C-250 DEG C and carrying out winding for molding in the range of the winding process speed of 2,500-3,000 m/min to prepare a finished product. The fiber for the safe air bag, which is produced by the process, can completely replace a nylon 66 fiber, is used for spinning terylene safe air bag fabrics and greatly reduces the processing cost.
Owner:ZHEJIANG HAILIDE NEW MATERIAL

Method for preparing low-melting-point polyester composite fiber by adopting continuous polymerization and melt direct-spinning

The invention relates to a method for preparing a modified copolyester composite fiber, in particular to a method for preparing a low-melting-point polyester composite fiber by adopting continuous polymerization and melt direct-spinning. The method comprises the following steps: slurry is prepared from raw materials in proportion and added continuously into an esterification system for an esterification reaction, an obtained oligomer is uniformly mixed with polyether, the mixture enters a homogenizing kettle for transesterification and pre-polycondensation, a product is uniformly mixed with a chain extender for final polycondensation, and an obtained low-melting-point polyester melt and a common polyester melt enter a composite spinning assembly to prepare the low-melting-point polyester composite fiber which comprises a common polyester core layer and a low-melting-point polyester cortex layer. The method has the advantages as follows: a side reaction of thermal degradation of polyether components is inhibited effectively, and the color and spinnability of the low-melting-point polyester melt are improved; the problem of poor performance of composite spinning of the low-melting-point polyester on the cortex layer and the common polyester on the core layer due to large dynamic viscosity difference of the melt is solved, and the composite fiber is well formed; the production efficiency of the low-melting-point polyester composite fiber is improved.
Owner:CHINESE TEXTILE ACAD

Three-dimensional oil-water separating material based on static spinning technology and preparation method thereof

The invention provides a three-dimensional oil-water separating material based on the static spinning technology and a preparation method thereof, belonging to the technical field of water treatment. The method specifically comprises the following steps: (a) preparing a static spinning solution; (b) selecting a proper solvent to directly receive static spinning nano fibers to obtain a nano fiber solution; (c) shaping and freezing the nano fiber solution, and drying through a freezing drying machine to obtain the three-dimensional nano fibers; (d) pre-oxidizing, carbonizing and activating the three-dimensional nano fibers to obtain three-dimensional carbon nano fibers; (e) wrapping the three-dimensional carbon nano fiber glue with lipophilic and hydrophobic films so as to obtain the final three-dimensional oil-water separating material. According to the preparation method of the three-dimensional oil-water separating material, the composition and structure of the material are easily controlled; the mechanical performance and hydrophobic performance of the materials can be effectively improved; the oil-water separating effect is good; the material can be recycled and has a wide application prospect in the oil-water separation field.
Owner:INST OF URBAN ENVIRONMENT CHINESE ACAD OF SCI +1

Processing method of high-strength low-shrinkage nylon 6 fine denier filament

The invention discloses a processing method of a high-strength low-shrinkage nylon 6 fine denier filament, belonging to the technical field of nylon filament processing. The method comprises the following steps: preparing materials: adding the nylon 6 slices into a bin of nitrogen protective gas to obtain a material to be melted; melting: introducing the material to be melted into a screw extruder for melting to obtain a melt; forming: introducing the melt from the upper part of a spinning box, and ejecting from a spinneret orifice of a spinneret plate to obtain a filament bundle; cooling: introducing the filament bundle into a slow-cooling area for slow cooling, forming through side-blowing air cooling, and further cooling through a channel; oiling and pre-interlacing: oiling the cooling-formed filament bundle through an oil lip or oil wheel, and pre-interlacing; drafting: feeding the filament bundle to be drafted through a feeding roller, drafting through a heat roller, and then performing relax-type setting to obtain the drafting-set filament; and re-interlacing and re-oiling: re-interlacing and re-oiling the drafting-set filament before packaging to obtain the high-strength low-shrinkage nylon 6 fine denier filament. The method can adapt to different purposes of products, and can be applied to the occasions having rigorous requirements on the breaking strength and dry heat shrinkage.
Owner:CHANGSHU POLYESTER

Self-enhanced polylactic acid fiber and preparation method thereof

The invention relates to a self-enhanced polylactic acid fiber and a preparation method thereof. The self-enhanced polylactic acid fiber provided by the invention is a uniform mixture of a vertical compound crystal polylactic acid micro-fiber and a polylactic acid substrate. In 100 weight parts of self-enhanced polylactic acid fiber, 1-30 parts of vertical compound crystal polylactic acid micro-fiber and 70-99 parts of polylactic acid substrate are contained. The preparation method of the fiber comprises the following steps: firstly, respectively carrying out vacuum drying on PLLA (poly L lactic acid) and PDLA (poly D lactic acid); physically mixing PLLA with PDLA after being dried; fusing the mixture; collecting primary fibers under the conditions that a spinning temperature is 225-245 DEG C and a spinning speed is 500-2500 meters per minute; and thermally drafting and thermally shaping the primary fibers. Compared with the common polylactic acid fiber, the self-enhanced polylactic acid fiber disclosed by the invention has the advantages of higher constant temperature mechanical strength, higher high temperature mechanical strength and lower boiling water shrinkage, so that the use demand is met and the application field is expanded.
Owner:NINGBO INST OF MATERIALS TECH & ENG CHINESE ACADEMY OF SCI

Method and apparatus for producing high strength, high modulus polyethylene filament by melt drawing

The invention discloses a method for producing polythene fiber with high strength and high modulus by melting fiber drawing and a device thereof. The method includes steps as follows: blend composition of polythene with super high molecular weight and three element blend composition of polythene with super high molecular weight are used as raw material, the raw material is spout fibre adobe after melted through a screw extruder, the fibre adobe is preset drafted after cooling, then low power drafted after once heating, then high power drafted after twice heating, finally is processed heat processing for obtaining polythene fiber with high strength and high modulus. The screw extruder, a cooling mechanism, a drafting machine processing preset drafting, an once heating mechanism, a low power drafting machine, a twice heating mechanism, a high power drafting machine, a heat processing mechanism, a winding reeling machine are arranged in the device orderly. The invention provides a producing method with simple technique, short producing flow, low cost and no pollution aiming at problem that UHMWPE melting spout fibre process has difficult to spin, and provides a device with compact equipment and easy to operate.
Owner:闫镇达

Production technique of three-dimensional curly hollow polyester staple fibers

The invention discloses a production technique of three-dimensional curly hollow polyester staple fibers, wherein the production technique comprises the steps of: utilizing regenerative PET material as raw material; sequentially performing the following procedures to obtain a finished product: pre-treating, drum drying, melting spinning, cooling forming, winding, stretching, curling, oiling, cutting and heat setting, wherein the drum drying duration is 9.5-10.5 h, a spinneret plate in the melting spinning procedure is three-dimensional hollow helical, the cross section of a spinneret orifice is a sealed space formed by sealing the circular arcs of two concentric circles, the temperatures of the threaded rod of a threaded rod extruding machine and the box body of a spinning box are 265-275 DEG C; a circular air blowing asymmetrical cooling forming mode is utilized, the circular blowing blast temperature is 20-24 DEG C, and the circular blowing wind speed is 4.7-5.7 m / s; the total stretching fold is 2.5-2.7 folds, the main curling pressure of a curling wheel is 0.05-0.1 MPa, and no backpressure exists; the heat setting temperature is 175-180 DEG C, and the heat setting duration is 10-14 min. The production technique of the invention has the advantages of saving the cost and protecting the environment, and the prepared finished product not only has good three-dimensional configuration and bulkiness, but also has better thermal stability.
Owner:HANGZHOU BEST CHEM FIBER
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