986results about How to "Easy to prepare" patented technology

The invention discloses a cisatracurium besilate content testing method which comprises the following steps: respectively weighing a test substance and a reference substance in a measuring flask, adding hydrochloric acid for dissolving and metering a volume to a scale, shaking up to prepare a corresponding solution, finally, measuring the solution according to an ultraviolet-visible spectrophotometry, measuring absorbance at a place of a maximum adsorption wavelength of 280nm, and calculating the content of cisatracurium besilate according to an anhydrous substance. According to the cisatracurium besilate content testing method, the solution is simply and conveniently prepared, no organic solvent is used, and the pollution to the environment and the harm to a human body are small. The cisatracurium besilate content testing method is higher in testing speed, and the time of testing each batch of products in average only needs 30 min. A place of a maximum adsorption wavelength of 280 nm is selected, so that the testing accuracy is ensured. The cost of a reagent used in a process of checking each batch of samples does not exceed 20 yuan; the testing cost of each batch of samples by adopting a high-performance liquid chromatography method is not less than 200 yuan, so that the cost of enterprises is greatly lowered.

The application discloses a kind of nano magnetic flocculants and its preparation method and application, belong to drinking water processing technical field, including the following steps: step S1, modified ferroferric oxide nanosphere is ultrasonically dispersed in ammonia alcohol solution, while stirring, slowly drop adding tetraethyl orthosilicate, continue stirring after drop, after centrifugal separation, wash, obtain silica coated ferroferric oxide nanoparticles;Step S2, phenylalanine modified chitosan is added into glacial acetic acid solution, after completely swelling and dissolving, add silica coated ferroferric oxide nanoparticles and ultrasonic treatment, under low pressure ultraviolet lamp, then with anhydrous ethanol wash purification, vacuum drying to constant weight, obtain nano magnetic flocculants;The method of the application is simple and easy to operate, the nano magnetic flocculants prepared can be quickly adsorbed to the surface of sulfonamide antibiotics, produce flocculation and can be magnetically separated, very suitable for trace sulfonamide antibiotics in drinking water source efficient removal.

The present application provides a rhodiolide composition with a core-shell-shell structure, a preparation method thereof comprising the steps of: 1) EGCG inclusion: adding beta-cyclodextrin and EGCG into water, ultrasonic, forming an inclusion compound; 2) liposome assembly: weighing soybean phospholipid and cholesterol, dissolving in chloroform to form a uniform solution; weighing rhodiolide, dissolving in the uniform solution, rotary evaporation to remove chloroform, then adding the inclusion compound and PBS buffer into the container, hydrating, forming a liposome wrapping rhodiolide and inclusion compound; 3) shell loading: weighing collagen, mixing with chitosan solution uniformly to form a complex; adding the complex into the liposome, the complex is coated on the outer layer of the liposome, centrifugal purification, obtaining a rhodiolide composition with a core-shell-shell structure. The present application belongs to the technical field of cosmetic raw materials, and the rhodiolide composition provided has the advantages of high stability, good transdermal effect, and significant anti-aging effect.

This invention discloses a method for preparing a heavy metal ion adsorbent, the heavy metal ion adsorbent itself, and its applications. The preparation method includes the following steps: obtaining a mixture of steel slag and red mud; adding water to the mixture obtained in the above step and wet-milling it using a ball mill to obtain slurry 1; introducing CO2 gas into slurry 1 under stirring conditions to carbonize the modified porous framework particles in slurry 1 to obtain slurry 2; and filtering slurry 2 to obtain a solid, washing the solid until the pH is neutral, and drying it to obtain the heavy metal ion adsorbent. This invention uses two industrial solid wastes, steel slag and red mud, as reaction raw materials, resulting in low cost. It prepares a porous adsorbent material loaded with nano-calcium carbonate at room temperature, exhibiting high adsorption efficiency, and realizing high-value utilization of steel slag and red mud for wastewater treatment.

This invention discloses a copper-based ternary chalcogenide semiconductor material, its preparation method, and its applications. The material is prepared by mixing CuSn(OH)6 nanomaterials, thioacetamide, ethylenediaminetetraacetic acid, and water and carrying out a hydrothermal reaction to obtain Cu3SnS4 nanomaterials. This semiconductor material exhibits excellent photoelectrochemical properties. Photoelectrochemical sensors constructed based on this material demonstrate high detection accuracy, fast response speed, low detection limit, and strong stability, enabling rapid and accurate real-time detection of microplastic content. The preparation method is simple, low-cost, and suitable for industrial production.

This invention discloses a sealing glass with good wettability to titanium alloys, comprising the following components in weight percentage (wt.%): 30-50 wt.% SiO2, 1-5 wt.% Al2O3, 10-30 wt.% B2O3, 10-20 wt.% TiO2, 5-9 wt.% CaO, 1-5 wt.% SrO, 0.1-0.5 wt.% BaO, 2-8 wt.% ZrO2, 1-2 wt.% La2O3, 0-1 wt.% CeO2, and 0.1-0.5 wt.% CoO. This invention also provides a method for preparing sealing glass, comprising the following steps: weighing raw materials according to a mass percentage of a glass composition, mixing them evenly, heating and melting them into a glass melt; after the glass melt is uniform, pouring the molten glass melt into deionized water for rapid cooling and quenching, then drying to obtain glass melt fragments; then ball milling the dried glass fragments into glass powder, drying and sieving to ensure the glass powder particle size is less than 100 micrometers, thus obtaining the desired sealing glass material powder. This invention has a linear thermal expansion coefficient of (50-70)×10⁻⁶ in the range of 20-300 °C. ‑7 / ℃; glass softening temperature is 610-660℃; advantages include chemical stability of level IV or above.

The application relates to an acetic acid-regulated sodium metaaluminate-doped calcium-aluminum-phosphorus defluorination material based on eggshell, a preparation method and application thereof, and belongs to the technical field of defluorination water treatment. The method is as follows: eggshell powder, a phosphorus source and sodium metaaluminate are added into a mixed solvent composed of acetic acid and water, mixed and dispersed to form a uniform reaction system; the pH of the reaction system is adjusted to be alkaline; the adjusted reaction system is transferred into a closed reaction container to perform a solvothermal reaction; after the reaction is completed, the obtained solid product is separated and washed; and the washed product is dried. In the application, acetic acid is used for regulating the dissolution and conversion of the eggshell calcium source and the material crystallization process, sodium metaaluminate is used for introducing aluminum components and adjusting the material structure, so as to construct an Al-Ca-P synergistic defluorination system. The obtained material can be used for removing fluorine ions in fluorine-containing water bodies. The application has the dual characteristics of resource utilization of waste eggshells and preparation of defluorination functional materials, and has the advantages of simple process, easily-obtained raw materials and high application value.

The present application provides a kind of high stability injection with cetrolix acetate freeze-dried composition and its preparation method, wherein, freeze-dried composition is made by active ingredient cetrolix acetate, mannitol, trehalose, glacial acetic acid, edetic acid disodium and injection water, filter sterilization, filling, after freeze-drying, target product is white freeze-dried block, moisture≤0.5%, reconstitution time<30s, acidity pH value is 4.0-6.0, acetate content≤0.4mg / branch, total impurity≤2.5%, cetrolix content is 90.0%-105.0% of the marked amount, under the condition of 40 degrees Celsius high temperature, 5000Lx illumination, place 30 days, total impurity increase≤1.2%, no obvious polymer is generated, the whole preparation method is simple, can significantly improve product anti-degradation, anti-aggregation capacity, prolong the shelf life, while ensuring that product quality indicators meet the standard.

This invention discloses a strain of *Neocallimastix* LGM-ZA9 and its application in the preparation of a coumarin-degrading feed additive. *Neocallimastix* LGM-ZA9 is classified as *Neocallimastix* sp., with accession number CGMCC No. 17592, and its optimal growth temperature is 39℃. The fermentation broth of *Neocallimastix* LGM-ZA9 can be used to degrade the anti-nutritional factor coumarin. The method is simple: the coumarin-containing material to be degraded is mixed with the fermentation broth, sterilized, and then the fermentation broth is added for anaerobic fermentation to degrade the coumarin. This preparation method is simple, highly operable, and can significantly reduce the coumarin content, providing a new method for feeding ruminants with sweet clover as a high-quality forage.

This invention discloses a manufacturing process for composite 7-series aluminum alloy sheets. The composite 7-series aluminum alloy sheets are formed by laminating and rolling multiple layers of 7-series aluminum alloy sheets and multiple layers of 1-series aluminum alloy connecting plates. The 7-series aluminum alloy sheets are composed of the following components by weight percentage: Si: ≤0.22%, Cr: ≤0.23%, Fe: ≤0.35%, Cu: 2.0-3.5%, Mg: 3.5-4.5%, Zn: 6.5-10.0%, Ti: 0.015-0.2%, Zr: 0.05-0.15%, rare earth cerium alloy: 0.015-0.05%, total impurities ≤0.1%, and the remainder being aluminum. This invention uses a lamination method to roll multiple layers of 7-series aluminum alloy sheets and multiple layers of 1-series aluminum alloy connecting plates, which effectively improves plasticity, toughness, and strength. Compared with existing single 7-series materials, it has higher material strength, better impact resistance and weldability, can adapt to corrosion resistance in complex environments, and extends service life.

The invention discloses a bimetallic oxide supported catalyst as well as a preparation method and application thereof. The bimetallic oxide supported catalyst comprises a bimetallic oxide carrier and a metal active component supported on the surface of the bimetallic oxide carrier; the bimetallic oxide carrier contains a divalent metal element oxide and a trivalent metal element oxide; the divalent metal element oxide is selected from at least one of oxides of Mg, Ca, Sr, Zn and Mn; the trivalent metal element oxide is selected from at least one of oxides of Al, In, Fe, Cr and Ce; the metal active component is selected from at least one of Pd, Pt, Ru, Ni and Co; in the bimetallic oxide supported catalyst, the mass of the metal active component is 0.1-20 wt% of the mass of the metal oxide carrier.

The application discloses an epoxy asphalt binder and a preparation method thereof, and belongs to the technical field of asphalt preparation, in particular relates to the binder which is composed of modified asphalt, epoxy resin material, compatilizer and anti-aging agent, and the mass ratio of the modified asphalt, the epoxy resin material, the compatilizer and the anti-aging agent is 100:15-60:5-10:0.1-0.5.The epoxy asphalt binder prepared by the application has excellent bonding performance and flexibility, in particular, the bonding performance at high temperature is significantly better than that of modified emulsified asphalt or polymer modified asphalt, and the flexibility is better than that of epoxy resin binder.

The application provides a double-effect time sequence nano healing agent for cross-species distant grafting and a grafting method thereof, and belongs to the technical field of plant grafting. The application initiates a double-component time sequence cooperation + nano targeted anchoring slow release + stock-scion homologous signal adaptation integrated technology system, which comprises a pre-antioxidant dredging agent and a main-effect healing promoting film forming agent; and is used for a grafting incision in a process and in stages. The application first applies an amino modified nano silicon slow release carrier, a composite enzymatic dredging system and a homologous leaf signal extraction liquid to a distant grafting scene, and solves the problems of grafting incision oxidation browning, callose deposition, poor vascular bundle connection, high cyst rate, slow healing and false activity in cross-species distant grafting through six-effect cooperation of antioxidant barrier, enzymatic dredging, nano targeted delivery, biomimetic skeleton film forming, homologous signal adaptation and bacteriostatic stress resistance, and is suitable for grafting of the same family but different species, such as Ebenaceae, Rutaceae, Bignoniaceae and Myrtaceae, and has a high survival rate.

This invention relates to an air electrode material and its preparation method. The preparation method includes: using metal salts of Ce, Pr, La, Ba, and Sr, metal salts of Co, and a fluorine source as raw materials, and preparing a fluorine-containing perovskite precursor according to a stoichiometric ratio; pretreating the precursor and then sintering it to obtain a composite powder; the composite powder includes a fluorine-containing perovskite main phase and a fluorine-containing CeO2 nanophase; pulverizing and sieving the composite powder to obtain air electrode powder; the fluorine-containing perovskite main phase is an A-site high-entropy perovskite oxide; the fluorine-containing CeO2 nanophase is precipitated through the self-assembly of some Ce elements during sintering; the fluorine-containing CeO2 nanophase is dispersed inside the main phase grains or at grain boundaries, and forms a strongly coupled heterogeneous interface with the main phase. This invention solves the technical problems of poor surface exchange activity, bulk diffusion transport, and long-term stability of existing air electrodes.

This invention relates to the field of separation membrane technology, and more specifically, to a highly selective PVA separation membrane, its preparation method, and its applications. The PVA separation membrane provided by this invention, modified with α-cyclodextrin and / or α-cyclodextrin derivatives, significantly improves the selectivity of the PVA separation membrane. It can be used to separate mixtures of organic matter and water, such as alcohol-water systems, and is suitable for the separation and preparation of high-purity products. The preparation method employed in this invention is simple and easy to operate, and does not introduce new impurities, making it applicable to the industrial production of high-purity products.

The embodiment of the present application relates to a kind of copper intermetallic compound porous materials and its preparation method and application, wherein, preparation method includes: metal Mg, Zn, Cu, M is mixed, is handled by induction smelting, and MgZnCuM alloy ingot is obtained;MgZnCuM alloy ingot is treated by spinning, and MgZnCuM precursor is obtained;MgZnCuM precursor is placed in gas phase de-alloying system and is treated by first vacuum heat treatment, and copper intermetallic compound porous material MgCuM is obtained;MgCuM has double continuous structure.The preparation method is simple and easy to operate, pore size is adjustable, and pore distribution is uniform, and the preparation process is environment-friendly and pollution-free.

This invention relates to the field of water treatment, specifically to an iron-doped biomass resource-based water treatment catalyst, its preparation method, and its application. The preparation of the water treatment catalyst includes the following steps: Step 1, drying and dehydrating recovered pigeon manure; Step 2, finely sieving the dried pigeon manure; Step 3, heat-treating the purified pigeon manure in a muffle furnace to obtain resource-based biochar; Step 4, ball milling dopamine hydrochloride, ferric chloride hexahydrate, and resource-based biochar at a mass ratio of 1:(5-15):(80-100); Step 5, calcining the ball-milled material in a tube furnace at 850-950℃. The water treatment catalyst provided by this invention can rapidly reduce the antibiotic content in wastewater, while accelerating antibiotic removal under ammonia nitrogen conditions. It achieves long-term continuous purification during long-term reaction, exhibiting good stability and removal effect, and is beneficial for achieving low-cost treatment of agricultural waste and efficient purification of new pollutant wastewater.

The present application relates to a kind of automatic material dumping and box withdrawing method suitable for AGV car, which adopts the material dumping and box withdrawing structure including material box dumping mechanism, empty box conveying belt being arranged below material box dumping mechanism, material box transfer mechanism capable of transferring material box between material box dumping mechanism and empty box conveying belt, and comprising the following steps: S1, dumping material;S2, exit empty box.The present application realizes AGV car automatic turnover material box to dump bar material on one hand, turnover is stable, ensures that bar material is all fallen on feeding platform, reduces labor intensity and manpower cost;On the other hand, it realizes automatic empty box withdrawal, to facilitate AGV car to carry out next feeding action in time, effectively improves production efficiency;At the same time, opening direction is unchanged when empty box is withdrawn, to facilitate next material preparation.

This invention relates to a carbon-coated electrode with controllable interface microenvironment, its preparation method, and its application. The carbon-coated electrode comprises a gas diffusion electrode substrate, a copper catalyst layer, and a carbon coating. The copper catalyst layer coats the outside of the gas diffusion electrode substrate, and the carbon coating coats the outside of the copper catalyst layer. The carbon coating forms a dense porous structure on the outside of the copper catalyst layer. The carbon particles in the carbon coating are 15–25 nm in size, and the copper catalyst layer contains several copper nanoparticles with a size of 60–100 nm. During fabrication, copper nanoparticles, a dispersant, and a binder are mixed to form a mixture containing copper nanoparticles, which is then uniformly sprayed onto the surface of the gas diffusion electrode to form the copper catalyst layer. Finally, a mixture of carbon-based nanomaterials and a dispersant is sprayed onto the surface of the copper catalyst layer to form the carbon coating. This invention uses a carbon coating to create hydrophobicity at the electrode interface, improving the interface microenvironment and enhancing the activity of CO electroreduction for ethylene production.

The application discloses a blood perfusion adsorbent for removing endotoxins and free radicals, and a preparation method and application thereof. The adsorbent (P-PEI Cu / TA) has simple preparation process, low cost, good blood compatibility, endotoxin adsorption performance and the ability of removing free radicals generated by oxidative stress, can remove endotoxins in blood of patients with sepsis, and remove free radicals generated by oxidative stress caused by endotoxins. The development of the blood perfusion adsorbent of the application is helpful to extracorporeal blood perfusion treatment of patients with sepsis and reduction of medical cost.

The present application relates to the technical field of supported metal nanoparticle catalysts, in particular to a supported nickel-based carbide acetylene selective hydrogenation catalyst, a preparation method and application thereof. The catalyst is formed by supporting a bimetallic carbide active component on a nanometer gallium oxide carrier, the bimetallic carbide is Ni3GaC 0.7 , and the loading amount of Ni in the catalyst is 1-40 wt.%. A nickel salt is loaded on a nanometer gallium oxide material by an impregnation method, then a NiO / Ga2O3 catalyst is obtained by calcining in air; then the catalyst is treated by heating in a mixed gas of carbon dioxide and hydrogen, and a supported Ni3GaC 0.7 / Ga2O3 catalyst is obtained. The acetylene selective hydrogenation reaction performance test results show that the Ni3GaC 0.7 / Ga2O3 catalyst exhibits excellent selectivity (about 85%) in the hydrogenation reaction, and long-term performance test also shows that the supported catalyst has good stability.

This invention belongs to the field of biosensor technology, specifically relating to an aflatoxin B1 sensor based on exchange catalysis and photocurrent polarity reversal, its preparation method, and its application. The sensor includes a reference electrode, a photosensitive substrate electrode, an AFB1-specific aptamer-trigger chain conjugate, a basement exchange catalytic nucleic acid amplification system, and an h-Zn1Cd5S-hairpin H conjugate. The sensor constructed by this invention is easy to operate, has a fast response speed, good repeatability, high detection sensitivity, and specificity. It can avoid interference from signal fluctuations, and its preparation method is simple, showing broad application prospects in aflatoxin B1 detection.

This invention relates to the field of catalyst technology, and in particular to a formaldehyde reforming hydrogen production catalyst, its preparation method, and its application. The formaldehyde reforming hydrogen production catalyst of this invention comprises a Cu-O-Zn solid solution and mordenite zeolite; the mass ratio of the Cu-O-Zn solid solution to the mordenite zeolite is 50-100:100. This formaldehyde reforming hydrogen production catalyst of this invention has advantages such as low reaction temperature, high formaldehyde conversion rate, high H2 selectivity, low CO selectivity, good stability, and long service life, and has broad market application prospects. This catalyst is not only suitable for formaldehyde systems, but can also be applied to other organic aldehydes such as acetaldehyde, propionaldehyde, butyraldehyde, and benzaldehyde for reforming to produce hydrogen, demonstrating high versatility and practicality in the research field of catalytic reforming of organic aldehydes to produce clean energy hydrogen. The preparation method of this invention is simple, the raw materials are readily available, and it is easy to scale up for industrial production.

The invention relates to perovskite quantum dot glass powder and a preparation method thereof, the chemical formula of the glass powder is CsPb (Ax B1-x) 3, A and B are one or more of Cl, Br or I, x is more than or equal to 0 and less than or equal to 1, and the total molar amount of the components is 100 mol%. According to the perovskite quantum dot glass powder, the fluorescence wavelength can be adjusted through component change, the preparation method is simple and low in toxicity, and the perovskite quantum dot glass powder has high stability and does not need an annealing process. The method can be widely applied to the fields of display devices, lighting equipment, photovoltaic devices, photoelectric sensors and the like.

The application discloses a method for preparing non-spherical nano-silica particles by self-assembly induction, which comprises synthesis of silica particle seeds and further growth of the seeds: by preparing monodispersed seed particles, trace amounts of amphoteric electrolytes are added into the seed growth solution to induce anisotropic growth of the seeds, the types and proportions of the electrolytes are adjusted to make the monodispersed seeds generate silica sol of non-spherical silica particles with different morphologies, and then a series of post-treatments such as water replacement solvent, filtration and concentration are conducted to obtain non-spherical ultra-high-purity silica sol with a mass fraction of more than 18%, a primary particle size of 40-80 nm and a morphology of peanut-shaped, short-chain-shaped and long-chain-shaped, etc. The application also relates to the non-spherical ultra-high-purity silica sol and application thereof in CMP. The preparation method of the application adopts a self-assembly mode of monodispersed seeds to prepare non-spherical particles, and the particle morphology can be further adjusted by adjusting the dosage or types of the self-assembly induction agent.

The present application belongs to the technical field of biomass catalytic conversion, and particularly relates to a method for preparing polyols by hydrogenation of furfural and its derivatives. The method comprises the following steps: taking furfural and its derivatives as raw materials, hydrogen as hydrogen source, and simultaneously adding a catalyst La2CuO4 / Cu to perform ring-opening reaction to obtain polyols. The catalyst La2CuO4 / Cu has excellent catalytic activity in the reaction of hydrogenation conversion of furfural and its derivatives into polyols, has high activity and selectivity for the rupture of C-O bonds of reactants, improves the yield of polyols, and has mild reaction conditions, realizes recovery and long-time use without deactivation of the catalyst, and reduces the utilization cost.

The present application relates to a kind of high-resolution patterning electrochromic display device and its preparation method.The high-resolution patterning electrochromic display device, including the first transparent electrode layer, buffer layer, electrochromic layer containing multiple hole array arrangement, gel electrolyte layer filled in aperture and second transparent electrode layer arranged in sequence.

The application discloses a kind of tetraphenyl ethylene-chalcone derivative preparation and its application preparation and its application.The structure is as follows: the method includes: 4-(1,2,2-triphenyl ethenyl) acetophenone, aldehyde derivative, sodium hydroxide (provides alkaline condition, pH=8.3~8.5), is placed in anhydrous ethanol, under the condition that heating temperature is 80 DEG C, reflux reaction 12h, after reaction is ended, the functional organic material is separated and purified.The functional organic material synthesized according to the above method has larger conjugated system, and has significant pressure-induced color change characteristics.The functional organic material disclosed in the application has low preparation cost, simple operation, simple method, and the material shows significant pressure-induced color change characteristics, can be applied to pressure-induced color change, luminescent material, printing and dyeing, color printing and anti-counterfeiting technical field.

The application discloses a flexible perovskite solar cell based on an in-situ cross-linking organic small molecule and a preparation method thereof, realizes synchronization of a cross-linking process and a perovskite growth process, thereby achieving the effect of small molecule in-situ cross-linking regulation of perovskite crystallization, and can simply prepare a high-efficiency and mechanically stable flexible perovskite solar cell. Based on the in-situ cross-linking strategy, the perovskite thin film growth greatly reduces the dependence on a flexible conductive substrate through a simple doping method, and a perovskite thin film with high crystalline quality, large grain size and low defect density is obtained on the flexible conductive substrate. Based on the perovskite thin film, not only a high-efficiency flexible perovskite solar cell can be prepared, but also the preparation of a large-area flexible device is applicable. In addition, the organic small molecule is aggregated at a perovskite grain boundary after in-situ cross-linking, effectively releases mechanical stress in the bending process, and reduces the Young's modulus of the perovskite thin film, so that the obtained flexible device has excellent mechanical stability.

This application discloses a crystal, a rare-earth-doped crystal, its preparation method, and its applications, belonging to the field of crystal materials. The chemical formula of the crystal is [Gd(L)]. 1.5 (DMA)] n Formula I; in Formula I, L is a ligand formed by deprotonated benzene polycarboxylic acid; benzene polycarboxylic acid is selected from any one of terephthalic acid, phthalic acid, and isophthalic acid; DMA is N , N -Dimethylacetamide; n ∞ represents continuous repetition and infinite extension. The crystal is rare-earth doped, and the chemical formula of the rare-earth doped crystal is [Gd]. 1‑x% (L) 1.5 (DMA)] n :x% Ln 3+ Equation II; in Equation II, x = 0.1~10; Ln 3+ Selected from Tb 3+ Or Eu 3+ Any one of the following. It has potential application value in fields such as fluorescent materials, multicolor display materials, long afterglow materials, X-ray detection and imaging materials, radiation detection dosimeters, and optical information encryption. The preparation method used in this application can be easily achieved through solution reaction under relatively mild conditions, with low cost and strong industrial feasibility.