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9143 results about "Alkene" patented technology

In organic chemistry, an alkene is an unsaturated hydrocarbon that contains at least one carbon–carbon double bond. The words alkene and olefin are often used interchangeably (see nomenclature section below). Acyclic alkenes, with only one double bond and no other functional groups, known as mono-enes, form a homologous series of hydrocarbons with the general formula CₙH₂ₙ. Alkenes have two hydrogen atoms fewer than the corresponding alkane (with the same number of carbon atoms). The simplest alkene, ethylene (C₂H₄), with the International Union of Pure and Applied Chemistry (IUPAC) name ethene, is the organic compound produced on the largest scale industrially. Aromatic compounds are often drawn as cyclic alkenes, but their structure and properties are different and they are not considered to be alkenes.

Electrically heated substrates, assemblies, systems, and processes for catalytic, chemical, and sorbent applications

An article for joule heating is described, including a three-dimensional substrate on and / or in which a pyrolyzate of a phenolic resin or polymer forms an electrically conductive carbon network. Such articles may be incorporated in structured materials applications, which may include support, sorbent, and or catalyst components. Also described are methods of fabricating such articles and structured materials, and apparatus comprising same, and methods of use of such articles and structured materials and apparatus for conducting material transformation processes requiring input of heat for their performance, such as CO2 adsorption, methane pyrolysis for hydrogen and carbon production, hydrogen-assisted conversion of CO2 to hydrocarbons, including catalytic conversion of CO2 to olefins, catalytic conversion of CO2 to propane (liquefied petroleum gas), and catalytic conversion of CO2 to renewable natural gas, reverse water gas shift reaction, steam ethane cracking, propane cracking, steam methane reforming, and dry methane reforming.
Owner:SUSTEON INC

Dual reactor system for simultaneous decontamination and cracking of plastic derived oil to circular chemicals

A process for upgrading plastic derived oil includes contacting the plastic derived oil with a mixed catalyst in a first reactor, where the mixed catalyst includes a decontamination catalyst and a cracking catalyst different from the decontamination catalyst. The first reactor reduces concentrations of halogen-containing compounds in the plastic derived oil. The process includes passing the first reactor effluent to a second reactor and contacting the first reactor effluent with the cracking catalyst to produce a second effluent comprising light olefins and naphtha range hydrocarbons. The process includes separating used mixed catalyst from the first reactor to produce a used decontamination catalyst and a second used cracking catalyst, and regenerating the decontamination catalyst and cracking catalyst in separate regenerators to reduce exposure of the cracking catalyst to halogen-containing compounds produced during regeneration of the used decontamination catalyst.
Owner:SAUDI ARABIAN OIL CO +1

Wear-resistant high-strength composite polyurethane sieve plate and preparation method thereof

The invention discloses a wear-resistant high-strength composite polyurethane sieve plate and a preparation method thereof, and belongs to the technical field of polyurethane sieve plate processing.The preparation method comprises the following steps that modified polyurethane is added into xylene, the temperature of a reaction system is increased to 90-100 DEG C, stirring is conducted till the system is dissolved and clarified, and a polyurethane sieve plate is obtained; the preparation method comprises the following steps: adding olefin double bond modified aluminum oxide powder and a catalyst into a reaction system, taking composite polyurethane prepared from modified aluminum powder reinforced modified polyurethane as a polyurethane sieve plate base material, and carrying out reinforced crosslinking on the composite polyurethane by using o-cresol formaldehyde epoxy resin and modified nylon fiber; the strong acid and alkali corrosion resistance of the composite polyurethane sieve plate is effectively improved, and the service life of the composite polyurethane sieve plate is effectively prolonged.
Owner:ANHUI YIXIANG FILTER MATERIAL CO LTD

Dual reactor system for decontamination and conversion of plastic derived oil to hydrocarbon intermediates

A process for upgrading a plastic derived oil includes providing the plastic derived oil comprising hydrocarbons and greater than or equal to 100 ppmw halogen-containing compounds and contacting the plastic derived oil with an MMO catalyst in a first reactor at reaction conditions to remove halogens from the plastic derived oil to produce a first reactor effluent with less than 100 ppmw halogen-containing compounds. The process includes contacting the first reactor effluent with an adsorbent to produce a treated first reactor effluent, passing the treated first reactor effluent to a second reactor, and contacting the treated first reactor effluent with a cracking catalyst in the second reactor. Contacting with the cracking catalyst may cause hydrocarbons in the treated first reactor effluent to undergo catalytic cracking to produce a second reactor effluent comprising light olefins, naphtha range hydrocarbons, or combinations thereof.
Owner:SAUDI ARABIAN OIL CO

High-temperature-resistant and high-pressure-resistant lubricating oil and preparation method thereof

The invention relates to the field of intelligent preparation, and provides high-temperature-resistant and high-pressure-resistant lubricating oil and a preparation method thereof.The preparation method comprises the steps that a-olefin synthetic oil in a preset proportion is added into a blending kettle provided with a stirring device, then an antioxidant preservative, an extreme-pressure phosphorus-containing ash-free anti-wear agent and an amine high-temperature antioxidant are sequentially added into the blending kettle, stirring is conducted, and the high-temperature-resistant and high-pressure-resistant lubricating oil is obtained; the preparation method comprises the following steps: uniformly stirring at a first constant temperature to obtain a primary mixture, sequentially adding an antirust agent, a metal cleaning agent and a pour point depressant into the mixture, continuously stirring at a second constant temperature, intelligently controlling the stirring time by deeply analyzing the stirring state of the mixture in the stirring process, and finally preparing the high-temperature-resistant and high-pressure-resistant lubricating oil. Therefore, the quality and the performance of the high-temperature-resistant and high-pressure-resistant lubricating oil product can be effectively ensured.
Owner:SUMACH CHEM CO LTD

Modified hydrated filler as well as preparation method and application thereof

The invention relates to the technical field of low-carbon olefin hydration, and discloses a modified hydrated filler as well as a preparation method and application thereof. The modified hydrated filler comprises a filler matrix, and a silane layer, a modified layer A and a modified layer B which are sequentially coated on the outer surface of the filler matrix from inside to outside, the modified layer A contains a pyrrolyl group, an amido group and a furyl group; the modified layer B contains phenoxy, pyrrolyl, furyl, sulfonic acid group, phosphate group and acylamino. The modified hydrated filler provided by the invention can obviously improve the mixing effect of water and alkene and promote the improvement of the yield of low-carbon alcohol.
Owner:CHINA PETROLEUM & CHEMICAL CORP +1

Process of making 2-[(3R)-2-[4-amino-3-(2-fluoro-4-phenoxy- phenyl)pyrazolo[3,4-d]pyrimidin-l-YL]piperidine-l-carbonyl]-4- methyl-4[4-(oxetan-3-YL)piperazin-l-YL]-pent-2-enenitrile and solvate forms thereof

PCT designated stage expiredWO2025029842A2Organic active ingredientsAntipyreticPiperazidinePhenyl group
Disclosed herein are novel methods for preparing 2-[(3R)-2-[4-amino-3-(2-fluoro-4-phenoxy-phenyl)pyrazolo[3,4-d]pyrimidin-1-yl]piperidine-1-carbonyl]-4-methyl-4[4-(oxetan-3-yl)piperazin-1-yl]-pent-2-enenitrile, including various solvate forms and intermediates thereof. Also disclosed herein are novel solvate forms and intermediates of 2-[(3R)-2-[4-amino-3-(2-fluoro-4-phenoxy-phenyl)pyrazolo[3,4-d]pyrimidin-1-yl]piperidine-1-carbonyl]-4-methyl-4[4-(oxetan-3-yl)piperazin-1-yl]-pent-2-enenitrile.
Owner:PRINCIPIA BIOPHARMA INC

Dielectric material based on multi-benzocyclobutene as well as preparation method and application thereof

The invention belongs to the technical field of dielectric materials, and particularly relates to a dielectric material based on polybenzocyclobutene as well as a preparation method and application of the dielectric material. According to the multi-benzocyclobutene-based dielectric material provided by the invention, different halogenated hydrocarbon, olefin and other raw materials are used, and on the basis of containing more than two benzocyclobutene groups, a specific group can be introduced into a connecting group so as to improve the dielectric property and thermal stability of the material; meanwhile, specific groups can be introduced into R2 and R3 through secondary Heck reaction to further improve the dielectric property and thermal stability of the material, so that the dielectric material with excellent comprehensive properties such as dielectric property and thermal stability is provided, and the technical problem of lack of dielectric materials for high-frequency and high-speed printed circuit boards (PCBs) in the prior art can be solved.
Owner:WUHAN DESYTEK ENVIRONMENTAL PROTECTION NEW MATERIAL CO LTD

Battery and preparation method thereof

The invention discloses a battery and a preparation method thereof. The battery comprises a positive electrode lithium supplementing material and an electrolyte, the positive electrode lithium supplementing material comprises at least one of lithium nickelate, lithium ferrite and lithium oxide; the electrolyte comprises a silicon-based fluorophosphate compound as shown in a formula I: # imgabs0 #, wherein R1, R2 and R3 are independently H, F, alkyl of C1-C4, fluoroalkyl of C1-C4, alkenyl of C2-C4, fluoroalkenyl of C2-C4, alkynyl of C2-C4, fluoroalkynyl of C2-C4, cycloalkane of C5-C7, phenyl substituted by R4 or benzyl substituted by R5; r1, R2, R3, R4 and R5 are independently alkyl groups of C1-C4, alkylene groups of C2-C4, alkyne groups of C2-C4, fluoro alkyl groups of C1-C4, fluoro alkylene groups of C2-C4 or fluoro alkyne groups of C2-C4. The compound shown in the formula I is added into the electrolyte, so that the problems of gas expansion and lithium precipitation caused by a positive electrode lithium supplementing material can be solved, and the battery performance is improved.
Owner:GUANGZHOU TINCI MATERIALS TECH

Desulfurization adsorbent for low-carbon olefins and preparation method thereof

The invention discloses a desulfurization adsorbent for low-carbon olefins and a preparation method of the desulfurization adsorbent, and belongs to the technical field of preparation of desulfurizers. The desulfurization adsorbent is a 13X molecular sieve with larger K < + > ion exchange aperture, so that the acting force between adsorbed molecules and cations is weak, the adsorption heat is obviously reduced, the olefin adsorption capacity is weakened, the polymerization reaction of olefin is obviously inhibited, the content of effective components can be further improved, and the adsorption capacity is improved; in the forming process of the adsorbent, a macromolecular polymer and a mesoporous high-thermal-conductivity material are added, local heat accumulation in the adsorption process is reduced, local temperature rise is relieved, meanwhile, heat is rapidly taken away, the adsorption temperature rise is small, and unexpected shutdown, olefin leakage and other dangers are avoided; in the forming process of the adsorbent, metal components are added, the adsorption sites of the adsorbent are further increased, the adsorption speed is higher, and the desulfurization efficiency is higher.
Owner:REZEL ENGINEERING CORP

Organic silicon cooling liquid and preparation method thereof

The invention discloses an organic silicon cooling liquid and a preparation method thereof, the product has low viscosity and high flash point, and relates to the field of application of single-phase cooling liquid for heat dissipation of heating equipment, and the specific method comprises the following steps: uniformly mixing olefin and a catalyst at 20-30 DEG C, heating to 35-45 DEG C, dropwise adding hydrogen-containing siloxane, and controlling the temperature of the reaction liquid to be in a range of 60-130 DEG C; after adding, continuously stirring; cooling after the reaction is finished, and removing residual olefin to obtain a final product with a general formula of (CH3) 3SiO-[R1R2SiO] nSi (CH3) 3, wherein R1 is an alkyl group ranging from 8 to 16; r2 is a methyl group or a trimethylsiloxy group; n is equal to 1-2. The prepared single-phase organic silicon cooling liquid has the performance of high flash point and low viscosity, is low in surface tension, good in fluidity, more comprehensive in coverage, better in heat dissipation effect, good in compatibility with materials of a data center, free of swelling and other damage with related materials, and safe and long-acting.
Owner:JIANGXI HITO CHEM

Shrinkage-resistant light, soft and elastic sole foaming material and preparation method thereof

ActiveCN121378942ASolesElastomerMicrosphere
The invention discloses an anti-shrinkage light, soft and elastic sole foaming material and a preparation method thereof, and belongs to the technical field of footwear products. The light, soft and elastic sole foaming material is formed by chemically foaming an EVA (Ethylene Vinyl Acetate) composite raw material, the EVA composite raw material is prepared from 50 to 70 parts of EVA, 20 to 40 parts of olefin thermoplastic elastomer, 10 to 20 parts of styrene elastomer, 1.5 to 3 parts of maleic anhydride grafted ethylene-octylene copolymer compatilizer, 0.4 to 0.8 part of peroxide cross-linking agent, 3 to 4 parts of foaming agent, 1 to 1.5 parts of zinc oxide, 1 to 1.5 parts of polyethylene wax substance and 0.5 to 1.5 parts of poly (butylene succinate). 0.3 to 1 part of polyamide 12 microspheres and 2 to 3 parts of nano montmorillonite. The foaming material can resist shrinkage when being used as a shoe sole part, and has good rebound performance and the like, so that the high-quality requirement of sneakers, the mass production stability and the like are met.
Owner:ANTA (CHINA) CO LTD

Lipid compounds

PCT designated stage expiredWO2025096940A1Organic active ingredientsPowder deliveryNanoparticleAlkene
The present invention relates to lipids that include novel triazole, and alkyl- and alkene-substituted amine compounds, intermediates in their synthesis, and uses of such triazole, and alkyl- and alkene-substituted amine compounds in, for example, lipid nanoparticle compositions for drug delivery and cancer treatments.
Owner:SPARK THERAPEUTICS INC

Supported Co-based catalyst with nano molybdenum carbide additive as well as preparation method and application of supported Co-based catalyst

The invention belongs to the technical field of catalysts, and particularly relates to a supported Co-based catalyst with a nano molybdenum carbide auxiliary as well as a preparation method and application of the supported Co-based catalyst. The preparation method comprises the following steps: depositing molybdenum oxide on the surface of a carrier material by adopting an atomic layer deposition method, then carrying out carburizing treatment to obtain a molybdenum carbide catalyst, depositing cobalt oxide on the surface of the molybdenum carbide catalyst by adopting the atomic layer deposition method, and then carrying out reduction treatment to obtain the supported cobalt-based catalyst with the nano molybdenum carbide assistant. According to the preparation method provided by the invention, the size of molybdenum carbide and the dispersity and valence state of cobalt are controlled by regulating and controlling the deposition times of molybdenum oxide, and the prepared catalyst has excellent catalytic activity and stability in the hydroformylation reaction of long-chain olefin with the carbon atom number being greater than or equal to 5.
Owner:INST OF COAL CHEM CHINESE ACAD OF SCI

Bidirectional asynchronous stretching high-temperature-resistant polypropylene film for capacitor with three-layer structure and preparation method of polypropylene film

The invention discloses a polypropylene film for a bidirectional asynchronous stretching high-temperature-resistant three-layer structure capacitor and a preparation method of the polypropylene film. The film comprises a first surface layer, a second surface layer and a middle layer clamped between the two surface layers, the middle layer is made of polypropylene, the first surface layer is made of a cycloolefin copolymer (COC), and the second surface layer is made of polypropylene; the mass of the middle layer accounts for 85wt%-88wt% of the total mass, the mass of the first surface layer accounts for 5wt%-7wt% of the total mass, and the mass of the second surface layer accounts for 7wt%-8wt% of the total mass. The temperature resistance can be effectively improved by utilizing the characteristics of the cycloolefin copolymer, the film-forming property is improved by controlling the proportion content of the cycloolefin copolymer, the temperature resistance of the film can be improved to 125 DEG C or above, and the temperature resistance of the film is greatly improved. When the COC content is controlled to be 5%-7%, the film-forming property and the temperature resistance can be both considered, and the temperature reaches 125 DEG C.
Owner:HUBEI LONGCHEN TECH CO LTD

Method for visible light-mediated chemical modification of polypeptide and protein based on cysteine

A method for visible light-mediated chemical modification of a polypeptide or protein based on cysteine includes the following steps: allowing a cysteine residue on a cysteine-containing oligopeptide, polypeptide, or protein to undergo a reaction with an activating reagent to generate a free radical precursor in situ; and subjecting the free radical precursor to desulfurization under photocatalytic condition, and allowing the generated free radical intermediate to undergo an addition reaction with an olefin or an alkyne, such that sulfhydryl removal and carbon-carbon bond construction are achieved to produce a chemical modification product of the polypeptide and protein. The method cleverly avoids the influence on the chiral center, and thus the chirality of the amino acid residue can be retained. The method is conducive to well avoiding the occurrence of side reactions, and thus the efficiency of the entire conversion is very high.
Owner:SHANGHAI JIAOTONG UNIV

Olefin production process

The present invention addresses the problem of providing a method for producing olefins that can sufficiently remove polyamides from waste plastics. [Solution] The method for producing olefins according to the present invention includes a thermal decomposition step of thermally decomposing a waste plastic raw material containing polyolefins and polyamides to obtain a hydrocarbon stream, a separation step of separating a thermal decomposition product of the polyamides from the hydrocarbon stream that has undergone the thermal decomposition step, and a catalytic cracking step of catalytically cracking the hydrocarbon stream that has undergone the separation step in the presence of a catalyst containing zeolite to obtain olefins.
Owner:SUMITOMO CHEM CO LTD

Method for synthesizing deuterated olefin under catalysis of palladium membrane by taking D2O as deuterium source

The invention discloses a method for synthesizing deuterated olefin under catalysis of a palladium membrane by taking D2O as a deuterium source, and belongs to the technical field of synthesis of deuterated olefin building blocks. According to the method, a three-chamber electrolytic tank separated by a palladium membrane and an ion exchange membrane is used as a reactor, the palladium membrane is used as a working electrode, an electrolyte deuterium aqueous solution is used as an electrolyte, deuterium water is electrolyzed through a constant-potential electrolysis method, and formed active deuterium is transmitted to one side of an organic reaction taking absolute ethyl alcohol or cyclohexane as an organic solvent; and catalyzing an alkyne compound by using a palladium membrane modified by sodium thiophenol to perform reduction deuterization so as to synthesize a deuterated olefin compound with high selectivity, and further synthesizing a corresponding deuterated drug. The invention provides a green, efficient, high-universality and low-cost amplification synthesis method for synthesizing a deuterated olefin building block containing a functional group easy to reduce and hydrolyze, and the method has a wide application prospect.
Owner:TIANJIN UNIV

Reversible cross-linked polyolefin elastomer and preparation method thereof

PendingCN120248482AElastomerPolymer science
The invention belongs to the field of olefin polymers, and relates to a reversible cross-linked polyolefin elastomer and a preparation method thereof. The reversible cross-linked polyolefin elastomer is a reversible cross-linked polyolefin elastomer in which a cross-linked network is formed through three non-covalent bonds, namely hydrogen bonds, ionic bonds and coordinate bonds, and the hydrogen bonds and the cross-linked bonds account for 0.1-85% by taking the sum of the three non-covalent bonds, namely the hydrogen bonds, the ionic bonds and the coordinate bonds as 100%; the ionic crosslinking bond accounts for 0.5-90%; and the coordination crosslinking bond accounts for 9-99%. Compared with a reversible cross-linked polyolefin elastomer in the prior art, the reversible cross-linked polyolefin elastomer prepared by the invention contains hydrogen bonds, ionic bonds and coordinate bonds at the same time, and a synergistic effect is generated through combination of reversible cross-linked interaction of the coordinate bonds, the hydrogen bonds and the ionic bonds; therefore, the material has excellent physical and mechanical properties and also has recoverability and self-repairability.
Owner:CHANGZHOU HANWEI POLYMER CO LTD

Electrically heated substrates, assemblies, systems, and processes for catalytic, chemical, and sorbent applications

An article for joule heating is described, including a three-dimensional substrate on and / or in which a pyrolyzate of a phenolic resin or polymer forms an electrically conductive carbon network. Such articles may be incorporated in structured materials applications, which may include support, sorbent, and or catalyst components. Also described are methods of fabricating such articles and structured materials, and apparatus comprising same, and methods of use of such articles and structured materials and apparatus for conducting material transformation processes requiring input of heat for their performance, such as CO2 adsorption, methane pyrolysis for hydrogen and carbon production, hydrogen-assisted conversion of CO2 to hydrocarbons, including catalytic conversion of CO2 to olefins, catalytic conversion of CO2 to propane (liquefied petroleum gas), and catalytic conversion of CO2 to renewable natural gas, reverse water gas shift reaction, steam ethane cracking, propane cracking, steam methane reforming, and dry methane reforming.
Owner:SUSTEON INC

Method for preparing fuel from waste polyolefin through noble-metal-free low-temperature aromatization

The invention discloses a method for preparing fuel from waste polyolefin through noble-metal-free low-temperature aromatization, which comprises the following steps: in the atmosphere of synthesis gas, carrying out catalytic cracking on polyolefin serving as a raw material by adopting a binary mixed catalytic system to obtain aromatic hydrocarbon; the binary mixed catalytic system comprises Zr-ZnO and a molecular sieve; the catalytic cracking temperature is less than or equal to 300 DEG C. According to the low-temperature aromatization method disclosed by the invention, methanol is generated in situ through the synthesis gas, and the methanol and olefin generated by polyolefin cracking are subjected to Prins reaction, so that the aromatization reaction can be realized at the pyrolysis temperature far lower than that in the prior art, precious metals are not needed, the additional value and the application range of a plastic recovery product are greatly enhanced, and the method is suitable for industrial production. And the cost of the recovery process is reduced.
Owner:ZHEJIANG UNIV

Polypropylene film for film capacitor and preparation method thereof

The invention discloses a polypropylene film for a film capacitor, the polypropylene film is composed of polypropylene and a cyclic olefin polymer, a plurality of gaps are distributed in the film, the gaps are approximately annular on the cross section of the film, and the inner diameter of the approximately annular gaps is 20-120nm. The invention also provides a preparation method of the polypropylene film, which comprises the following specific steps: putting the polypropylene and the cyclic olefin polymer into an extruder, heating and melting; the melt is extruded through a T-shaped die head and attached to a piece casting roller through an air knife for piece casting, and the temperature of the piece casting roller is 85-95 DEG C; the method comprises the following steps: preheating a cast sheet, longitudinally stretching at the stretching rate of 4-7 times and at the temperature of 135-150 DEG C, preheating the longitudinally stretched sheet at the temperature of 145-160 DEG C, transversely stretching at the stretching rate of 7-10 times and at the stretching temperature of 165-180 DEG C, and then entering a shaping area at the temperature of 168 DEG C; and carrying out corona treatment, rolling, curing and slitting on the heat-set film to obtain the product. The polypropylene film has good high temperature resistance and high pressure resistance, and is suitable for the field of capacitors.
Owner:XIAMEN CHANGSU IND CO LTD

Preparation and application of cationic compound and compound thereof

The invention discloses preparation and application of a cationic compound and a compound thereof, belongs to the technical field of medicines, and particularly relates to a cationic compound which can be added into an original lipid compound. The invention also discloses the lipid compound, which can be specifically delivered to the lung, has the characteristics of small toxicity and good targeting property, solves the problem of difficult targeting delivery of nucleic acid drugs, and promotes the development of nucleic acid drugs. The prepared lipid compound can effectively target the lung, lung targeting can be achieved without adding any cationic lipid with positive charges into the lipid compound, and the tail of the cationic lipid needs to be provided with one or two olefins. Compared with a compound formed by a traditional DOTAP lipid material, the cationic lipid developed by the invention has lower hemolytic toxicity and better lung targeting property.
Owner:ZHEJIANG UNIV OF TECH +1

Catalyst for olefin polymerization process, propylene polymer and production method thereof

The invention belongs to the technical field of propylene polymerization, and particularly relates to a catalyst for olefin polymerization, an isotacticity-adjustable propylene polymer containing an ultra-high molecular weight polypropylene component and a production method of the isotacticity-adjustable propylene polymer, and the method comprises the following steps: in the presence of hydrogen and a polymerization catalyst, propylene or propylene reacts with one or more optional comonomers; at least one part of the obtained material flow containing the polypropylene component I is continuously subjected to polymerization reaction for 0.05-3.0 hours in a pipeline positioned outside the reactor or a subsequent reactor connected with the pipeline in series and in the presence of a mixture DH of a hydrogenation catalyst and an external electron donor; a propylene polymer product containing 0.03 wt%-15.0 wt% of an ultra-high molecular weight polypropylene component is obtained; the molar ratio of the hydrogenation catalyst to the total amount of hydrogen is 1 / 10000 to 1 / 100. According to the invention, the polypropylene product containing the ultra-high molecular weight component with lower content is prepared, and the isotacticity of the ultra-high molecular weight polypropylene component can be flexibly adjusted.
Owner:CHINA ENERGY INVESTMENT CORP LTD +1

Preparation method of low-halogen alkali-soluble photosensitive resin and solder resist ink

The invention relates to the technical field of electronic materials, in particular to a preparation method of low-halogen alkali-soluble photosensitive resin and solder resist ink. Comprising the following steps: adding amino resin, alcohol olefin and a catalyst A into a solvent, mixing, and carrying out an ether exchange reaction to obtain an initial etherified product; adding peroxide into the initial etherification product, and carrying out epoxidation reaction to obtain an epoxy resin intermediate; adding an olefine acid compound, a catalyst B and a polymerization inhibitor into the epoxy resin intermediate, and carrying out ring-opening esterification reaction to obtain an epoxy acrylate intermediate; and adding acid anhydride into the epoxy acrylate intermediate, and carrying out carboxylation reaction to obtain the low-halogen alkali-soluble photosensitive resin. The problem of high halogen content of the existing alkali-soluble photosensitive resin is solved, and the solder resist ink prepared from the alkali-soluble photosensitive resin has high sensitivity, high resolution, high heat resistance, high acid and alkali resistance and high electrical insulation property.
Owner:GUANGDONG SHUO CHENG TECH CO LTD

Method for Synthesizing a Covalent Organic Framework Material

The present invention relates to a novel method for synthesizing olefin covalent organic framework foams, and polyimide, imine, hydrazone or Ketoenamine covalent organic frameworks (COFs). The method is a green synthetic strategy, including: under non-solvent condition, performing condensation reaction of a methyl-containing monomer and an aldehyde monomer with participation of acid anhydride or carboxylic acid compound to prepare olefin COFs; performing condensation reaction of a multihead acid anhydride or a multihead carboxylic acid monomer and an amino monomer with participation of acid anhydride or carboxylic acid compound to prepare amide COFs; and performing condensation reaction of the aldehyde monomer and the amino monomer with participation of acid anhydride, imidazole or carboxylic acid compound to prepare imine COFs. The COFs obtained by using the method have large specific surface area, regular and adjustable porous structure, and high crystallinity. The method effectively avoids use of organic solvent and risk of high pressure in the reaction process, and is suitable for large-scale preparation of COF materials.
Owner:YOCOF MATERIAL (SUZHOU) CO LTD

Iron-based catalyst for catalyzing CO2 hydrogenation to prepare low-carbon olefin and preparation method of iron-based catalyst

The invention relates to an iron-based catalyst for catalyzing CO2 hydrogenation to prepare low-carbon olefin and a preparation method thereof, and the preparation method comprises the following steps: preparing a zirconium oxide carrier, grinding ZrOCl2. 8H2O, calcining in a muffle furnace to obtain ZrO2, and grinding to obtain the zirconium oxide carrier; the preparation method comprises the following steps: respectively dissolving a Fe source, a Co source and a K source in water, adding the zirconia carrier, stirring and evaporating to obtain a suspension, drying the suspension, and calcining to obtain a FeCoK / ZrO2 catalyst; wherein in the FeCoK / ZrO2 catalyst, the loading capacity of Fe-Co is 12.2 wt%, the molar ratio of Co / (Fe + Co) is 0.15 to 2, and the molar ratio of K to Fe is 0.2 to 0.7. The FeCoK / ZrO2 catalyst prepared by the preparation method disclosed by the invention has a very high conversion rate on CO2 and selectivity on low-carbon olefins, optimizes the adsorption activation path on CO2, and has very good catalytic activity.
Owner:CHINA PETROLEUM & CHEMICAL CORP +2

Single-phase refrigerant medium and preparation method thereof

The invention discloses a single-phase refrigerant medium and a preparation method thereof.The preparation method comprises the following preparation steps that S1, in an inert gas atmosphere, a dimethyl cyclosiloxane mixed ring body and 1, 1, 3, 3-tetramethyldisiloxane react under the action of a second catalyst, and after impurities are removed, a hydrogen-terminated polysiloxane intermediate is obtained; s2, in an inert gas atmosphere, adding the end hydrogen-containing polysiloxane intermediate and a first catalyst into a solvent, then adding isolated diene for reaction, adding alpha-olefin after the reaction is performed for a period of time, and performing low-temperature removal to obtain the single-phase refrigerant medium. The single-phase refrigerant medium has the advantages of being good in fluidity, resistant to high and low temperature, good in insulativity, good in thermal conductivity, high in safe usability and the like, does not contain fluorocarbon compounds, is environmentally friendly, is simple in preparation method and is suitable for industrial production.
Owner:NINGBO RUNHE HIGH TECH MATERIAL CO LTD

Comb-type polyphosphate polymeric dispersant and preparation method thereof

The invention discloses a comb-type polyphosphate polymeric dispersant and a preparation method thereof, the dispersant is prepared by preparing a phosphate monomer from acrylate and phosphorus pentoxide, then copolymerizing the phosphate monomer with phenyl alkene or alkyl alkene, and finally adding alkali liquor for neutralization. A phosphate-polyether bifunctional side chain is introduced to a main chain, a phosphate group provides electrostatic repulsion, and a polyether group enhances steric hindrance, so that the dispersing agent can meet the requirements of strong adsorption and long-range stability at the same time, and a more durable and effective stabilizing effect is provided for a dispersion system.
Owner:GUANGZHOU FANGZHONG CHEM CO LTD