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1265 results about "Solvent free" patented technology

Solvent-free refers to a substance that contains little or no solvent. Paint, adhesives, hash oil and epoxy are substances that normally contain very little solvent. When adhesive contains less than 5% solvent, it is considered a solvent-free adhesive. Solvent-free epoxy resin is solid and contains no water or solvent as diluents.

High-stability endotoxin-free PHA nano-emulsion and preparation method thereof

ActiveCN120585676ACosmetic preparationsToilet preparationsEndotoxin removalNanoparticle
The invention discloses a high-stability endotoxin-free PHA nano-emulsion and a preparation method thereof, and belongs to the technical field of biodegradable high polymer material compositions and processing thereof. The nano-emulsion is characterized in that the endotoxin content is not higher than 0.10 EU / g, the median particle size d50 is 100-200 nm, and the PDI is not higher than 0.15, and the nano-emulsion is stable in long-term storage. The preparation method is a continuous solvent-free process and comprises the steps of melt extrusion, high-pressure thermal emulsification and deep endotoxin removal. By adopting the specific pH-insensitive cationic polymer emulsifier and the crystallization inhibitor, the chemical contradiction that an efficient alkaline purification process is incompatible with a nano-emulsion stable system is solved, physical aging is inhibited, and an unexpected technical effect is obtained. The invention also discloses an O / W type cream containing the nano emulsion.
Owner:DU BAI CHENG NEW MATERIAL TECH (SHANGHAI) CO LTD +1

Method for preparing single-benzene-ring liquid chemicals through solvent-free hydrogenation degradation of polystyrene waste plastics based on bifunctional catalyst

The invention discloses a method for preparing a single-benzene-ring liquid chemical through solvent-free hydrogenation degradation of polystyrene waste plastics based on a bifunctional catalyst. According to the method, Nb2O5 is taken as a carrier, 1-3wt% of noble metal ruthenium is loaded to prepare a bifunctional catalyst, and high-molecular-weight polystyrene is efficiently degraded into single-benzene-ring liquid chemicals such as benzene, methylbenzene and ethylbenzene through hydrogenation reaction under a solvent-free condition. Precious metal ruthenium hydrogenates a polystyrene long chain to generate a short-chain hydrocarbon intermediate, then a carrier # imgabs0 # acid site drives beta-cracking and hydrogen transfer reaction, and a single-benzene-ring product is directionally generated through the synergistic effect of the short-chain hydrocarbon intermediate and the carrier # imgabs0 # acid site. The method has the advantages of no solvent, reduced equipment cost, high reaction efficiency, simple reaction operation, mild reaction conditions, simple catalyst preparation process, high activity, selectivity and good stability, and is suitable for industrial production, and no other solvents preempt acidic sites. The method not only can realize cyclic utilization of resources, but also can alleviate the current environmental pollution problem.
Owner:DALIAN UNIV OF TECH

Solvent-free UV (ultraviolet) dielectric insulation protective coating as well as preparation method and application thereof

The invention provides a solvent-free UV dielectric insulation protective coating as well as a preparation method and application thereof. The high-surface-energy and high-glass-transition-temperature UV-curable coating is prepared by combining flexible modified polyurethane acrylate, flexible acrylate, rigid acrylate with high glass transition temperature, a high-functionality acrylate cross-linking agent, methyl methacrylate with high dilutability and high glass transition temperature as well as a plurality of photoinitiators, auxiliaries, pigment and filler powder and the like. The invention relates to a dielectric insulation protective coating with high adhesive force. The prepared coating is a solvent-free 100% solid single component, is complete in mixing and dissolving, convenient to construct, high in light curing energy utilization rate, high in production efficiency and suitable for large-scale automatic large-scale flow line production, and compared with PSA back glue used for a traditional PET blue film, the outer surface of the coating has higher surface energy, and the coating has the advantages of being high in light curing energy utilization rate and high in production efficiency. And the film has considerable dielectric insulation performance and good edge covering protection performance, and meets the development requirements of a higher charging voltage platform of a fast-charging electric vehicle in the future.
Owner:LINKTECH SILICONE MATERIAL CO LTD

Solvent-free process for preparing lithium-ion batteries

A solvent-free process employs a multifunctional carbon black to prepare compositions and electrodes for lithium-ion batteries. The multifunctional carbon black provides two or more desirable characteristics, acting, for example, as a conductive carbon additive, as a fibrillizing agent and / or as a mechanical reinforcement. In one example, an electroactive material, e.g., graphite or a lithium transition metal compound, a binder and a multifunctional carbon black are combined in one or more steps. High shear mixing is used to process the binder in the presence of the multifunctional carbon black. The resulting composition can be formed into a film which can be applied onto a suitable substrate to produce an electrode.
Owner:CABOT CORP

Polyurethane modified epoxy resin adhesive, preparation method and application

The invention discloses a polyurethane modified epoxy resin adhesive as well as a preparation method and application thereof, and the polyurethane modified epoxy resin adhesive is prepared from the following components in parts by mass: 7-10 parts of E51 type bisphenol A diglycidyl ether, 3.5 parts of a phenolic aldehyde amine T31 curing agent and 1-3 parts of synthetic polyurethane, the synthetic polyurethane is prepared from polyether triol, polyether amine, isophorone diisocyanate and glycerol carbonate, and a blending system of the synthetic polyurethane and bisphenol A diglycidyl ether is adopted to be subjected to covalent crosslinking with phenolic aldehyde amine T31, so that the adhesive has high toughness and strength guarantee; the synthetic polyurethane prepared by the method is obtained through simple, green and efficient solvent-free synthesis, and the synthesized product has certain fluidity at room temperature, so that the subsequent stirring preparation process of an adhesive is facilitated. And a solvent-free synthesis method is adopted, so that the use of a toxic organic solvent in the traditional polyurethane synthesis process is avoided, and the synthesis process is greener.
Owner:BEIJING FORESTRY UNIVERSITY

Solvent-free vanillin-hydroxyethyl acrylate double-system closed waterborne polyurethane emulsion adhesive, and preparation method and use method of solvent-free vanillin-hydroxyethyl acrylate double-system closed waterborne polyurethane emulsion adhesive

The invention discloses a solvent-free vanillin-hydroxyethyl acrylate double-system closed waterborne polyurethane emulsion adhesive as well as a preparation method and a use method thereof, and belongs to the field of waterborne polyurethane emulsion adhesives. The invention is mainly prepared from the following components in parts by weight: 40 to 50 parts of soft segment monomer, 50 to 60 parts of hard segment monomer, 20 to 40 parts of sealing agent, 0.02 to 0.15 part of catalyst, 0.4 to 0.6 part of emulsifier, 0.2 to 0.6 part of initiator, 4 to 12 parts of neutralizer, 5 to 15 parts of functional monomer and 340 to 360 parts of deionized water. According to the double-system closed waterborne polyurethane emulsion adhesive disclosed by the invention, rapid crosslinking curing of the adhesive can be realized through thermocuring, the highest hardness of an adhesive layer can reach about 26 MPa, the adhesive strength is high, and the mechanical property is relatively good.
Owner:QUZHOU UNIV

Packaging material, method for manufacturing same, and packaging bag

PCT designated stage expiredWO2025154535A1Flexible coversWrappersPolymer scienceSolvent free
This packaging material has a structure in which a transparent vapor-deposited barrier film, a stretched nylon film, and an unstretched polypropylene film are laminated in this order. The transparent vapor-deposited barrier film and the stretched nylon film are laminated with an adhesive layer formed of a cured product of a solventless adhesive agent therebetween. The ratio of the Young's modulus in the MD direction of the unstretched polypropylene film with respect to the thickness of the unstretched polypropylene film is 9.0 MPa / μm or more.
Owner:TOPPAN HOLDINGS INC

Polyurethane super-strong adhesive as well as preparation method and application thereof

The invention belongs to the technical field of adhesives, and particularly relates to a polyurethane super-strong adhesive as well as a preparation method and application thereof. The preparation method comprises the following steps: mixing branched-chain multi-mercapto mercaptan with an epoxy compound, adding a catalyst for reaction, and then adding a neutralizer for terminating the reaction to prepare an epoxy prepolymer; the preparation method comprises the following steps: mixing an epoxy prepolymer with branched chain multi-mercapto mercaptan to prepare a mixture; and mixing the mixture with isocyanate, reacting to obtain a product, and defoaming the product to obtain the polyurethane super-strong adhesive. The sulfur element is introduced into a polymer molecular chain, so that the bonding performance between the base cloth (base cloth) and the coating is remarkably improved, meanwhile, the water resistance, solvent resistance and low temperature resistance are also greatly improved, the method is suitable for humid, low-temperature and organic solvent environments, no solvent participates in the preparation process, and the environment-friendly requirement is met.
Owner:QILU UNIVERSITY OF TECHNOLOGY (SHANDONG ACADEMY OF SCIENCES)

Environment-friendly furniture protective film and preparation method thereof

ActiveCN120923834ACellulosePolymer science
The invention relates to the technical field of environment-friendly high polymer materials, in particular to an environment-friendly furniture protective film and a preparation method thereof. The technical problems that a traditional furniture protection film is insufficient in toughness and short in service life are solved. According to the protective film disclosed by the invention, a polylactic acid, polyhydroxyalkanoate and dimer fatty acid ester flexibilizer blending material is taken as a matrix, a cyanoethylation lignin-cellulose nanocrystal compound reinforcing agent is added to form a dense nano network, and a dynamic cross-linking agent containing disulfide bonds and a functional auxiliary agent are introduced. According to the invention, a solvent-free ultraviolet light / damp and hot dual-curing system is adopted for coating and curing to prepare the coating. The furniture protection film is excellent in mechanical property, toughness is remarkably improved, and the furniture protection film has multiple functions such as high barrier property and the like and has the self-repairing capacity and the full-life-cycle environment-friendly characteristic.
Owner:SHENGFENG (HUBEI) NEW MATERIAL TECH CO LTD

Preparation method and application of sacha inchi oil

The invention relates to the field of extraction of sacha inchi oil, in particular to a preparation method and application of sacha inchi oil, and aims to solve the problems of large loss of heat-sensitive components, solvent residue and low oil yield in the traditional process. The ratio of cellulase to pectinase to xylanase to lipase is 3: 2: 1: 0.5, and carrying out enzymolysis for 2-3 hours at the pH value of 4.5-5.5 and the temperature of 45-50 DEG C; the obtained enzymolysis product is subjected to 28-40kHz ultrasonic treatment for 20-30 minutes, and then is subjected to two-stage gradient squeezing (pre-squeezing at 50-55 DEG C to final squeezing at 35-40 DEG C) in combination with 0.1 mu m ceramic membrane filtration, so that efficient oil extraction and active ingredient protection are realized. The oil yield of the sacha inchi oil is increased to 50.0%, the content of alpha-linolenic acid is larger than or equal to 42%, the content of vitamin E reaches 158 mg / 100 g, no solvent is left, and the sacha inchi oil is suitable for the fields of functional food and cosmetics.
Owner:YUNNAN SEEDSHARE DEV CO LTD

Dual-curing solvent-free high-temperature-resistant epoxy resin structural adhesive as well as preparation method and application thereof

The invention discloses a dual-curing solvent-free high-temperature-resistant epoxy resin structural adhesive as well as a preparation method and application thereof. The structural adhesive comprises the following components in percentage by weight: 1.5-5% of a latent curing agent, 2-5% of a high-heat-resistant curing agent, 1-5% of nano filler, 0.1-0.3% of a curing accelerator and the balance of epoxy resin. By accurately screening epoxy resin monomers, optimizing a dual curing agent system and introducing the high-temperature-resistant nanofiller, room-temperature stability, medium-temperature rapid curing and gelling and high-temperature complete curing are realized, and the final heat-resistant temperature is greater than or equal to 300 DEG C. Through the synergistic effect of the epoxy resin, the medium-temperature curing agent and the high-temperature curing agent, the crosslinking stability at different temperature stages is ensured. In addition, through introduction of the inorganic nano filler, the high-temperature mechanical property and the heat-resistant stability of the material are further improved. The preparation method does not need to use a solvent, and the prepared epoxy resin structural adhesive has excellent heat resistance and mechanical strength and is suitable for the fields of high-temperature structural adhesives, aerospace composite materials, high-temperature-resistant coatings and the like.
Owner:HUNAN YISIDI TECH CO LTD +1

Method for preparing diglyceride oil by solvent-free enzymatic method

The invention provides a method for preparing diglyceride oil by a solventless enzymatic method, which comprises the following steps: S1, mixing saturated fatty acid A and saturated fatty acid B to prepare a liquid eutectic mixture; s2, mixing the eutectic mixture, glycerol and lipase in a reaction system, and carrying out esterification reaction to obtain diglyceride; s3, separating the prepared diglyceride, adding the saturated fatty acid A and / or the saturated fatty acid B into the reaction system again to form a liquid eutectic mixture again, and repeating the step 2; wherein in the step S1, the saturated fatty acid A and the saturated fatty acid B are selected from C10-C20 alkanoic acid, in the step S2, the mass ratio of the eutectic mixture to the glycerol is 1: (1-5), and the temperature of the esterification reaction is 35-78 DEG C. The method solves the problem that the high-melting-point saturated fatty acid is difficult to utilize in the existing technology for preparing the diglyceride oil by the solvent-free enzymatic method.
Owner:HUBEI CHUYI NEW MATERIAL CO LTD

Preparation method of soybean oil base polyhydric alcohol

The invention relates to a preparation method of soybean oil base polyhydric alcohol, in particular to a method for preparing soybean oil base polyhydric alcohol by directly using soybean oil. The soybean oil diluted by using a solvent reacts with hydrogen peroxide with the weight percentage being 30% for 2-5 hours at the temperature of 60-70 DEG C under catalysis of a catalyst with the weight percentage being 3-5%; vacuum distillation is conducted after the reaction is ended, and the solvent is evaporated; then low alcohol is added in a reactor to be subjected to a reaction for 4-6 hours under the pressure of 0.3-0.4 MPa and at the temperature of 70-80 DEG C, then the reaction is stopped, and the soybean oil base polyhydric alcohol is obtained. The method saves the using amount of hydrogen peroxide, reduces the post-treatment steps, and simplifies the production procedures, and accordingly the product cost is declined directly.
Owner:YIWU QUANCE NEW MATERIAL CO LTD

Self-repairable lipoic acid-based underwater binder and preparation method thereof

The invention discloses a self-repairable lipoic acid-based underwater binder and a preparation method thereof, and relates to the technical field of polymer binders. The binder comprises the following raw material components: lipoic acid and vinyl cyclosiloxane, the lipoic acid and the vinyl cyclosiloxane are subjected to chemical crosslinking through a solvent-free thermal / light synergistic polymerization process, and the underwater binder with good self-repairing performance and binding performance is prepared. The preparation method disclosed by the invention is simple and environment-friendly in process, and the prepared lipoic acid-based underwater binder has firm binding property, good universality and excellent self-repairing characteristic, and can realize rapid and stable binding underwater.
Owner:GUILIN UNIVERSITY OF TECHNOLOGY

Composite anti-corrosion coating for medium heavy-duty anti-corrosion environment and preparation method of composite anti-corrosion coating

The invention relates to the technical field of anti-corrosion coatings, in particular to a composite anti-corrosion coating for a medium heavy-duty anti-corrosion environment and a preparation method of the composite anti-corrosion coating. According to the technical scheme, the composite anti-corrosion coating for the medium heavy anti-corrosion environment comprises the following components in percentage by mass: a bottom coating component, a middle transition layer component and a surface coating component, and the mass ratio of the bottom coating component to the middle transition layer component to the surface coating component is 33: 17: 50; the durability is improved through multi-dimensional material innovation, a fluorocarbon resin modified waterborne epoxy system is adopted for the bottom coating, and a nano graphene directional arrangement technology is combined, so that a labyrinth effect is formed, and a corrosion medium is blocked; a solvent-free polyurea and microcapsule self-repairing system is introduced into the surface coating, so that automatic repairing after damage is realized; the middle transition layer enhances the interlayer barrier function through the oriented graphene composite material, and the three layers cooperate to construct a compact protection network, so that the medium permeation path is obviously delayed, and the full-life-cycle maintenance cost is greatly reduced.
Owner:TIANJIN JIZHI ENG CONSULTING CO LTD

Preparation of lipoic acid modified epoxy resin-based sealant and circuit board sealing and unsealing process method of lipoic acid modified epoxy resin-based sealant

The invention belongs to the technical field of electronic sealants, and relates to preparation of a lipoic acid modified epoxy resin-based sealant and a circuit board sealing and unsealing process method thereof. The preparation method comprises the following steps: mixing epoxidized soybean oil and a lipoic acid monomer, stirring and reacting at 50-90 DEG C for 20-40 minutes to prepare a precursor, pouring the precursor into a mold, and curing at 50 DEG C for 8 hours to obtain the sealant. And sealing the circuit board by using the precursor, keeping at 50 DEG C for 8 hours, and finally soaking the sealed circuit board in absolute ethyl alcohol at 50 DEG C for 72 hours to realize unsealing. The method adopts a solvent-free method, and is simple in process, low in cost and environment-friendly. The prepared sealant can adhere to various base materials, is stable in air and underwater and has excellent transparency, weather resistance and detachability, a new thought is provided for design and preparation of the bio-based electronic sealant, and meanwhile, the epoxidized soybean oil can be replaced to construct various functional sealants.
Owner:CHANGCHUN UNIV OF TECH

MXene-based aerogel as well as normal-pressure preparation method and application thereof

The invention belongs to the technical field of aerogel, and discloses MXene-based aerogel and a normal-pressure preparation method and application thereof.The preparation method comprises the steps that mixed dispersion liquid of chitosan and conductive filler is mixed with glutaraldehyde, standing and crosslinking are conducted, and hydrogel is obtained; in the hydrogel, the conductive filler accounts for 20-75% of the mass of a solid substance, the chitosan accounts for 15-55% of the mass of the solid substance, and the glutaraldehyde accounts for 1-20% of the mass of the solid substance; the filler is selected from MXene, a carbon nano tube, graphene, boron nitride or MOF (Metal Organic Framework); the hydrogel is frozen at the temperature ranging from-20 DEG C to-80 DEG C; and carrying out normal pressure drying on the frozen hydrogel at 25-80 DEG C to obtain the aerogel. The solvent exchange-free normal-pressure drying preparation process breaks through the limitation of solvent exchange on the size, the high cost of a large amount of solvent is saved, large-area extensible preparation can be realized on the basis of energy conservation and environmental protection, and meanwhile, the prepared aerogel has relatively high mechanical strength, and the application range is widened.
Owner:SHANDONG UNIV

Preparation method of high-temperature-resistant durable super-hydrophobic powder coating and application of coating to heat distribution pipeline

According to the preparation method of the high-temperature-resistant durable super-hydrophobic powder coating, integrated powder coating particles are prepared by mixing through a tabletting-crushing-sieving technology, and finally, one end of a solid nano-material in the integrated powder coating particles is embedded into a bottom layer, and the other end of the solid nano-material protrudes out of the surface of the coating, so that a nano-fiber bridging interface strengthening structure is formed. According to the invention, the low surface energy material, the solid nano material and the thermoplastic film-forming resin are effectively combined together to construct firm and stable integrated powder coating particles, so that the overall performance is synergistically enhanced, and the protection capability of a micron-scale structure to a nano-scale structure is greatly improved; the solvent-free durable super-hydrophobic powder coating is directly prepared through electrostatic spraying, so that the technological process is simplified; the solid, solvent-free and environment-friendly super-hydrophobic powder coating is prepared, has excellent high-temperature resistance and super-hydrophobic performance, and has potential advantages in the aspect of anti-corrosion and anti-drag application of a heat distribution pipeline.
Owner:TIANJIN UNIV +2

Preparation method of linear reaction type phosphorus-nitrogen-silicon synergistic flame-retardant solvent-free polyurethane coating

The invention relates to the field of polyurethane, and discloses a preparation method of a linear reaction type phosphorus-nitrogen-silicon synergistic flame-retardant solvent-free polyurethane coating, which comprises the following steps: S1, carrying out exchange reaction on phosphonate and alcohol amine ester to obtain a phosphorus-nitrogen polyol intermediate; s2, carrying out condensation polymerization on the phosphorus-nitrogen polyol intermediate and chlorosilane to obtain phosphorus-nitrogen-silicon polyol; s3, mixing polyester / polyether polyol, a chain extender and an amine / metal catalyst to obtain a component A; mixing and reacting isocyanate, part of polyester / polyether polyol and phosphorus-nitrogen-silicon polyol to obtain a component B; mixing the component A and the component B, spraying the mixture on release paper, and curing. Through a synergistic flame-retardant mechanism of phosphorus, nitrogen and silicon, the balance of efficient flame retardance, mechanical properties and excellent coating properties is realized. The solvent-free system realizes zero emission of volatile organic compounds, and the linear reaction type design ensures that the mechanical properties and durability of the coating are not influenced.
Owner:ZHEJIANG SCI-TECH UNIV

Modified thermoplastic solid-solution anticorrosive paint, preparation method thereof and application of modified thermoplastic solid-solution anticorrosive paint on surface of pneumatic actuator

The invention discloses a modified thermoplastic solid-solution anticorrosive coating, a preparation method thereof and application of the modified thermoplastic solid-solution anticorrosive coating on the surface of a pneumatic actuator, and belongs to the field of industrial equipment surface protection materials. Two novel modifiers are designed to construct a multi-protection system. Wherein the layered double hydroxide-silane covalent grafting modifier takes magnesium-aluminum layered double hydroxide as a matrix, and after covalent modification by a silane coupling agent, the matrix is compounded with a quinoline derivative in an intercalation manner, so that the interface bonding and barrier properties are improved; according to the polyaniline-graphene covalent grafting modifier, few layers of graphene and polyaniline are copolymerized and then grafted with a polyurethane prepolymer, so that the toughness and the conductive corrosion resistance of a coating are enhanced. The coating is prepared by taking polyethersulfone as a matrix, compounding the modifier, nano silicon dioxide and other components, mixing, dissolving, dispersing at a high speed and ultrasonically defoaming. The coating has the advantages of high interface adhesion, strong corrosion resistance, dynamic fatigue resistance, environmental protection, no solvent and the like, and is suitable for surface protection of key components such as a pneumatic actuator shell.
Owner:WUXI CHENGTIANNUO ACTUATOR MFG CO LTD

A puncture-resistant film and its preparation process

This application relates to the technical field of polymer materials, and specifically discloses a puncture-resistant film and its preparation process. A puncture-resistant film is composed of an outer layer, an intermediate layer, and an inner layer, and the outer layer, the intermediate layer, and the inner layer are all bonded by a solvent-free adhesive; the outer layer is a PET film layer; the intermediate layer is a nylon film layer; the inner layer is mainly prepared from the following raw materials in parts by weight: 36-48 parts of LDPE resin, 20-38 parts of LLDPE resin, 5-10 parts of MLLDPE resin, 1-5 parts of HDPE resin, 5-8 parts of nano-organic montmorillonite, 0.5-1 part of nano-silica sol, 5-8 parts of compatibilizer, 0.3-0.5 part of antiblocking agent, 0.3-0.5 part of slip agent, 0.1-0.3 part of antistatic agent, and 0.1-0.2 part of processing aid. This application can improve the puncture resistance of the film.
Owner:HAINING YUEHAI COLOR PRINTING CO LTD

Solvent-free polyaspartic acid ester polyurea floor coating and preparation method thereof

The invention provides a solvent-free polyaspartic acid ester polyurea floor coating and a preparation method thereof, the coating comprises a main agent and a curing agent, the main agent comprises polyaspartic acid ester resin, a functional auxiliary agent and a pigment filler; the functional auxiliary agent comprises a dispersing agent, a defoaming agent, a flatting agent, a water absorbent and a coupling agent, and the pigment filler comprises pigment and filler; the curing agent comprises a hydroxyl cyclic ketone compound modified polyisocyanate composition. By optimizing and modifying the components in the radix asparagi polyurea coating, a terrace material can be endowed with excellent properties in the aspects of rapid curing, high-humidity constructability, performance retention rate after curing, leveling wettability, good adhesive force with various coating substrates, high and low temperature resistance, high strength and the like, and the comprehensive performance is excellent; the method is suitable for different terrace application fields.
Owner:REALTEC CHEM RTC SHANGHAI

Cellulose-doped cesium-tungsten bronze modified epoxy silane infrared stealth coating material as well as preparation method and application thereof

PendingCN120888237ACoatingsEpoxyCellulose
The invention belongs to the technical field of infrared stealth, and particularly relates to a cellulose doped cesium tungsten bronze modified epoxy silane infrared stealth coating material as well as a preparation method and application thereof. Through the ternary collaborative design of cellulose, cesium tungsten bronze and epoxy silane, and by adopting a physical blending-chemical grafting process, the problems of high toxicity, low hardness and complex process of the existing coating are solved. The prepared coating has a good infrared stealth effect, the pencil hardness can reach 9H, and the thermal decomposition temperature is gt; and the preparation process is solvent-free, low-temperature and efficient, the low-infrared-emissivity effect, high hardness and good wear resistance are achieved, the coating is suitable for direct coating of military equipment (such as unmanned aerial vehicles), the original structure does not need to be changed, and the application prospect is wide.
Owner:QILU UNIVERSITY OF TECHNOLOGY (SHANDONG ACADEMY OF SCIENCES)

Super-soft anti-corrosion solvent-free polyester coating and preparation method thereof

The invention relates to the technical field of coatings, and discloses a super-soft anticorrosive solvent-free polyester coating and a preparation method thereof. The solvent-free polyester coating comprises a component A and a component B, wherein the component A comprises modified polyester polyol, polycarbonate diol, modified organic silicon, a catalyst, an auxiliary agent and an inorganic filler; the component B is polymethylene polyphenyl isocyanate; the solvent-free polyester coating prepared by the invention has the advantages of ultrahigh solid content, accurate regulation and control of coating thickness, high reaction film-forming speed, primer and topcoat integration, ultrahigh flexibility, and favorable adhesive force and corrosion resistance to a base material.
Owner:SHAANXI HANGKAI ENVIRONMENTAL PROTECTION TECHNOLOGY CO LTD +1

Degradable preservative film and preparation method thereof

The invention discloses a degradable preservative film and a preparation method thereof. The film takes nano chitosan / agarose in a ratio of 1: 1 as a matrix, contains 0.5-5wt% of PVA (Polyvinyl Alcohol), 1-4wt% of protein powder or starch, 0.2-3wt% of tea polyphenol / carvacrol, 5-20wt% of glycerol and optional 5-15wt% of polylactic acid, and is cross-linked with sodium alginate. And carrying out tape casting at 55-65 DEG C, and carrying out gradient drying at 40-50 DEG C, thereby obtaining the product. The film is compact and flexible, the breaking strength is larger than or equal to 69 MPa, the oxygen permeability is low, the inhibition zone on six germs is enlarged by 3-4 mm, 98% of natural soil is degraded 20 days later, and no toxic smoke is generated during incineration. The biodegradable film is solvent-free in preparation, can be produced by existing equipment, is lower than a traditional biodegradable film in cost, can be in direct contact with food, remarkably prolongs the fresh-keeping period of fruits and vegetables, replaces PE and PVC, and solves white pollution.
Owner:JINLIN MEDICAL COLLEGE

High-adaptability mud-resistant polycarboxylate superplasticizer and preparation method thereof

ActiveCN120590586AHydrophilic monomerEpoxy
The invention belongs to the technical field of high-molecular polymer materials, and particularly relates to a high-adaptability anti-mud polycarboxylic acid water reducing agent and a preparation method thereof. The preparation method comprises the following steps: heating epoxy-terminated allyl polyether and phytic acid to 40-80 DEG C in the absence of a solvent or a diluted solvent, and reacting to obtain a phytate-terminated high-steric-hindrance polyether monomer; and adding the obtained high-steric-hindrance polyether monomer, an unsaturated polyether monomer and an unsaturated carboxylic acid monomer into water, stirring and heating to 60-80 DEG C, dropwise adding an initiator to carry out a copolymerization reaction, and adding alkali for neutralization after the reaction is completed, thereby obtaining the high-adaptability anti-mud polycarboxylic acid water reducer. Compared with a phosphate-terminated hydrophilic monomer, the phytate-terminated high-steric-hindrance polyether monomer is adopted as the mud-resistant monomer, and compared with the phosphate-terminated hydrophilic monomer, the phytate-terminated high-steric-hindrance polyether monomer has higher steric hindrance and can better reduce intercalation adsorption of clay to the water reducing agent, so that the mud resistance is remarkably improved, and the adaptability of the polycarboxylic acid water reducing agent to mud-containing concrete is improved.
Owner:FOSHAN KAIJUN NEW BUILDING MATERIALS TECH CO LTD

Solvent-free anti-doodling cover agent as well as preparation method and application thereof

The invention relates to the technical field of coatings, in particular to a solvent-free anti-doodling cover agent as well as a preparation method and application thereof. The solvent-free anti-doodling finishing agent is prepared from the following raw materials in percentage by mass: 80 to 95 weight percent of solvent-free methyl phenyl silicone resin, 1 to 5 weight percent of a curing agent, 3 to 8 weight percent of an adhesion enhancer, 0.5 to 3 weight percent of an anti-doodling auxiliary agent and 0 to 6 weight percent of an optional delustering agent. The core is that the adhesion enhancer is an enhanced silane coupling agent and is prepared by carrying out molecular-level chemical bonding on a titanium compound, the silane coupling agent and a self-made antifouling agent. The finishing agent disclosed by the invention has the advantages of high adhesive force, excellent stain resistance, adjustable glossiness and the like, and is suitable for base material protection of various scenes such as building outer walls, household crystal plating and artistic coatings.
Owner:FOSHAN SITECH CHEM TECH

Solvent-free composite aluminized film bubble bag packaging machine

The invention belongs to the technical field of bubble bag packaging, and discloses a solvent-free composite aluminized film bubble bag packaging machine which comprises a conveyor and a packaging table, the conveyor is located on the left side of the packaging table, a conveying belt is arranged at the bottom of the packaging table, and a heating soldering iron is fixedly installed on the left side wall of the packaging table. Guide mechanisms are arranged on the left side and the right side of the heating soldering iron, a heat sealing table is fixedly installed in the middle of the packaging table, and an air cylinder is fixedly installed at the top of the heat sealing table. According to the bubble bag winding and unwinding device, a two-way screw rod rotates through operation of a first motor, the distance between two sets of sliding blocks is further shortened, so that two sets of supporting plates expand outwards to fix a mounting roller, a first gear controls a rotating disc to rotate through operation of a second motor, and winding and unwinding of bubble bags are completed; according to the device, the winding drum can be conveniently and rapidly taken and placed, so that the winding drum is rapidly disassembled and assembled, the packaging efficiency is further improved, and time and labor are saved.
Owner:SUZHOU JINFEIXIN NEW MATERIAL TECH CO LTD

Recyclable paper-based laminate and a beverage carton made therefrom

The present invention concerns a paper-based barrier multilayer packaging material structure (1) being formed as a unitary sheet and comprising from its outer surface to its inner surface, the following layers: —a polymer dispersion coating (9) having a thickness of 1 to 10 μm, —a paperboard (8) having a grammage of between 120 g / m2 and 500 g / m2, —a water-based or solvent-less adhesive (7) having a thickness of 1 to 10 μm, —a barrier metallized paper layer (MBPL) having substance weight between 30-120 g / m2, preferably 45 to 90 g / m2 and a Water Vapour Transmission Rate (WVTR) of 10 to 0.1 g / m2 / d, preferably a WVTR of 1.0 to 0.1 g / m2 / d measured at 38° C. and 90% RH, and an Oxygen Transmission Rate (OTR) comprised between 100 and 0.1 cc / m2 / d, measured at 23° C. and 50% RH, preferably an OTR comprised between 1.0 and 0.1 cc / m2 / d. —at least one layer of a polymer dispersion coating (2) having a thickness of 1 to 25 μm, preferably of 5 to 15 μm.
Owner:SOCIETE DES PRODUITS NESTLE SA

Transfer device for solvent-free flat coating paint production

The invention belongs to the technical field of coating production, and particularly relates to a transfer device for solvent-free flat coating production, which comprises a rack, a conveying belt is arranged on the rack, and a coating barrel side-by-side conveying auxiliary assembly is further arranged on the rack; the side-by-side conveying auxiliary assembly comprises a limiting frame fixedly connected to one end of the upper side of the rack, a plurality of equidistant plates are arranged on the limiting frame at equal intervals, the equidistant plate at the rearmost end is fixedly connected with the limiting frame, and the other equidistant plates are slidably connected with the limiting frame. According to the auxiliary assembly for side-by-side conveying of the coating barrels, when the multiple coating barrels are placed on the conveying belt side by side to be conveyed, the conveying belt can be divided into the multiple conveying channels matched with the coating barrels in diameter through the multiple equidistant plates, and the situation that when the multiple coating barrels are conveyed side by side, the conveying channels are blocked is avoided; the situation that the adjacent coating barrels collide due to factors such as vibration of the conveying belt and external force, and then the coating barrels deviate or even topple over is avoided, and normal conveying of the coating barrels is guaranteed.
Owner:JIANGSU YABANG ENVIRONMENTAL PROTECTION TECHNOLOGY CO LTD