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4151 results about "Yield rate" patented technology

Method for synthesizing molecular sieve under solvent-free condition through grinding solid phase raw materials

The invention relates to a method for preparing a molecular sieve, aiming to provide a method for synthesizing a molecular sieve under a solvent-free condition through grinding solid phase raw materials. The method comprises the following steps of: grinding and mixing the pre-weighed solid raw materials which include silicon sources, metal atom sources, an organic template agent, and an alkalinity regulator, putting the grinded material into a reactor, and performing a crystallization reaction for 1-8 days at a temperature ranged from 80 DEG C to 180 DEG C; and drying for over 12 hours at a temperature of 80 DEG C after washing the reaction product thoroughly by using deionized water to obtain a final product. A ZSM-5 molecular sieve, a Beta molecular sieve, a ZSM-39 molecular sieve, and a SOD molecular sieve, which have a good crystallinity and a controllable silicon-aluminum ratio, can be prepared through the method provided by the invention. The synthetic route only involves a mixture of the raw materials without a use of any solvents, which simplifies the synthetic process compared to the traditional method, improves the yield rate and the single reactor utilization rate greatly, reduces the production cost greatly, saves energy and reduces emission, and has a wide industrial application prospect.
Owner:淮安六元环新材料有限公司

Method for preparing lithium carbonate by extracting lithium from lepidolite

The invention relates to a method for preparing lithium carbonate by extracting lithium from lepidolite. The method comprises the following steps of: a. calcination and defluorination at a high temperature; b. grinding; c. autoclaving; d. impurity removal; e. condensation; f. sodium separation by freezing; g. ithium precipitation by carbonization, wherein, in the step c, the grinded lepidolite, calcium oxide and sodium salt are thrown into a high-pressure kettle for autoclaving; the lepidolite is decomposed in the continuous stirring state; and alkali metal in the lepidolite is subject to ion exchange, turned into salt and dissolved out. In the step d, an autoclaving mother solution and autoclaving residues are obtained after separation and autoclaving; sodium hudroxide with slightly excess amount according to the Lithia content in the autoclaving mother solution is added and evenly stirred, then activated carbon is added for filtering and impurity removal. In the step g, CO2 is led to a sodium separation mother solution till the PH value of the solution is equal to between 9 and 10; the mother solution is heated, stirred, carbonized and subject to centrifugal water spinning and separation to obtain coarse lithium carbonate; backwashing and drying are carried out to the coarse lithium carbonate, thereby obtaining a product of lithium carbonate. The method has the advantages that: the method has high lithium yield rate; residues can be utilized; and sodium salt can be recycled, etc.
Owner:GANFENG LITHIUM CO LTD

Green biological active feed

The invention discloses a green biological active feed, which relates to the technical field of feeds. The green biological active feed is prepared from the following materials in part by weight: 40 to 80 parts of straw, 5 to 30 parts of corn four, 5 to 25 parts of cake dregs, 5 to 25 parts of wheat bran, 0.1 to 0.2 part of complex bacteria and 0.1 to 0.2 part of complex enzyme. During preparation, the straw is crushed and then is uniformly mixed with the corn flour, the cake dregs and the wheat bran; the complex bacteria and the complex enzyme are mixed into the mixture; water is added into the mixture to ensure that the water content reaches 45 to 50 percent, and the mixture is filled in a big tank, sealed and stored for later use; or the mixture is baked or dried by natural wind for storage and later use. The green biological active feed has the following advantages of: (1) improving the balance of intestinal flora, and improving the feed utilization rate; (2) promoting the growth of meat livestock and poultry, and shortening the breeding cycle; (3) strengthening the body conditions of laying hens, ducks and geese, and having a significant strengthening action on prolonging theegg-laying peak period; (4) strengthening the body condition of female domestic animals, and improving the yielding rate; (5) strengthening the body conditions of the livestock and poultry, enhancingthe disease prevention and disease resisting capacities, and reducing the sickness rate; and (6) purifying the culture environment, and improving the meat quality due to no public nuisances and no residues.
Owner:徐贵阁

Welding quality analysis device based on infrared vision and analysis method thereof

The invention discloses a welding quality analysis device based on infrared vision and an analysis method thereof. The analysis device comprises an infrared vision collecting system that is adjustably and fixedly connected to a welding facility, a vision processing system, in which welding defect intelligent recognition algorithm is embedded, and a feed control system, which can evaluate the welding quality, give an alarm, and adjust the parameters of the welding facility. The analysis method comprises the following steps: (1) collecting the infrared vision information of a molten pool or an area near a molten pool in real time through infrared sensing; (2) processing the infrared vision information by the welding defect intelligent recognition algorithm so as to obtain the weld seam positions and welding defect characteristics; (3) evaluating the welding quality in real time, and controlling the welding facility and giving an alarm aiming at different welding defects. According to the provided intelligent analysis device and intelligent analysis method, the welding process can be monitored in real time, the welding defects can be recognized, the welding seam position can be traced, the welding quality can be evaluated, the welding loss can be reduced, and the finished product yield rate can be increased.
Owner:HUAZHONG UNIV OF SCI & TECH

Method for comprehensive utilization of V-Ti-bearing iron ore concentrate by using tunnel kiln reduction-grinding - separation

The invention relates to an iron powder production method by using a tunnel kiln to reduce concentrate pellets containing carbon vanadium ferrotitanium with titanium slag and vanadium pentoxide as combined products. Concentrate pellets are made from vanadium-titanium iron concentrate through crashing and damp milling. The iron powder and tailings are obtained by putting the concentrate pellets into the tunnel kiln to be reduced, crashing, wet-grinding, magnetic separation and gravity separation. The tailings are soaked with titania waste acid to eliminate remnants magnesium and iron. Then the tailings are filtrated and dried to obtain a new material. And then the new material is added with sodium salt to do salt roast and then to be soaked by water, then titanium slag and sodium vanadate are obtained respectively after the water soaking. At last, the vanadium pentoxide is obtained by ammonium vanadate precipitating and calcination deaminase to the sodium vanadate liquid. The invention eliminates the disadvantage of high energy consumption by electric furnace smelting and bad separating effect of vanadium and titanium, difficult control of vanadium and titanium trend and low yield rate of extracting vanadium and titanium through converter blowing iron molten, etc. The invention has the advantages of high yield rate of vanadium, titanium and iron and high resources utilization rate and explores a novel practical way for comprehensive utilization of vanadium, titanium and iron concentrate ore.
Owner:攀枝花锐龙冶化材料开发有限公司

Method for extracting iron titanium vanadium from high-titanium iron concentrate

The invention discloses an iron-titanium-vanadium extracting method from high-titanium ferrovanadium concentrate ore. By adopting the method to make steel, fine TiCI4 and V2O5 have the advantages that: technological processes are simple and reasonable; energy consumption is low; yield rate of iron-titanium-vanadium is high and three wastes (waste gas, waste water and waste slag) are fewer. The method comprises the steps: iron smelting: a high furnace or an electric furnace is adopted to smelt iron to make melten iron containing vanadium and chromium and make titanium-enriched slag as byproduct and the rate of vanadium reduced and added into iron is 60-78 percent; single-slag steel-making: melten iron containing vanadium and chromium is put into a converter furnace directly to make steel by the function of oxygen blowing, and steel slag containing vanadium and chromium is obtained as byproduct; carbonized titanium-vanadium-chromium slag with 80-95 percent of carbonization rate is made by smelting reduction carbonization by the electric furnace smelting selection; TiCl4 containing vanadium is made by selective chlorination of carbonized titanium-vanadium-chromium slag in a fluidized bed at low temperature, and residual slag of chlorination containing CrCl3 is byproduct; vanadium titanium separation: VOCI3 is directly reduced by cycloolefine or naphthenic acid to make VOCl2 which can not dissolve in TiCI4, while the VOCI3 can be dissolved in TiCI4. Then the fine TiCI4 is made and the slurry TiCI4 containing rich vanadium is also made as byproduct; V2O5 is extracted from the rich vanadium containing slurry TiCI4.
Owner:张荣禄
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