The invention relates to a multistage
hydrogen dissolution liquid phase hydrogenation method. The method is as below: mixing a cycle liquid material with raw oil, and heating in a
heating furnace; introducing the
hydrogen divided into n paths into a
heating furnace for heating; mixing a first path of
hydrogen and
liquid phase material in a mixer to conduct a first stage of hydrogen
dissolution, sending the rest (n-1) paths of hydrogen through an inlet of a reactor
bed layer into a hydrogen oil
mixture component of the reactor, and mixing the (n-1) paths of hydrogen with a mixture from reaction of a previous
bed layer, so as to conduct a second stage of hydrogen
dissolution, conducting stripping to obtain reaction by-products
hydrogen sulfide and
ammonia, arranging a reaction
pressure control system on the top of the reactor, and arranging an exhaust
system in each stage of reactor; and sending the reaction products into a stripping
tower, arranging a hydrogen oil mixer in the stripping
tower, conducting stripping to obtain by-products
hydrogen sulfide and
ammonia to enhance hydrogen
solubility, sending part of the oil product from
tripping into a product tank, and a recycling the other part of the oil product. The method discharges
hydrogen sulfide and
ammonia from the
reactor system while conducting a
catalytic hydrogenation reaction, a
solid-phase catalyst contacts with a
liquid phase reactant to improve the efficiency of reaction.