The invention discloses a
triphenyl phosphate standard substance structure identification method, and relates to the technical field of
fluorine-containing gas emission reduction, and the method comprises the following steps: obtaining a standardized
analysis sample through
fluorine-containing matrix separation, target substance enrichment and
solvation treatment; a multi-dimensional chromatographic
system and a heart
cutting technology are adopted, and temperature
programming optimization is combined to realize separation and purification of a sample; carrying out multi-dimensional
structure analysis and confirmation by using
gas chromatography-
mass spectrometry,
infrared spectroscopy and
nuclear magnetic resonance technologies; a five-stage progressive identification
algorithm is constructed, and systematic identification is realized by combining a confidence
evaluation system and a
fluorine-containing interference correction technology; establishing a
structural integrity verification and purity quantitative evaluation standard, and outputting a standardized identification report; a method applicability
database is established through multi-type fluorine-containing environment
verification and process condition adaptability testing. The method effectively solves the problem of accurate identification of
triphenyl phosphate in a complex fluorine-containing matrix, and realizes effective removal of interference components such as light gas,
hydrofluorocarbon, perfluorinated compounds and the like.