305 results about "Dimethylacetamide" patented technology

The present invention relates to the field of the preparation of polyurethane elastic fibers, and relates to a preparation method for a bio-based polyurethane elastic fiber, comprising: preparing polyether polyol from sucrose, glycerol, dimethylamine and propylene oxide; adding a solvent, i.e., N,N-dimethylacetamide, and polyether polyol and polyisocyanate into a reaction tank, and adding p-Toluenesulfonyl semicarbazide and aluminum methylenebis(2,4-di-tert-butylphenoxy) phosphate to prepare a spinning solution; and subjecting the spinning solution to spinning and oil application by means of dry spinning technology to obtain the bio-based polyurethane elastic fiber. The present invention ensures that the properties of polyurethane elastic fibers do not deteriorate or are partially enhanced, while the cost and performance advantages are achieved.

The application discloses a preparation method of a hydrophilic oil-water separation anti-pollution membrane and the anti-pollution membrane and application thereof, and prepares MNRs material; the MNRs material is dispersed in dimethylacetamide, is uniformly stirred, polyvinylpyrrolidone is added, and stirring is continued, and a first mixture is obtained through ultrasonic treatment; the first mixture is mixed with polyvinylidene fluoride to obtain a second mixture, and the second mixture is stirred; the treated second mixture is dip-coated on a carrier, the dip-coated carrier is treated in deionized water to obtain an ultrafiltration membrane; the ultrafiltration membrane is soaked in a tea polyphenol solution with a Tris-HCl buffer solution, and is shaken to obtain the hydrophilic oil-water separation anti-pollution membrane. The hydrophilic oil-water separation anti-pollution membrane has excellent separation efficiency and flux recovery rate for four different oil-water mixtures of kerosene, gasoline, edible oil and n-hexane. The preparation process of the oil-water separation membrane is simple, the cost is low, and the reaction condition is mild; when the oil-water separation membrane is applied to organic wastewater separation, the oil-water separation membrane has the advantages of high efficiency, good removal performance and good recycling performance.

The application relates to a preparation method of a hollow fiber membrane composite thermal insulation material, which comprises the following steps: adding 18-22% of polyurethane, 4-8% of polyethylene glycol 2000 and 72-76% of N,N-dimethylacetamide into a spinning reaction kettle to mix, stir and defoam to prepare homogeneous casting solution; based on a non-solvent induced phase separation method, the homogeneous casting solution is coated on the surface of a polyester braided tube through a spinneret by adopting a concentric circle composite spinning technology, is gathered on a spinning wheel after a coagulation bath to form a reinforced polyurethane hollow fiber membrane assembly which is arranged in parallel and obliquely crosses and is mutually bonded, and the fiber membrane assembly is hot-pressed to prepare the hollow fiber membrane composite thermal insulation material under the conditions of a temperature of 60-150 DEG C and a pressure of 120-470 MPa. Since the coating layer and the braided tube are both through porous structures, the prepared composite material has good air permeability.

The invention discloses a preparation method of a polyimide-boron nitride nanosheet heat-conducting composite film. The preparation method comprises the following steps: firstly, dispersing boron nitride nanosheets into N, N-dimethylacetamide containing poly (diallyldimethylammonium chloride) to prepare slurry; meanwhile, 4, 4 '-diaminodiphenyl ether reacts with pyromellitic dianhydride to prepare a polyamide acid solution. And mixing the two materials, forming a layered structure through vertical and horizontal temperature gradients by adopting a bidirectional freezing casting technology, and freezing by liquid nitrogen to obtain the aerogel in oriented arrangement. And performing hot pressing and step-by-step thermal imidization treatment to obtain the heat-conducting composite film. According to the method, the highly-oriented arrangement of boron nitride nanosheets is constructed through bidirectional freezing casting, and the composite film has excellent heat-conducting property and keeps good mechanical strength and flexibility in combination with the surface modification effect. The process is simple and controllable, and is suitable for the fields of flexible electronics, 5G heat dissipation, battery thermal management and the like.

The present invention belongs to the technical field of fabric color fixing agents and provides a novel acidic color fixing agent free of bisphenol S and a preparation method thereof; the acidic color fixing agent is composed of the following components in parts by weight: 15-25 parts of water, 10-15 parts of phenol, 15-25 parts of dimethylacetamide, 2-5 parts of sodium sulfite, 10-15 parts of acetic acid, 5-7 parts of concentrated sulfuric acid, 15-20 parts of acrylic acid, 2-5 parts of ethylene glycol dimethyl ether, and 1-3 parts of sorbitol; the preparation method comprises the following steps: mixing a formula amount of phenol, dimethylacetamide, acrylic acid, acetic acid, and sodium sulfite, heating, adding concentrated sulfuric acid to react, cooling, adding a formula amount of water, and adding a formula amount of ethylene glycol dimethyl ether and sorbitol to obtain the product. Compared with the prior art, the present invention does not contain bisphenol S, has a good color fixing effect, can effectively improve various fastnesses such as water fastness, perspiration fastness, and seawater resistance, has little effect on the color change of the fabric after treatment, and has good tolerance to hardness ions.

The invention discloses a compound fluralana external preparation for dogs, a preparation method and application, belongs to the technical field of veterinary drugs, and solves the problems that an existing preparation is poor in skin surface permeability, a solvent is easy to volatilize, and use experience and drug effect exertion are influenced. The preparation is prepared from the following raw materials: fluralana, moxidectin, ethyl butylacetamidopropionate and N, N-dimethylformamide. The preparation method comprises the following steps: adding N, N-dimethylacetamide, acetone, an auxiliary adjuvant, a transdermal penetration enhancer, an antioxidant and a surface film-forming agent; according to the invention, the combination of the fluralab and the moxidectin can play a synergistic effect and expand an anti-parasitic spectrum so as to achieve an internal and external driving effect; both the fluralab and the moxidectin belong to high-fat-soluble substances, parasites can be quickly repelled and killed by adding novel adjuvant natural parasite expelling ingredients, and meanwhile, the skin permeability can be improved by adding the efficient transdermal penetration enhancer, and the risk that medicine residues are licked by pets is reduced.

The invention relates to a polyimide composite film for realizing high-dispersion carbon nanotubes through chemical anchoring and a preparation method of the polyimide composite film, which are used for solving the problems that carbon nanotubes in the existing carbon nanotube / polyimide composite material are easy to agglomerate, poor in interfacial compatibility and low in grafting efficiency. The preparation method comprises the following steps: S1, ultrasonically dispersing aminated carbon nanotubes in anhydrous dimethylacetamide to obtain a stable dispersion liquid; s2, slowly dropwise adding pyromellitic dianhydride into the stable dispersion liquid under an ice bath condition, and enabling the pyromellitic dianhydride to react with the aminated carbon nanotubes under the assistance of triethylamine to form anchor points; s3, adding a diamine monomer 4, 4 '-diaminodiphenyl ether, and gradually adding the residual pyromellitic dianhydride to carry out in-situ polymerization; and S4, preparing a wet film by adopting a curtain coating or spin coating method, and carrying out step-by-step thermal imidization at 80-300 DEG C to obtain the covalent composite film. Controllable covalent connection of the carbon nanotubes and pure polyimide chain segments can be achieved on the molecular level, and therefore the composite film with excellent heat conductivity, electromagnetic shielding performance and mechanical performance is obtained.

The application discloses a preparation method of superfine nanofiber antibacterial and mosquito-repellent high-efficiency low-resistance air filtration membrane, which comprises the following steps: dissolving cellulose acetate, cinnamyl aldehyde and polyhexamethylene biguanide hydrochloride in a solvent, fully stirring to form a spinning solution, wherein the solvent is a mixed solution of acetone, N, N-dimethylacetamide and water; and performing electrostatic spinning on the spinning solution to obtain the superfine nanofiber antibacterial and mosquito-repellent high-efficiency low-resistance air filtration membrane. The manufacturing steps of the application are simple and not complicated; cellulose acetate has excellent mechanical properties, hydrophobicity and thermal stability, and is an ideal material for air filtration membrane; the liquid property of cinnamyl aldehyde can effectively dilute cellulose acetate, so that the overall binding energy of the mixed solution system is reduced, the diameter of the prepared fiber is reduced, and meanwhile, the mild binding force of cinnamyl aldehyde minimally affects the interaction between cellulose acetate molecules.

The present application relates to photosensitive polyimide oligomer, preparation method and polyimide photosensitive resin composition prepared by the same, the present application provides the molecular formula of photosensitive polyimide oligomer, which is prepared from 1, 4, 5, 8-naphthalene tetracarboxylic anhydride, N, N-dimethylacetamide, triethylamine, tetramethyl benzene dimethyl diisocyanate, hydroquinone methyl ether, dibutyl tin dilaurate and hydroxyethyl acrylate according to the molar ratio of 2.5:10-15:1.2-1.6:3.0:0.0035-0.0045:0.007-0.01:2-2.5.The good solubility group is introduced into the molecular structure, so that it has good solubility in active diluent, and the polyimide oligomer can be photocured reaction;The device printed by the polyimide photosensitive resin composition prepared by the same has small shrinkage, high precision, and has the excellent performance of photosensitive polyimide oligomer, and has certain toughness and excellent weather resistance.

The present invention relates to a kind of water-resistant honeycomb activated carbon and preparation method thereof, belong to the technical field of activated carbon. A kind of preparation method of water-resistant honeycomb activated carbon comprises the following steps: 1) after heating and firing the coconut shell raw material after cleaning; 2) under nitrogen atmosphere, cyano-modified polyphenylene sulfide, polyetherimide, accelerator and activated carbon powder are mixed uniformly and then heated to react, cooled and washed, and dried; 3) N, N-dimethylacetamide is added to activated carbon intermediate and heated and extracted, solid is filtered and taken, put into anhydrous ethanol and soaked, solid is filtered and taken, after washing; 4) modified activated carbon is placed in anhydrous ethanol, tetrabutyl titanate is added and stirred and mixed, ferric nitrate solution is added by spraying under stirring, ultrasonic treatment is carried out after the addition of materials is completed, solid is filtered and taken, and microwave drying is carried out after centrifugation. The water-resistant honeycomb activated carbon prepared by the present invention has higher stability, water resistance and adsorption.

A process to produce cellulose ester fibers is provided, the process comprising: a. mixing cellulose ester and at least one solvent at a temperature ranging from about 60 ℃ to less than 90 ℃ to produce a cellulose ester dope; wherein the solvent comprises N, N-dimethylformamide, N, N-dimethylacetamide, or dimethyl sulfoxide, or mixtures thereof; and b. spinning the cellulose ester dope through at least one spinneret to produce the cellulose ester fibers; wherein the cellulose ester fibers have improved color over cellulose ester fibers produced from dope mixed outside about 60 ℃ to less than 90 ℃.

The invention discloses a catalyst for synthesizing 1, 3-dioxane-2-ketone as well as a preparation method and application of the catalyst. The catalyst is prepared from the following components in percentage by mass: 60wt%-90wt% of a component A, 5wt%-20wt% of a component B and 5wt%-30wt% of a component C, wherein the component A is one or more of N, N-dimethyl formamide, N, N-dimethylacetamide, N, N-diethyl formamide and urea, and the component B is one or more of N, N-dimethyl formamide, N, N-dimethylacetamide, N, N-diethyl formamide and urea; the component B is one or more of lithium carbonate, sodium carbonate, potassium carbonate, cesium carbonate, calcium carbonate and magnesium carbonate; and the component C is 1-butyl-3-methylimidazolium tetrafluoroborate and / or 1-butyl-3-methylimidazolium hexafluorophosphate, and the component C is 1-butyl-3-methylimidazolium hexafluorophosphate. According to the present invention, the components of the catalyst have the mutual synergistic promotion effect, the reaction substrate can be adsorbed and activated, the reaction condition is mild, the product yield is high, the catalyst can be recovered and regenerated, and the environmental pollution is low.

The invention relates to the technical field of production of flurala drops, in particular to a flurala drop preparation method based on online monitoring. The preparation method comprises the following preparation processes: sequentially adding weighed dimethylacetamide and acetone into a liquid preparation tank, adding fluralana and tetrahydrofuran polyglycol ether into the liquid preparation tank, stirring until the materials are uniformly mixed, monitoring raw material data, production data and product data by using a monitoring and collecting system in the preparation process, and recording and storing the raw material data, production data and product data through a monitoring and recording system. Data collected by the monitoring and collecting system is used as a reference, production is controlled and commanded through the monitoring and controlling system, and the monitoring and recording system records and stores the data and sends the data to the monitoring and analyzing system for statistical analysis and machine learning training. Key links such as raw material parameters, environmental process parameters and intermediate product and finished product quality data are monitored online in real time through the monitoring and collecting system, the production dynamic state is comprehensively mastered, and it is guaranteed that all procedures are strictly executed according to the process requirements.

The invention relates to the technical field of organic synthesis, in particular to a preparation method of crude poly (p-phenylene terephthamide). According to the method, phase-to-phase switching between non-aqueous suspension and ionic liquid homogeneous phase is adopted, and AB type end group balance, alternating end sealing and interface confinement branching are combined to realize end group accurate control and molecular weight distribution convergence. The method comprises the following steps: emulsifying an N-methyl pyrrolidone / calcium chloride solution in paraffin oil; carrying out polycondensation with p-phenylenediamine and paraphthaloyl chloride at a low temperature, and adding p-aminobenzoyl chloride to carry out dynamic balance on an end group; after layering, transferring into 1-butyl-3-methylimidazole chloride / N, N-dimethylacetamide for continuous polycondensation; cooling and re-emulsifying, and alternately adding benzoyl chloride and p-toluyl chloride for end sealing; trimesoyl chloride is added to a phase interface to realize limited branching; and carrying out ionic liquid homogenization, amine termination and alcohol / water sedimentation washing to obtain the product. The method effectively relieves end group drift, inhibits high molecular weight tailing and improves the filtering performance, and is suitable for preparation of high-reliability aramid fibers.

This invention employs a washing solution containing solvents and metal removal agents. The washing solution contains two or more solvents, the distance between the Hansen solubility parameter of the washing solution and the Hansen solubility parameter of dimethylacetamide (HSP distance) is less than 1.0, and the content of metal impurities is 0.1 × 10⁻¹¹ parts by mass relative to the total of 100 parts by mass of the aforementioned solvents and metal removal agents. ‑9 10 or more by weight 2 ×10 ‑6 The amount is less than a certain percentage by weight. The washing solution described herein can improve the removal of impurities and dirt.

This application discloses a crystal, a rare-earth-doped crystal, its preparation method, and its applications, belonging to the field of crystal materials. The chemical formula of the crystal is [Gd(L)]. 1.5 (DMA)] n Formula I; in Formula I, L is a ligand formed by deprotonated benzene polycarboxylic acid; benzene polycarboxylic acid is selected from any one of terephthalic acid, phthalic acid, and isophthalic acid; DMA is N , N -Dimethylacetamide; n ∞ represents continuous repetition and infinite extension. The crystal is rare-earth doped, and the chemical formula of the rare-earth doped crystal is [Gd]. 1‑x% (L) 1.5 (DMA)] n :x% Ln 3+ Equation II; in Equation II, x = 0.1~10; Ln 3+ Selected from Tb 3+ Or Eu 3+ Any one of the following. It has potential application value in fields such as fluorescent materials, multicolor display materials, long afterglow materials, X-ray detection and imaging materials, radiation detection dosimeters, and optical information encryption. The preparation method used in this application can be easily achieved through solution reaction under relatively mild conditions, with low cost and strong industrial feasibility.

The present application relates to a method for treating N,N-dimethylacetamide wastewater. Reagent A and reagent B are provided; wherein, the reagent A is activated carbon for solid-loaded iron ions; the reagent B is an aqueous solution of hydrogen peroxide; the reagent A and the reagent B are sequentially added to N,N-dimethylacetamide wastewater to react. The above-mentioned method for treating N,N-dimethylacetamide wastewater, the activated carbon for solid-loaded iron ions is coordinated with the aqueous solution of hydrogen peroxide, has an excellent decomposition effect on the N,N-dimethylacetamide in N,N-dimethylacetamide wastewater, and has a high decomposition efficiency. Meanwhile, the operation of wastewater treatment is simple, the operation safety is high, the energy consumption is low, and the material is green and environmentally friendly, and the cost is low.

The invention belongs to the field of novel functional polymer materials, and discloses a preparation method of a selenium-containing polymer material capable of fixing metal ions, and the preparation method comprises the following steps: S1, adding PTMEG into a round-bottom reaction flask filled with inert gas, and placing the round-bottom reaction flask in an oil bath pan for melting; s2, MDI, dimethylglyoxime, DSe and anhydrous N, N-dimethylacetamide are sequentially added and fully mixed; s3, stannous octoate and CuCl2 are added at the same time; s4, keeping the temperature of the oil bath pan and continuously reacting; s5, after the reaction is finished, a polymer is precipitated out, and secondary cleaning is conducted through methyl alcohol. The preparation method has the advantages that oximido is introduced into a polyurethane molecular structure to fix metal ions, meanwhile, selenium is introduced in a covalent fixation mode, and through double-site introduction of the metal ions and the selenium, the molecular structure of the polyurethane is greatly improved; the NO catalytic release rate of the material can be regulated and controlled, so that the biocompatibility and applicability of the polymer material in a blood environment are improved, and the application scene is further widened.

The application belongs to the field of detection reagents, and particularly relates to a single-component luminol chemiluminescence substrate liquid and a preparation method thereof. The single-component luminol chemiluminescence substrate liquid comprises the following components: sodium acetate, sodium perborate, N-N dimethylacetamide, beta-cyclodextrin, luminol, 4-morpholinopyridine, p-acetylaminophenol, 4-hydroxyphenylacetic acid, phenothiazine-10-yl-propyl sulfonic acid sodium salt and isothiazolinone. The purpose of the application is to solve the technical defects that the luminol chemiluminescence substrate liquid in the prior art must be packaged in two components due to the instability of the luminous agent and the oxidizing agent in the liquid phase, leading to inconvenient use and easy introduction of operation errors, so as to provide a single-component luminol chemiluminescence substrate liquid and a preparation method thereof, which have high storage stability, high luminous performance and convenient use.

Solvent-based compositions for post-etch residue removal and related methods are provided. The composition comprises a first amine halide component. The composition comprises a second amine halide component. The composition comprises a hydrogen halide component. The composition comprises an organic solvent. The organic solvent comprises a cyclic compound having at least one electron-withdrawing substituent. The organic solvent does not comprise at least one of N-methyl-2-pyrrolidone, dimethylacetamide, or any combination thereof. The first amine halide component, the second amine halide component, the hydrogen halide component, and the organic solvent are present in an amount sufficient for the composition to remove a substance at an etch rate of at least 50 Angstroms / min.

This invention discloses an anticoagulant microsphere, its preparation method, and its application, belonging to the field of biomedical materials technology. The preparation method includes: preparing a droplet solution using polyethersulfone, polyvinylpyrrolidone, and dimethylacetamide; preparing polyethersulfone framework microspheres; preparing a functional monomer solution using acrylic acid monomer, 2-acrylamide-2-methylpropanesulfonic acid monomer, initiator, crosslinking agent, and deionized water; immersing the polyethersulfone framework microspheres in the functional monomer solution; polymerization; and post-treatment. This invention utilizes oil-phase isolated in-situ polymerization, allowing the functional monomers to polymerize within the aqueous phase inside the porous framework microspheres and form a stable bond with the pore walls, preventing adhesion and extravasation. The resulting PES-gel interpenetrating network composite structure exhibits excellent anticoagulant properties. The preparation process is simple, easy to scale up for production, the oil phase and ethanol are recyclable, the steps are modular, and the production window is wide, making it suitable for large-scale and continuous production.

The invention relates to a preparation method of a Co-based MOF material constructed based on H3BTTC. The preparation method comprises the following steps: adding a ligand and a metal salt into N, N-dimethylacetamide through a conventional solvothermal synthesis method, adding a tetrafluoroboric acid aqueous solution to adjust the pH value and polarity of the solution, heating and crystallizing in a drying oven, washing a product with a solvent for multiple times, and carrying out vacuum drying to obtain a target material. The method can accurately regulate and control pore channels, conditions are mild and efficient, the performance of the material in the fields of gas adsorption and separation, catalysis, sensing and the like is effectively improved, and the remarkable advantages are enhanced.

The application provides a preparation method of an elastomer material, a leakage-proof artificial blood vessel and a preparation method thereof, and belongs to the field of biomedical materials. Polyethylene glycol, hexamethylene diisocyanate and dibutyl tin dilaurate are dissolved in a mixed solution of a first solvent and tetrahydrofuran, a precursor solution is obtained after oil bath reaction at 50-80 DEG C for 3-24 hours, then a chain extender chitooligosaccharide is added for continuous reaction, and a polyurethane elastomer solution is obtained. The first solvent is one of N'N-dimethylacetamide and DMF. The application selects polyethylene glycol with good biocompatibility and degradability as a soft segment raw material, and selects chitooligosaccharide with a molecular weight of 1000-2500 as a chain extender, so that the prepared elastomer material has good in-vivo and in-vitro biocompatibility and degradability. The prepared polyurethane elastomer solution is sprayed on an artificial blood vessel, and a leakage-proof artificial blood vessel can be prepared. The tensile strength of the prepared leakage-proof artificial blood vessel is greater than or equal to 19 MPa, and the tear resistance can reach 162 kJ m ‑2 .

The embodiment of the invention discloses a polymer electrolyte for a magnesium battery and the magnesium battery. The polymer electrolyte consists of a eutectic solvent, a cross-linking agent and a photoinitiator, the eutectic solvent is any one of a Mg (TFSI) 2 / N-methylformamide system or a MgCl2 / 2-chlorine-N, N-dimethylacetamide system, and N-methylformamide or 2-chlorine-N, N-dimethylacetamide is a hydrogen bond donor in the eutectic solvent; the crosslinking agent is polyethylene glycol diacrylate, and the photoinitiator is 2, 2-dimethoxy-2-phenyl acetophenone. According to the polymer electrolyte provided by the invention, high ionic conductivity, excellent electrochemical stability and good magnesium ion reversible deposition and dissolution performance are realized, the cycling stability is enhanced, the structural stability is also considered, and the polymer electrolyte has excellent reversibility and application potential in a magnesium battery; and the cycling stability and the energy efficiency of the magnesium battery can be obviously improved.

The invention discloses a polyimide and epoxy resin composite modified fluorocarbon resin coating and a preparation method thereof. The composition of the polyimide and epoxy resin composite modified fluorocarbon resin coating, measured by weight percentage, comprises: 0.4-0.8% of a diamine monomer, 0.4-0.8% of a dianhydride monomer, 60-70% of N,N-dimethylacetamide, 10-20% of an epoxy resin, 0.2-0.5% of an epoxy curing agent, 1-2% of a fluorocarbon resin curing agent, and 15-25% of a fluorocarbon resin. The preparation method comprises the following specific steps: reacting the diamine monomer and the dianhydride in N,N-dimethylacetamide, then compounding the composite modifier with the epoxy resin and the epoxy curing agent in sequence to obtain a composite modifier, and adding the composite modifier and the fluorocarbon resin curing agent together to a fluorocarbon resin solution to obtain the polyimide and epoxy resin composite modified fluorocarbon resin coating. The polyimide and epoxy resin composite modified fluorocarbon resin coating has greatly improved performance in mechanical properties, heat resistance, adhesion, and other aspects compared to existing fluorocarbon resin coatings.

The invention provides a method for catalytically degrading polyolefin plastic by using a eutectic solvent, which comprises the following steps: placing polyolefin plastic particles, C4-C6 alkane, an amide-AlCl3 eutectic solvent, an initiator and polychloromethane in a reactor, and carrying out catalytic degradation reaction in an anhydrous and closed environment to obtain a hydrocarbon product; wherein the C4-C6 alkane is added before the polyolefin plastic particles and the amide-AlCl3 eutectic solvent coexist in the reactor; the amide-AlCl3 deep eutectic solvent is prepared from an amide compound and AlCl3; the amide compound is selected from one or more of chloroacetamide, formamide, acetamide, N-methylformamide, N-methylacetamide, N, N-dimethylacetamide, N, N-diethyl acetamide and N, N-dimethylformamide, and the amide compound is selected from one or more of chloroacetamide, formamide, acetamide, N-methylformamide, N-methylacetamide, N, N-dimethylacetamide, N, N-diethyl acetamide and N, N-dimethylformamide; the eutectic solvent is applied to catalytic degradation of polyolefin plastic for the first time, and the problems that a traditional method is low in efficiency and high in cost at low temperature are solved.

The application provides a wear-resistant enameled copper wire and a preparation method thereof, and belongs to the technical field of enameled copper wires.The preparation method comprises the following steps: repeatedly coating wear-resistant paint on a copper wire and curing the wear-resistant paint into a paint film, and then cooling and winding the copper wire to obtain the wear-resistant enameled copper wire.The preparation method of the wear-resistant paint comprises the following steps: adding 4,4'-diamino-4"-hydroxytriphenylmethane and 2,2-bis-[4-(4-aminophenoxy)phenyl]propane into a polymerization bottle, adding N,N-dimethylacetamide, stirring and dissolving, adding 3,3',4,4'-benzophenonetetracarboxylic dianhydride, stirring and polymerizing, and obtaining a polyamic acid solution one; adding 4,4'-diamino diphenyl ether into the polymerization bottle, adding N,N-dimethylacetamide, stirring and dissolving, adding pyromellitic dianhydride, stirring and polymerizing, and obtaining a polyamic acid solution two; adding the polyamic acid solution one and the polyamic acid solution two into the polymerization bottle, adding a silane coupling agent, stirring, adding N,N-dimethylacetamide and a peroxide initiator, and stirring uniformly to obtain the wear-resistant paint; and the wear resistance of the wear-resistant enameled copper wire can be effectively improved.

The application discloses a drainage bag with an antibacterial functional layer and a preparation process thereof, and relates to the technical field of medical materials, and comprises the following steps: adding modified montmorillonite into N, N'-dimethylacetamide, uniformly mixing through ultrasonic, adding a polyurethane film, ultrasonic immersion for 60-120 min, drying, and obtaining a drainage bag substrate; adding polylactic acid into N, N-dimethylformamide, uniformly stirring and mixing, adding modified nano zinc oxide, uniformly mixing through ultrasonic, and then performing electrospinning to obtain an antibacterial coating fiber film; placing the antibacterial coating fiber film on the inner side surface of the drainage bag substrate, high-frequency heat sealing, assembling, and obtaining the drainage bag.

This invention relates to the field of fine chemical catalysis technology, specifically to an improved ion-gel confined palladium-on-carbon catalyst, its preparation method, and its applications. The catalyst uses N,N-dimethylacetamide (DMAc) as a solvent and potassium acetate as a base, with the addition of a catalytic amount of antioxidant 168 [(tris(2,4-di-tert-butylphenyl) phosphite)], and the reaction is carried out under milder CO pressure (1.0-1.6 MPa) and temperature (90-110 °C). This improved catalyst, in synergy with the optimized process, unexpectedly enables the high conversion and selectivity of 4-bromobenzyl sulfone derivatives to 4-methylsulfonylbenzoic acid derivatives, while maintaining the catalyst's excellent recyclability and stability. This invention provides a highly efficient, green, and easily industrialized synthetic route for the target product.

This invention discloses a PVDF-modified ultrafiltration membrane based on a tannic acid crosslinking network, its preparation method, and its applications. The membrane is prepared by a phase inversion membrane fabrication method using polyethyleneimine, tannic acid, polyvinylidene fluoride (PVDF), and N,N-dimethylacetamide (NDM). The pyrogallol structure abundant in the tannic acid molecule can coordinate with metal ions and also form a robust covalent crosslinking network with the amine-rich polyethyleneimine through Michael addition and Schiff base reactions. This network firmly anchors TA to the membrane surface and pores, solving the problem of TA loss in traditional modifications. The introduction of TA imparts lasting hydrophilicity to the membrane, significantly improving pure water flux and separation efficiency. Simultaneously, the hydrophilic and positively charged surface synergistically constructed by TA and PEI effectively inhibits the adsorption and deposition of pollutants, endowing the membrane with excellent antifouling performance and operational stability. This PVDF membrane, prepared through a green and simple co-crosslinking strategy, shows broad application prospects in complex water treatment and bioseparation.