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32 results about "Diisopropanolamine" patented technology

Diisopropanolamine is a chemical compound with the molecular formula used as an emulsifier, stabilizer, and chemical intermediate. Diisopropanolamine can be prepared by the reaction of isopropanolamine or ammonia with propylene oxide.

Material for concrete floor support plate

ActiveCN120271310AFiberSulfate
The invention belongs to the technical field of floor support plates, and particularly relates to a material for a concrete floor support plate, which is prepared from 150 to 170 parts of cement, 30 to 35 parts of mineral admixture, 200 to 250 parts of sand, 100 to 120 parts of gravel, 40 to 45 parts of fiber, 5 to 10 parts of early strength agent and 140 to 150 parts of water. The early strength agent comprises the following components in parts by weight: 20-30 parts of a polycarboxylate superplasticizer, 5-10 parts of modified nano zeolite powder, 5-9 parts of lithium acetate, 3-5 parts of a complexing agent, 5-10 parts of calcium sulfate and 1-4 parts of diisopropanolamine. The fibers, the mineral admixture and the early strength agent are added into the formula, early hydration of cement is promoted, dry shrinkage and cracking caused by too fast later hydration of cement are avoided, the compressive strength and breaking strength of the concrete floor support plate are effectively improved, the maintenance period of the concrete floor support plate is shortened, and the production cost is reduced.
Owner:SHAANXI TIANLI HENGTAI NEW BUILDING MATERIALS CO LTD

Continuous production method of high-stability N-methyldiisopropanolamine

The invention relates to the technical field of petrochemical engineering, in particular to a continuous production method of high-stability N-methyldiisopropanolamine. The method comprises the following steps: heating and reacting methylisopropanolamine and propylene oxide under the action of a specific catalyst to generate an N-methyldiisopropanolamine crude product; then adding the crude product into a rectifying tower, and extracting a high-purity N-methyldiisopropanolamine product from a side line at the middle upper part; the used catalyst is citric acid modified zeolite loaded copper-chromium bimetal. According to the production method disclosed by the invention, by optimizing an active site structure and a rectification separation path of the catalyst, efficient and stable operation of a reaction process is realized, and the thermal stability of a final product is remarkably improved.
Owner:MAOMING YUNLONG IND DEV +1

Production method for co-production of isopropanolamine and DL-2-aminopropanol

The invention belongs to the technical field of raw material preparation, and particularly relates to a production method for co-production of isopropanolamine and DL-2-aminopropanol. The production method for co-production of isopropanolamine and DL-2-aminopropanol comprises the following steps: adding ammonium carbonate, ammonium carbamate, epoxypropane and water into a high-pressure reaction kettle, uniformly stirring, heating to 88-90 DEG C, preserving heat for 30-35 minutes under 0.8 MPa, then heating to 100-103 DEG C, reacting for 40-45 minutes under 1.0 MPa, cooling to room temperature, filtering, washing, and drying to obtain the DL-2-aminopropanol. And after the reaction is finished, carrying out post-treatment to obtain a mixture of isopropanolamine and DL-2-aminopropanol. According to the production method for co-production of isopropanolamine and DL-2-aminopropanol, the process is simple, parameters are easy to control, reaction conditions are relatively mild, it is guaranteed that a large amount of monoisopropanolamine and DL-2-aminopropanol are generated, and meanwhile generation of by-products diisopropanolamine and triisopropanolamine is reduced.
Owner:SHANDONG DIAM CHEM CO LTD

A compound, a method of preparation and use in desulfurization and a desulfurizer composition

The application provides a compound, a preparation method, and application in desulfurization and a desulfurizer, a structural formula of the compound is as follows: the preparation method is as follows: diisopropanolamine, ethylene glycol diglycidyl ether, and a solvent are uniformly mixed and then are added into a high-temperature and high-pressure reaction kettle, reaction is carried out at 80-120 DEG C for 4-8 h, the solution is poured out after cooling, and the solution is distilled under reduced pressure to obtain a solid product steric amine; then the prepared steric amine and N-methyldiethanolamine are uniformly mixed at a mass ratio of 1-2:2-3, and are compounded into a 40-50 wt% aqueous solution, and the desulfurizer is preferably applied to natural gas desulfurization.
Owner:CHINA PETROLEUM & CHEMICAL CORP +1

Alkaline composition, its use and a process for cleaning substrates comprising cobalt and copper

The presently claimed invention relates to an alkaline composition for cleaning a substrate comprising i) copper or copper alloy and ii) cobalt or cobalt alloy, the composition comprising: a) at least one pH adjustor selected from diglycolamine, 4,4-diethoxy-N,N-dimethyl-1-butanamine, 3-dimethylaminopropan-1-ol, dimethylaminoethoxyethanol, N,N-dimethylisopropanolamine, ethylethanolamine, N-methyldiethanolamine, 2-(2-(methylamino)ethoxy)ethanol, 3-(methylamino)propane-1,2-diol, 2-[2-[2-(2-methoxy- ethoxy)ethoxy]ethoxy]ethylamine, 2-[2-(2-aminoethoxy)-ethoxy]-ethanol, N-butyldiethanolamine, diisopropanolamine, N-methyldiisopropanolamine, monoethanolamine, 3-dimethylamino-1,2-propandiol, 2- amino-1-butanol, 2-(2-(2-(2-aminoethoxy)ethoxy)ethoxy)ethanol, prolinol, 1-methyl-2-pyrrolidinemethanol, 1-methyl-2-pyrrolidinemethanol, 1-methyl-3-pyrrolidinol, 2-amino-2-methyl-1-propanol, N,N-dimethylethanolamine, butylethanolamine, diethylethanolamine, 3-methoxypropylamine, 4-(2-hydroxyethyl)morpholine, 4-(dimethylamino)cyclohexanol, 2-amino-2-methyl-1, 3-propanediol, or diisopropylamine; b) at least one complexing agent selected from C2 to C12 hydrocarbon having at least two sulfonic acid or carboxylic acid groups; c) at least one polymeric dispersing agent having a weight average molecular weight ≥ 1000 g / mol; and d) a solvent comprising water.
Owner:BASF SE

A method for preparing a composite tanning agent, a composite tanning agent and a tanning method thereof

This invention relates to a method for preparing a composite tanning agent, the composite tanning agent itself, and the tanning method thereof. The method involves preparing 5-50 parts by weight of glutaraldehyde, 5-20 parts by weight of diisopropanolamine, 5-50 parts by weight of zirconium sulfate, and 2-50 parts by weight of phosphate ester. A measured amount of water is added to a reaction vessel, and stirring is started. Diisopropanolamine is added and stirred until completely dissolved, with the temperature controlled at ≤40℃. Glutaraldehyde is slowly added, and after the addition is complete, the mixture is stirred for 30-60 minutes to obtain an aldehyde-amine modified intermediate. Zirconium sulfate is added to the intermediate, and the reaction is stirred for 40-60 minutes, controlling the pH of the entire system to 3.5-4.0. Phosphate ester is added, and the reaction is stirred for 20-30 minutes, adjusting the pH of the entire system to 3.8-4.2. The mixture is then filtered to obtain the composite tanning agent. The obtained composite tanning agent has the following advantages when tanning leather: low free aldehydes, high stability, high tanning efficiency, excellent leather-forming properties, and is environmentally friendly and chromium-free.
Owner:ANHUI ZEOLITE NEW MATERIAL TECH CO LTD

A low-carbon cement concrete steam-curing enhancer and its application

ActiveCN119898989BCeramic shaping apparatusActive agentMonoisopropanolamine
The invention discloses a kind of low carbon cement concrete steam curing strengthening agent and application thereof, the present invention screens and obtains a kind of strengthening agent for high iron phase cement clinker, and the strengthening agent can be adapted to steam curing process, and quickly improves the early strength and ultimate strength of concrete member.The strengthening agent includes 0.5-5 parts of nano-calcium carbonate, 0.02-0.2 parts of alcoholamine additives, 0-2 parts of inorganic salts, 0.01-0.2 parts of surfactants; Alcoholamine additives are selected from diethanol monoisopropanolamine, monoethanol diisopropanolamine, triethanolamine, triisopropanolamine, and inorganic salts are selected from aluminum sulfate, sodium metaaluminate, sodium chloride, sodium sulfate, calcium chloride, and the surfactant includes at least one of polydimethylsiloxane, fluorosilicone, and ethylene glycol siloxane.The present invention reverses the effect decline problem caused by the combination of alcoholamine strengthening agent and steam curing process by adjusting the temperature system and strengthening agent component before steam curing, so that strengthening agent and steam curing process produce synergistic effect.
Owner:ANHUI CONCH IND TECHNOLOGY RESEARCH INSTITUTE CO LTD

Method for preparing repair material for hydraulic concrete from solid waste material

PendingCN121850556AMarine site engineeringSpontaneous combustionSodium thiocyanate
The invention provides a method for preparing a repair material for hydraulic concrete by using a solid waste material. The preparation method comprises the following steps: mixing 55-65% of a material A (water-quenched slag and copper slag), 30-40% of a material B (citric acid gypsum, red mud and spontaneous combustion coal gangue) and 4-6% of a catalytic complexing activator (cane molasses, iron ion catalytic complexing agent sodium thiocyanate leftovers, polyether amine, calcium ion catalytic complexing agent diisopropanolamine borate and water), and carrying out ball milling to obtain the concrete; the repairing material and water are uniformly stirred according to the ratio and then are brushed or sprayed on the base surface of the defective concrete, so that the effects of resisting scouring, resisting erosion and freezing and thawing can be achieved, the effect of further cracking and falling off of the concrete is inhibited, and the durability of the hydraulic concrete is improved.
Owner:SHANDONG ZHONGSEN TECH

A compound, a method of preparing the same, and a composition containing the same

ActiveCN118439962BStrong absorption capacityExcellent selective absorption coefficientOrganic compound preparationGaseous fuelsDistillationStructural formula
The application provides a compound, a preparation method thereof and a composition containing the compound. A structural formula of the compound is shown as formula I. The preparation method of the compound is as follows: mixing diisopropanolamine and ethylene glycol diglycidyl ether, adding the mixture into a reaction kettle, adding a solvent, and reacting at 80-120 DEG C for 4-8 h, and then distilling at 50-80 DEG C under reduced pressure, collecting the distillation product, and obtaining the compound; mixing the compound and N-methyldiethanolamine in a mass ratio of (1-2):(2-3), and uniformly mixing to obtain a 20-60 wt% aqueous solution, and obtaining the composition.
Owner:CHINA PETROLEUM & CHEMICAL CORP +1

Water-resistant silicon-based antioxidant as well as preparation method and application thereof

The invention provides a water-resistant silicon-based antioxidant as well as a preparation method and application thereof, and belongs to the technical field of wood-plastic composite material preparation aids. The invention discloses a preparation method of 3-(3, 4-dichlorophenyl)- The preparation method comprises the following steps: carrying out aminolysis reaction on 2, 5-di-tert-butyl-4-hydroxyphenyl) methyl propionate and diisopropanolamine, and then carrying out grafting reaction on methyl phenyl dichlorosilane and hydroxyl of the aminolysis product to introduce an organic silicon chain segment; finally, the reaction intermediate of dichlorodiethylsilane and N-methyl-3-aminopropyltrimethoxysilane participates in chain segment polymerization, and a coupling agent chain segment is introduced. A chain segment of a final product contains amide, amino, trimethoxy and ethyoxyl groups, so that wood flour, inorganic filler and the like are favorably combined with plastic, and an organic silicon-based antioxidant product with antioxidant and coupling functions is obtained. The product is used in wood-plastic composite material processing, and has the effects of enhancing the water boiling resistance and water boiling loss resistance of the wood-plastic surface.
Owner:HUANGSHAN QIANGLI CHEM CO LTD

Process for gas-solid phase synthesis of isopropanolamine

The invention belongs to the technical field of preparation of isopropanolamine, and particularly relates to a process for gas-solid phase synthesis of isopropanolamine. The gas-solid phase isopropanolamine synthesis process comprises the following steps: (1) preparing a copper-doped silicoaluminophosphate carrier; (2) preparing a modified copper-doped silicoaluminophosphate catalyst; and (3) taking epoxypropane and ammonia gas as reaction gases, taking the modified copper-doped silicoaluminophosphate as a catalyst, and carrying out gas-solid phase reaction in the fixed bed reactor to prepare the isopropanolamine. According to the process for gas-solid phase synthesis of isopropanolamine, copper-doped silicoaluminophosphate is used as a catalyst carrier, cobaltosic oxide and ferric oxide are loaded as catalyst active components, and the process is applied to gas-solid phase reaction of epoxypropane and nitrogen to prepare isopropanolamine. Due to the addition of the catalyst, ring opening of epoxypropane is effectively activated while the activation energy of the nucleophilic reaction of ammonia gas is reduced, the content of monoisopropanolamine in a product is increased, and the content of diisopropanolamine and the content of triisopropanolamine are reduced.
Owner:SHANDONG DIAM CHEM CO LTD

Preparation method of phenyl diisopropanolamine

The invention discloses a preparation method of phenyl diisopropanolamine, and belongs to the technical field of organic chemical synthesis. The preparation method comprises the following steps: adding aniline and a Na2SiO3 / D301 catalyst into a reaction kettle, heating, adding epoxypropane, carrying out a ring-opening addition reaction, carrying out a constant-temperature reaction until the pressure is not reduced any more, cooling, and filtering and separating the Na2SiO3 / D301 catalyst to obtain phenyl diisopropanolamine. The Na2SiO3 / D301 catalyst is adopted to catalyze the ring-opening addition reaction of aniline and epoxypropane, compared with a traditional autocatalysis method, reactants are more quickly activated, the reaction efficiency is higher, the reaction is more complete, the prepared phenyl diisopropanolamine is high in yield and purity, aniline residues are few, purification treatment is not needed, and the method is suitable for industrial production. The separation of the catalyst can be realized only by simple filtration, and the method is green, environment-friendly, simple in process flow and suitable for industrialization.
Owner:ZHEJIANG LYUKEAN CHEM +1

Process for the preparation of a coarse-pored polyether for polyurethane rigid foam

The application belongs to the technical field of organic synthesis and relates to a preparation method of coarse-pore polyether for polyurethane rigid foam. First, phenolic substances, glucose and an acidic catalyst are subjected to an acetalization reaction to obtain a phenyl glycoside, then the phenyl glycoside, diisopropanolamine and triisopropanolamine are used as a composite initiator, potassium hydroxide is used as a catalyst, and an alkylene oxide is grafted to form a polymer with a molecular weight of 500-800, and after neutralization, adsorption, dehydration and filtration, an intermediate is obtained, then the intermediate is put into a polymerization kettle, a double-metal cyanide complex catalyst is used as a reaction catalyst, and quantitative propylene oxide is continuously grafted, and after removal of low-boiling impurities, the coarse-pore polyether is obtained. The polyurethane rigid foam prepared from the coarse-pore polyether has uniform and relatively coarse pores, and the foam compression strength is obviously improved while maintaining good heat preservation performance.
Owner:HUAIAN CHEN HUA NEW MATERIALS CO LTD

An N,N,N',N'-tetrakis(2-hydroxypropyl) adipamide curing agent, its preparation method and applications

The present invention provides an N,N,N',N'-tetrakis(2-hydroxypropyl) adipamide curing agent, a preparation method thereof and an application thereof, belonging to the technical field of powder coating curing agents. The curing agent is obtained by atomizing and feeding dimethyl adipate, diisopropanolamine, a catalyst and a solvent, and carrying out stepwise reaction under normal pressure and stepwise crystallization. There is no need to evacuate the vacuum throughout the process, the synthesis reaction effect is good, the product yield and purity are high, and the by-products are few. When used in high-temperature resistant powder coatings, the cured coating film has very excellent high-temperature yellowing resistance performance, and the surface fineness is good, and it can be used in fields with high requirements for high-temperature yellowing and appearance.
Owner:HUANGSHAN HUAHUI TECHNOLOGY CO LTD

Negative electrode binder, preparation method, lithium battery negative electrode and lithium battery

The invention discloses a negative electrode binder, a preparation method, a lithium battery negative electrode and a lithium battery. The negative electrode binder is obtained by polymerizing organic alcohol amine and acrylic acid, and at least comprises the following molecular formula: # imgabs0 #; wherein R1, R2 and R3 are respectively and independently selected from hydrogen or C1-C3 hydroxyl groups; the organic alcohol amine is one of ethanol amine, diethanol amine, isopropanolamine and diisopropanolamine. Amido in the organic alcohol amine reacts with carboxyl in the acrylic acid to generate amido bonds, so that the flexibility and toughness of the negative electrode binder are improved; meanwhile, hydroxyl in the organic alcohol amine and hydroxyl alcohol groups on the silicon surface have higher affinity. Therefore, the bonding degree of the adhesive to the silicon surface under the electrolyte infiltration condition is further improved. Therefore, the organic alcohol amine and the propylene compound cooperate with each other, so that the negative electrode binder has excellent flexibility, toughness, binding power and stability.
Owner:HANGZHOU TRANSFAR FINE CHEM CO LTD +2

An engineered decarboxylase polypeptide and methods of making isopropanolamine

The application discloses an engineered decarboxylase polypeptide and a method for preparing isopropanolamine, which can synthesize isopropanolamine from L-threonine or a fermentation broth containing L-threonine by using the engineered decarboxylase polypeptide. Compared with a naturally occurring wild-type decarboxylase, the engineered decarboxylase polypeptide has improved properties, such as increased enzyme activity, increased thermal stability, good substrate tolerance and the like. The reaction conditions tolerated by the engineered decarboxylase polypeptide are more relaxed, and the reaction is more conducive to scale-up. The method for preparing isopropanolamine provided by the application can avoid the process of flammable and explosive toxic epoxide compounds or ammonia under high temperature and high pressure, greatly saves energy and equipment investment, and does not contain the classic diisopropanolamine, triisopropanolamine and polyether impurities in chemical synthesis, and has important industrial application value.
Owner:ENZYMASTER NINGBO BIO ENG CO LTD

A highly selective amine absorbent and its preparation method

The present invention relates to a highly selective amine-based absorbent and its preparation method, belonging to the technical field of industrial desulfurization. The absorbent of the present invention comprises a primary absorbent, an organic sulfur removal accelerator, an auxiliary agent, and deionized water. The primary absorbent comprises an alcoholamine containing a tertiary amine structure and / or containing steric hindrance. The alcoholamine containing a tertiary amine structure and / or containing steric hindrance comprises one or more of methyldiethanolamine, diisopropanolamine, 2-(tert-butylamino)ethanol, tert-butylaminoethoxyethanol, and 2-amino-2-methyl-1-propanol. The present invention uses sterically hindered amines to inhibit CO2 absorption, reducing regeneration energy consumption by 40%, thereby addressing the technical problems of high CO2 co-absorption rates and high regeneration energy consumption in the prior art.
Owner:RUIRAN(SHANGHAI)ENVIRONMENTAL ENG TECH CO LTD

Aqueous epoxy resin and a method for producing the same, aqueous epoxy resin sizing agent and a method for producing and using the same

ActiveCN120988250BCarbon fibresEpoxyFiber
The application belongs to the technical field of carbon fiber preparation, and relates to a water-based epoxy resin and a preparation method thereof, a water-based epoxy resin sizing agent and a preparation method and application thereof. The water-based epoxy resin is obtained by reacting N,N-bis(2-hydroxypropyl)succinamic acid with a terminal carboxyl group and diisopropanolamine modified epoxy resin with a terminal hydroxyl group. The water-based epoxy resin sizing agent is obtained by mixing the water-based epoxy resin and water. The application is to apply the water-based epoxy resin sizing agent to the sizing treatment of carbon fibers. The application does not need additional catalysts, complex emulsification steps and additives, and the process is simple.
Owner:DONGHUA UNIV

A resin rust preventive, its preparation method and application

The application discloses a resin rust inhibitor and a preparation method and application thereof, and relates to the technical field of rust prevention. The resin rust inhibitor provided by the application comprises 0.5-2 parts of tetraglycidyl-4,4'-diamino diphenyl methane, 1-5 parts of diisopropanolamine, 0.02-0.15 parts of a silane coupling agent and 0.01-0.1 parts of nano-SiO2. The tetraglycidyl-4,4'-diamino diphenyl methane has high adhesion, and can improve the adhesion of the water-based rust inhibitor to metal. The introduction of the diisopropanolamine and the nano-SiO2 improves the high-temperature and low-temperature resistance of the resin, and makes the resin have better water solubility and be fully compatible with the water-based system. The water-based rust inhibitor obtained by taking the resin rust inhibitor as the main component has excellent adhesion and high-temperature and low-temperature resistance, and still has good adhesion at a low temperature of-20±2 DEG C, and does not excessively lose at a high temperature of 89±1 DEG C.
Owner:GUANGZHOU SINOMACH LUBRICATION TECH CO LTD +1

Composite cement grinding aid and preparation method thereof

ActiveCN118754498BPropanoic acidSulfite salt
The present invention discloses a composite cement grinding aid and a preparation method thereof, and belongs to the technical field of cement admixtures. It is made of the following raw materials in parts by weight: 30-40 parts of alcoholamine compounds, 10-15 parts of sodium sulfite, 20-30 parts of red mud modified biochar, 5-10 parts of dilauryl thiodipropionate, 5-10 parts of sodium humate, 5-10 parts of molasses, and 30-40 parts of water. The alcoholamine compound is composed of monoethanol diisopropanolamine and diisopropyl monoethanolamine in a mass ratio of 2: 1. The grinding aid of the present invention utilizes solid waste red mud and plant straw to comprehensively modify biochar materials, which on the one hand improves the utilization rate of solid waste red mud and plant straw and reduces production costs; on the other hand, the biochar after red mud modification and the alcoholamine compound act synergistically according to a specific ratio to improve the grindability of the material and increase the hourly output of cement. At the same time, it can also improve the distribution of cement particles and stimulate hydration power, thereby improving the early strength and late strength of cement.
Owner:SHANDONG HONGYI TECH +1

Carbon dioxide adsorbent with low energy consumption and long service life and preparation method thereof

The invention discloses a carbon dioxide adsorbent with low energy consumption and long service life and a preparation method thereof, and the carbon dioxide adsorbent comprises the following components: 8-12% of ethanolamine, 5-7% of N-methyldiethanolamine, 18% of N-methylmonoethanolamine, 51-55% of hydroxyethyl ethylenediamine and 12-14% of diisopropanolamine. The preparation method comprises the following steps: firstly, conveying ethanolamine, N-methyldiethanolamine, N-methylmonoethanolamine, hydroxyethyl ethylenediamine and diisopropanolamine into a reaction kettle through a feeding pump and a feeding pipe according to a proportion, heating materials in the reaction kettle to carry out chemical reaction, and continuously stirring by adopting a variable-frequency speed-regulating stirrer, so that the materials in the reaction kettle are fully mixed; and after the mixing is finished, the carbon dioxide adsorbent with low energy consumption and long service life in the reaction kettle is output through a discharge pipe under the action of a discharge pump. The prepared carbon dioxide adsorbent has the advantages of high absorption efficiency, long service life, low energy consumption, low loss and the like.
Owner:FOSHAN JIALIDA ENVIRONMENTAL PROTECTION TECH

Compositions comprising a specific hyperbranched copolymer and 1,3-propanediol and / or N-hydroxyoctanamide

The present invention relates to a composition comprising a specific hyperbranched copolymer (HBC) of monomeric dodecenyl succinic anhydride, diisopropanolamine and bis(dimethylaminopropyl)amine, and comprising the compounds 1,3-propanediol and / or N-hydroxyoctanamide. It has been found that the hyperbranched copolymer synergistically enhances the antimicrobial action of 1,3-propanediol and / or N-hydroxyoctanamide.
Owner:DSM IP ASSETS BV

A material for concrete floor deck

ActiveCN120271310BFiberCrushed stone
The present invention belongs to the technical field of floor decking, and in particular to a material for concrete floor decking, wherein the material comprises 150-170 parts of cement, 30-35 parts of mineral admixture, 200-250 parts of sand, 100-120 parts of crushed stone, 40-45 parts of fiber, 5-10 parts of early strength agent, and 140-150 parts of water; the early strength agent comprises the following components in parts by weight: 20-30 parts of polycarboxylate water reducer, 5-10 parts of modified nano zeolite powder, 5-9 parts of lithium acetate, 3-5 parts of complexing agent, 5-10 parts of calcium sulfate, and 1-4 parts of diisopropanolamine. The present invention adds fiber, mineral admixture, and early strength agent to the formula, promotes early hydration of cement, avoids excessively fast hydration of cement in the later stage, causes shrinkage and cracking, effectively improves the compressive strength and flexural strength of the concrete floor deck, shortens the curing period of the concrete floor deck, and reduces production costs.
Owner:SHAANXI TIANLI HENGTAI NEW BUILDING MATERIALS CO LTD

Light-aging-resistant polyurethane composition, polyurethane composite material and application of light-aging-resistant polyurethane composition and polyurethane composite material

PendingCN121591988APolymer sciencePtru catalyst
The invention belongs to the field of polyurethane materials, and particularly relates to a light-aging-resistant polyurethane composition, a polyurethane composite material and application of the light-aging-resistant polyurethane composition and the polyurethane composite material. The polyurethane composition comprises aliphatic isocyanate, an isocyanate reactant, a catalyst and an optional auxiliary agent, wherein the isocyanate reactant comprises micromolecular polyol, polycaprolactone polyol and alcohol amine; the alcohol amine is selected from at least one of diethanol amine, 3-hydroxymethyl piperidine, 2-butylaminoethanol, diisopropanolamine and 1-(cyclohexyl amino) propane-2-alcohol. According to the invention, the mechanical property, the glass transition temperature and the light aging resistance of the aliphatic polyurethane composite material can be effectively improved.
Owner:WANHUA CHEM BEIJING

Process for the gas-solid phase synthesis of isopropanolamine

The application belongs to the technical field of isopropanolamine preparation, and particularly relates to a gas-solid phase synthesis process of isopropanolamine. The gas-solid phase synthesis process of isopropanolamine comprises the following steps: (1) preparing a copper-doped phosphosilicic aluminum carrier; (2) preparing a modified copper-doped phosphosilicic aluminum catalyst; and (3) taking propylene oxide and ammonia gas as reaction gas, taking the modified copper-doped phosphosilicic aluminum as a catalyst, and performing a gas-solid phase reaction in a fixed bed reactor to prepare isopropanolamine. The gas-solid phase synthesis process of isopropanolamine takes the copper-doped phosphosilicic aluminum as a catalyst carrier, loads three cobalt tetroxides and two iron trioxides as catalyst active components, is applied to the gas-solid phase reaction of propylene oxide and nitrogen gas to prepare isopropanolamine, the addition of the catalyst reduces the activation energy of the nucleophilic reaction of ammonia gas and effectively activates the ring opening of propylene oxide, the content of mono-isopropanolamine in the product is increased, and the contents of di-isopropanolamine and tri-isopropanolamine are reduced.
Owner:SHANDONG DIAM CHEM CO LTD

Additive composition for strength enhancement of cementitious compositions

PendingCN121175282ASucrosePropanolamine
There is provided a composition for use as an additive to enhance the strength of a cementitious composition, the composition comprising: an alkanolamine comprising ethanol diisopropanolamine (EDIPA) and optionally at least one selected from the group consisting of triisopropanolamine (TIPA), diethanol isopropanolamine (DEIPA), triethanolamine (TEA), and tetra-(2-hydroxyethyl) ethylenediamine (THEED); at least one retarder selected from the group consisting of gluconate, sucrose, corn syrup and molasses; and at least one accelerator selected from the group consisting of thiocyanate, sodium chloride and calcium chloride wherein the alkanolamine and the accelerator are present in a mass ratio of 0.2 to 4.0 and the accelerator and the retarder are present in a mass ratio of 1 to 10. When hydrated, the additive enhances the short-term and long-term strength of the cement.
Owner:GCP APPLIED TECHNOLOGIES INC

Water-borne epoxy resin and preparation method thereof, water-borne epoxy resin sizing agent and preparation method and application thereof

ActiveCN120988250ACarbon fibresEpoxyFiber
The invention belongs to the technical field of carbon fiber preparation, and relates to waterborne epoxy resin and a preparation method thereof, and a waterborne epoxy resin sizing agent and a preparation method and application thereof. The water-borne epoxy resin is obtained by reacting N, N-bis (2-hydroxypropyl) succinamic acid of which the end group contains carboxyl with diisopropanolamine modified epoxy resin of which the end group is hydroxyl. The water-borne epoxy resin sizing agent is obtained by mixing the water-borne epoxy resin and water. According to the application, the water-borne epoxy resin sizing agent is used for sizing treatment of carbon fibers. The water-borne epoxy resin sizing agent prepared by the method does not need additional catalysts, does not need complex emulsification steps and additives, and is simple and convenient in process.
Owner:DONGHUA UNIV

Process for the production of dl-2-amino propanol with isopropanolamine

The application belongs to the technical field of raw material preparation, and particularly relates to a production method of co-producing isopropanolamine and DL-2-aminopropanol. The production method of co-producing isopropanolamine and DL-2-aminopropanol comprises the following steps: adding ammonium carbonate, ammonium carbamate, propylene oxide and water into a high-pressure reaction kettle, stirring until uniform, heating to 88-90 DEG C, keeping at 0.8 MPa for 30-35 min, then heating to 100-103 DEG C, reacting at 1.0 MPa for 40-45 min, and after the reaction is completed, post-treatment is performed to obtain a mixture of isopropanolamine and DL-2-aminopropanol. The production method of co-producing isopropanolamine and DL-2-aminopropanol is simple in process, easy to control in parameters, and relatively mild in reaction conditions, so that a large amount of isopropanolamine and DL-2-aminopropanol is generated while the generation of by-products diisopropanolamine and triisopropanolamine is reduced.
Owner:SHANDONG DIAM CHEM CO LTD