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1595 results about "Carbon disulfide" patented technology
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Carbon disulfide is a colorless volatile liquid with the formula CS₂. The compound is used frequently as a building block in organic chemistry as well as an industrial and chemical non-polar solvent. It has an "ether-like" odor, but commercial samples are typically contaminated with foul-smelling impurities.
Absorbent composition containing molecules with a hindered amine and a metal sulfonate, phosphonate or carboxylate structure for acid gas scrubbing process
An acid gas absorbent comprising a metal sulfonate, phosphonate or carboxylate of a hindered amine and a process for the selective removal Of H2S as well as other acidic components such as carbon disulfide, carbonyl sulfide and oxygen and sulfur derivatives of C1 to C4 hydrocarbons from mixtures containing such acidic components and CO2 using said absorbent.
Owner:EXXON RES & ENG CO
Systems and methods for producing oil and/or gas
Owner:SHELL OIL CO
Process for the manufacture of carbon disulphide and use of a liquid stream comprising carbon disulphide for enhanced oil recovery
InactiveUS8097230B2Less carbon dioxideReduce rateCarbon disulfidePhysical/chemical process catalystsSulfurCarbon disulfide
The invention provides a process for the manufacture of carbon disulphide by reacting carbon monoxide with elemental sulphur to form carbonyl sulphide and disproportionating the carbonyl sulphide formed into carbon disulphide and carbon dioxide, the process comprising contacting a gaseous stream comprising carbon monoxide with a liquid elemental sulphur phase containing a solid catalyst at a temperature in the range of from 250 to 700° C. to obtain a gaseous phase comprising carbonyl sulphide, carbon disulphide and carbon dioxide. The invention further provides the use of a liquid stream comprising carbon disulphide, carbonyl sulphide and carbon dioxide obtainable by such process for enhanced oil recovery.
Owner:SHELL OIL CO
Cyanuric acid-based heavy metal chelating flocculant and preparation method thereof
InactiveCN101863544AOvercome the defect that the ion concentration is difficult to reach the standardIncrease steric hindranceWater/sewage treatment by flocculation/precipitationEpoxyHeavy metal chelation
The invention belongs to the technical field of heavy metal wastewater treatment, and in particular relates to cyanuric acid-based heavy metal chelating flocculant and a preparation method thereof. In the method, cyanuric acid is adopted as a basic framework; and polyamine is connected to a molecule through epoxy chloropropane, and reacts with carbon disulfide in an alkaline condition to prepare the heavy metal chelating flocculant of which the molecule contains a plurality of branches and a plurality of dithio formate functional groups. The method overcomes the defects that the conventional monofunctional flocculant has small flocculating body, and poor precipitation performance, and when polymeric chelant chelates heavy metals, steric clash is great, and the residual heavy metal ion concentration is difficult to meet the standard and the like. The flocculant has the advantages of simple preparation process, mild condition, easy operation and control, high yield, high raw material utilization, less three waste discharge and environmental protection of technical process, convenient popularization and industrialization realization and suitability for treatment of various types of heavy metal wastewater, such as smelting wastewater, electroplating wastewater, nonferrous metals processing wastewater, mining and beneficiating wastewater, printed circuit board wastewater, battery plants and the like.
Owner:HUNAN UNIV OF SCI & TECH
Process for the manufacture of carbon disulphide
InactiveUS7763227B2Significant costSignificant designCarbon disulfideHydrocarbon from carbon oxidesHydrogenCarbonyl sulfide
A process for the manufacture of carbon disulfide comprising the following steps: (a) reacting carbon monoxide with hydrogen sulfide to form carbonyl sulfide and hydrogen; (b) contacting the carbonyl sulfide formed in step (a) with a catalyst effective for disproportionating carbonyl sulfide into carbon disulfide and carbon dioxide.
Owner:SHELL OIL CO
Prepn of antioxidant for lubricant oil
InactiveCN1191340CEffective protectionImprove solubilityAdditivesAntioxidantInternal combustion engine
The preparation of antioxidant for lubricant oil includes the condensation reaction between the mixture liquid containing shielding phenol, aldehyde and CS2 and added dialkyl amine at 40-120 deg.c and product separation and collection. The prepared antioxidant has the integrated structure of both free radical terminator and peroxide decomposing agent and has the capacity of trapping free radical and decomposing hydrogen peroxide to protect the oxidation safety of oil product. Containing S element in its structure makes it possess certain antiwear effect. The product of the present invention is liquid, easy to dissolve and compatible with other functional additives, and may be used in industrial lubricant oil and internal combustion engine oil.
Owner:CHINA PETROLEUM & CHEM CORP +1
Reactive formulations for a neutralization of toxic industrial chemicals
InactiveUS7125497B1Efficiently neutralizedHydrogen peroxideLiquid degasificationBoron trichlorideMalathion
Decontamination formulations for neutralization of toxic industrial chemicals, and methods of making and using same. The formulations are effective for neutralizing malathion, hydrogen cyanide, sodium cyanide, butyl isocyanate, carbon disulfide, phosgene gas, capsaicin in commercial pepper spray, chlorine gas, anhydrous ammonia gas; and may be effective at neutralizing hydrogen sulfide, sulfur dioxide, formaldehyde, ethylene oxide, methyl bromide, boron trichloride, fluorine, tetraethyl pyrophosphate, phosphorous trichloride, arsine, and tungsten hexafluoride.
Owner:NAT TECH & ENG SOLUTIONS OF SANDIA LLC
Carbon disulfide process
The specification discloses a process for the manufacture of carbon disulfide from sulfur dioxide and carbon monoxide comprising two catalytic reactions. In the first reaction, sulfur dioxide and carbon monoxide are converted to carbonyl sulfide and carbon dioxide. In the second reaction, carbonyl sulfide is disproportionated to carbon disulfide and carbon dioxide. The second reaction is conducted in the presence of a solvent, which continuously removes the carbon disulfide product so as to drive the reaction to completion.
Owner:JES TECH LLC
Lignin-based dithiocarbamate heavy metal ion capture agent and preparation method
InactiveCN102784622AReduce manufacturing costThe synthesis method is simpleOther chemical processesWater/sewage treatment by sorptionAminationDithiocarbamate
The invention discloses a preparation method of a lignin-based dithiocarbamate heavy metal ion capture agent. The method comprises the steps of: (1) adding water into lignin and stirring them, adding an alkaline conditioning agent to adjust the pH to 9-11, then adding an oxidizing agent, conducting heating to raise the temperature to 80-90DEG C for reacting for 1-2 hours; (2) adding an amination reagent, maintaining the reaction temperature at 80-90DEG C, then adding formaldehyde to react for 5-6 hours; (3) cooling the solution to room temperature, adjusting the pH value to 10-11, then adding carbon disulfide to perform an esterification reaction for 4-5 hours at 40-45DEG C; and (4) adding a modifier for reacting for 1-2 hours, then carrying out pumping filtration, and then conducting washing 2-3 times with water and absolute ethyl alcohol, thus obtaining a solid product, i.e. the lignin-based dithiocarbamate. The lignin-based dithiocarbamate heavy metal ion capture agent provided in the invention has the advantages of simple preparation process, low production cost, excellent performance, adaptability to treatment of various heavy metal ion polluted wastewater, good stability, and wide applicable range.
Owner:GUANGXI UNIV
Absorbent composition containing molecules with a hindered amine and a metal sulfonate, phosphonate or carboxylate structure for acid gas scrubbing process
Owner:EXXON RES & ENG CO
Antibacterial and environment-friendly deodorant of microorganism strains
The invention relates to an antibacterial and environment-friendly deodorant of microorganism strains and a preparation method thereof. The traditional method for removing odor generally uses essence to cover up the odor or pumping odor physically or uses ozone to oxidize and degrade the odor or uses a chemical method. The methods also can alleviate the odor to a certain extent, but finally the problem can not be solved really and fundamentally and the essence and chemical deodorization also have secondary pollution. The microbial deodorization technology utilizes the effects of high-efficient absorption, absorption and metabolism of particular microorganism strains which can convert or degrade odorant, to purify the odorous gases of amyl mercaptan, benzene methanethiol, methyl sulfide, ethanethiol, hydrogen sulfide, sulfur dioxide, p-benzyl mercaptan, ammonia, dimethylamine, trimethylamine and carbon disulfide and the like which are emitted from human life areas, domestic sewage and domestic garbage and the like and to convert the odorous components of amyl mercaptan, benzene methanethiol, methyl sulfide, ethanethiol, hydrogen sulfide, sulfur dioxide, p-benzyl mercaptan, ammonia, dimethylamine, trimethylamine and carbon disulfide and the like into matters without harm and odor, thus achieving the purpose of thoroughly improving air quality and protecting health of people. The preparation method utilizes a fermentation method of microorganism strains to prepare deodorant products.
Owner:王峰
Amphiprotic high-molecule chelated flocculating agent and preparation method thereof
InactiveCN101585572AReduce flocculation and settling performanceLow costWater/sewage treatment by flocculation/precipitationIndustrial waste waterPolyamine
The invention relates to amphiprotic high-molecule chelated flocculating agent for various heavy metal waste water treatments and preparation method thereof. The amphiprotic high-molecule chelated flocculating agent of the invention is formed by following steps: configuring a basic skeleton by cationic dimethyl diallyl ammonium chloride and acrylamide copolymer; reacting with aldehydes and polyamine through Mannich to connect the polyamine to the high-molecule chain; then reacting with carbon bisulfide in alkaline condition. The invention mainly overcomes the disadvantages that the existing high-molecule chelating agent has excessive flocs negative charge caused by the suspension of part chelating radical because the space steric resistance of high-molecule chain and chelated radical are not matched so as to reduce the flocculating settling performance and the traditional heavy metal waste water processing method has complicated technique, high cost, low efficiency and cannot be suitable for large-scaled heavy metal waste water treatment. The invention is widely applied to the heavy metal waste water treatment of various types, in particular suitable for removing the heavy metal ions in industrial waste water and domestic sewage.
Owner:HUNAN UNIV OF SCI & TECH
Preparation method of positive material for lithium-sulfur battery
ActiveCN102832379AGood dispersionUniform particle sizeCell electrodesCarbon compositesCarbon nanotube
Owner:SHANGHAI INST OF SPACE POWER SOURCES
Chelating agent capable of simultaneously processing multiple heavy metallic ions
InactiveCN101081827AMeet the use requirementsReduce contentOrganic chemistryWater/sewage treatmentPrinted circuit boardPolyamine
The present invention discloses one kind of chelating agent capable of treating several kinds of metal ion simultaneously. The chelating agent is synthesized with polyamine or polyethylene imine as basic skeleton and carbon disulfide in alkaline condition, where, polyamine or polyethylene imine and carbon disulfide have weight ratio of 1 to 0.6-2.0. The chelating agent of the present invention can form chelate precipitate simultaneously with several kinds of metal ion, and is especially suitable for use in purifying waste water, chemical intermediate and chemicals for printed circuit board containing metal ions.
Owner:TIANJIN RUIJI CHEM
Systems and methods for producing oil and/or gas
InactiveUS20070251686A1Enhanced overall recoveryCut fingerFluid removalVibration devicesCarbon disulfideChemistry
A system comprising a carbon disulfide formulation storage; a mechanism for releasing at least a portion of the carbon disulfide formulation into a formation; and a mechanism for creating a pulse in the carbon disulfide formulation in the formation.
Owner:SHELL OIL CO
Method for oil shale pollutant sorption/NOx reburning multi-pollutant control
A method of decreasing pollutants produced in a combustion process. The method comprises combusting coal in a combustion chamber to produce at least one pollutant selected from the group consisting of a nitrogen-containing pollutant, sulfuric acid, sulfur trioxide, carbonyl sulfide, carbon disulfide, chlorine, hydroiodic acid, iodine, hydrofluoric acid, fluorine, hydrobromic acid, bromine, phosphoric acid, phosphorous pentaoxide, elemental mercury, and mercuric chloride. Oil shale particles are introduced into the combustion chamber and are combusted to produce sorbent particulates and a reductant. The at least one pollutant is contacted with at least one of the sorbent particulates and the reductant to decrease an amount of the at least one pollutant in the combustion chamber. The reductant may chemically reduce the at least one pollutant to a benign species. The sorbent particulates may adsorb or absorb the at least one pollutant. A combustion chamber that produces decreased pollutants in a combustion process is also disclosed.
Owner:BATTELLE ENERGY ALLIANCE LLC
Oil-soluble self-vulcanizing molybdenum catalyst, and preparation method, use method and application of oil-soluble self-vulcanizing molybdenum catalyst
InactiveCN103349999AImprove catalytic performanceReduce yieldOrganic-compounds/hydrides/coordination-complexes catalystsHydrocarbon oil crackingSlurry reactorFiltration
The invention provides an oil-soluble self-vulcanizing molybdenum catalyst, and a preparation method, a use method and an application of the oil-soluble self-vulcanizing molybdenum catalyst. The preparation method comprises the following steps of (1) sequentially putting a molybdenum source, water, sodium sulfide, a solvent and inorganic acid in a container under the protection of nitrogen, uniformly mixing and stirring, cooling to 5-50 DEG C for reaction for 10-150min, (2) adding alkylamine and carbon disulfide, uniformly stirring, heating to 60-200 DEG C for reaction for 3-10h, and (3) after reaction, sufficiently cooling a product, performing suction filtration, sufficiently washing with methanol, and drying to obtain the oil-soluble self-vulcanizing molybdenum catalyst. The oil-soluble self-vulcanizing molybdenum catalyst can be vulcanized and decomposed to form a molybdenum disulfide active component in situ, is used for a slurry reactor hydrocracking technology for poor heavy oil with a high metal content, a high carbon residue content and a high sulfur content, can reduce the coke yield, and keeps long-period operation of a device.
Owner:CHINA UNIV OF PETROLEUM (EAST CHINA)
Gas pipeline drag reduction agent and preparing method thereof
The invention relates to a gas line drag reduction agent and a preparation method thereof, relating to the technical field of the composite of high-molecular compound and piping systems. The drag reduction agent consists of carbon bisulfide, hydrazine hydrate and long chain acid, the mol ratio of which is 1.8:1:1 to 2.2:1:1. The preparation method comprises the following steps: step one, CS2 is taken according to proportional quantity, dripped into the mixed liquor of the hydrazine hydrate and water with proportional quantity under agitation, reflowed for certain time in the temperature range of 90 to 95 DEG C, then cooled for 30 to 60 minutes in ice water bath and pumped and filtered, the mother liquor continues to react for two times, products of the third time are merged, washed by using ethanol and ether sequentially, and recrystallized by using boiling water so as to obtain symmetrical diaminothiourea clear crystal; and step two, symmetrical diaminothiourea with proportional quantity and the long chain acid with proportional quantity are dissolved in a pyridine solvent with nitrogen protection, reflowed at the temperature of 140 to 220 DEG C by adopting a temperature programming method, and react for 3 to 4 hours, then the mixture is cooled to the room temperature and recrystallizated by using the ethanol of 95 percent to obtain the brown product.
Owner:PIPECHINA SOUTH CHINA CO
Ethylenediamine-based heavy metal chelating agent and preparation method thereof
InactiveCN101857296AOvercoming the defect of spatial mismatchOvercome the defects of large steric hindrance and difficulty in reaching the standard concentration of residual heavy metal ionsWater/sewage treatmentEthylenediamineHeavy metal chelation
The invention belongs to the technical field of removal, purification and entrapment of heavy metal ions in a water body, and in particular relates to an ethylenediamine-based heavy metal chelating agent and a preparation method thereof. The ethylenediamine-based heavy metal chelating agent is prepared by directly reacting ethylenediamine, carbon disulfide and solid alkali in absolute ethyl alcohol or a mixed solvent consisting of absolute ethyl alcohol and diethyl ether in a certain volume ratio. The method overcomes the defect of steric effect of polymer chains when the conventional polymeric chelating agent chelates the heavy metal ions, and also overcomes the defect that floccules have excessive negative charge to obstruct the further growth of the floccules because of mismatched space of chelation groups of small molecules with multiple functional groups. The product is solid powder, has high stability and is convenient to store and transport. The method has the advantages of simple synthetic process, mild reaction conditions, easy operation and control, high reaction speed, high efficiency, recyclable solvent, high utilization rate of raw materials, less discharge of three wastes, environmental-friendly technical process, conventional equipment and easy industrial production.
Owner:HUNAN UNIV OF SCI & TECH
Treatment method of acid heavy metal wastewater
ActiveCN102964014AImprove recycling ratesSignificant technological progressSludge treatment by de-watering/drying/thickeningWater/sewage treatmentViscous liquidCavitation
The invention provides a treatment method of acid heavy metal wastewater, comprising the following steps of: removing massive impurity of the wastewater by the means that the wastewater passes through grids, and adjusting the pH to 8-9; adding 20-80mg / L heavy metal collecting agent before entering a coagulating floatation tank, and adding 0.5-4.0mg / L biological flocculants before entering the floatation tank; removing organic matter, heavy metal and suspended solids by means of cavitation air floatation; subsiding the water discharged in an air floatation way by a wobble plate, and filtering in a continuous microfiltration device to remove suspended solids and colloid; concentrating air floatation slag by the sludge of a floatation slag tank and a sedimentation tank, putting 20-60mg / L cationic polyacrylamide, and recovering in a drying way; and adding 1320kg of deionized water, 400kg of sodium hydroxide and 380kg of polyethylenimine into the reaction kettle, controlling the temperature of the reaction kettle to be below 25 DEG C, slowly and dropwise adding 1008kg of carbon disulfide, and cooling to room temperature to obtain the heavy metal collecting agent of orange viscous liquid.
Owner:URUMQI DEAN DONGSHENG ENVIRONMENTAL PROTECTION EQUIP CO LTD
A preparation method of a sulfur-supported graphene aerogel composite material
InactiveCN103996830ASimple processShort preparation cycleCell electrodesSecondary cellsLithium-ion batteryPolymer
The invention relates to a preparation method of a sulfur-supported graphene aerogel composite material, and belongs to the technical field of lithium ion battery cathode materials. The preparation method mainly includes steps of: subjecting a graphene oxide dispersion liquid, ethanol and sulfur / carbon disulfide which are main raw materials to a hydrothermal reaction at 100-200 DEG C for 6-48 h to obtain sulfur-supported graphene aerogel, and obtaining the sulfur-supported graphene aerogel composite material covered by a polymer through a chemical oxidation method. According to a sulfur-supported graphene aerogel cathode prepared by the preparation method, graphene is staggered and connected to form a three-dimensional conductive network, the supramaximal surface area can absorb more sulfur, and covering by the polymer can overcome a problem of volume expansion of sulphur and a problem of material smashing in charge-discharge processes. In addition, the composite material prepared by the preparation method can be directly used as a pole piece, thus omitting tedious processes, such as pulping and coating in traditional electrode preparation. The preparation method is prone to industrial production.
Owner:SHANGHAI UNIV
Method for preparing 2-mercaptobenzothiazole
The invention discloses a method for preparing 2-mercaptobenzothiazole, which comprises the steps of: adding carbon disulfide, aniline and sulfur into a reaction kettle; and heating the mixture, finishing a reaction under the reaction pressure of 6.8 to 9.5MPa to obtain a crude product, namely a melt, pressing the melt into a crystallizer loaded with carbon disulfide, controlling the initial temperature of the crystallization, reducing the temperature, beginning to discharge hydrogen sulfide when the material temperature in the crystallizer is reduced to be between 70 and 100 DEG C, controlling the discharge time of hydrogen sulfide to be between 20 and 60min, cooling the obtained product to be between 15 and 20 DEG C, filtering the obtained product to obtain a filter cake and carbon disulfide mother liquor, washing the filter cake for 2 to 5 times by using carbon disulfide in an amount which is 1 to 3 times mass of the filter cake, and drying the scrubbed filter cake to obtain the 2-mercaptobenzothiazole at the mass percentage concentration of over 98 percent. By the method, no 'waste water' and 'waste gas' are discharged, and asphalt-like wastes are greatly reduced. The circulation of crystallization mother liquor realizes the recycling of intermediate products, and the total yield of the process is improved to be over 94 percent.
Owner:TIANJIN UNIV +1
Method for preparing di-dithiocarbamate modified chitosan beads
InactiveCN102504312AGood dispersionLarge specific surface areaOther chemical processesWater/sewage treatment by sorptionBenzaldehydeMining industry
The invention relates to a method for preparing di-dithiocarbamate modified chitosan beads. The method comprises the following steps of: after dissolving 5 g of chitosan in an acetic acid solution at first, solidifying the chitosan in a sodium hydroxide solution to form chitosan beads with the diameter of 2-3 mm, wherein the solidifying time is 8-26 h; and, after carrying out Shiff alkali reaction, etherification, amination and elimination of benzaldehyde of the chitosan beads, grafting carbon disulfide under an alkaline condition to obtain di-dithiocarbamate modified chitosan. Compared with the original chitosan, the chitosan disclosed by the invention as a water treatment agent has stronger adsorption property and can be applied to treatment of heavy metal ions in wastewater, such as electroplating wastewater, battery wastewater, wastewater in mining industries and the like; the adsorption selectivity of the chitosan is increased; furthermore, the chitosan can be recycled for many times; and the purpose of rationally utilizing resources is achieved.
Owner:上海同纳环保科技有限公司
Method for preparing dithiocarbamate-based modified porous starch
InactiveCN101759809AImprove adsorption capacityHigh removal rateWater contaminantsWater/sewage treatment by sorptionDesorptionAlpha-amylase
The invention relates to a method for preparing dithiocarbamate-based modified porous starch. The method comprises the steps that: using starch as the raw material; carrying out enzymolysis on the starch for 1 to 26 hours under the condition that the pH is between 4 and 6 and the temperature is between 30 and 60 DEG C by a complex enzyme consisting of a saccharifying enzyme and an alpha-amylase; drying the obtained product to prepare porous starch; and after carrying out crosslinking, etherification and aminating modification on the porous starch, grafting the product with carbon disulfide under the alkaling conndition to obtain the dithiocarbamate-based modified porous starch. Compared with the conventional porous starch, the dithiocarbamate-based modified porous starch of the invention has strong absorption characteristic and high adsorptive selectivity. When the adsorption effect is reduced, the dithiocarbamate-based modified porous starch is taken out and immersed in 2mol.L-1 of HNO3 solution to carry out desorption, the desorption ratio is over 90 percent, and the absorption effect is not reduced by repeated desorption. The invention has commendable economic and social benefits, and can be used for treatment of heavy metal ions in waste water in galvanization, battery and mining industries and the like.
Owner:TONGJI UNIV +1
Method for dissolving cellulose
The invention discloses a method for dissolving cellulose, characterized by: using at least one from the group consisting of wood pulp, cotton pulp, hemp pulp, bamboo pulp, bagasse pulp, grass fibered pulp, cellulose non-woven fabric or steam exploded cellulose pulp as cellulose raw material, uniformly stirring the cellulose raw material, NaOH and water at a temperature of -15-50 DEG C to obtain a cellulose solution. The prepared cellulose concentrated solution has good spinnability and film forming property. The method breaks through a dissolution method of traditional gluing technology, does not relate to carbon disulfide and other substance causing serious environmental pollution, and is green and environmentally friendly. According to the invention, the cellulose raw material can be directly rapidly dissolved at room temperature, without heating or precooling a solvent. The method has the advantages of saving energy, and reducing energy consumption. By using raw materials having low cost, the method has the advantages of simple operation, small investment, high productivity, and is easy to realize large-scale industrial production.
Owner:NANHUA UNIV +1
Method for preparing anode of lithium sulfur battery
InactiveCN101958414AReduce dispersionHigh discharge specific capacityCell electrodesCarbon disulfideCarbon film
The invention relates to a method for preparing an anode of a lithium sulfur battery, which comprises the following steps of: 1) pretreating a metal sheet: cutting the metal sheet with neat surface into a circular sheet, cleaning by using cotton balls absorbed with acetone, performing ultrasonic cleaning by using distilled water, taking out, and airing; and 2) preparing a carbon sulfur composite material: putting the treated metal sheet into a cavity of a sputtering device, carrying carbon disulfide vapor into the cavity by using sputtering gas, forming plasma by using the sputtering gas, sputtering high-purity graphic target by using the sputtering gas, depositing a carbon film on the pretreated metal sheet, decomposing the carbon disulfide vapor in the plasma formed by the sputtering gas, depositing the generated sulfur and carbon sulfur groups in the carbon film to realize sulfur doping, and preparing the carbon sulfur composite material through deposition, wherein the metal sheet on which the carbon sulfur composite material is deposited is the anode of the lithium sulfur battery. The preparation method is favorable for improving the cyclical stability of the battery, and can avoid reduction of conductivity of the anode caused by an adhesive and shorten the preparation period of the anode of the battery.
Owner:WUHAN INSTITUTE OF TECHNOLOGY
Oil solubility compound-type suspended bed hydrocracking catalyst as well as preparation method thereof
ActiveCN103977822AImprove catalytic performanceReduce yieldPhysical/chemical process catalystsHydrocarbon oil crackingSolubilityReaction temperature
The invention discloses an oil solubility compound-type suspended bed hydrocracking catalyst, wherein the catalyst is prepared by the following steps: 1) enabling compounds of metal elements in the VIB family, the VIIB family or the VIII family in a periodic table of elements as metal sources with alkali metal sulfide or alkali metal hydrosulfide according to the mole ratio of (0.5 to 1)-(2 to 1), thereby obtaining a metal element compound at a reduction state; 2) adding the metal element compound at the reduction state and amine substances into a reaction medium according to the mole ratio of (1:0.6)-(1 to 2), and meanwhile dropwise adding carbon disulfide with the corresponding quantity into the reaction medium according to the mole ratio of (1 to 1)-(2 to1) with the metal element compound at the reduction state, warming to react at the reaction temperature of 30-110 DEG C for 2-10 hours; 3) filtering and washing the product obtained by the step 2) so as to obtain the oil solubility compound-type suspended bed hydrocracking catalyst. The catalyst prepared by the invention can inhibit the coke yield, and improve the light oil yield.
Owner:CCTEG CHINA COAL RES INST
Preparation method of magnetic fluorescence dual functional thermo-sensitive nano particle
InactiveCN101775112AAvoid reunionReduce quenchingLuminescent compositionsPotassium hydroxideBenzyl chloride
The invention discloses a preparation method of a magnetic fluorescence dual functional thermo-sensitive nano particle. The preparation method comprises the following steps: (1) preparing a nano particle core by a routine method, then packing the magnetic nano particle with a layer of silicon dioxide, performing cholromethylation on the silicon dioxide by utilizing a chloromethyl silane coupling agent, and leading benzyl chloride wrapped on the surface of the nano particle to react with carbon disulfide in the dimethylsulfoxide solution of potassium hydroxide so as to obtain a magnetic fluorescence nano particle the surface of which is modified with an RAFT reagent; and (2) utilizing the magnetic fluorescence nano particle obtained in step (1), a thermo-sensitive monomer, a sacrificed RAFT reagent and an initiating agent to form a polymerizing system and dissolving in solvent, carrying out reversible addition-fragmentation chain transfer (RAFT) living radical polymerization, and then performing separating to obtain the magnetic fluorescence dual functional thermo-sensitive nano particle with a nuclear shell structure. RAFT polymerization is directly carried out on the surface of the magnetic silicon oxide nano particle, thus facilitating the magnetic fluorescence dual functional nuclear shell structure to keep the stability of the structure and performance in the actual application process.
Owner:SUZHOU UNIV
Method for preparing tetraalkyl thiuram disulphide by utilizing micro-structured reactor
The invention relates to a method for preparing tetraalkyl thiuram disulphide by utilizing a micro-structured reactor, which comprises the following steps: simultaneously injecting solution of raw material secondary amine and carbon disulfide into the micro-structured reactor through pumps for condensation reaction; injecting the obtained solution of N,N-dialkyl dithiocarbamate and oxyful into another micro-structured reactor for oxidation reaction; and re-crystallizing, filtering, washing and drying the reaction product to obtain the product of tetraalkyl thiuram disulphide. In the method, the operating conditions are easy to control; blockage cannot occur in the process; the operation is convenient; the product has good selectivity; and continuous safety production is realized under theconditions of no acid or alkali and no catalyst.
Owner:NANJING UNIV OF TECH
Method for preparing silica gel supported dithiocarbamate heavy metal chelating resin
InactiveCN102060995ALarge adsorption capacityImprove adsorption capacityOther chemical processesHeavy metal chelationSilica gel
The invention relates to a method for preparing heavy metal chelating resin, in particular to a method for preparing silica gel supported dithiocarbamate heavy metal chelating resin and adsorption of heavy metals such as lead, cadmium, copper, mercury and the like by the resin. The method comprises the following steps of: reacting carbon disulfide with a polyamine compound to generate a dithiocarbamate compound; and grafting the dithiocarbamate compound onto the surface of silicon dioxide, wherein a halogen group is modified on the surface of the silicon dioxide. By the method, the adsorption capacity of dithiocarbamate chelating resin is effectively improved; and the problem that silica gel is dissolved due to too high alkalinity of a reaction system (pH value is more than 11), or the dithiocarbamate compound cannot be generated through reaction due to too low alkalinity (the pH value is less than 10) when a dithiocarbamate functional group is prepared by reacting the silica gel with the carbon disulfide in the conventional synthetic route is solved, wherein an amino group is modified on the surface of the silica gel.
Owner:CENT SOUTH UNIV
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