2888 results about "Filter cake" patented technology

The invention discloses high-purity hafnium oxide and a preparation method thereof, and relates to the technical field of hydrometallurgy. The preparation method of the high-purity hafnium oxide comprises the following steps: crushing a hafnium oxide raw material to obtain hafnium oxide powder; sequentially carrying out alkali fusion, water immersion and filtration treatment on the hafnium oxide powder to obtain a hafnium hydroxide filter cake; dissolving the hafnium hydroxide filter cake in a sulfuric acid solution to obtain a hafnium sulfate solution; adding sodium sulfate into the hafnium sulfate solution to obtain hafnium-containing double salt; dissolving the hafnium-containing double salt in a sulfuric acid solution, heating, evaporating, cooling and crystallizing to obtain hafnium sulfate crystals; dissolving the hafnium sulfate crystal in concentrated hydrochloric acid to obtain a hafnium oxychloride solution, heating, evaporating, cooling and crystallizing to obtain a hafnium oxychloride crystal; dissolving the hafnium oxychloride crystal in pure water, adding an oxalic acid solution, and precipitating to obtain hafnium oxalate; and calcining hafnium oxalate to obtain high-purity hafnium oxide. The preparation method of the high-purity hafnium oxide is green, environment-friendly, simple and efficient.

The invention relates to the technical field of tailing mud treatment, and discloses a solid-liquid separator for treating tailing mud, which comprises a support frame, the top of the support frame is fixedly provided with a vertical plate I and a vertical plate II, the outer wall of the vertical plate II is fixedly provided with a fixed seat, and the top of the fixed seat is fixedly provided with a central control box; a cross beam is fixedly assembled between the first vertical plate and the second vertical plate, a sliding groove is formed in the outer wall of the cross beam, a filter plate is arranged on the outer wall of the cross beam, a circular groove is formed in the inner wall of the filter plate, and a solid-liquid separation assembly is arranged on the inner wall of the circular groove. An electric telescopic rod II is started under the control of a weighing display instrument, so that an arc-shaped plate can lift a lapping block to move up and down, a filter plate can perform high-frequency vibration, a filter cake can quickly fall off from the filter plate, discharging is more thorough, meanwhile, the cleanliness of equipment is improved, and the device is high in discharging speed and convenient to use. And the influence of filter cake residues on the next filtering process can be effectively avoided, and the discharging efficiency is improved.

The invention relates to the technical field of sulfur-iodine circulating hydrogen production, in particular to a thermochemical iodine-sulfur-barium circulating hydrogen production process and a thermochemical iodine-sulfur-barium circulating hydrogen production system, which comprises the following steps: reacting excessive Ba < 2 + > with sulfuric acid in a Bunsen reaction product to obtain barium sulfate so as to obtain a first reaction mixed solution containing HI, BaSO4, H2O, BaI2 and a small amount of unreacted I2; sequentially carrying out cyclone separation, liquid removal and filter pressing to obtain a barium sulfate filter cake and a second mixed solution containing HI, H2O and BaI2; the method comprises the following steps: crushing a barium sulfate filter cake, performing high-temperature decomposition, returning gas generated by decomposition to participate in Bunsen reaction, and dissolving BaO generated by decomposition into Ba < 2 + >; and reboiling the second mixed solution to obtain hydrogen iodide steam, cooling a product obtained by decomposing the hydrogen iodide steam, carrying out gas-liquid separation to obtain hydrogen, and returning liquid obtained by gas-liquid separation to participate in the Bunsen reaction of the next cycle. Barium circulation is introduced, the process is simplified, the dosage of elemental iodine is reduced, and the cost is low.

The invention provides a method for synthesizing 1, 2-bis (4-vinyl phenyl) ethane, which comprises the following steps: adding a first solvent, methyl triphenyl phosphine halide and strong alkali into a reaction flask, and uniformly stirring to obtain a first mixed solution; heating the first mixed solution and carrying out reflux reaction for 1 hour; dropwise adding a 1, 2-bis (p-formaldehyde phenyl) ethane solution until the reflux reaction is finished to obtain a second mixed solution; reducing the temperature of the second mixed solution to room temperature, and adjusting the pH value of the second mixed solution to obtain a first solution; layering the first solution, and taking an organic layer; adding a polymerization inhibitor into the organic layer to obtain a second solution; concentrating the second solution to obtain a 1, 2-bis (4-vinyl phenyl) ethane crude product; adding a poor solvent into the crude product, stirring and crystallizing; filtering the crystal to obtain a filter cake, adding a second solvent into the filter cake, and washing and drying the filter cake to obtain 1, 2-bis (4-vinyl phenyl) ethane; the method for synthesizing the BVPE is simple and low in raw material cost, and the synthesized BVPE is high in purity and free of product isomeride.

The invention relates to a process for recycling and regenerating a waste lithium iron phosphate positive electrode material by using a specific chelating agent. The method comprises the following steps: carrying out heat treatment on a waste lithium iron phosphate positive electrode material, putting separated waste lithium iron phosphate powder into a ball milling tank, adding organic acid and a chelating agent, and carrying out ball milling; after the ball milling is finished, adding hydrogen peroxide, uniformly stirring and mixing, adjusting the pH value to 2-3 by using nitric acid, and filtering to obtain a filter cake which is iron phosphate; adding saturated sodium carbonate into the filtrate, precipitating, and recovering lithium carbonate; putting the iron phosphate, the lithium carbonate, the iron source, the lithium source and the phosphorus source in the step S3 into a ball mill for ball milling, and performing high-temperature solid-phase sintering after ball milling to obtain a regenerated lithium iron phosphate material; the chelating agent disclosed by the invention is prepared from (9ci)-2-(2-propenyl)-1-cyclopentene-1-carboxylic acid, 2-mercaptobenzimidazole carboxylic acid, an ethylene boric anhydride pyridine complex and potassium persulfate. The regenerated lithium iron phosphate material prepared by the method has excellent electrochemical performance.

The invention belongs to the technical field of denitration catalyst preparation, and discloses a meerscham-TiO2 composite carrier loaded manganese cerium medium and low temperature denitration catalyst and a preparation method and application thereof, the preparation method comprises the following steps: (1) mixing meerschaum and nitric acid, then heating and stirring for reaction, then carrying out suction filtration and washing, and drying to obtain a meerschaum-TiO2 composite carrier loaded manganese cerium medium and low temperature denitration catalyst; after the treated sepiolite is drained, drying and screening are conducted, and nitric acid acidified sepiolite is obtained; and (2) mixing the meerschaum acidified by nitric acid and TiO2, then adding the manganese source precursor solution into the acidified meerscham-TiO2, then dipping and stirring, dropwise adding a potassium permanganate solution into the solution, then adding a cerium nitrate solution, stirring and then carrying out suction filtration, drying, grinding and screening the obtained filter cake, and then calcining to obtain the catalyst. According to the invention, the acidified sepiolite and TiO2 are compounded, so that complementary advantages of the two carrier materials are realized, and the obtained catalyst not only has good denitration efficiency, but also can significantly reduce the production cost.

The preparation method comprises the following steps: S1, preparing a phosphoric acid solution, a hydrogen peroxide solution, a Ti salt, a phosphor salt solution and a ferrite solution; s2, Ti salt and the ferrite solution are mixed, and a titanium iron salt solution is obtained; mixing the phosphoric acid solution and the phosphorus salt solution to obtain a phosphorus source solution; s3, adding the titanium iron salt solution into a reaction kettle, and adding the hydrogen peroxide solution; s4, adding the phosphorus salt solution into the reaction kettle to obtain yellow slurry; s5, after the color of the slurry is heated to be white, white slurry is obtained; s6, carrying out solid-liquid separation on the white slurry to obtain an iron phosphate dihydrate filter cake; and S7, drying and calcining the iron phosphate dihydrate filter cake to obtain the Ti-doped battery-grade anhydrous iron phosphate. The titanium-doped iron phosphate is firstly prepared by a one-step method, the pH value of the reaction system is controlled by controlling the molar ratio of the iron element to all phosphorus elements in total phosphorus, ammonium phosphate and phosphoric acid in the reaction system, and the retention of the Ti element in the finished product and the regulation and control of the iron-phosphorus ratio in a specified range are ensured.

The invention provides three-stage extrusion type coal slime filter pressing equipment and a working method. The filter pressing equipment structurally comprises a thrust plate, a filter plate, filter cloth, a cross beam, a pressing plate, a pressing hydraulic system, a sealing unit, a feeding unit, a control unit and the like; columnar protruding structures arranged in an array mode are arranged on the outer surface of the filter plate, and each columnar protruding structure is in the structural form that a cone and a semicircle are combined. According to the requirements of the size and the dehydration rate of the filter plate, the columnar bulge structures are arranged on the surface of the filter plate by adopting a topological optimization method, so that the dehydration rate of the coal slime is improved, and the separation of a filter cake is facilitated; the pressing plate is of a sectional structure and is divided into three sections from left to right, and each section is connected with piston rods of the corresponding three hydraulic cylinders and corresponds to a three-stage extrusion working mode. And when the previous-stage extrusion pressure reaches 40% of the threshold pressure, the next-stage extrusion procedure is started. 40% of the extrusion threshold pressure can be set to ensure that the first two-stage extrusion is not finished when the third-stage extrusion process is started, so that the optimal extrusion mode of three-stage simultaneous extrusion is formed, the coal slime dehydration rate is increased to the greatest extent, and the filter pressing effect is improved. By adopting the three-stage extrusion mode, the dehydration process of each sub-area can be freely, flexibly and independently controlled, the toothpaste extrusion type collaborative filter pressing effect is achieved, the coal slime dehydration rate is higher, and the filter pressing effect is better.

The invention belongs to the technical field of reaction crystallization type solid-liquid separation, and particularly relates to filtering equipment with a reaction aging crystallization function. The device comprises a reaction kettle and a centrifugal filter disc which is located in the reaction kettle and can rotate and ascend and descend, and a reserved channel for materials to ascend and filter cakes to descend is formed between the disc edge of the centrifugal filter disc and the inner wall of the reaction kettle; the upper disc surface of the centrifugal filter disc is provided with a filter surface, a kettle cavity of the reaction kettle is communicated with a liquid accumulation cavity positioned in the centrifugal filter disc through the filter surface, the liquid accumulation cavity is communicated with a mother liquor outlet through a transition channel, and a slag outlet for discharging filter cakes is formed in the bottom of the reaction kettle. Through vertical reciprocating motion of the filter disc and multi-dimensional motion of rotation, rapid filtering and centrifugal discharging functions of materials needing reaction, aging and crystallization operation are achieved, smoothness of a filtering medium channel can be effectively guaranteed, and the effects of being simple in structure and compact in structure are achieved.

The invention discloses a novel electrolytic tank pipeline filter and a self-cleaning system. The novel electrolytic tank pipeline filter comprises a multi-stage filtering part, the self-cleaning system and an intelligent control system, the multi-stage filtering part comprises multi-stage filter elements arranged in the material pipeline, and the multi-stage filter elements are arranged from large to small according to the filtering particle size to form a filtering gradient; the self-cleaning system acts on the multi-stage filter element part at the same time or in a time-sharing manner on the basis of a fluid reverse recoil principle; the self-cleaning system is combined with pulsating flushing control, so that the filter element is separated from a filter cake at low loss; the multi-stage gradient filtration is adopted, impurities are efficiently and accurately intercepted, the filter elements with the particle sizes from large to small are arranged in a gradient mode, the first-stage titanium alloy filter element intercepts large particles, the second-stage polytetrafluoroethylene membrane filters tiny impurities, the efficiency is improved through graded interception, the loss of the filter elements is reduced, and the material purity and the hydrogen production quality are guaranteed. The multi-element self-cleaning technology is adopted, low-loss deep cleaning is achieved, and the self-cleaning system integrates multiple technologies such as fluid reverse backflushing, pulsating flushing, ultrasonic vibration and a pulsed electric field.

A lithium manganese iron phosphate substrate, cathode material, and their preparation method, as well as a lithium battery, belonging to the field of lithium-ion battery technology. The preparation of the lithium manganese iron phosphate substrate comprises the following steps: dissolving soluble ferrous salt, soluble manganese salt, phosphoric acid, and lithium hydroxide in deionized water to react, obtaining Material A; filtering Material A, taking the filter cake and drying it to obtain Material B; Heat treating Material B in an inert gas atmosphere to obtain the lithium manganese iron phosphate substrate. By coating the surface of the carbon-free nano lithium manganese iron phosphate substrate with metal oxides or metal salts and carbon, the coating layer formed on the surface of the composite lithium manganese iron phosphate material effectively prevents the reaction between the lithium battery and the electrolyte.

The invention discloses a method for reducing the content of aged starch and soluble miscellaneous sugar in alpha-cyclodextrin, and belongs to the technical field of alpha-cyclodextrin synthesis, the method comprises the following steps: liquefaction, conversion, primary filtration, inclusion, secondary filtration, complexing agent removal and post-treatment; the conversion comprises the following steps: adding alpha-CGTase and isoamylase into the starch liquefied liquid at 38-42 DEG C, adjusting the pH value to 5.30-5.70, and carrying out conversion to obtain a conversion liquid; the primary filtration comprises the following steps: carrying out enzyme deactivation treatment on the conversion liquid, filtering, washing a filter cake with water, and combining the washing liquid with the filtrate to obtain primary filtrate; and the secondary filtration comprises the following steps: filtering the material liquid containing the complex, taking a filter cake, and washing the filter cake with water to obtain the inclusion compound. The preparation method of the alpha-cyclodextrin is improved, so that the alpha-cyclodextrin with high yield and high stability is obtained, and the industrial controllability is realized.

The invention discloses a method for preparing MHP by cyclic utilization of manganese precipitation post-solution, which comprises the following steps: mixing sodium hydroxide, magnesium oxide and manganese precipitation post-solution to obtain compound alkali slurry; mixing the laterite-nickel ore liquid subjected to iron and aluminum removal with the compound alkali slurry, and carrying out precipitation reaction to obtain MHP slurry; carrying out thickening treatment on the MHP slurry to obtain a dense underflow; filtering the dense underflow to obtain an MHP filter cake and filtrate; directly carrying out manganese precipitation treatment on the filtrate to obtain manganese slag and manganese-precipitated liquid; and reusing the manganese-deposited liquid in the preparation of the compound alkali slurry. According to the invention, a sodium hydroxide and magnesium oxide compounded system is utilized, so that the MHP precipitation process can be simplified to one step. And meanwhile, part of the manganese-deposited liquid is recycled to the alkali preparation process, so that the wastewater treatment cost is reduced, and the magnesium content in the MHP can be reduced by controlling the circulation amount of the manganese-deposited liquid, and the cost of preparing crystals through subsequent fine extraction of the MHP is reduced.

The invention discloses a method for producing lithium dihydrogen phosphate by using a low-lithium-concentration strong-basicity lithium-containing leaching solution, and relates to the technical field of lithium salt production. The method specifically comprises the following steps: adding a sodium phosphate or sodium hydrogen phosphate solution into the lithium-containing leaching solution, reacting to obtain slurry, carrying out solid-liquid separation, washing the obtained filter cake, adding water, slurrying, adding phosphoric acid, completely dissolving to obtain a solution, adding a precipitant into the solution, adjusting the pH value to alkalescence, precipitating, and drying to obtain the lithium-containing leaching solution. And carrying out solid-liquid separation on the obtained precipitate, washing the obtained filter cake, adding water for slurrying, adding phosphoric acid, continuously stirring for reaction, completely dissolving to obtain a clear lithium dihydrogen phosphate solution, and treating to obtain the battery-grade lithium dihydrogen phosphate. According to the method, efficient extraction of lithium is successfully realized, a lithium dihydrogen phosphate product with a high additional value is generated, a large amount of acid consumption in the alkali liquor neutralization process is avoided, the consumption of alkali in the solution is relatively low, and the solution can be returned to the previous procedure for cyclic utilization.

The invention relates to the technical field of swimming pool filtration, in particular to a composite treatment method of a filter aid for swimming pool filtration, which comprises the following steps: S1, adding the filter aid: adding a powdered activated carbon filter aid into a filter through a feeding pump, and forming an activated carbon filter aid filter cake in the filter; s2, filtering: intercepting or adsorbing impurities when the water in the to-be-treated pond is filtered through an activated carbon filter aid filter cake and a filter, and continuously or intermittently supplementing a powdered activated carbon filter aid in order to maintain the filtering efficiency; s3, backwashing: when the pressure difference of the filter reaches a set value, backwashing is started, and intercepted and adsorbed pollutants and the activated carbon filter aid filter cake slurry are discharged into a drainage system together. The device has the effects of efficiently removing chloramine and other disinfection by-products, peculiar smell, pigment and other pollutants, guaranteeing the water quality safety of the swimming pool and maintaining normal operation of the swimming pool.

The invention relates to a method for treating a waste iron phosphate positive electrode material by a phosphoric acid-hydrogen peroxide method matched with a specific complexing agent. The method comprises the following steps: crushing the positive electrode material of the waste lithium iron phosphate battery, adding the crushed positive electrode material into deionized water, and stirring to prepare slurry; heating the slurry, dropwise adding a phosphoric acid-hydrogen peroxide mixed solution and a complexing agent, adding a NaOH solution to adjust the pH value to 3.5, and filtering to obtain a filtrate and a filter cake; adding a NaOH solution into the filtrate, and adjusting the pH value to 10 to obtain lithium phosphate; performing evaporative crystallization on the filter cake to obtain trisodium phosphate; the complexing agent is prepared by adding pentasodium salt of amino trimethylene phosphonic acid, triallyl citrate, epoxysuccinic acid and DMF (Dimethyl Formamide) into a reaction kettle, mixing, adding ammonia water to adjust the pH value to be 10, and distilling to remove the DMF after the reaction is finished. The precipitation rate of Fe reaches up to 99.99%, the leaching rate of Li reaches up to 99.91%, and efficient separation and recycling of lithium and iron are achieved.

The invention relates to the technical field of oil-gas field development, in particular to a zwitterionic polymer filtrate reducer and a preparation method thereof.The zwitterionic polymer filtrate reducer is prepared from an acrylamide monomer, a hydrophilic monomer, a rigid monomer, a salt-tolerant monomer, a copolymerization adjusting monomer, starch, aluminum oxide powder, KH560 modified nano-silica, a cationic monomer and an anionic monomer; mixing an acrylamide monomer, a hydrophilic monomer, a rigid monomer, a salt-tolerant monomer, a copolymerization adjusting monomer, a cationic monomer, an anionic monomer and a solvent to obtain a monomer mixed solution; introducing nitrogen to remove oxygen; adding an initiator, heating and carrying out copolymerization reaction; adding starch and continuously stirring to obtain a material flow A; uniformly mixing KH560 modified nano silicon dioxide and aluminum oxide powder, and adding the mixture into the material flow A; and drying, crushing and grinding to obtain zwitterionic polymer filtrate reducer powder. When in contact with a well wall, the filtrate reducer can be spread and adhered to the surface of the well wall to form a low-permeability, flexible, thin and compact filter cake, so that the filter loss of a drilling fluid is reduced.

The invention discloses a method for preparing a carbon monoxide oxidation catalyst by using titanium gypsum and a waste hydrogenation catalyst, which comprises the following steps: crushing and pickling the waste hydrogenation catalyst, washing with clear water until the waste hydrogenation catalyst is neutral, and drying to obtain pretreated waste catalytic powder; uniformly mixing and stirring titanium gypsum and the pretreated waste catalytic powder to obtain gypsum doped pretreated waste catalytic powder; mixing a plant extract, crop powder and gypsum, doping the pretreated waste catalytic powder, uniformly stirring, feeding into mixed bacteria consisting of bacillus and aspergillus, and fermenting under a stirring condition to obtain a biological activated mixture; adding water into the biological activation mixture for hydrothermal reaction, filtering, separating and washing the material after the hydrothermal reaction is finished, roasting the washed filter cake, naturally cooling the roasted material, and crushing to obtain the carbon monoxide oxidation catalyst. According to the invention, the titanium gypsum and the waste hydrogenation catalyst are combined, and the biomass material is used for activating treatment, so that the use of chemical precursors is reduced, and the oxidation catalyst with excellent catalytic performance is obtained.

Belonging to the field of petrochemical engineering, the invention discloses a catalytic slurry oil purification device, which comprises a tank body, and a feed end and a discharge end respectively arranged at two ends of the tank body. An upper partition plate and a lower partition plate are fixedly connected to the inner wall of the tank body, a discharging opening is formed in the upper partition plate, and a feeding opening is formed in the lower partition plate; the interior of the tank body is divided into three independent cavities by the upper partition plate and the lower partition plate; according to the scheme, the filter element is sleeved with the hollow cylinder, and the rotatable first spiral flow deflector is further arranged between the inner wall of the hollow cylinder and the outer wall of the filter element; a rotatable first spiral flow deflector is further arranged between the inner wall of the hollow cylinder and the outer wall of the filter element; a shear force generated by rotation of the first spiral flow deflector can prevent a filter cake on the surface of the filter element from forming a compact thick layer; a filter cake layer can be controlled within a relatively thin thickness range, and the rising speed of the pressure difference is delayed, so that the operation duration of a single filtering period is prolonged; and the single-time continuous treatment capacity of the device is greatly improved.

The present application relates to the technical field of battery materials, and provides iron phosphate having low sulfur content and a high iron-phosphorus ratio, a preparation method therefor, and a use thereof. The preparation method for the iron phosphate having low sulfur content and a high iron-phosphorus ratio comprises: providing amorphous iron phosphate; adding water and phosphoric acid into the amorphous iron phosphate for slurrying treatment, and then heating and aging to obtain an aged slurry; carrying out slurry washing and filter pressing on the aged slurry to obtain a first filter cake; adding water and a first pH regulator into the first filter cake for slurry washing to obtain a first slurry having a pH value range of 3.0-5.0, and carrying out filter pressing on the first slurry to obtain a second filter cake; and rinsing, drying and calcining the second filter cake to obtain iron phosphate having low sulfur content and a high iron-phosphorus ratio. The present application facilitates preparation of iron phosphate having low sulfur content, a high iron-phosphorus ratio, and a large specific surface area. The iron phosphate can be used for preparing lithium iron phosphate having good electrochemical performance, and the lithium iron phosphate can be further used for preparing a positive electrode sheet and a secondary battery having good electrochemical performance.

The invention provides a method and system for separating and washing red mud in aluminum oxide production, and the method comprises the following steps: pretreating red mud slurry to improve the filtering performance of the red mud slurry; filtering the pretreated red mud slurry under set filtering conditions to form a red mud filter cake; in the filtering process, when the thickness of the dehydrated red mud filter cake reaches a set thickness, dehydrating the red mud filter cake so as to reduce the moisture content of the dehydrated red mud filter cake; performing multi-stage countercurrent washing on the dehydrated red mud filter cake to obtain a countercurrent washing solution; and carrying out purification treatment and concentration treatment on the countercurrent washing liquid, and returning the countercurrent washing liquid subjected to purification treatment and concentration treatment to the multi-stage countercurrent washing step as a washing liquid for cyclic utilization. The problem that the resource recycling rate is low in the red mud separating and washing process in aluminum oxide production is effectively solved.

The application provides a reverse water gas shift catalyst, a preparation method and application thereof, and the reverse water gas shift catalyst prepared by the preparation method has excellent catalytic activity and high CO selectivity in a reverse water gas shift reaction. The preparation method comprises the following steps: contacting a precipitating salt solution with a precipitant aqueous solution and performing co-precipitation, and simultaneously controlling the reaction temperature to be 40-80 DEG C and the pH to be 6-8; optionally performing aging after the co-precipitation is completed; filtering the obtained precipitate to obtain a filter cake, washing the filter cake, then drying the filter cake, and calcining the filter cake at 300-500 DEG C to obtain the reverse water gas shift catalyst; wherein the precipitating salt solution is a mixed aqueous solution of a soluble salt of divalent metal ions and a soluble salt of trivalent metal ions, the divalent metal ions are selected from divalent ions of Mg and / or Zn, and the trivalent metal ions are selected from trivalent ions of Al, In and / or Ga.

The invention discloses a low-resistance and easy-to-clean frame filter and a filtering method, and relates to the technical field of filtering equipment, the frame filter comprises a washing liquid storage tank, a gas-liquid mixing device, a rotary distribution head, a filter plate fixing device, filter cloth, a filter frame, a sieve plate, a washing pipe, a sieve plate supporting sleeve, a filtrate storage tank and a washing nozzle. According to the invention, a material flowing space is constructed between the sieve plates by using the sieve plate supporting sleeve, so that the filtrate flow of a traditional plate-and-frame filter is shortened, and the filtering resistance is obviously reduced; the gas-liquid mixing device is combined with high-pressure gas, so that the cleaning effect is effectively enhanced; after the filter plate fixing device is loosened, the filter cloth and the filter cake can be easily separated and fall off. According to the invention, a traditional plate frame type filter is transformed, so that the formed frame type filter can remarkably reduce the filtering pressure and energy consumption, greatly improve the filtering efficiency and the filter cake washing rate, reduce the maintenance cost and prolong the service life of equipment, and is suitable for various filtering scenes.

The invention discloses a preparation method of basic magnesium chloride, which comprises the following steps: dissolving magnesium chloride in water, heating to 50-95 DEG C, and stirring for 1-2 hours to obtain a colorless and transparent first solution; magnesium oxide is added into the first solution, alkali is added to adjust the pH to be 8-10, heat preservation is conducted, stirring continues for 1-4 h, and a second solution is obtained; pulping the second solution into a crystallization kettle, crystallizing, centrifuging, washing, drying a filter cake at 80-105 DEG C to obtain a white product basic magnesium chloride, and circulating mother liquor water for the synthesis reaction. The synthesis process provided by the invention is simple, high in product yield and yield and suitable for mass production, a common chemical synthesis kettle can meet production requirements, high-temperature and high-pressure procedures are avoided, and the production cost is reduced. The method is low in energy consumption, high in safety, free of wastewater and sewage discharge, green and environment-friendly.

The invention belongs to the technical field of waste PET (Polyethylene Terephthalate) recovery, and particularly relates to a continuous production system and process for efficiently recovering and refining PTA (Purified Terephthalic Acid) from waste PET and application. According to the continuous production system and process for efficiently recovering and refining the PTA from the waste PET, through mutual cooperation of the enzymolysis unit, the first solid-liquid separation unit, the filter cake dissolving and decolorizing unit, the electrolysis unit, the second solid-liquid separation unit and the recrystallization unit, continuous production of'obtaining the refined PTA by taking the waste PET as a raw material 'is realized; besides, by adjusting the runner structure in the electrolysis assembly of the electrolysis unit, the situation of electrolysis interruption caused by the fact that TA generated by electrolysis is prone to being deposited on the surface of the anode plate is avoided, guarantee is provided for continuous proceeding of the whole degradation and recovery process, and the system and the process have important significance on efficient degradation and recovery of waste PET.

The invention provides a rapid preparation method of tungsten trioxide, which specifically comprises the following steps: step 1, weighing crude tungstic acid, dissolving in ammonia water, heating and stirring to obtain an ammonium tungstate solution; step 2, slowly dropwise adding the ammonium tungstate solution in the step 1 into a poor solvent to obtain an ammonium paratungstate suspension, and step 3, filtering the ammonium paratungstate suspension in the step 2 to obtain an ammonium paratungstate filter cake, and leaching the ammonium paratungstate filter cake with the poor solvent; 4, the ammonium paratungstate filter cake in the step 3 is placed in a drying oven to be dried; and (5) roasting the ammonium paratungstate filter cake in the step (4) at high temperature to obtain a faint yellow irregular flaky tungsten trioxide product. According to the preparation method, a mixed solvent crystallization and high-temperature roasting two-step process is adopted, the solubility of ammonium tungstate in water is reduced by adding a poor solvent, so that an ammonium tungstate solution rapidly reaches a saturated state and is separated out, the crystallization process of ammonium paratungstate is accelerated, and the preparation speed and the crystallization rate of a tungsten trioxide product are high.

A method for recycling various metals from sintering machine head ash comprises the steps that S1, the sintering machine head ash is subjected to pulping and magnetic separation, and tailing pulp and iron-containing concentrate are separated; s2, settling the tailing pulp to obtain bottom mud and supernate, carrying out filter pressing on the bottom mud to obtain silver-containing tailings and beneficiation water, and mixing the supernate and the beneficiation water to obtain mixed waste liquid; s3, treating the mixed waste liquid to obtain a heavy filter cake and high-salt waste water, and concentrating and separating out salt to obtain potassium sodium salt, condensed water and high-chlorine waste liquid; and S4, leaching the silver-containing tailings by using the high-chlorine waste liquid to obtain a silver-rich liquid, and carrying out an iron powder replacement reaction to obtain crude silver. Through the steps of magnetic separation, sedimentation, leaching and replacement, iron, silver, potassium, sodium and other metals are efficiently recycled, the process is simplified, and the efficiency is improved.

The invention belongs to the technical field of wastewater treatment and recycling, and relates to a low-pressure ultrafiltration sewage treatment method and device based on bioelectrochemical enhancement and application. The treatment device consists of a water inlet tank, a constant water level water tank, a cathode, a resistor, a membrane assembly, a biological filter cake layer, a pre-filtering layer-anode, an ultrafiltration membrane, a water collecting device, a data acquisition module and a computer. The treatment device is used for treating effluent of a secondary sedimentation tank of a sewage plant and tail water of livestock and poultry breeding wastewater; on the basis of retaining nitrogen and phosphorus resources, deep removal of heavy metals and antibiotics is realized, propagation of resistance genes is inhibited, and safe reuse of nitrogen and phosphorus resources in effluent of sewage plants and tail water of livestock and poultry breeding wastewater can be realized. In the invention, low-pressure ultrafiltration adopts transmembrane pressure difference generated by gravitational potential energy to realize continuous flow filtration, coupled bioelectrochemistry utilizes electric energy generated by biodegradation of organic matters to realize reduction of heavy metals and deep removal of reinforced antibiotics, and the method has the advantages of greenness, low carbon and sustainability.

A filter and method for removing solids from FCC oil slurries and concentrates thereof is provided. The filter comprises a main tank (4), a first filter cylinder, a second filter cylinder and a third filter cylinder, each of which is composed of a main conduit and a number of secondary conduits with porous outer walls surrounding the main conduit, each of which is fitted with a single turn of first filter membrane around its outer periphery, a filter cake scraper (7) installed inside the main tank above the third filter cylinder, and a deslagging bin (8) installed at the bottom of the main tank. The present invention can achieve complete solid-liquid separation of FCC oil slurry and its concentrate, and fully automatic, intelligent operation.

The invention particularly relates to a computer-implemented method for optimizing the output of a decanter during operation using an enhanced artificial intelligence (AI) engine, the method comprising a. Operating the decanter according to a plurality of operating parameters; b. Treating the physical input comprising sludge and polymer by a decanter and producing a physical output comprising a centrifugal filtrate and a filter cake; c. Determining a plurality of substance parameters based on the physical output; d, transmitting the plurality of material parameters and the plurality of operation parameters to an enhanced AI engine; e. Determining, by the enhanced AI engine, a quality value for each of the plurality of substance parameters; f. Predicting, by the enhanced AI engine, a plurality of adjusted operating parameters; and further operating the decanter based on the plurality of adjusted operating parameters.