1454 results about "Buffering agent" patented technology

The invention discloses an intelligent fish and rice symbiosis ecological control system and method based on the Internet of Things. The system comprises a fish breeding area, a rice irrigation area and a circulating water channel arranged between the fish breeding area and the rice irrigation area. The central control platform is used for collecting a dissolved oxygen (DO) value and a pH value in a water body in real time through a plurality of water quality sensors configured in the system; the dissolved oxygen DO value and the pH value are water quality data; and analyzing the dissolved oxygen DO value, generating a water quality regulation and control instruction, and regulating the oxygenation equipment according to the water quality regulation and control instruction. The automatic buffering agent adding device is used for automatically adding a buffering agent according to an instruction sent by the central control platform; the oxygenation equipment comprises an aeration device and is used for adjusting the content of dissolved oxygen in the water body. According to the intelligent fish and rice symbiosis ecological control system based on the Internet of Things, the fish culture area, the rice irrigation area and the circulating water channel are integrated, effective management and control of the fish and rice symbiosis ecological system are achieved, the water body environment is optimized, and the symbiosis benefits of fishes and rice are improved.

The invention is about a method of marking ink which is only used to defend fake. The composition of it is: lipidol or lipid, surface active agent, integration agent, water, buffering agent. Their mass percents are: 1,2-hexylene glycol: 5%-15%, butanol: 1-5%, DH-1: 5-10%, EDTA: 0.1-0.5%, MS-1: 0.1-1%, water: the rest. The process is: a. dissolving the colorant in water, b. put the correct percent of 1,2-hexylene glycol and butanol into the solvent, then dropping the MS-1 and EDTA solution when mixing the solvent for 30-50 min, c. put the rest precent of water into the printing ink box. The picture and word would be shown red fluorescence in the UV but blank in the usual light.

The invention discloses an efficient wet desulfurization synergist and a preparation method thereof, and relates to the technical field of flue gas desulfurization. The efficient wet desulphurization synergist comprises the following raw materials in parts by weight: 10-20 parts of sodium formate, 5-10 parts of citric acid, 20-30 parts of binary acid, 5-6 parts of a surfactant, 15-20 parts of magnesium salt, 12-18 parts of sodium salt and 2-5 parts of a pH buffer agent. The preparation method comprises the following steps: reacting cyanuric chloride with lauryl amine to generate a monosubstituted compound; then reacting with L-asparaginic acid to generate a disubstituted compound; reacting with diethylenetriamine to generate a bis-triazine ring compound; and finally, reacting with sodium 2-chloroethanesulfonate to generate the surfactant. The high-efficiency wet desulphurization synergist prepared by the invention has a desulphurization effect.

The invention relates to a fluorine-containing binder for a sulfide all-solid-state battery and a preparation method and application thereof.The binder is formed by copolymerizing isoprene and lithium perfluorovinyl ether sulfonate, specifically, the lithium perfluorovinyl ether sulfonate, a chelating agent, an emulsifying agent, ferrous sulfate, a reducing agent and an acid-base buffering agent are dissolved in water, cooling is conducted in the inert atmosphere, and the fluorine-containing binder for the sulfide all-solid-state battery is obtained. And adding isoprene, an initiator and a molecular weight regulator, and carrying out polymerization reaction to obtain the fluorine-containing binder. The isoprene can enhance the solubility of the lithium perfluorovinyl ether sulfonate fragment in the non-polar solvent, so that the whole polymer is dissolved in the non-polar solvent; the perfluorovinyl ether lithium sulfonate has a large space proportion of fluorocarbon groups, and has a shielding effect on hydrocarbon groups on isoprene, so that the stability of the whole polymer can be improved. The fluorine-containing binder prepared by the preparation method disclosed by the invention is a binder with high elasticity, high ionic conductivity and high stability.

The present disclosure provides agronomically stable liquid agricultural compositions, methods of formulation thereof, and methods of application thereof. The agricultural compositions comprise nitrogen-fixing microorganisms and one or more of a buffering agent, a microbial stabilizer, and a physical stabilizer. The disclosed liquid agricultural compositions have a longer shelf life and greater ease of application than other existing dry and liquid formulations. The disclosed liquid agricultural compositions are stable for a period of thirty days or longer with low toxin accumulation and high microbial stability. The compositions are suitable for use on agricultural plant tissues or the environs thereof for providing a source of fixed atmospheric nitrogen to the agricultural plant. The compositions are used to increase crop yield and decrease yield variance.

Methods of treating a nerve injury are disclosed. The methods include administering to a target site of the nerve injury a thermally stable preparation having a purified amphiphilic peptide in an aqueous biocompatible solution, being configured to self-assemble into a hydrogel, and administering to the target site a buffer having an effective amount of an ionic salt and a biological buffering agent to form the hydrogel. The methods include administering to the target site a biological material suspension in an amount effective to treat the nerve injury. The methods include administering to the target site an anti-scarring agent in an amount effective to treat the nerve injury. The target site is associated with central nervous system tissue or peripheral nervous system tissue. The nerve injury includes spinal cord injury and peripheral nerve injury.

The invention discloses a pharmaceutical composition for promoting aTreg cell differentiation and application thereof, and relates to the field of biological medicine, and the pharmaceutical composition comprises zinc salt, a basic cell culture medium, fetal calf serum, antibiotic, L-glutamine and a pH buffer agent. According to the application, the basic cell culture medium is used for providing basic nutrition required by cell growth for lymphocytes, the fetal calf serum is used for providing growth factors, hormones, adhesion proteins and nutrient substances required by cell growth for the lymphocytes, and the antibiotics are used for preventing bacterial infection; l-glutamine provides key amino acid for cell energy metabolism and participates in synthesis of protein and nucleic acid, zinc salt provides zinc ions, and under the comprehensive action, the proportion of Treg cells and aTreg cells differentiated from lymphocytes in peripheral blood mononuclear cells is increased.

S-Beta-hydroxybutyric acid compositions for oral delivery are effective in rapidly raising blood ketone levels without causing acute acidosis or gastrointestinal (GI) distress when consumed in sufficiently dilute form and / or as a gel or suspension. By limiting added beta-hydroxybutyrate salts containing alkali or alkaline earth metal ions, beta-hydroxybutyric acid solutions, gels, or suspensions can deliver exogenous ketone bodies without significantly altering electrolyte balance. Although aqueous beta-hydroxybutyric acid solutions are moderately acidic with a pH of about 3.5 to 4, when diluted with sufficient water, the water acts as a pseudo buffering agent that offsets otherwise harsh acidic effects when consumed orally. Gels and suspensions can also ameliorate acidic effects by partially encapsulating the beta-hydroxybutyric acid. Beta-hydroxybutyric acid can be pure S-beta-hydroxybutyric acid or a non-racemic mixture enriched with S-beta-hydroxybutyric acid relative to R-beta-hydroxybutyric acid.

The invention discloses a selective exchange film sealing concentrated solution based on layered double hydroxides. The selective exchange film sealing concentrated solution comprises divalent metal ions, a corrosion inhibitor, a pH buffering agent and a wetting agent. The invention also discloses a preparation method and application of the compound. The closed thin film obtained based on the layered double-metal hydroxide selective exchange thin film closed concentrated solution has excellent compactness, double protection on the aluminum alloy anode oxide film is achieved through selective exchange of interlayer anions of the closed thin film, and the corrosion resistance of the aluminum alloy anode oxide film is improved and enhanced; and on the premise that the aluminum alloy anode oxide film is protected from being corroded, the alkali resistance of the aluminum alloy anode oxide film is improved and enhanced, and the color fixing performance of the dye is achieved.

The invention discloses positive electrode slurry for preventing formation of gel and a preparation method of the positive electrode slurry. The method comprises the following steps: S1, drying a positive electrode active material under the protection of inert gas; s2, carrying out surface modification by using a functionalized silane coupling agent; s3, drying the conductive agent under a high-temperature vacuum condition; s4, under the protection of inert gas, lithium alkyl sulfonate, a polyhydric alcohol chelating agent and polyvinylidene fluoride are subjected to a reaction to prepare a modified binder; s5, mixing and dispersing the modified active material, the conductive agent, the modified binder and the acidic buffer agent in a low-dew-point drying chamber; s6, performing ultrasonic treatment on the slurry under a vacuum condition; and S7, adding a cross-linked fluorosilane coupling agent, mixing at a low speed and precisely filtering to obtain the anti-gel positive electrode slurry. According to the invention, through a multi-synergistic anti-gel mechanism, the problem that the positive electrode material slurry is easy to form gel is solved, and the prepared slurry has excellent stability, rheological property and coating performance, so that the electrochemical performance of the battery is improved.

The present application relates to a chelated iron desulfurizer, which is composed of a high-price soluble iron salt, a chelating agent, a pH buffer and water, wherein the chelating agent is a compound of sodium polyetheramine tetraacetate and at least one of N,N-diethylcarboxylic acid-based ethylenediamino-3-hydroxysuccinic acid, a polycarboxylic acid chelating agent or an amino acid-derived chelating agent; or the chelating agent is a compound of tetrasodium N,N-diethylcarboxylic acid-based ethylenediamino-3-hydroxysuccinic acid and at least one of sodium polyetheramine tetraacetate, a polycarboxylic acid chelating agent or an amino acid-derived chelating agent. Compared with the existing commonly used desulfurizers EDTA or NTA, the chelating ability of the present application's chelated iron desulfurizer is significantly improved, the iron ion regeneration ability is significantly enhanced, and the desulfurization effect is comparable to EDTA or NTA.

The invention provides a copper-nickel alloy foil and a preparation method and application thereof, and belongs to the technical field of lithium ion battery negative electrode current collectors, and the preparation method comprises the following steps: preparing a copper-nickel composite electrolyte, and adding a coordination agent, a pH buffer agent and an additive into the copper-nickel composite electrolyte to obtain a mixed electrolyte; the coordination agent comprises a main coordination agent and an auxiliary coordination agent, and the main coordination agent comprises at least one of trisodium citrate, potassium sodium tartrate and sodium pyrophosphate; the auxiliary coordination agent comprises at least one of ammonia water, glycine and triethanolamine; and a cathode and an anode are placed in the mixed electrolyte, the pH of the mixed electrolyte is controlled to be 6-10, direct current is applied for electrochemical deposition, and the copper-nickel alloy foil is obtained. According to the method, the alkalescence system is adopted, the main coordination agent and the auxiliary coordination agent are used, full coordination of free Cu < 2 + > and Ni < 2 + > is achieved, precipitation is avoided, the hydrogen evolution phenomenon is greatly reduced, and the alloy foil quality is improved.

The invention relates to a modified acrylic emulsion as well as a preparation method and application thereof. The water-based acrylic resin comprises the following components in percentage by weight: 30 to 40 percent of acrylate monomer and / or methacrylate monomer, 2 to 4 percent of hydroxyl acrylate monomer, 0.2 to 0.8 percent of polymerizable unsaturated acid monomer, 0.4 to 1.5 percent of crosslinking monomer, 0.6 to 0.8 percent of monomer containing N heterocyclic ring, 0.4 to 1 percent of organic silicon monomer, 0.5 to 1.5 percent of polymerizable emulsifier, 0.08 to 0.16 percent of persulfate, 0.02 to 0.08 percent of pH buffering agent, 0.3 to 1 percent of neutralizer and the balance of water. And the balance of deionized water. The water-based bi-component polyurethane wood lacquer prepared from the modified acrylic emulsion provided by the invention has the advantages of good adhesive force on a melamine board, fast hardness increase, very excellent anti-adhesion effect, better water resistance, chemical resistance and stain resistance, and is very suitable for water-based coating of the melamine board.

The invention discloses a preparation method of a vitamin C liposome preparation capable of improving encapsulation efficiency, the vitamin C liposome preparation is prepared by an ethanol injection-high pressure microjet circulation homogenization method, the homogenized liposome is small in particle size and uniform in distribution, and meanwhile, by combining a dialysis purification and buffer agent pH regulation process, the encapsulation efficiency of the vitamin C liposome preparation is improved. The prepared vitamin C liposome preparation can still keep high stability under the condition that cholesterol is not contained, and the problem that in the prior art, a vitamin C liposome preparation is low in encapsulation efficiency is effectively solved.

The present invention provides a detection reagent and a detection method for calcium hardness, magnesium hardness and total hardness of water. The detection reagent comprises a liquid color developing component, a liquid buffer component, a first liquid masking agent component and a second liquid masking agent component. The liquid color developing component comprises a color developing agent that can react with both calcium ions and magnesium ions. The liquid buffer component adjusts the pH value of the color developing reaction to be greater than 12. The first liquid masking agent component is used to mask the calcium ions and magnesium ions in the water quality, and the second liquid masking agent component is used to mask the calcium ions in the water quality. The detection reagent can simultaneously measure the calcium hardness, magnesium hardness and total hardness in the water quality. The detection method has high accuracy, good parallelism, convenience and rapidity, and the detection time of the three indicators of calcium hardness, magnesium hardness and total hardness of a single sample is short.

The invention relates to the technical field of glass cleaning agents, in particular to an environment-friendly cover plate glass cleaning agent and a preparation method thereof. The environment-friendly cover plate glass cleaning agent comprises the following raw materials in percentage by weight: 12-20% of inorganic base, 8-12% of a surfactant, 5-8% of a chelating agent, 3-5% of a humectant, 1-3% of an adsorbent, 1-3% of a dispersing agent, 0.3-1% of a buffering agent and the balance of deionized water, the surfactant is dodecyl glucoside and dodecyl ethyoxyl sulphobetaine, and the weight range ratio of the dodecyl glucoside to the dodecyl ethyoxyl sulphobetaine is (3-1): 1; the chelating agent is one or more of sodium gluconate, sodium polyaspartate and sodium polyepoxysuccinate. According to the present invention, the degradable surfactant and the degradable chelating agent are adopted, and the dispersant is added to modify the nanometer titanium dioxide, such that the low pollution property is achieved while the high decontamination efficiency and the anti-fingerprint ability are considered.

The present invention provides a sulfur autotrophic denitrification filler and a preparation method thereof. The sulfur autotrophic denitrification filler of the present invention comprises the following raw materials in parts by weight: 50-100 parts of sulfur powder, 5-20 parts of pH buffer, 10-50 parts of medical stone, and 0-10 parts of additives; wherein the pH buffer is one or more of sodium carbonate, sodium bicarbonate, sodium hydroxide, and potassium hydroxide; and the additive is one or more of amide substances and epoxy resins. The sulfur autotrophic denitrification filler has good filler strength and a long service life, and can be conducive to the attachment of denitrifying thiobacillus to the surface of the sulfur autotrophic denitrification filler, thereby increasing the microbial concentration per unit volume of the filler and increasing the reaction rate.

The present invention relates to a highly concentrated, stable pharmaceutical formulation of a pharmaceutically active anti-HER2 antibody, such as e.g. Trastuzumab (HERCEPTIN™), Pertuzumab or T-DM1, or a mixture of such antibody molecules for subcutaneous injection. In particular, the present invention relates to formulations comprising, in addition to a suitable amount of the anti-HER2 antibody, an effective amount of at least one hyaluronidase enzyme as a combined formulation or for use in form of a co-formulation. The formulations comprise additionally at least one buffering agent, such as e.g. a histidine buffer, a stabilizer or a mixture of two or more stabilizers (e.g. a saccharide, such as e.g. α,α-trehalose dihydrate or sucrose, and optionally methionine as a second stabilizer), a nonionic surfactant and an effective amount of at least one hyaluronidase enzyme. Methods for preparing such formulations and their uses thereof are also provided.

The invention provides N-Fe co-doped biochar, a preparation method and application of the N-Fe co-doped biochar in production of medium-chain carboxylic acid by anaerobic digestion. The preparation method comprises the following steps: S1, pretreating a nitrogen-rich biomass raw material; s2, pyrolyzing and carbonizing the pretreated nitrogen-rich biomass raw material to obtain N-doped biochar; s3, adding FeCl3. 6H2O, a stabilizer, a buffer agent and N-doped biochar into an organic solvent, and uniformly mixing to obtain a mixed solution; s4, performing microwave-assisted solvent heat treatment on the mixed solution to obtain a precursor mixed solution; and S5, carrying out centrifugal washing on the precursor mixed solution, filtering, and drying to obtain the N-Fe co-doped biochar. On one hand, the required nitrogen element is obtained by using the nitrogen-rich biomass raw material, and the use of an exogenous nitrogen-containing material is avoided; on the other hand, the biochar is kept in a good dispersion state in a solution through microwave solvent heat treatment, agglomeration of particles is avoided, the electrical conductivity, the thermal conductivity and the mechanical strength of the biochar are improved, and the N-Fe co-doped biochar can also be used for producing medium-chain carboxylic acid through anaerobic digestion.

The invention discloses a kind of high-efficiency and environment-friendly developer for PCB board, and the developer includes the following components by mass: 60-100 parts of organic alkali composition; 30-80 parts of cosolvent; 30-70 parts of defoamer; 40-70 parts of surfactant; 20-50 parts of antioxidant; 15-45 parts of penetrant; 30-50 parts of buffer; 10-20 parts of inhibitor; The invention also discloses a preparation process of high-efficiency and environment-friendly developer for PCB board. The present invention develops PCB board by using organic alkali composition, fully dissolves dry film by ether group, hydroxyl group and amine group, avoids solid precipitation caused by traditional carbonate development, thereby effectively improving the efficiency and quality of PCB development process; penetrant and cosolvent are added at the same time, significantly improving the penetration and dissolution effect of developer on dry film, further improving development efficiency; and with the antioxidant, buffer etc. added therein, the antioxidant capacity of developer and PCB board can be improved, and the stability of developer during use is ensured.

The invention discloses an aluminum etching solution and a preparation method and application thereof, the aluminum etching solution is composed of the following raw materials in percentage by mass: 55-75% of phosphoric acid, 1.5-8.5% of nitric acid, 2-10% of glacial acetic acid, 1-6% of an additive and the balance of deionized water, and the additive is composed of a surfactant accounting for 0.005-1% of the total mass of the aluminum etching solution and a buffering agent accounting for 1-5% of the total mass of the aluminum etching solution; all the raw materials can be used for etching aluminum-silicon-copper after being uniformly mixed, and the method has the advantages that the lateral erosion amount is small, the etching depth-to-width ratio can reach 2.23 or above, meanwhile, the etching taper angle is large, the etching rate is controlled between 5800-6200 / min, and the requirement of the market for the etching rate can be met.

The present invention relates to a highly concentrated, stable pharmaceutical formulation of a pharmaceutically active anti-HER2 antibody, such as e.g. Trastuzumab (HERCEPTIN™), Pertuzumab or T-DM1, or a mixture of such antibody molecules for subcutaneous injection. In particular, the present invention relates to formulations comprising, in addition to a suitable amount of the anti-HER2 antibody, an effective amount of at least one hyaluronidase enzyme as a combined formulation or for use in form of a co-formulation. The formulations comprise additionally at least one buffering agent, such as e.g. a histidine buffer, a stabilizer or a mixture of two or more stabilizers (e.g. a saccharide, such as e.g. α,α-trehalose dihydrate or sucrose, and optionally methionine as a second stabilizer), a nonionic surfactant and an effective amount of at least one hyaluronidase enzyme. Methods for preparing such formulations and their uses thereof are also provided.

The invention relates to the technical field of hair dyes, and particularly discloses a mild hair dye capable of coloring quickly and a preparation method of the mild hair dye. The hair dye comprises an agent A and an agent B. The agent A comprises glycerin, cetostearyl alcohol, myristyl alcohol, flaxseed gum, a stevia rebaudiana extract, tea tree oil, fructo-oligosaccharide, a surfactant, an oxidation dye, a chelating agent, an antioxidant, an emulsifier, grease, a hair conditioner, essence, a pH regulator and water. The agent B comprises cetostearyl alcohol, an emulsifier, grease, glycerol, a chelating agent, a buffering agent, hydrogen peroxide, a stabilizer and water. The hair dye disclosed by the invention can shorten the hair dyeing time, so that the retention time of the hair dye on scalp and hair is shortened, and the irritation and damage of the hair dye to the scalp and the head are reduced.

The invention relates to the technical field of biomass energy utilization, in particular to a method for producing biogas by biomass fermentation, which comprises the following steps: pretreating raw materials, collecting agricultural wastes, forestry residues, organic household garbage and other biomass raw materials, sorting and crushing the biomass raw materials until the particle size is 1-3mm, putting the biomass raw materials into a soaking pool and adding biogas slurry for soaking, adding a compound enzyme preparation, and stirring and soaking for 12-24 hours at 30-40 DEG C; draining the pretreated raw materials, inoculating microbial flora, and transferring into an anaerobic fermentation tank; in the initial stage of fermentation, the temperature in the tank is 28-32 DEG C, the pH value is 6.5-7.0 and is kept anaerobic, after the gas production rate is increased, the temperature is adjusted to 35-38 DEG C, the pH value is 7.0-7.2, and a buffering agent is added in good time. According to the method, the biomass raw materials are subjected to fine pretreatment, so that complex organic components in the biomass raw materials can be fully decomposed, more organic matters which are originally difficult to utilize by microorganisms are converted into fermentable substrates, the gas production efficiency is remarkably improved, and compared with a traditional method, the biogas yield can be remarkably increased.

The invention relates to the technical field of nutrient element extraction, and discloses a step-by-step extraction method of organic selenium in natural selenium-rich agricultural products, which comprises the following steps: cleaning, drying and crushing the natural selenium-rich agricultural products into fine powder; then sequentially using an aqueous solution containing a buffer agent, low-concentration ethanol and a high-concentration organic solvent for ultrasonic-assisted extraction to respectively obtain water-soluble, hydrophilic, hydrophobic and fat-soluble organic selenium compounds; and finally, combining the extracting solutions in the steps, and carrying out rotary evaporation concentration and purification treatment to obtain the high-purity organic selenium compound. Through a step-by-step extraction method, different types of organic selenium compounds in natural selenium-rich agricultural products are efficiently extracted by using the aqueous solution, the low-concentration ethanol and the high-concentration organic solvent respectively under low-temperature and mild conditions, so that high purity and biological activity are kept, meanwhile, the process flow is simplified, and the production cost is reduced. The energy consumption and the use of organic solvents are reduced, the environmental pollution is reduced, and the method is suitable for large-scale industrial production.

The invention discloses eye drops containing L-ergothioneine and a preparation method of the eye drops. The eye drops are prepared from the following components in parts by weight: 0.0015 to 15 parts of L-ergothioneine, 0.001 to 0.01 part of a bacteriostatic agent, 0.05 to 15 parts of a buffering agent and the balance of normal saline, and the pH value of the eye drops is 5.0 to 7.0. Experiments show that L-ergothioneine can prevent and reverse denaturation of crystalline lens protein, the prepared eye drops containing L-ergothioneine can prevent and reduce opacity of crystalline lens protein, and the prevention and treatment effects on cataract are better than those of existing eye drops.

An antiperspirant active composition of high efficacy includes aluminum dichlorohydrate (ADCH), a buffering agent, and a calcium salt. The buffering agent may be an amino acid, such as glycine. The composition has an aluminum to chloride (Al:Cl) molar ratio ranging from 0.91 to 1.25 and a size exclusion chromatography HPLC peak 4 of at least 30% and peak 5 of at least 10%.

The invention belongs to the technical field of biomedicine, and particularly relates to a paris polyphylla exosome, a preparation method thereof and application of the paris polyphylla exosome in treatment of psoriasis, in the method, fresh paris polyphylla rhizomes are cleaned and washed with a buffering agent, the washed paris polyphylla rhizomes and the buffering agent are mixed according to the mass ratio of 1: (1.5-2.5), after mixing, crushing and filtering are conducted, and the paris polyphylla exosome is obtained; the preparation method comprises the following steps: extracting paris polyphylla from paris polyphylla to obtain a paris polyphylla crude extract for later use, carrying out differential centrifugation on the paris polyphylla crude extract, taking supernate and concentrating to obtain an exosome crude extract, sequentially adding the exosome crude extract into cane sugar with the concentration of 15%, 30%, 45% and 60%, and carrying out cane sugar gradient purification to obtain the paris polyphylla exosome. The paris polyphylla exosome is in the shape of a cup-shaped circle and has a complete double-layer membrane structure, the protein concentration is 3.5-4.5 ug / ml, the particle size is 100-200 nm, and the paris polyphylla exosome is beneficial to improvement of psoriasis, is good in curative effect and fast in effect taking, and has high economical efficiency and safety.

The invention relates to the technical field of OLED (Organic Light Emitting Diode) manufacturing process etching processes, in particular to a silver etching solution for an OLED manufacturing process as well as a preparation method and application of the silver etching solution. The silver etching liquid comprises nitric acid, phosphoric acid, a buffer agent, a metal ion chelating agent and an ionic liquid inhibitor, the ionic liquid inhibitor comprises 1-butyl-3-methylimidazole phosphate, the metal ion chelating agent is selected from at least one of pyromellitic acid, diethylenetriamine pentaacetic acid and ethylenediamine tetramethylene phosphoric acid, and the buffer agent is selected from at least one of sodium chloride, sodium chloride and sodium chloride. The buffering agent comprises acetic acid, and all the components are prepared according to a specific mass ratio. The etching solution can balance the etching rate of silver and indium tin oxide, avoid silver residues and black spot defects, prolong the service life of the solution, reduce the use of a volatile buffer agent, adapt to the OLED fine manufacturing process, improve the product yield and reduce the production cost, and is suitable for etching of a metal substrate in the OLED manufacturing process.

According to the method for preparing the nanocrystalline nickel foil through the electro-deposition method and the nanocrystalline nickel foil prepared through the method, a nickel plate serves as an anode, a titanium plate serves as a cathode, the anode and the cathode are both placed in electrolyte, and the nanocrystalline nickel foil is prepared on the titanium plate through electro-deposition by adopting a pulse power source; the electrolyte comprises water and the following components by concentration: 300-500g / L of nickel sulfate; 5-15 g / L of nickel chloride; 0.01 to 0.2 g / L of a wetting agent; 20-60 g / L of a buffer agent; 0.05-2 g / L of a brightener; the pH value of the electrolyte is 2-4, and the electro-deposition temperature is 40-60 DEG C; the buffering agent is selected from one or two of citric acid and sodium citrate; and the brightener is selected from one or more of butynediol propoxide, butynediol ethoxylate, sodium sulfopropyne ether, propynol ethoxylate and glycerol monopropyne ether. Based on the method, the problem that in the prior art, the nickel foil prepared through an electro-deposition method is large in fine grain size is solved.