3231 results about "Oil phase" patented technology

The invention relates to the field of oil exploitation, and discloses a polymer with a heavy oil cold recovery function as well as a preparation method and application thereof. After the polymer disclosed by the invention enters a stratum, hydrophobic groups on a polymer chain can be adsorbed on an oil-water interface, the aggregation state of micelles is destroyed, the size of the micelles is greatly reduced, and released energy can provide energy required by emulsification. And meanwhile, after the amphiphilic groups are adsorbed to an oil-water interface, the tension of the oil-water interface is reduced, a low-surface-tension oil phase is automatically diffused to a high-surface-tension water phase, and spontaneous permeation emulsification viscosity reduction of the thick oil is realized without external force or under the low-power condition by virtue of the Malangori effect.

The invention discloses a self-crosslinking temperature-resistant salt-resistant emulsion type fracturing fluid thickening agent and a preparation method thereof, and belongs to the technical field of oilfield chemistry. The raw materials adopted by the invention comprise 30 to 50 parts of an oily solvent, 15 to 25 parts of deionized water, 10 to 20 parts of acrylamide, 5 to 10 parts of acrylic acid, 2 to 4 parts of 2-acrylamido-2-methylpropanesulfonic acid, 0.05 to 0.2 part of a crosslinking monomer, 0.5 to 1 part of a quaternary ammonium salt type hydrophobic association monomer, 4 to 8 parts of an emulsifier and 1 to 2 parts of a phase inversion agent. The self-crosslinking emulsion is formed through water phase-oil phase mixing, high-speed emulsification, low-temperature initiation polymerization and phase inversion treatment. Based on physical-chemical double-crosslinking temperature control cooperation, a salt-resistant-hydrophobic double-shielding mechanism and an integrated design without an exogenous crosslinking agent, the contradiction between the temperature-resistant and salt-resistant performance of a traditional thickening agent and the process complexity is broken through, and a technical support is provided for efficient development of high-temperature and high-salt oil and gas reservoirs.

The invention provides water-in-oil type emulsion gel loaded with probiotics and a preparation method of the water-in-oil type emulsion gel, and belongs to the technical field of probiotic products, the water-in-oil type emulsion gel loaded with the probiotics comprises a water phase and an oil phase, and the internal water phase is composed of gel and probiotic suspension; and the external oil phase consists of edible oil, a lipophilic emulsifier and at least one oil gelator. According to the water-in-oil emulsion gel, the stability of entrapped probiotics can be remarkably improved, meanwhile, the activity of the entrapped probiotics in the processing, storage and digestion processes is improved, particularly, the normal-temperature storage time is prolonged by 3 months, and a scientific basis is provided for normal-temperature food development.

The application belongs to the technical field of daily chemical industry, and particularly relates to an emulsion and a preparation method thereof. The emulsion provided in the application comprises an emulsifier, glycerol, oil-phase active substance, pentaerythritol tetra(ethylhexanoate) and water; the emulsifier is a lipopeptide; the weight percentage of the lipopeptide and the glycerol is not less than 3%; the weight ratio of the oil-phase active substance and the pentaerythritol tetra(ethylhexanoate) is 1:3-10; the ratio of the sum of the weights of the lipopeptide and the glycerol to the sum of the weights of the oil-phase active substance and the pentaerythritol tetra(ethylhexanoate) is 1:3-10; and the ratio of the sum of the weights of the lipopeptide, the glycerol, the oil-phase active substance and the pentaerythritol tetra(ethylhexanoate) to the weight of the water is 1:1-4. The emulsion is prepared by using sodium bacillomycin, glycerol and pentaerythritol tetra(ethylhexanoate), can effectively inhibit the diffusion of the oil-phase active substance at the interface of the emulsion, reduce the oxidative degradation of the oil-phase active substance, and greatly prolong the effective action time of the oil-phase active substance in the emulsion.

The invention relates to an oral mucosa repairing medicine and a preparation method thereof, and belongs to the technical field of medicines, the medicine comprises barnacle peptide, salivary lactobacillus, resveratrol, a biphasic adhesion matrix, hydroxyapatite, vitamin B family and other components. The preparation method comprises the following steps: sequentially carrying out enzymolysis on barnacle gooseneck by pepsin and lumbrukinase to obtain barnacle peptide. The double-phase adhesion matrix comprises a water-phase matrix, an oil-phase matrix and lecithin; the water-phase matrix contains a chondroitin sulfate-chitosan quaternary ammonium salt compound, sodium alginate and other components; the oil-phase matrix comprises sesame oil, beeswax, a polylactic acid-glycolic acid copolymer and the like. According to the invention, barnacle peptide and salivary lactobacillus are prepared by adopting a special method and are matched with resveratrol for use, so that multi-target and multi-path promotion of oral mucosa repair can be realized; the chondroitin sulfate-chitosan quaternary ammonium salt compound is prepared through electrostatic and physical embedding, the chondroitin sulfate-chitosan quaternary ammonium salt compound is matched with other components to prepare the biphasic adhesion matrix, the biocompatibility is good, the adhesion is high, and the action time of a sustained-release drug is well prolonged.

The invention discloses an ultra-low-density high-strength resin proppant capable of being carried by clear water or low-viscosity slickwater. The proppant is prepared by dispersing, polymerizing and curing a mixture comprising 15 to 50 weight percent of vinyl monomer, 5 to 10 weight percent of acrylate monomer and 50 to 70 weight percent of unsaturated resin. The preparation method comprises the following steps: controlling the resin composition in a water phase by virtue of a dispersing agent and a rotating speed to form spherical liquid drops with the particle size of 12-140 meshes and the sphericity of nearly 100%; then, the temperature ranges from 30 DEG C to 80 DEG C; the propping agent provided by the invention has ultra-low density, can be carried by clear water or low-viscosity slickwater, is suitable for low-viscosity fracturing fluid, low-displacement construction and small-scale fracturing, can realize ultra-far-end seam net support, and greatly increases the oil and gas drainage area. The breaking rate under the closing pressure of 20-90 MPa is lower than 2%, the surface is weakly lipophilic, and the oil-phase flow conductivity is higher than the water-phase flow conductivity.

The invention relates to the field of hydrogel materials, in particular to a preparation process of intragastric volume hydrogel, a product and application. The preparation process comprises the following steps: S1, preparing a KGM filtrate: adding konjaku flour into an acid solution for swelling, performing high-temperature treatment after swelling, and then adding an alkali solution to terminate the reaction to obtain the KGM filtrate; s2, preparing an oil phase mixture; s3, preparing KGM particles: mixing the oil phase mixture and the KGM filtrate, stirring and emulsifying, and then adding a cross-linking agent for cross-linking reaction to obtain the KGM particles; s4, hydrogel preparation: washing the KGM particles, and freeze-drying to obtain KGM microspheres, namely a hydrogel product. According to the invention, the konjac flour is selected as a main raw material to prepare the intragastric volume hydrogel particles, and the obtained product has good hydrophilicity, different swelling characteristics and an adjustable degradation period, can prolong the emptying time of the hydrogel in the stomach, and has a wide application prospect.

The utility model discloses reaction equipment with high crude methyl ester yield, which comprises a stirring kettle and a material circulating system, the material circulating system comprises a circulating pump, a spray pipe arranged in the stirring kettle and a mixing nozzle arranged on the spray pipe, and a bottom outlet of the stirring kettle is connected with a feed port of the circulating pump through a first pipeline. An outlet of the circulating pump is connected with the spray pipe through a second pipeline; the mixing nozzle comprises a first sprayer and a second sprayer, and an outer flaring in the lower portion of the second sprayer is in clearance fit with the conical head through a connecting piece. The material circulating system can realize bottom-out and top-in of materials, so that the mixing of an oil phase and an enzyme water phase is promoted through the reciprocating circulation. In addition, the material circulating system is provided with a plurality of mixing nozzles, the flow speed of spraying of the first spray head is large, so that a negative pressure suction gap is formed at the joint of the second spray head and the first spray head, materials in the stirring kettle can enter the mixing nozzles under the action of negative pressure, an oil phase and an enzyme water phase are intensively mixed, and the yield of fatty acid methyl ester is improved.

The invention discloses an integrated oil phase emulsion explosive and a preparation method thereof. The emulsion explosive is prepared from the following raw materials: a water-phase component, an oil-phase component and an emulsifier for emulsifying the water-phase component and the oil-phase component, wherein the water-phase component contains a modified oxidant formed by loading a nitrate oxidant component on p-aminophenyl POSS (Polyhedral Oligomeric Silsesquioxane); the preparation process of the modified oxidizing agent comprises the following steps: A, fully dispersing a nitrate oxidizing agent component and p-aminophenyl POSS in an aqueous solution, so that the nitrate oxidizing agent component is fully attached to the p-aminophenyl POSS; and B, separating a solid-phase component, namely the modified oxidant, from the solution system obtained in the step B. According to the integrated oil phase emulsion explosive and the preparation method thereof provided by the invention, the sensitivity and the power can be well considered.

The invention belongs to the field of nano preparations, and discloses a preparation method of nano microspheres coated with a nicotinamide mononucleotide shell membrane structure, which comprises the following steps: coating NMN in a pregel formed by chitosan and sodium tripolyphosphate, heating and stirring, adjusting the pH value to separate out chitosan-coated nano microspheres, drying to remove moisture on the surfaces of the nano microspheres, and drying to obtain the nano microspheres coated with the nicotinamide mononucleotide shell membrane structure. Then selecting a water phase and an oil phase in a proper proportion, preparing a chitosan / sodium alginate composite nano-microsphere with sodium alginate as an outer membrane by adopting an emulsion cross-linking method, and washing and drying to obtain the NMN nano-microsphere with a core-shell structure. According to the invention, NMN is coated in the nano-microsphere which is composed of two materials and has a nuclear membrane structure, so that the stability of NMN in a natural environment can be improved, hydrolysis of NMN by gastric acid and gastrointestinal tract enzyme in a drug delivery process can be prevented, the bioavailability of NMN is improved, and a drug sustained release effect is achieved.

The utility model belongs to the technical field of recovery of coking chemical products in the metallurgical coking industry, and particularly relates to a crude benzene oil-water separation integrated device which is characterized by comprising an oil-water separation area, an oil phase collection area and a water phase collection area, and a partition plate is annular and defines the oil-water separation area in the middle and the oil phase collection area surrounding the oil-water separation area; a crude benzene diversion weir is arranged between the periphery of the top of the partition plate and the oil phase collecting region; a flow guide expansion head and a flow guide baffle are arranged at the bottom of the inlet liquid guide pipe, and a dispersion flow channel in the transverse circumferential direction is formed between the flow guide expansion head and the flow guide baffle; a drainage pipe at the bottom of the oil-water separation area is provided with a diversion collector for transversely draining and collecting separated water from the periphery. The crude benzene oil-water separation device has the beneficial effects that the existing crude benzene oil-water separation process is improved, oil-water separation and reflux are integrated, and the equipment integration device saves the occupied area, simplifies the process flow and is convenient to operate and maintain.

The invention relates to the technical field of membrane separation, in particular to a high-flux high-salt rejection rate reverse osmosis membrane as well as a preparation method and application thereof. The preparation method comprises the following steps: sequentially contacting a porous base membrane with a water phase solution and an oil phase solution to generate an interfacial polymerization reaction to form a primary reverse osmosis membrane, and sequentially contacting the primary reverse osmosis membrane with a nitrous acid or salt solution thereof and a hydrosulfite solution to obtain the reverse osmosis membrane with high flux and high salt rejection rate, the water-phase solution contains a water-phase cosolvent, and the oil-phase solution contains an oil-phase cosolvent. According to the preparation method, cosolvents are creatively added into a water-phase solution and an oil-phase solution in an interfacial polymerization reaction process to regulate and control the microstructure of a polyamide layer, and a diazo reaction promotes further crosslinking of residual aniline groups, so that in-situ densification regulation and control of a polyamide network structure are realized; the trade-off effect of the water flux and the salt rejection rate of the traditional reverse osmosis membrane is successfully broken through.

The invention relates to the technical field of microcapsule encapsulation, and a novel preparation method is adopted to prepare microcapsule perfume. The microcapsule takes natural gelatin and paraffin as composite wall materials, a gradient structure is formed by optimizing the mass ratio (1: 2.5-1: 3.75), the gelatin provides mechanical support, and the paraffin endows hydrophobicity and thermal control release characteristics. Dissolving a solution in which the mass volume ratio of gelatin to water is (1: 2.5)-(1: 3) under an ultrasonic condition; mixing the molten paraffin with the liquid spice and the emulsifier to form an oil phase; the oil phase and the gelatin solution are mixed through magnetic stirring at the rotating speed larger than or equal to 800 rpm till the solid phase and the liquid phase are completely fused; after cooling and curing, separating to obtain the solid microcapsule. And when the temperature reaches the melting point (45-65 DEG C) of paraffin, the wall material is molten and quickly releases the perfume, and the slow release performance is excellent at normal temperature. The material is wide in application field and high in compatibility, and has the advantages of being green, safe, high in environmental stability and controllable in trigger release.

The invention relates to the technical field of water treatment, in particular to a reverse osmosis membrane and a preparation method thereof. The preparation method of the reverse osmosis membrane comprises the following steps: soaking a base membrane in a water phase solution, taking out the base membrane, drying the surface of the base membrane, coating the base membrane with an oil phase solution, carrying out interfacial polymerization reaction, curing, coating with a modifier solution, and drying to obtain the reverse osmosis membrane, the modifying agent comprises 2, 4, 6-tri (4-aminophenyl)-1, 3, 5-triazine-1, 3, 5-tri (4-methyl phenyl) benzene. The successfully grafted COFs can improve the water permeability of the membrane to a certain extent, and also can improve the pollution resistance, acid resistance and oxidation resistance of the membrane, so that the service life of the membrane is prolonged. According to the invention, different effects of the same type of imino COFs introduced to the reverse osmosis membrane are further compared, so that the excellence of the selected imino COFs is highlighted.

The invention discloses a water-in-oil emulsion, a preparation method, application, a membrane and a cosmetic product containing the same. The water-in-oil emulsion is prepared from the following components in parts by weight: 0.25 to 50.00 parts of water phase, 0.45 to 80.00 parts of oil phase, 0.025 to 5.00 parts of emulsifier, 1 part of sterol and / or sterol derivative, 0.01 to 30.0 parts of powder and 0 to 3 parts of polymer. The water-in-oil emulsion disclosed by the invention can form a liquid crystal structure which is regularly and orderly arranged in space according to a certain direction, has low film forming continuity, hydrophobicity, flexibility of a wax film and excellent air permeability, and also has certain migration resistance of a high-molecular polymer film, but the brittleness is improved. In addition, the brittleness of a layer of uniform and continuous three-dimensional network structure film formed on the skin by the polymer can be improved, and the flexibility and uniformity are improved.

The present invention relates to the field of water treatment technology, and more particularly to a kind of reverse osmosis membrane and preparation method thereof.The preparation method of the reverse osmosis membrane includes:Basement membrane is soaked in aqueous phase solution, after taking out surface drying, oil phase solution is coated on basement membrane and carries out interfacial polymerization reaction, after solidification, coating modifier solution, after drying, obtain reverse osmosis membrane;The modifier includes 2,4,6-tris (4-aminophenyl) ‑1,3,5-triazine ‑1,3,5-tris (4-methylphenyl) benzene.The COFs successfully grafted by the present invention can improve the water permeability of membrane to a certain extent, and can also improve the anti-pollution property, acid resistance and oxidation resistance of membrane, and then improve the service life of membrane.The present invention further compares the different effects that the same type of imino COFs are introduced into reverse osmosis membrane, so as to highlight the excellence of the imino COFs selected by the present invention.

The invention provides a 180 DEG C-resistant microcapsule type cementing wall-fixing agent for water-based drilling fluid as well as a preparation method and application thereof, and belongs to the technical field of drilling. The preparation method of the wall fixing agent comprises the following steps: (1) respectively adding the macromolecular hydrophilic colloid and the emulsifier into deionized water, and stirring until the macromolecular hydrophilic colloid and the emulsifier are completely dissolved to obtain a water phase; (2) adding phenolic resin, the MUF prepolymer solution and nano SiO2 into an organic solvent under a stirring condition, and uniformly stirring to obtain an oil phase; (3) adding the oil phase obtained in the step (2) into the water phase obtained in the step (1), and carrying out shear emulsification to obtain an oil-in-water emulsion; and evaporating to remove the organic solvent in the system, filtering, washing, and drying to obtain the product. Under the multi-element synergistic effect of hydrogen bonds or coordinate bonds, Van der Waals force and the like, the microcapsule type cementing wall-fixing agent can accelerate the interface to form a compact cemented network structure, the cementing strength of rock particles is remarkably improved, and the purpose of strengthening the stability of a well wall is achieved.

The invention relates to the technical field of pharmaceutical preparations, in particular to a multiple nano emulsion adjuvant and a preparation method thereof. The multiple nano emulsion adjuvant is prepared from 2.73 to 6.37 g of an oil phase matrix based on 100 g of a raw material system, 0.10 to 0.25 g of a sterol compound; 0.212 to 0.424 g of a nonionic surfactant; 0.00050 to 0.00200 g of a triterpenoid saponin type active adjuvant; 0.010 to 0.020 g of an anionic polymer modifier; 0.005 to 0.015 g of a cationic polymer modifier; 70-90 g of a buffer solution; the total mass of the raw materials is 100 g. The nano emulsion adjuvant prepared by the invention can be stored for 6 months at 2-8 DEG C under a low sterol condition, the particle size change does not exceed + 5%, no crystallization or layering is generated, and the stability of the active adjuvant is remarkably improved.

The invention relates to the technical field of membrane separation, in particular to a preparation method of a pH-step-by-step thermocuring regulation sodium-magnesium separation nanofiltration membrane. The method comprises the following steps: (1) pre-treating a base membrane; (2) preparation and treatment of an aqueous phase solution: S1, preparing the aqueous phase solution according to mass fraction: sequentially adding 1.2%-1.6% of piperazine, 0.10%-0.14% of triaminopyrimidine and 0.14%-0.18% of polyethylene glycol into deionized water, and stirring until the piperazine, the triaminopyrimidine and the polyethylene glycol are completely dissolved to form the aqueous phase solution; s2, adjusting the pH value of the water-phase solution to 10-11 by using hydrochloric acid; s3, pouring the water-phase solution of which the pH is adjusted on the surface of the pretreated base membrane, standing, and blow-drying to form a uniform water-phase layer; (3) interfacial polymerization reaction: S1, preparing an oil phase solution: adding 0.10-0.14% of trimesoyl chloride into n-hexane, and performing ultrasonic treatment until the trimesoyl chloride is completely dissolved; s2, pouring the oil-phase solution on the surface of the base membrane subjected to water-phase treatment, and after reaction, pouring out redundant solution to form a polyamide separation layer, so as to obtain a membrane sheet; (4) performing a step-by-step thermocuring process; and (5) cleaning and storing.

The invention belongs to the technical field of grease preparation, and particularly relates to a preparation method and application of diglyceride oil with a weight reducing effect. Comprising the following steps: firstly, adding grease into a basic nutrient solution, adding strains for fermentation, and filtering to obtain a glycolysis product; adding glycerol into the glycolysis product, carrying out lipase esterification reaction, and carrying out centrifugal separation to obtain an oil phase; the method comprises the following steps: degrading triglyceride by adopting dominant strain fermentation, then adding glycerol, and carrying out esterification reaction under the action of dominant compound lipase to obtain the diglyceride oil. According to the method, the 1, 3-diglyceride can be selectively generated, the proportion of dominant grease of the 1, 3-diglyceride can be increased, and research shows that the prepared diglyceride oil has good weight reduction and fat reduction effects and has a good application prospect.

The present invention relates to the technical field of nanofiltration membranes, and particularly relates to a high-temperature resistant nanofiltration membrane and a preparation method thereof. The nanofiltration membrane is prepared by this method. The method includes preparing a nano-layer; coating a CHO-SiO2 nano-particle solution with a required mass concentration on the surface of a porous support layer to form a base membrane containing the nano-layer; preparing a high-temperature resistant nanofiltration membrane; immersing the base membrane in an aqueous solution, taking out the base membrane after the first immersion treatment and air-drying the water droplets on its surface; secondly, immersing the base membrane in an oil-phase solution, taking out the base membrane after the second immersion treatment and performing a drying treatment to obtain a high-temperature resistant nanofiltration membrane; the aqueous solution includes polyamine, an acid absorbent, inorganic salts and a first organic solvent; the polyamine is a bis-benzene N-heterocyclic derivative; the oil-phase solution includes polyacyl chloride. The present invention can solve the problem that the directly introduced nano-particles are liable to fall off after film formation in the prior art.

The invention relates to the technical field of functional materials, in particular to a chitosan nanocapsule as well as a preparation method and application thereof. The preparation method of the chitosan nanocapsule comprises the following steps: (a) mixing and emulsifying a chitosan solution, an oil-in-water emulsifier and essential oil to form an oil-in-water emulsion, adding an aqueous solution of sodium tripolyphosphate into the oil-in-water emulsion, and stirring to obtain a first mixture; (b) adding the first mixture into an oil phase solvent containing a water-in-oil emulsifier, and stirring to obtain a multiple emulsion; and (c) adding an aqueous solution of a dialdehyde cross-linking agent into the multiple emulsion, carrying out a cross-linking reaction, collecting a solid-phase substance, and drying. The physical / chemical double-crosslinking chitosan nanocapsule is obtained by utilizing physical crosslinking between the chitosan and the sodium tripolyphosphate and chemical crosslinking between the chitosan and the binary aldehyde crosslinking agent, so that the encapsulation efficiency and the encapsulation efficiency of the nanocapsule are remarkably improved; meanwhile, the nanocapsule also has pH responsiveness and has a slow release effect after pH response.

The invention belongs to the technical field of functional finishing of textiles, and particularly relates to microcapsule emulsion with a pH indicating function, preparation of the microcapsule emulsion and application of the microcapsule emulsion in a textile finishing agent. The invention provides a preparation method of a microcapsule emulsion with a pH indication function, which comprises the following steps: reacting isocyanate with polyol to obtain a polyurethane prepolymer, mixing and dissolving the polyurethane prepolymer with a pH indicator solution, an acrylate monomer and an initiator to obtain an oil phase, and taking an aqueous solution of a polymer emulsifier as a water phase; then mixing and emulsifying the oil phase and the water phase, adding a chain extender, heating to carry out chain extension reaction, cross-linking to a certain degree to form a polyurethane-polyurea-polyacrylate hybrid shell layer on an oil-water interface, and coating a core material pH indicator to obtain the microcapsule emulsion with the pH indication function. According to the invention, the pH indicator is coated in the form of microcapsules for the first time, and industrial production and processing can be carried out.

The invention provides a composite nanofiltration membrane as well as a preparation method and application thereof, and the preparation method comprises the following steps: reacting a water phase solution and an oil phase solution on the surface of a base membrane to obtain a primary composite nanofiltration membrane; wherein the water phase solution contains piperazine and polyacrylamide, and the oil phase solution contains trimesoyl chloride. The nanofiltration membrane provided by the invention is high in pure water flux, good in membrane surface hydrophilicity, strong in pollution resistance, high in mechanical strength and durability, low in cost and capable of stably running for a long time.

The invention provides efficient gelatin hemostatic microspheres as well as a preparation method and application thereof, the preparation method comprises the following steps: mixing a gelatin solution with a tannic acid solution, and uniformly stirring to obtain a tannic acid modified gelatin aqueous solution; uniformly mixing span-80 with liquid paraffin to obtain an oil phase; adding the tannic acid modified gelatin aqueous solution into an oil phase, and uniformly stirring to obtain a mixed solution; the mixed solution is subjected to a cross-linking reaction under the ice bath condition, after the cross-linking reaction is completed, a reaction solution and acetone are mixed, liquid paraffin is removed after standing, and the tannic acid modified hemostatic microspheres are obtained after drying; mixing the tannic acid modified hemostatic microspheres with an adsorbent, and dehydrating to obtain the gelatin hemostatic microspheres. The prepared gelatin hemostatic microspheres can be attached to the surface of tissue and have the effects of high water absorption and rapid hemostasis.

The invention belongs to the technical field of oilfield auxiliaries, and particularly relates to an oil-soluble demulsifier for a heavy oil field and a preparation method of the oil-soluble demulsifier. The oil-soluble demulsifier for the heavy oil field, provided by the invention, is prepared from a block polymer emulsion, nonylphenol polyoxyethylene ether, modified nanoparticles and a cross-linking agent. According to the invention, methoxystyrene, dodecyl vinyl ether, N, N-dimethylaminopropyl acrylamide and 2-acrylamide-2-methylpropanesulfonic acid are adopted to prepare a quaternary block comb-shaped polymer, the quaternary block comb-shaped polymer and nonylphenol polyoxyethylene ether are subjected to molecular-level cross-linking through a cross-linking agent, nano modified particles are added, and the quaternary block comb-shaped polymer is prepared. The prepared demulsifier can be rapidly adsorbed on an oil-water interface and respectively adsorb an oil phase and a water phase, so that the tension of the oil-water interface is reduced, rapid separation of the oil phase and the water phase is realized, and the demulsification performance is improved.

The invention relates to composite vegetable oil microcapsule powder and a preparation method thereof, and belongs to the technical field of biology. The composite vegetable oil microcapsule powder provided by the invention is prepared from an oil phase, a water phase and auxiliary materials. The preparation method comprises the following steps: preparing an oil phase and a water phase, emulsifying, homogenizing, drying and mixing to obtain the composite vegetable oil microcapsule powder. By optimizing emulsification parameters, an oil phase and a water phase are fully mixed to obtain a more stable emulsion, so that grease is better embedded in a wall material, and the microencapsulation effect is improved; a spray drying technology is adopted, and parameters are reasonably set, so that the drying efficiency is improved, and grease oxidation and wall material deformation are avoided; by reasonably setting mixing parameters, the components are uniformly mixed, so that the stability of the product is ensured, and the quality of the product is improved; the process provided by the invention improves the stability and encapsulation efficiency of the product, prolongs the shelf life of the product, and has better market competitiveness.

The application belongs to the technical field of oil and gas field development, and provides a phase permeability improver, a fracturing fluid system containing the same, and respective preparation methods and applications. The phase permeability improver is obtained by copolymerization and hydrolysis of acrylamide AM, a functional monomer 2-acrylamido-2-methylpropanesulfonic acid AMPS, and cationic hydrophobic monomers A and B; the cationic hydrophobic monomer A is at least one of tetradecyl dimethyl allyl ammonium chloride, hexadecyl dimethyl allyl ammonium chloride, and octadecyl dimethyl allyl ammonium chloride; the cationic hydrophobic monomer B is at least one of methacryloyloxyethyl trimethyl ammonium chloride, acryloyloxyethyl trimethyl ammonium chloride, and acryloyloxyethyldimethyl benzyl ammonium chloride; the phase permeability improver and the fracturing fluid system containing the same can significantly reduce the water phase permeability after fracturing operation, while having a smaller influence on the oil phase permeability, and have a significant effect of stabilizing oil and controlling water, and can significantly improve the stable production effect of fracturing operation in a low-permeability oil reservoir.

The invention provides an acne-removing suspension oil essence and a preparation method thereof. The acne-removing suspension oil essence comprises a water phase and oil phase particles dispersed in the water phase, the oil phase comprises grease, salicylic acid and an oil-soluble acne-removing component; the water phase comprises a thickening agent, a humectant, a water-soluble acne-removing component and water. Compared with a single water type acne-removing essence, the acne-removing suspension oil essence provided by the invention has the advantages that through the matching of the salicylic acid, the oil-soluble acne-removing component and the water-soluble acne-removing component, the acne-removing effect is more efficient, the oil phase of the product can suspend in the water phase, and the coexistence of the oil phase and the water phase is realized under the condition of not adding an emulsifier, so that the oil-water suspension oil essence has a good application prospect. Irritation caused by an emulsifier is reduced, and the acne cream is friendly to acne skin, especially sensitive acne skin.

The invention discloses a method for improving water flux and anti-pollution capacity of a polyamide reverse osmosis membrane and application of the method, and belongs to the technical field of water treatment membranes.The method comprises the steps that a water-phase solution containing polyamine monomers and an oil-phase solution containing polyacyl chloride monomers are respectively subjected to droplet formation into a water-phase solution containing polyamine monomers and an oil-phase solution containing polyacyl chloride monomers through a droplet generator, and the water-phase solution containing polyamine monomers and the oil-phase solution containing polyacyl chloride monomers have the particle size of 10-200 microns; water phase solution droplets and oil phase solution droplets with the specific surface area of 3 * 10 < 4 >-6 * 10 < 5 > m < 2 > / m < 3 > are sequentially sprayed on the ultrafiltration substrate membrane through a moving spray head system, so that the water phase solution droplets and the oil phase solution droplets are fully contacted to generate an interfacial polymerization reaction, and after the spraying process is finished, heat treatment is performed to obtain the polyamide reverse osmosis membrane. According to the method disclosed by the invention, the traditional interfacial polymerization method is improved, a new additive is not introduced, and the water flux and the anti-pollution capacity of the polyamide reverse osmosis membrane are further improved on the basis of reducing the solvent dosage.