3180results about "Microballoon preparation" patented technology

The invention discloses crack-chloride ion double-triggered subsea tunnel corrosion-resistant concrete and a preparation method thereof, and relates to the field of subsea tunnel engineering materials. The concrete is prepared from the following components in parts by weight: 400 to 500 parts of Portland cement, 50 to 80 parts of fly ash, 60 to 100 parts of superfine mineral powder, 1000 to 1100 parts of coarse aggregate, 700 to 800 parts of fine aggregate, 140 to 160 parts of water, 10 to 20 parts of self-repairing microcapsules and 1 to 5 parts of a water reducing agent, the self-repairing microcapsule comprises a capsule wall material, a self-repairing material and a layered dihydroxyl composite metal oxide. A crack-chloride ion double-response system is constructed, and the limitation of traditional single trigger repair is broken through. When a crack with a certain width appears in the concrete, the capsule wall of the self-repairing microcapsule is broken to release the repairing component, so that effective filling of the crack is realized; and meanwhile, the layered double-metal hydroxide can directionally adsorb chloride ions to form a stable compound, so that the migration rate of the chloride ions is remarkably reduced.

A core-shell particle having an organic polymer core which is completely covered by a first inorganic oxide shell, wherein the first inorganic oxide shell has a silica (SiO2), an alumina (Al2O3), or a titania (TiO2); wherein the first inorganic oxide shell has a layer of a magnetic material which is disposed directly on the polymer core; further having a mesoporous second inorganic oxide shell, wherein the mesoporous second inorganic oxide shell covers the first inorganic oxide shell; wherein the mesoporous second inorganic oxide shell has silica (SiO2), alumina (Al2O3), or a titania (TiO2).

The invention provides methods for the preparation of particles including one or more agents, e.g., therapeutic or diagnostic agents. The particles can be formed by creating droplets of a first liquid, e.g., including an agent, and removing the first liquid, e.g., through its dispersal in a second liquid and / or evaporation, to solidify the droplets. Advantageously, the process of forming the particles does not significantly alter the structure or activity of the agents and may enhance the stability of the agents. For example, the particles may be stored for long periods of time without significant loss of activity, and in some embodiments, without the need for refrigeration. These particles may be used to generate stabilized pharmaceutical compositions for storage or other logistical purposes, pharmaceutical suspensions, pharmaceutical powder formulations (e.g., inhalable powders, injectable powders), creams or other topical pastes, nutraceuticals, or cosmetics.

The invention discloses a high-temperature-resistant astaxanthin microcapsule and a preparation method and application thereof, and relates to the field of nutritional products, the microcapsule comprises: a, a core material: astaxanthin oil selected from haematococcus pluvialis or krill oil; b, double-layer wall materials: an inner-layer wall material is formed by crosslinking sodium alginate and whey protein through an ionic gel method; the outer-layer wall material is formed by electrostatic adsorption of chitosan and Arabic gum; and c, an antioxidant synergist: a rosemary extract. A double-layer embedding structure is adopted outside astaxanthin oil, sodium alginate on the inner layer is combined with whey protein to form a compact network structure through ionic bonds, chitosan on the outer layer and Arabic gum form a compact composite film on the surface of a primary embedded microsphere through electrostatic attraction, so that the double-layer embedded microcapsule has the advantages that the astaxanthin oil has good stability, and the astaxanthin oil has good stability. The temperature resistance limit of a traditional single-layer microcapsule is broken through, the stability of the astaxanthin in a high-temperature baking environment is remarkably improved, the astaxanthin can stably exist in high-temperature baked food, and the anti-oxidation effect and the like of the astaxanthin are fully exerted.

The present invention belongs to the field of microbead preparation technology, and specifically relates to a microbead production process with adjustable internal phase based on microfluidic technology and its application. The microbead production process includes the following steps: (1) raw material transportation: the required materials are transported to the microfluidic chip separately through a pump under heat preservation conditions; (2) logistics shearing: the required materials are sheared in the microfluidic chip to obtain composite droplets; (3) cooling and molding: after the sheared droplets are cooled, they are cooled and solidified using a cooling medium to form microbead particles; (4) product collection: the microbead particles and the cooling medium are subjected to solid-liquid separation, filtered, and collected to obtain microbeads. The microbead production process of the present invention can quickly realize the continuous production of double-layer microbeads, realize the precise regulation of the inner layer of the double-layer microbeads, and quickly and accurately control the particle size of the microbeads; at the same time, it can quickly realize the production conversion between single-layer microbeads and double-layer microbeads.

The invention discloses water-based anti-forgery ink, a preparation method thereof, an obtained printed matter and application thereof, and relates to the technical field of printing forgery prevention. The water-based anti-forgery ink comprises the following components in percentage by mass: 15%-30% of water-based resin, 5%-20% of acrylic resin, 0.5%-10% of an auxiliary agent, 2%-5% of a first fluorescent developing substance, 3%-10% of a first microcapsule and the balance of water, a capsule core of the first microcapsule contains a second fluorescent color developing substance, a capsule shell is made of a first temperature-sensitive high polymer material, and the first temperature-sensitive high polymer material is subjected to reversible phase transformation at a first threshold temperature T1; the second fluorescent color-developing substance is different from the first fluorescent color-developing substance. According to the invention, multiple hidden anti-counterfeiting mechanisms are arranged and can be triggered under specific conditions, so that the cracking difficulty is increased; and the anti-counterfeiting verification requirements in some important occasions can be met.

The invention relates to the field of building material preparation, in particular to a high-strength concrete material and a preparation method thereof.According to the high-strength concrete material, through the synergistic effect of core-shell type temperature-sensitive resin particles, a pH response type expanding agent and industrial solid waste composite micro powder, multi-environment self-adaptive crack resistance and mechanical property breakthrough are achieved. The core component is prepared from 180 to 240 parts of cement, industrial solid waste composite micro powder (30 to 50 parts of fly ash-based nano SiO2 and 50 to 70 parts of steel slag micro powder), 10 to 15 parts of core-shell resin particles and 8 to 12 parts of pH response type expanding agent. According to the preparation process, multi-section intelligent stirring (ultra-high-speed shearing and dispersing of the nanometer material) and dynamic maintenance of the internet of things are adopted, the hydration process is precisely regulated and controlled, and the finally prepared material has excellent compressive strength and anti-cracking performance. The method is suitable for severe scenes such as ocean engineering and plateau buildings, and has wide application prospects.

The invention belongs to the technical field of microbead preparation, and particularly relates to a microbead production process with an adjustable internal phase based on a microfluidic technology and application of the microbead production process. The micro-bead production process comprises the following steps: (1) conveying raw materials: respectively conveying required materials to a micro-fluidic chip through a pump under a heat preservation condition; (2) material flow shearing: shearing the required material in the micro-fluidic chip to obtain composite liquid drops; (3) cooling and forming: cooling and curing the sheared liquid drops by using a cooling medium after the sheared liquid drops are cooled, so as to form microbead particles; and (4) product collection: carrying out solid-liquid separation on the microbead particles and a cooling medium, filtering, and collecting to obtain the microbeads. According to the microbead production process disclosed by the invention, continuous production of double-layer microbeads can be quickly realized, accurate regulation and control of inner layers of the double-layer microbeads are realized, and the particle sizes of the microbeads are quickly and accurately controlled; and meanwhile, the production conversion of single-layer microbeads and double-layer microbeads can be quickly realized.

The invention relates to the technical field of self-thermal-insulation mortar, in particular to self-thermal-insulation mortar and a preparation method thereof. Comprising the following components: Portland cement, a gradient graphene aerogel skeleton, metal organic framework nanoparticles, photo-thermal-phase change coupling microcapsules, magnetic field orientation Fe3O4 nanosheets, self-repairing microcapsules, silicon carbide nanowire aerogel, a water reducing agent and a fiber reinforced material. The gradient graphene aerogel skeleton, the photo-thermal-phase change coupling microcapsules and other materials with excellent thermal insulation performance are introduced, and a multi-layer thermal insulation structure is constructed. The gradient graphene aerogel skeleton has extremely low heat conductivity coefficient and high porosity, and can effectively prevent heat transfer; the photo-thermal-phase change coupling microcapsules can absorb and release a large amount of heat in the phase change process, and the heat preservation effect of the mortar is further improved.

The invention relates to the technical field of food, and particularly discloses a compound prebiotics embedded probiotic microcapsule and a preparation method and application thereof.The green tea leaves serve as main raw materials, water extraction is conducted on the green tea leaves, meanwhile, ultrasonic-assisted treatment is adopted, active ingredients in the green tea leaves can be more effectively released, the extraction time is shortened, and the content of probiotics in the green tea leaves is increased; the extraction rate of active ingredients in the green tea leaves is improved; then, lactobacillus acidophilus is adopted to ferment the extract liquid, so that the green tea fermentation liquid contains more antioxidant active ingredients, combined polyphenol in the extract liquid can release micromolecular polyphenol in the fermentation process, the content of substances such as flavone and polyphenol in the green tea fermentation liquid is increased, and the antioxidant activity is further improved; and then the modified dietary fiber is used as a main wall material of the microcapsule to embed the green tea fermentation liquor and the probiotics, so that the stability of active substances and the probiotics in the green tea fermentation liquor is improved, and the green tea fermentation liquor can play a role in protection and slow release in the simulated digestion process.

The present disclosure relates to methods that enable the continuous formation of droplets and dehydration of droplets to provide pharmaceutically relevant particles that can be used for therapy. In particular, the methods disclosed herein allow the controlled continuous droplet formation and dehydration that produce circular particles having low internal void spaces comprising bioactive therapeutic biologies.

The utility model discloses a device for preparing a double-droplet microsphere. The device comprises a fluid injection unit, a liquid injection unit and a control unit, the micro-fluidic chip comprises a cover glass, one side of the cover glass is provided with a dispensing needle a, the dispensing needle a is connected with an internal phase glass capillary tube, the internal phase glass capillary tube is partially nested in an intermediate phase glass capillary tube, the intermediate phase glass capillary tube is partially nested in an external phase glass capillary tube, and the external phase glass capillary tube is connected with the external phase glass capillary tube. A dispensing needle b is vertically arranged above one end, which is overlapped with the inner phase glass capillary, of the intermediate phase glass capillary, and a dispensing needle c is vertically arranged above one end, which is overlapped with the intermediate phase glass capillary, of the outer phase glass capillary; and a micro-droplet collection unit. According to the utility model, through the coaxially arranged glass capillary tube and the dispensing needle head communicated with the glass capillary tube, the double-droplet microsphere is prepared, meanwhile, the groove is formed in the dispensing needle head, so that the construction of a coaxial glass capillary tube micro-fluidic chip is facilitated, the preparation equipment is simple, and the operation is simple.

The invention provides novel liquid-liquid phase separation microparticles (LLPS MPs) as well as a preparation method and application thereof. The liquid-liquid separation (LLPS) system is micron liquid drops formed by driving under the electrostatic attraction effect of positively charged polyelectrolyte and negatively charged inorganic salt or organic salt in an aqueous solution. Polyoxometallate (POM) is used to stabilize it by electrostatic attraction and precipitate LLPS MPs having a ridge structure. According to the preparation method, [{(B-alpha-PW9O34) Co3 (OH) (H2O) 2 (O3PC (O) (C3H6NH3) PO3)} 2Co] 14-(Co7-POM) with photocatalytic water oxidation activity is selected to deposit micron particles, so that the micron particles have enhanced photocatalytic water oxidation activity, and meanwhile, the micron particles can be recycled through simple and feasible solid-liquid separation.

The invention relates to the technical field of super-hydrophobic anti-icing coatings, in particular to a low-temperature thermochromic super-hydrophobic anti-icing coating and a preparation method thereof. According to the specific technical scheme, low-temperature thermochromic phase change microcapsules and nanoscale hydrophobic silicon dioxide particles are dispersed in an organic solvent, an adhesive and a curing agent are added, and the super-hydrophobic surface with the micro-nano hierarchical structure, the latent heat regulation function and the temperature visual feedback function is constructed through a spraying method. The obtained coating has excellent super-hydrophobicity, and water drop adhesion can be effectively reduced; the phase change microcapsules contained in the coating release latent heat during low-temperature solidification, and surface temperature reduction and icing are remarkably delayed; and meanwhile, the color of the coating is obviously and reversibly changed along with the reduction of the temperature, so that the visual early warning of the low-temperature icing risk is realized. The problems that a traditional super-hydrophobic coating is insufficient in low-temperature anti-icing long-term effect and lacks an early warning function are solved, the super-hydrophobic coating is suitable for low-temperature anti-icing occasions, and the sensing-regulation-protection integrated function is achieved.

The invention provides marine concrete with salt corrosion resistance and self-repairing and a preparation method thereof.The marine concrete is prepared from, by weight, 190-210 parts of cement, 91-100 parts of a natural mineral activating group, 10-15 parts of a composite corrosion inhibitor, 30-35 parts of an exciting agent, 3-6 parts of a high-efficiency water reducing agent, 4-8 parts of a polyamide / polyether sulfone copolymer and 20-25 parts of microcapsules; the preparation method comprises the following steps: preparing the composite corrosion inhibitor and the microcapsule; mixing the cement, the natural mineral activating group, the composite corrosion inhibitor, the exciting agent and the high-efficiency water reducing agent, adding the treated polypropylene fibers and the microcapsules, reacting and curing. According to the invention, the long-acting protection and self-repairing functions of the marine concrete in a high-salt environment are realized by utilizing the cooperation of multiple physical and chemical mechanisms of various formula materials.

The invention relates to the technical field of concrete materials, and discloses rapidly-reinforced high-performance sprayed concrete for an existing tunnel lining and a preparation method of the rapidly-reinforced high-performance sprayed concrete. The sprayed concrete is prepared from the following raw materials in parts by weight: 300 to 350 parts of low-calcium high belite sulphoaluminate cement, 80 to 100 parts of superfine slag powder, 3 to 8 parts of a trigger type activating agent, 5 to 15 parts of slow-release particles, 2 to 5 parts of nanogel, 800 to 900 parts of fine aggregate, 800 to 900 parts of coarse aggregate, 30 to 50 parts of copper-plated steel fiber, 0.8 to 1.2 parts of polypropylene fiber, 30 to 40 parts of a viscosity-adjusting accelerator, 10 to 20 parts of a water reducing agent and 160 to 180 parts of water. The sprayed concrete is high in compressive strength and good in durability, the double threats of chemical corrosion and chloride ion permeation / steel bar corrosion are cooperatively solved, and the requirement for rapid reinforcement of tunnels and underground engineering is met.

The invention relates to the field of oil storage microcapsules, and discloses a porous covalent organic framework oil storage microcapsule as well as a preparation method and application thereof. Under the catalysis of p-toluenesulfonic acid, 4, 4 ', 4' '-(1, 3, 5,-triazine-2, 4, 6-triyl) triphenylamine and trialdehyde phloroglucinol monomers are promoted to be subjected to condensation reaction in the repeated oscillation process, a product is purified to prepare a 4, 4', 4 ''-(1, 3, 5,-triazine-2, 4, 6-triyl) triphenylamine covalent organic framework, and by means of a periodic pore structure of the covalent organic framework, the covalent organic framework can be used for preparing the covalent organic framework. And the lubricating oil is adsorbed and stored and can be controllably separated out to provide lubrication during working, so that a high-performance self-lubricating effect can be realized. In addition, covalent organic frameworks are used as hard particles to be doped into a polymer matrix to modify the polymer matrix, so that the wear resistance of the polymer matrix can be greatly enhanced, and the performance of the self-lubricating bearing material is improved.

The invention relates to the technical field of microcapsule encapsulation, and a novel preparation method is adopted to prepare microcapsule perfume. The microcapsule takes natural gelatin and paraffin as composite wall materials, a gradient structure is formed by optimizing the mass ratio (1: 2.5-1: 3.75), the gelatin provides mechanical support, and the paraffin endows hydrophobicity and thermal control release characteristics. Dissolving a solution in which the mass volume ratio of gelatin to water is (1: 2.5)-(1: 3) under an ultrasonic condition; mixing the molten paraffin with the liquid spice and the emulsifier to form an oil phase; the oil phase and the gelatin solution are mixed through magnetic stirring at the rotating speed larger than or equal to 800 rpm till the solid phase and the liquid phase are completely fused; after cooling and curing, separating to obtain the solid microcapsule. And when the temperature reaches the melting point (45-65 DEG C) of paraffin, the wall material is molten and quickly releases the perfume, and the slow release performance is excellent at normal temperature. The material is wide in application field and high in compatibility, and has the advantages of being green, safe, high in environmental stability and controllable in trigger release.

The invention provides a well wall heat insulation hollow microsphere and a preparation method thereof. A sealed vacuum cavity is formed in the well wall heat insulation hollow microsphere, a polymer layer is arranged on the surface of the well wall heat insulation hollow microsphere, the polymer layer is provided with cationic groups and anionic groups, and aerogel nano powder is embedded in the polymer layer. The invention also provides a preparation method of the well wall heat insulation hollow microsphere. The well wall heat insulation hollow microspheres have high compressive strength, and the heat conductivity coefficient is reduced; efficient well wall adsorption can be achieved through the synergistic effect of anion groups and cation groups, the defects that a traditional heat insulation material is prone to breaking, fast in heat conduction and ineffective in adsorption under the high-temperature and high-pressure environment of an ultra-deep well are overcome, and the material is suitable for an ultra-deep and ultra-deep oil and gas well drilling fluid system. A multistage pore heat insulation system is constructed through the zwitterionic polymer and the aerogel nano-powder, and a rough surface structure can be provided to assist the microspheres in adsorbing well wall rocks.

The invention provides a microbial slow-release porous composite material for sewage treatment as well as a preparation method and application thereof. The preparation method comprises the following steps: dropwise adding an organic ligand solution into a precursor solution consisting of a nanocellulose solution and a cobalt source solution; mixing the reaction solution with polyvinyl alcohol, injecting the mixture into a mold, and performing directional freezing to obtain an aerogel matrix; carrying out hydrophobic modification on the aerogel matrix to obtain a modified aerogel matrix; mixing the microbial suspension with sodium alginate, and homogenizing at high pressure to obtain a gel precursor emulsion; the preparation method comprises the following steps: dropwise adding a calcium chloride solution to gelatinize to obtain gel particles, and then cross-linking and drying by glutaraldehyde to obtain sustained-release capsule particles; dispersing the sustained-release capsule particles in deionized water to obtain dispersion liquid; and dipping the modified aerogel matrix in the dispersion liquid. An aerogel matrix with a hierarchical porous structure is compounded with a sustained-release capsule with a pH response mechanism, so that physical adsorption, chemical catalysis and biodegradation for sewage treatment are realized.

The present disclosure relates to methods that enable the continuous formation of droplets and dehydration of droplets to provide pharmaceutically relevant particles that can be used for therapy. In particular, the methods disclosed herein allow the controlled continuous droplet formation and dehydration that produce circular particles having low internal void spaces comprising bioactive therapeutic biologics.

The invention provides a 180 DEG C-resistant microcapsule type cementing wall-fixing agent for water-based drilling fluid as well as a preparation method and application thereof, and belongs to the technical field of drilling. The preparation method of the wall fixing agent comprises the following steps: (1) respectively adding the macromolecular hydrophilic colloid and the emulsifier into deionized water, and stirring until the macromolecular hydrophilic colloid and the emulsifier are completely dissolved to obtain a water phase; (2) adding phenolic resin, the MUF prepolymer solution and nano SiO2 into an organic solvent under a stirring condition, and uniformly stirring to obtain an oil phase; (3) adding the oil phase obtained in the step (2) into the water phase obtained in the step (1), and carrying out shear emulsification to obtain an oil-in-water emulsion; and evaporating to remove the organic solvent in the system, filtering, washing, and drying to obtain the product. Under the multi-element synergistic effect of hydrogen bonds or coordinate bonds, Van der Waals force and the like, the microcapsule type cementing wall-fixing agent can accelerate the interface to form a compact cemented network structure, the cementing strength of rock particles is remarkably improved, and the purpose of strengthening the stability of a well wall is achieved.

The invention relates to the technical field of silicon dioxide surface modification, in particular to a silicon dioxide hollow sphere with an MOF composite layer, a manufacturing method and a dielectric loss prediction method. The silicon dioxide hollow sphere comprises a hollow spherical structure formed by silicon dioxide, an amino silane layer grafted on the surface of an inner core layer through a covalent bond, a ZIF-8 crystal layer growing in situ by taking amino as a nucleation site, and thiol groups distributed on the outer surface of an MOF crystal. According to the silicon dioxide hollow sphere with the MOF composite layer, the manufacturing method and the dielectric loss prediction method, the silicon dioxide hollow sphere with the MOF composite layer has good compatibility and stability in an LCP matrix, the dielectric loss is small, and the performance of a high-frequency FPC is effectively improved.

The invention discloses a multi-shell photo-thermal phase change microcapsule and a preparation method thereof, the multi-shell photo-thermal phase change microcapsule comprises a capsule wall and a capsule core, the capsule core is an organic phase change material, the capsule wall comprises a titanium dioxide layer, a graphene layer and a polydopamine layer, the graphene layer is located outside the titanium dioxide layer, and the polydopamine layer is located outside the graphene layer. The multi-shell photo-thermal phase change microcapsule disclosed by the invention can realize full-wave band capture, and is high in photo-thermal conversion efficiency and good in shell stability.

The invention provides a slow-release corrosion-resistant microcapsule applied to reinforced concrete, the slow-release corrosion-resistant microcapsule comprises a capsule core and a capsule wall, and the capsule core comprises a composite corrosion inhibitor, self-repairing microspheres, nano hydrotalcite and an anti-freezing agent; the capsule wall comprises a three-layer structure including an inner layer film, a middle layer film and an outer layer film. The mass ratio of the capsule core to the capsule wall is 1: (0.3-0.5); and the thickness of the capsule wall is 10-17 microns. A pH triggering inner layer, a dynamic self-repairing middle layer and a hydrophobic protection outer layer are designed through three layers of intelligent response capsule walls, and on-demand release and long-term stability of a corrosion inhibitor are achieved; the crack repairing efficiency is remarkably improved through the synergistic effect of the chemical repairing material and the biological spores in the capsule core; the dynamic cross-linked network endows the capsule wall with self-healing ability, resists physical damage, improves the durability of the concrete, prolongs the service life of the concrete, also can enhance the wear resistance of the concrete, and reduces the wear in the use process.

The invention relates to the technical field of functional materials, in particular to a chitosan nanocapsule as well as a preparation method and application thereof. The preparation method of the chitosan nanocapsule comprises the following steps: (a) mixing and emulsifying a chitosan solution, an oil-in-water emulsifier and essential oil to form an oil-in-water emulsion, adding an aqueous solution of sodium tripolyphosphate into the oil-in-water emulsion, and stirring to obtain a first mixture; (b) adding the first mixture into an oil phase solvent containing a water-in-oil emulsifier, and stirring to obtain a multiple emulsion; and (c) adding an aqueous solution of a dialdehyde cross-linking agent into the multiple emulsion, carrying out a cross-linking reaction, collecting a solid-phase substance, and drying. The physical / chemical double-crosslinking chitosan nanocapsule is obtained by utilizing physical crosslinking between the chitosan and the sodium tripolyphosphate and chemical crosslinking between the chitosan and the binary aldehyde crosslinking agent, so that the encapsulation efficiency and the encapsulation efficiency of the nanocapsule are remarkably improved; meanwhile, the nanocapsule also has pH responsiveness and has a slow release effect after pH response.

The invention discloses anti-attrition lubricating oil suitable for minimal quantity lubrication and a preparation method thereof, and belongs to the technical field of lubricating oil, molybdenum disulfide is nucleated and grows on the surface of porous cerium oxide nanosphere powder to form a cerium oxide and molybdenum disulfide compound, then modified silicon dioxide and tannic acid are pre-polymerized to form silicon dioxide prepolymer powder, and the silicon dioxide prepolymer powder is subjected to ball milling to obtain the anti-attrition lubricating oil suitable for minimal quantity lubrication. The preparation method comprises the following steps: taking a cerium oxide molybdenum disulfide compound as a core material, taking silicon dioxide prepolymer powder and an N-isopropylacrylamide polymer as a shell to obtain a composite temperature-sensitive microcapsule, and mixing the composite temperature-sensitive microcapsule with other raw materials to prepare the composite temperature-sensitive microcapsule. The outer-layer shell polymer chain of the composite temperature-sensitive microcapsule in the anti-attrition lubricating oil shrinks, the cerium oxide molybdenum disulfide compound inside is released, and controllable release of the inner core material is realized by using the temperature sensitivity of the shell polymer of the composite temperature-sensitive microcapsule and the external temperature change during operation.

The invention relates to the technical field of road construction and maintenance, and discloses a multi-polymer modified emulsified asphalt in-situ cold recycling mixture and a preparation process thereof, the multi-polymer modified emulsified asphalt in-situ cold recycling mixture comprises the following components by weight: 600-680 parts of nano hybrid emulsified asphalt; 250 to 350 parts of plasma activated recycled aggregate; 15 to 30 parts of a microcapsule phase change catalyst; 5 to 10 parts of bio-based interface reinforcing fiber; and 3-8 parts of a rare earth doped curing accelerator. According to the invention, through multi-technology cross-scale fusion of a quaternary polymer rigid-flexible synergistic system, a gradient emulsification-vacuum self-assembly process, double-shell intelligent catalytic release and rare earth gradient distribution-magnetic field induced fiber arrangement, the bottlenecks of unbalanced high and low temperature performance, easy interface stripping, poor aging resistance, extensive process regulation and control and the like of a traditional asphalt material are overcome; and the strength and toughness-durability-self-adaption performance synergistic jump is realized.

The invention relates to the technical field of anti-counterfeiting materials, and particularly discloses a composite color-changing agent, anti-counterfeiting color-changing ink and a preparation method of the anti-counterfeiting color-changing ink. The composite color-changing agent is a composite microsphere with a core-shell-satellite structure, the core is a temperature-sensing color-changing microcapsule and is composed of a temperature-sensing color-changing core material and a polymer wall material, the shell is a transparent polymer shell and wraps the core through in-situ polymerization, the satellite is a light-sensing color-changing material and is embedded and fixed on the shell, and the shell is a transparent polymer shell and is embedded and fixed on the shell. According to the composite color-changing agent, the light-sensitive material and the temperature-sensitive material are compositely inlaid through the polymer shell, so that the problem of poor compatibility of the light-sensitive material and the temperature-sensitive material is solved, the stability and the production efficiency are improved, and the imitation difficulty is increased.

The present invention relates to the technical field of cigarette processing, and in particular to a method for preparing a sustained-release flavor material, comprising the following steps: S1 adsorption: placing mesoporous hollow nano-silicon spheres in a flavor and fragrance solution, allowing the solution to stand for 2-5 hours, and obtaining mesoporous hollow nano-silicon spheres to which flavors and fragrances are added for standby use; S2 preparation of a composite flavor material: wrapping the mesoporous hollow nano-silicon spheres processed by the S1 step with a coating layer, and drying them under low temperature conditions after the coating is completed to obtain a composite flavor material. The purpose of the present invention is to enable flavors and fragrances to be prepared into a sheet or granular form, on the one hand, to reduce the volatilization of the flavor during storage, and on the other hand, to be easily added to a filter rod or a cigarette cartridge, so that the cigarette or cigarette cartridge can continuously release the flavor of the flavor when inhaled, thereby improving the consumer experience.