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6079 results about "Sodium phosphates" patented technology

Sodium phosphate is a generic term for a variety of salts of sodium (Na⁺) and phosphate (PO₄³⁻). Phosphate also forms families or condensed anions including di-, tri-, tetra-, and polyphosphates. Most of these salts are known in both anhydrous (water-free) and hydrated forms. The hydrates are more common than the anhydrous forms.

Vanadium sodium phosphate composite material as well as preparation method and application thereof

The invention relates to a vanadium sodium phosphate composite material as well as a preparation method and an application thereof. The general formula of the composite material provided by the invention is C1-xNx-LaNabMcVd(PO4)3, wherein C1-xNx is carbon or carbon doped with nitrogen, L is one or two selected from Li and K; M is one or more than one selected from Mg, B, Al, Ca, Ti, Cr, Mn, Fe, Co, Ni, Cu, Zn, Ce, Y, Zr, Nb, Mo, Sn, La, Ta and W; and x, a, b, c and d are mol percents, wherein x is more than or equal to 0 and less than 1, a is more than or equal to 0 and less than 2, b is more than 1 and less than or equal to 3, c is more than or equal to 0 and less than or equal to 1, and d is more than or equal to 1 and less than or equal to 2. The invention also provides a preparation method and an application of the composite material. The vanadium sodium phosphate composite material can be taken as cathode or anode material of a secondary sodium-ion battery, especially vanadium sodium phosphate composite material coated with carbon and nitrogen has higher coulombic efficiency and ion and electron conductivity and better cycling performance, is high in safety, low in price, simple in process and wide in application range and can be applied to energy storage equipment, a backup power supply, a spare power supply and the like.
Owner:INST OF PHYSICS - CHINESE ACAD OF SCI

Preparation method of carbon coated vanadium sodium phosphate positive electrode material

A preparation method of a carbon coated vanadium sodium phosphate positive electrode material comprises the steps: with glucose as a reducing agent and a carbon source and water as a dispersant, carrying out ball milling of NH4VO3, NaH2PO4.2H2O and glucose in water, carrying out spray drying, calcining, and thus obtaining the carbon coated vanadium sodium phosphate positive electrode material. The method has the advantages of low synthesis temperature, simple steps, easily obtained raw materials, and advantageous industrialization; the obtained carbon coated vanadium sodium phosphate positive electrode material has a structure with uniform primary particles, has the particle size of 100-200 nm, and has the characteristics of short sodium ion diffusion distance, fast transmission speed, high specific surface area, high electrical conductivity and fast ion transmission and the like. The obtained carbon coated vanadium sodium phosphate positive electrode material is assembled into a battery; in a voltage scope of 2.0-3.75 V and under 1 C multiplying power, the highest first charge and discharge capacity per gram can reach 93.5 mAh*g<-1>, the capacity retention rate can be up to 97.7% after cycling for 50 circles with the 1C multiplying power, and excellent electrochemical performance is showed.
Owner:CENT SOUTH UNIV

Anti-crack alkalis excited ecological cement

InactiveCN101456685AImprove impermeabilityExcellent volume shrinkageCement productionSlagMass ratio
The invention relates to anti-cracking alkali exciting ecological cement, which consists of A, B and C, and solid-phase mass ratio of the A to the B to the C is 5-10:75-90:5-15. The A is exciting agent, which comprises the following components by mass percentage: more than or equal to 80 percent of water glass of which modulus is 0.7 to 1.4, and less than or equal to 20 percent of one or a plurality of sodium sulfate, sodium phosphate, sodium carbonate, sodium chloride and magnesium chloride; and the A is prepared into solution containing more than or equal to 40 percent of solid for use. The B is a mineral additive, which comprises the following components by mass percentage: 30 to 70 percent of slag powder, and 30 to 70 percent of other additives, wherein the other additives comprise one or a plurality of siliceous dust, coal ash, metakaolin, red mud, burnt shale, colliery waste, steel slag and alloy slag, and is grinded to powder of which specific surface is 350 to 800m<2>/g. The C is active magnesium oxide, wherein mass content of MgO is more than or equal to 70 percent. The active magnesium oxide is calcined at a temperature of between 700 and 1,000 DEG C and then mixed and grinded with the B to become powder. The cement is the low-carbon discharge ecological cement with the advantages of high-early strength, durability, permeability resistance, corrosion resistance, freezing and thawing resistance, low heat of hydration, good cracking resistance, economy and environmental protection, and is used for civil construction, water conservancy, national defense, and oil well and mine passage support engineering.
Owner:WUHAN UNIV OF TECH

Method for recovering lithium from lithium iron phosphate

The invention discloses a method for recovering lithium from lithium iron phosphate. The method disclosed by the invention comprises the following steps: dissolving waste lithium iron phosphate slag with sulfuric acid and ferric sulfate, leaching iron, lithium and phosphorus, adding an oxidizing agent, reacting iron and phosphate radicals to produce an iron phosphate precipitate and a small amountof ferric hydroxide, converting lithium into a water-soluble lithium sulfate solution, filtering to obtain the lithium sulfate solution, adding sodium carbonate into the lithium sulfate solution to prepare a lithium carbonate product, and adding sodium phosphate or phosphoric acid to prepare lithium phosphate; dissolving the lithium phosphate with ferric sulfate again to obtain the lithium sulfate solution and a compound taking iron phosphate as a principle component, returning the lithium sulfate solution to the system to prepare lithium carbonate, and calcining the iron phosphate slag to remove organic matters and carbon in the slag; and slurrying to prepare cell grade iron phosphate. According to the method for recovering lithium from lithium iron phosphate disclosed by the invention,the lithium is totally converted into the product lithium carbonate in the method, the process flow is short, the cost is low, the lithium recovery rate is 97%, the metal lithium in the lithium iron phosphate can be effectively recovered, and all the slag is converted into the cell grade iron phosphate.
Owner:취저우화여우코발트뉴머터리얼컴퍼니리미티드 +1

Preparation method for wear resistant fire-retardant coating

The invention provides a preparation method for wear resistant fire-retardant coating with simple construction process, good wear resistance and relatively low cost. The raw material of the wear resistant fire-retardant coating selects plate-shaped tabular alumina, brown alumina and high-quality bauxite chamotte as aggregate, selects plate-shaped tabular alumina powder, flint clay powder, alpha-Al2O3 micropowder and ceramic powder as fine powder, selects 42.5 mass percent industrial phosphoric acid solution, solid aluminium dihydrogen phosphate and clay powder as bonding agents, selects fused magnesite as a curing agent and selects sodium borate and sodium hexametahposphate as sintering aids. The wear resistant fire-retardant coating can be directly smeared on the surfaces of a wear resistant fire-retardant material liner and a water cooling wall pipe, fills up technical blank of resisting the wear on metal by using a non metal coating at a high temperature of 900 DEG C, provides a new repairing method for a non metal wear resistant fire-retardant material liner, has simple construction process, can obviously improve working environment of workers, reduce the labor intensity and improve the working efficiency of maintaining a circulating fluid bed boiler heated surface metal pipe wall and the wear resistant fire-retardant material liner.
Owner:TONGDA REFRACTORY TECH CO LTD

Technology of enhanced-dispersion partial selective and bulk flotation of lead and zinc sulfide ores under low and high alkalinity

The invention discloses a technology of enhanced-dispersion partial selective and bulk flotation of lead and zinc sulfide ores under low and high alkalinity. During grading of the lead and zinc sulfide ores, sodium hexametahposphate is taken as a dispersion agent and directly added into a ball mill, the ores are ground till the ores with the size of 0.074mm account for 67%-70%, lime is taken as an adjusting agent, zinc sulfate and sodium sulfite are taken as inhibitors, dithiophosphate BA and diethyldithiocarbamate are taken as collectors, and selective flotation of part of lead minerals with good floatability can be performed under low alkalinity; then xanthate and the diethyldithiocarbamate are taken as collectors, and the flotation of the lead minerals is further performed under high alkalinity; copper sulfate is added in lead flotation tailings for activation, butyl xanthate is further taken as the collector for flotation of zinc blende and part of pyrite, and zinc-sulfur separation flotation is further performed on zinc-sulfur mixed concentrate; and sulfuric acid is added in zinc flotation tailings for activation, and the xanthate is taken as the collector for flotation of the remaining pyrite. By adopting the technology, the lead-silver recovery rate can be improved, the using amount of lime and sulfuric acid can be reduced, the circulating amount of middlings can be reduced, the ore dressing cost can be reduced and the grade of the concentrate can be improved.
Owner:KUNMING UNIV OF SCI & TECH

Acetylene sludge aerated concrete block and preparation method thereof

The invention provides an acetylene sludge aerated concrete block, which is prepared by processing the following raw materials in part by weight: 20-30 parts of acetylene sludge, 25-30 parts of coal ash, 5-10 parts of cement, 4-6 parts of modified attapulgite, 5-10 parts of water treatment sludge, 5-10 parts of soda residue, 5-10 parts of light calcium powder, 10-15 parts of lime, triethanolamine, 4-5 parts of gypse, 0.02-0.08 part of aluminium powder, oxidized paraffin wax soap, 0.01-0.02 part of calcium bicarbonate, 2-3 parts of chelky slag, 1-2 parts of lignocellulose, 0.3-0.5 part of water glass, 0.03-0.05 part of borax, 1-2 parts of sodium hexametaphosphate, 1-2 parts of hydroxy propyl methyl cellulose sodium and 1-2 parts of superfine polyvinyl alcohol, wherein the weight of the triethanolamine is 0.1-0.3 percent of that of the lime, and the weight of the oxidized paraffin wax soap is 3-5 percent of that of the aluminium powder. According to the invention, the acetylene sludge is added into the raw materials of the aerated concrete block, and meanwhile other conventional additives and modified nano additives are added; the aerated concrete block is prepared by adopting a proper technology and is low in cost and good in performance; the circulating economy effect of changing waste into valuable is realized; the pollution is reduced; and the prepared aerated concrete block has the characteristics of light volume weight, high thermal insulation performance, good sound absorption effect and high strength and can be used for non-bearing or bearing wall bodies.
Owner:广东合盛建筑工程有限公司

Chemical nickel-plating method for carbon fiber

The invention discloses a chemical nickel-plating method for carbon fiber, which is designed for overcoming the disadvantages of high cost, a large number of process steps and poor operability existing in the prior art. In the method, a chemical plating process is adopted; and a pre-treatment is performed on a raw material and chemical plating solution is prepared before the chemical plating. The pre-treatment process comprises the steps of: calcining by using a muffle furnace to remove glue; soaking in solution of absolute ethanol to remove oil; performing surface roughening and activating treatment by using solution of sodium hydroxide and solution of silver ammonia; sensitizing by using a sensitizer, namely stannous chloride; and performing surface reduction by using solution of sodium hypophosphite. The chemical plating solution consists of nickel sulfate hexahydrate, sodium hypophosphite, sodium pyrophosphate and sodium citrate. The chemical nickel-plating on the carbon fiber is finished by placing a pre-treatment product of the chemical plating into the chemical plating solution, and reacting, standing, filtering and drying under a chemical plating condition. The method has the characteristics that: the product has a uniform surface, a compact plating layer and uniform particles.
Owner:沈阳临德陶瓷研发有限公司

Technique for efficiently removing iron from kaolin

The invention relates to a technique for efficiently removing iron from kaolin by magnetic separation, which is characterized by comprising the following steps: (1) purifying kaolin raw ore to obtain a magnetic separation raw material; (2) adding water to the magnetic separation raw material obtained in the step (1) to prepare a mixed slurry with the solid content of 10-20 wt%, adding sodium hexametaphosphate accounting for 0.2-0.6 wt% of the magnetic separation raw material, slurrying, stirring for 20 minutes, and passing through a 325-mesh wet sieve; (3) carrying out high-gradient magnetic separation on the undersize slurry of the 325-mesh sieve in the step (2): while controlling the magnetic field intensity of the high-gradient magnetic separator at 1.0-1.8T and the slurry flow rate at 0.8-1.8cm/s, the slurry is subjected to magnetic separation by the high-gradient magnetic separator to obtain a concentrate slurry; (4) adding alum accounting for 1-6 wt% of the concentrate slurry into the concentrate slurry obtained in the step (3), flocculating, carrying out pressure filtration, drying, and packaging to obtain a magnetic concentrate; and (5) calcining the magnetic concentrate obtained in the step (4) to obtain the calcined kaolin. The technique has the advantages of high iron removal efficiency and obvious whitening effect.
Owner:CHINA UNIV OF GEOSCIENCES (WUHAN)
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