35319results about How to "Wide variety of sources" patented technology

The invention discloses a particle-typed composite fertilizer of humic acid and manufacturing method, which consists of dressing and karyosome, wherein the dressing contains nitrogen, phosphor and potassium. The manufacturing method comprises the following steps: graining humic acid; cladding; graining; solidifying fused fertilizer on the particle of humic acid; making the composite fertilizer dissolved into water without falling; fitting for large scale of agricultural product.

The invention discloses an edible biological preservative film and a preparation method thereof. The edible biological preservative film comprises the following components in parts by weight: 30-60 parts of a film former, 1-10 parts of a natural antioxidant, 1-10 parts of a natural bacterial inhibitor, 1-4 parts of a plasticizer and 0.5-4 parts of an emulsifier. The preparation method comprises the following steps: mixing the components in proportion to form preservative film liquid, and preparing the preservative film by adopting a tape-casting process. According to the preservative film, excellent film forming performances of materials such as marine polysaccharides, chitosan, gelatin and the like are utilized, the natural antioxidant and the natural bacterial inhibitor are selected and used, and the modification process is carried out through the plasticizer, the emulsifier and the like, so that the prepared preservative film is good in mechanical property, delays the spoilage of an aquatic product and can effectively prolong the shelf life of the aquatic product.

The invention discloses a composite natural polymer gel material with a cross-linking agent. The material comprises hydrogel, organogel, aerogel and bioplastics and mainly overcomes the problem of low mechanical strength of conventional natural polymer gel materials. According to the invention, a certain amount of the cross-linking agent is added into a natural polymer water-based solution or dispersion liquid, then stirring is carried out, the obtained mixture is placed in a non-solvent for physical cross-linking, and then washing is carried out so as to obtain composite natural polymer hydrogel; water in the composite natural polymer hydrogel is replaced with an organic solution so as to prepare composite natural polymer organogel; the composite natural polymer hydrogel or organogel is dried so as to prepare composite natural polymer aerogel; the composite natural polymer aerogel is subjected to hydrophobic treatment so as to obtain hydrophobic aerogel; the composite natural polymer aerogel is subjected to heat treatment so as to obtain carbon aerogel; and one or more selected from the above-mentioned gel materials are subjected to high-temperature pressing so as to prepare composite natural polymer bioplastics. The composite natural polymer gel material prepared in the invention has the advantages of excellent mechanical properties, a high specific surface area, high elongation at break, etc., and can be easily processed into molded products of a plurality of forms.

The invention relates to the field of bio-materials, and especially relates to an acellular matrix repairing gel and a new method for preparing the same. The invention discloses the acellular matrix repairing gel and the method for preparing the same, wherein the method includes steps of acellular treatment and gelatinization treatment on tissue and organs from mammal animals to prepare the acellular matrix repairing gel. The acellular matrix repairing gel is eliminated in immunogenicity of heterologous and foreign tissue, so that activity of extracellular matrix components of the tissue is maintained as more as possible. The gel can specially repair damaged tissue and organs of human body, is strong in applicability, is suitable for requirements of various irregular-shaped repair zones and different position environments in body and has a huge clinical value.

The invention discloses preparation methods for a macroporous alumina carrier and a hydrodemetallization catalyst. The preparation method for the macroporous alumina carrier includes the following steps: (1) dry pseudoboehmite gel powder is hydrothermally processed under high pressure; (2) the dry pseudoboehmite gel powder obtained in step 1 is kneaded into a plastic, and pore-expanding agent is added in step 1 or step 2; (3) the plastic obtained in step 2 is shaped, the shaped material is dried and baked, and thereby the macroporous alumina carrier is obtained. The impregnation method is adopted to prepare the hydrodemetallization catalyst. The hydrodemetallization catalyst prepared by the method has large pore volume and pore diameter, centrally distributed pores, moderate mechanical strength and high activity and activity stability.

The present invention relates to a nitrogen-doped porous carbon material for a lithium-air battery positive electrode, wherein the nitrogen-doped porous carbon material has an interconnected graded pore structure, N is uniformly doped in the C skeleton, N accounts for 0.2-15% of the carbon material atomic ratio, the graded pores comprise mass transfer pores and deposition holes, the deposition holes account for 40-95% of the total pore volume, and the mass transfer pores account for 4-55% of the total pore volume. According to the present invention, with application of the carbon material as the lithium-air battery electrode material, the space utilization rate of the carbon material during the charge-discharge process can be increased at a maximum, and the energy density and the power density of the lithium-air battery can be effectively increased; and the preparation process is simple, the material source is wide, the pore structure of the graded pore carbon material can be regulated, the regulation manner is diverse, and the nitrogen doping manner is easily achieved.

The invention belongs to the field of fine chemical materials, and more particularly relates to a method for preparing cellulose composite aerogel. The method is mainly characterized by taking a carbon material as a modifying agent, and comprises the following main processes of: firstly dissolving cellulose in a sodium hydroxide / thiourea aqueous solution, a sodium hydroxide / urea aqueous solution or other solvents to prepare a cellulose solution with a certain concentration, adding a carbon nanotube (CNT), graphene oxide (GOS), reduced graphene oxide (rGO) and other modifying agents, standing for carrying out gelation, carrying out solvent exchange on the obtained gel, and drying the composite gel to obtain the cellulose composite aerogel. The preparation technique provided by the invention has a simple process and convenience for operation, and can obviously shorten the time of forming the gel from the solution; and the prepared composite aerogel has higher compressive strength and modulus as well as good heat stability, and has wide application prospects in the biomedical, biological sensing and detecting and other fields.

The present invention provides a non-radical photo-crosslinked hydrogel preparation method, comprising the following steps: a component A is dissolved in a biocompatible medium to obtain a solution A, component B-hydrazide, hydroxylamine or primary amine high molecular derivative is dissolved in a biocompatible medium to obtain a solution B; the solution A and the solution B are evenly mixed to obtain a hydrogel precursor solution; under illumination, aldehyde group produced by light excitation of o-nitrobenzyl in the component A of the hydrogel precursor solution is crosslinked with hydrazone, hydroxylamine or primary amine group in the component B in the form of respective formation of oxime and Schiff base to produce the hydrogel. The present invention also provides a kit for the hydrogel preparation, and application of the hydrogel in tissue repair, beauty and as a cell, protein or drug carrier. The tissue surface light-situ gel can be achieved by the hydrogel, in particular, wound surface in-situ thin glue formation can be achieved, and the hydrogel is especially suitable for clinical wound surface tissue repair and isolation.

The invention discloses a credit recording system and method based on a block chain. The credit recording system comprises a plurality of user terminals which are connected to the block chain and used for acquiring and verifying credit data, wherein each user terminal is installed with an encryption module for encrypting target credit data to be transmitted to form encrypted credit data, a communication module for transmitting the encrypted credit data together with the block chain, and a storage module for storing the target credit data of the user terminal and other encrypted credit data transmitted by the block chain. The credit data are wide in sources, independent, reliable and real; the cleaning and sieving complexity of the credit data are lowered greatly; and the credit recording system and method have flexible and diverse application scenes and high extensibility.

The invention discloses a preformed material for post-tensioned prestressing pipeline vacuum grouting or mudjacking and a preparation method thereof. The preformed material includes the following components by weight percent: 65 to 95 percent of silicate cement, 0.01 to 3 percent of high-range water-reducing agent, 0 to 1 percent of stabilizing agent, 0.05 to 5 percent of retarding agent, 1 to 20 percent of expanding agent, 0.2 to 2 percent of corrosion inhibitor, 0.01 to 1 percent of air entraining agent and 0 to 30 percent of mineral materials, wherein by uniformly and proportionally mixing the silicate cement, the high-range water-reducing agent, the stabilizing agent, the retarding agent, the expanding agent, the corrosion inhibitor, the air entraining agent and the mineral materials, the post-tensioned prestressing pipeline vacuum grouting or mudjacking preformed material can be obtained. After being uniformly mixed and stirred with water with neutral pH value according to the water cement ratio ranging from 0.24 to 0.32, the preformed material can be used, the obtained grouting material has the advantages of low water cement ratio, favorable flowability, no water bleeding and delamination, and favorable pumpability; meanwhile, the preparation method of the preformed material is simple and the raw material sources of the preformed material are wide.

The invention discloses a heavy metal absorbent and a preparation method and use thereof. The heavy metal absorbent is prepared by using an inorganic mineral modified by a surfactant as a carrier and loading organic complexing agent on the carrier, wherein the inorganic mineral is bentonite, kaolin, kieselguhr, zeolite, aluminum oxide or iron oxide; the surfactant is cationic surfactant or nonionic surfactant; and the organic complexing agent is a compound containing a sulfydryl and an amino. The heavy metal absorbent has the advantages of stable performance, environment friendliness, high absorption capacity, high selectivity, convenient post-recovery treatment and the like. The absorption capacities of cadmium, mercury lead and other heavy metals all exceed 100mg / g, and the heavy metal absorbent can achieve good treatment effect in treatment of water and soil environments polluted by heavy metals.

The invention discloses a preparation method of large-size graphene oxide or graphene. The preparation method mainly utilizes graphite as a raw material and comprises that 1, under the action of an intercalator and an expanding agent, graphite fully releases interlayer spaces so that interlayer interaction is reduced and a graphene aggregate is obtained, 2, the graphene aggregate is oxidized by an oxidizing agent, and then the oxidized graphene aggregate is peeled in water under gentle mechanical action so that a large area of a dispersion liquid of graphene oxide is obtained, and 3, the peeled graphene oxide is reduced by a reducer or heat treatment so that high conductivity graphene is obtained. The preparation method utilizes cheap raw materials, has a simple process, can be controlled easily, realizes fast and high efficiency solid-liquid separation, is convenient for industrial large scale production, prevents graphene crystal structure destroy caused by high energy supersonic wave, high speed shearing or fluid crushing. The obtained graphene has a large size and high conductivity and can be popularized and used in fields of high efficiency heat management, flexible display, energy conversion and storage.

This invention refers to a kind of component of nick resistant talcum-powder-filling polypropylene, is characterized with strengthened toughness through latex and is composed of the following materials in amounts of weight: between 50 and 80 of polypropylene, between 5 and 35 of filler, between 5 and 25 of latex, between 0.5 and 5 of high molecular silicone elastomer, between 0.05 and 0.5 of nucleater, between 0.1 and 1.0 of stabilizer, between 0.2 and 1.5 of talcum powder surface passiation agent, between 0.05 and 1.0 of processing agent and between 0.3 and 2.0 of toner. The manufacturing method is to weigh the materials in amounts of weight, to mix polypropylene, filler, latex, high molecular silicone elastomer, nucleater, stabilizer, talcum powder surface passiation agent, processing agent and toner in homo mixer, then put them into double-screwed extruder for melting and extruding. After cooling, drying and pelleting, we can get the turnoff. The invention improves the nick resistance of polypropylene, ultraviolet radiation endurance and thermal endurance and the toughness and rigidity of the material reach good balance. It can meet the requirements of the material of automobile limbs. It can demold at a relatively high temperature, improves the moulding efficiency greatly and reduces the processing cost.

The invention provides high-strength and high-corrosion-resistance cast aluminum alloy and a pressure casting preparation method thereof. The alloy is prepared from, by a certain weight percent, Si, Mg, Fe, Mg, Zn, Sr, Cu, M and the balance Al, wherein M is at least one element of Ti, Zr and V, or the element RE is added in M. After the high-strength and high-corrosion-resistance cast aluminum alloy is subjected to pressure casting, the room temperature tensile strength sigma b of alloy not subjected to heat treatment is larger than or equal to 315 MPa, the room temperature ductility sigma of the alloy not subjected to heat treatment is larger than or equal to 3.0%, and good corrosion resistance is achieved; and the alloy can be applied to automobile parts without ageing or solid solution heat treatment, and the requirement for light automobile development is met.

The invention discloses preparation of a super-hydrophobic ice-covering-proof coating having a slowly-releasing function. The ice-covering-proof coating consists of the following substances in parts by mass: 1.5-5 parts of inorganic hollow or porous nanoparticles for adsorbing small molecular anti-icing substances, 2-5 parts of fluorine-containing polymer and 1-15 parts of solvent. The super-hydrophobic ice-covering-proof coating having the slowly-releasing function can be obtained by uniformly mixing the three substances and coating the mixture onto the surface of a substrate. At the normal temperature, the water contact angle of the coating is greater than 150 degrees, and the rolling angle is smaller than 7 degrees. At 10 DEG C below zero, the low-temperature contact angle of water is greater than 140 degrees, and the rolling angle is smaller than 12 degrees. During testing of the ice cover at 10 DEG C below zero, the ice cover is lowered by over 70 percent, and is still higher than 50 percent after testing is performed circularly for ten times in comparison to a blank sample.

The invention discloses a preparation method for high strength macro graphene conductive fiber. According to the method, graphite is oxidized to obtain a graphene oxide; the graphene oxide is dispersed in water or a polar organic solvent to prepare a spinning liquid sol with the mass concentration of 1-20%; the spinning liquid sol is transferred to a spinning device; the spinning liquid is continuously extruded from a spinning head capillary at a uniform speed; the extruded spinning liquid enters a solidification liquid; the solidified primary fiber is collected by using a polytetrafluoroethylene roller; a drying treatment is performed to obtain the graphene oxide fiber; the graphene oxide fiber is subjected to chemical reduction to obtain the graphene fiber. According to the present invention, the spinning process is simple; the operation is performed at the room temperature; no strong corrosive reagent is used; the process has the characteristics of green environmental protection; the prepared graphene fiber has characteristics of good conductivity, excellent mechanical property and good toughness, can be woven into the pure graphene fiber cloth, can further be woven into various fabrics with other fibers, and can further be added to the polymer as the conduction enhancing additive and the like; the prepared graphene fiber can replace the carbon fiber to use in a plurality of fields.

The invention discloses a restoration agent for lowering cadmium / lead effective state content in soil, which is composed of quicklime, calcium sulfate, wood charcoal, iron chloride and water, wherein the weight ratio of the quicklime, calcium sulfate, wood charcoal and iron chloride is (1-2):(1-2):(1-2):(0.5-1), and the water accounts for 30-45 wt% of the soil. The restoration agent can be used for treating heavily polluted soil; and common chemical passivators can only restore lightly polluted soil, and do not have obvious effect on heavy pollution. The restoration agent can be used for treating both acidic soil and neutral soil. The restoration agent has high remediation efficiency for cadmium polluted soil; the reaction mechanisms relate to chemical precipitation and physical adsorption; and when one action fails due to change of the outside conditions, the other action can perform the guarantee function. The restoration agent has certain control actions on the lead effective state content in the polluted soil.

The invention discloses a preparation method of an ultralight and hydrophobic nano fibrillated cellulose aerogel with high oil absorption, and relates to a preparation method of cellulose aerogel. The method disclosed by the invention aims to solve the problem that existing cellulose aerogel which is lower in oil absorption multiplying power and strong in hydrophilicity is not suitable for oil-water separating materials. The method comprises the following steps: I, preparing cellulose aqueous liquor; II, preparing a nano fibrillated cellulose aqueous dispersion liquid; III, preparing a strongly gelatinous nano fibrillated cellulose aqueous dispersion liquid; IV, freezing and drying; and V, carrying out hydrophobic modification to obtain the ultralight and hydrophobic nano fibrillated cellulose aerogel with high oil absorption. The preparation method of the ultralight and hydrophobic nano fibrillated cellulose aerogel with high oil absorption is simple in preparation process, wide in source of raw materials, low in cost and environment-friendly and green. The invention relates to the preparation method of the ultralight and hydrophobic nano fibrillated cellulose aerogel with high oil absorption.

The invention discloses a nitrogen and phosphorus removal method by using pyrite as biochemical filling, belonging to the field of simultaneous nitrogen and phosphorus removal of low-carbon and nitrogen ratio sewage. The basic principle is as follows: thiobacillus denitrificans is subject to autotrophic denitrification by using sulfur in pyrite as an energy source, and ferrous ions and iron ions generated in the process of denitrification are used to react with phosphate radical to form precipitation so as to remove phosphorus, thus integral nitrogen and phosphorus removal is realized. The method comprises three stages of the preparation of reactor filling, the starting of a reactor and the operation of the reactor, and has the advantages of high process efficiency, low operation cost and low sludge yield. The reactor of the invention also has the advantages of small floor space and convenient operation. The reactor can work continuously, can be used singly in waste water processing, and also can be used as a processing unit of a processing system.

The invention provides a medium which is suitable for planting dendrobe, particularly planting dendrobium officinale, and a method for utilizing the medium to plant dendrobium officinale. The dendrobium officinale medium comprises an upper medium layer, a middle medium layer and a lower medium layer from top to bottom in sequence; the upper medium layer is deal sawdust, the middle medium layer is the mixture of deal sawdust and peat, and the lower medium layer is the mixture of deal sawdust and deal bark blocks. The dendrobium officinale medium and the plant method of dendrobium officinale have the advantages of wide sources and low cost; the appearance and the quality of the dendrobium officinale obtained with the medium and the method are superior to that of the dendrobium officinale obtained with other mediums.

The invention discloses a plant polysaccharide cigarette filter tip and a preparation method thereof. Plant polysaccharide, starch, adsorbent, plasticizer, emulsifier, waterproofing agent and plant protein are blended according to a certain proportion, so that the filter tip is prepared. The preparation method includes the following steps: (a) the starch, water and the plasticizer are blended and stirred, so that modified starch solution is obtained; (b) the plant polysaccharide and the modified starch solution are blended; (c) under certain conditions, the emulsifier, the waterproofing agent and the adsorbent are added into the mixture of the plant polysaccharide and the modified starch solution, and after stirring, the mixture is injected into a long cylindrical mold made of anti-freezing, heat-proofing material and molded; (d) the semifinished product is placed into a freezing environment and frozen, i.e. prefreezing; (e) the semifinished product in step d is placed into a freeze dryer and freeze-dried; (f) the porous composite body is taken out of the mold and deburred, and thereby a filter tip stick is obtained. Material resources are rich, the cost is low, and the three wastes cannot be produced. The performance is good, the filter tip can reduce the nicotine content by 40.2 to 84.1 percent, the tar by 26 to 72.1 percent and the nicotinamide by 20 to 39.2 percent, and after use, waste can be biodegraded.

The invention discloses a controlled release fertilizer coated by vegetable oil based polyurethane and a preparation method thereof. The preparation method of the controlled release fertilizer coated by vegetable oil based polyurethane comprises the following steps of: 1) preheating the granular fertilizer; 2) heating plant oil polyhydric alcohol containing 2-6 hydroxys and isocyanate containing at least two isocyanate groups, and uniformly mixing the ingredients to form a vegetable oil based polyurethane coating liquid; 3) spray coating the vegetable oil based polyurethane coating liquid on the surfaces of the preheated fertilizer granules, repeatedly spray coating the vegetable oil based polyurethane coating liquid for 2-10 times after the vegetable oil based polyurethane coating liquid solid is solidified to obtain the controlled release fertilizer coated by vegetable oil based polyurethane. According to the controlled release fertilizer coated by vegetable oil based polyurethane and the preparation method thereof provided by the invention, the adopted coating material is extensive in resource, cheap and liable to obtain, non-toxic, harmless, simple in production process and good in controlled release effect of fertilizer.

The invention discloses a method for preparing large-size high-quality graphene with controllable number of layers, wherein graphite powder or flake graphite is mainly adopted as a raw material. The method specifically comprises the steps of intercalating the graphite raw material by virtue of an intercalating agent to initially weaken the intercalation interaction force and obtain different orders of graphite intercalation compounds (GICs); soaking the GICs in an appropriate expander, and then under the case that an auxiliary agent is added or not, enabling the intercalation materials to be quickly reacted with the expander to release a gases to obtain highly expanded wormlike graphene aggregate and further to cause the distances among graphene lamellar layers to be increased; and after certain processing, peeling, and then repeatedly centrifuging and dispersing to obtain a graphene dispersion with different numbers of layers. According to the method disclosed by the invention, the intercalation-expansion-peeling process is involved, raw materials are cheap, the reaction process is simple and easily controlled, and the number of layers of graphene is precisely controlled; the obtained graphene lamellar layers have the advantages of few defects, large size, high conductivity, high yield and the like, the large-scale industrial production is easily implemented, and the problems of high cost, low productivity, poor quality, small size, uncontrollable number of layers and the like in an existing graphene preparation technology are solved.

The invention discloses a nitrogen doped carbon quantum dot as well as a preparation method and an application thereof, belonging to the technical field of material science. The preparation method comprises the steps: after mixing organic acid and organic amine, directly performing a hydrothermal reaction to prepare a nitrogen doped carbon quantum dot water dispersion solution, and extracting and drying the nitrogen doped carbon quantum dot water dispersion solution to obtain a nitrogen doped carbon quantum dot solid. The size of the nitrogen doped carbon quantum dot is not more than 10 nm, the nitrogen content is not more than 50 percent, the surface of the nitrogen doped carbon quantum dot contains amino, carboxyl and hydroxyl; and the quantum efficiency is 39.8-50 percent. The preparation method is simple to operate, environment-friendly, low in equipment requirement; and the prepared nitrogen doped carbon quantum dot has excellent light emitting property, and can be widely applied to fields such as photoelectric materials, biological imaging and fluorescence probe.

The invention discloses slow-release fertilizer with the effect of soil remediation, which is prepared by polyhydroxyalkanoates which can be completely biodegraded, organic and inorganic nutrients and other substances, by slow-releasing the organic and inorganic nutrients, microorganism propagation and sustained and rapid growth of plants can be promoted, the bioactivity and water solubility of polycyclic aromatic hydrocarbons are quickened, and simultaneously, the defects of fertilizer loss and repeated fertilization can be avoided, thereby saving the cost and enhancing the soil remediation efficiency. The invention also discloses a soil pollution remediation method by utilizing the slow-release fertilizer, plants with the remediation effect are planted in the soil with the slow-release fertilizer, and efficient, environment-friendly and sustained remediation of the soil polluted by the polycyclic aromatic hydrocarbons (PAHs) can be realized by utilizing the microorganism-plant remediation technology.

The invention discloses a method for preparing a manganese series lithium ion sieve adsorbent, and relates to a method for preparing an inorganic adsorbent for adsorbing lithium from liquid lithium resources such as brine of salt lake, seawater and the like. In the method, a cubic crystal ion sieve precursor Li1.6Mn1.6O4 is prepared from Mn2O3 and LiOH or Li2CO3 serving as raw materials by using two sections of solid-phase reactions, wherein the precursor also can be used as an anode material of a lithium ion battery. The precursor is acidized to obtain a lithium ion sieve adsorbent MnO2.0.5H2O (or expressed as H1.6Mn1.6O4), and the ion sieve is the lithium adsorbent which has high selectivity on lithium. The method has the advantages of simple and readily available raw materials, simple process, high adsorption capacity of the ion sieve, low cost, high purity of products and is easy to realize industrial production.

The invention discloses a freeze beverage containing isomaltose hypgather and process for preparation, wherein the raw materials comprise the following constituents (by weight ratio): cow's milk and / or dairy product and / or dairy product analogues 0-90%, isomaltose hypgather 0. 01-10. 0%, sugar 4. 0-16. 0%, stabilizing agent 0. 1-1. 0%, sour flavor agent 0-0. 7%, edible flavoring essence 0. 01-0. 4% and balancing water.

The invention relates a kind of preparation method of bio-diesel oil under the condition of solid ac and alk catalyzing. The character is that under the condition of solid ac and alk catalyzing, gain the bio-diesel oil using the craft of exchange reaction of soja oil with carbinol. Afer the reaction, apart catalyser from reaction liquor by centrifugal machine till delimination in quiet placing, the above is rough output, the below is admixture of glycerol and carbinol. Distil the of above to gain bio-diesel oil and to gain the pure glycerin in the same way. The distilled carbinol can be used again and again. The invention has many advantages, for example, its raw material can be rebirth, its craft is easy and only need normal equipment. Even treat the used oil, the whole process is easier compared with the method in solid ac and alk catalyzing, besides, the process will not produce foul water so it is environmental. Every plant of the bio-diesel accords with standards compared with foreign similar competitive grade and the main plants are close to its of 0# (GB252-1994, superior product)diesel of China.