583 results about "Triethanolamine" patented technology

The invention discloses a method for preparing calcium hydroxide slurry with high specific surface area and high pore volume, which comprises the following steps: S1, adding an alcohol reagent into water to obtain a solution A; s2, adding an inorganic salt solution into the solution A, and uniformly mixing to obtain a solution B; s3, a reagent X is added into the solution B, ultrasonic mixing is performed to obtain a solution C, and the reagent X is a mixture of phenol or triethanolamine, ethidene diamine and ethylamine; and S4, adding calcium oxide powder into the solution C, continuously stirring, and reacting to obtain calcium hydroxide slurry. The invention provides a method for preparing calcium hydroxide slurry with high specific surface area and high pore volume, the calcium hydroxide slurry prepared by the method can form calcium hydroxide with high specific surface area and high pore volume when in use, and the method aims to solve the problems of low specific surface area and low pore volume of the existing calcium hydroxide. Therefore, the problem of desulfurization performance inactivation caused by blockage of calcium hydroxide (desulfurizer) pores by generated CaSO3 and CaSO4 in the desulfurization process is avoided.

The invention provides glycyrrhizic acid / glycyrrhetinic acid-triethanolamine composite hydrogel as well as a preparation method and application thereof, and belongs to the technical field of preparation of biological medicine carriers and composite materials. According to the invention, glycyrrhizic acid or glycyrrhetinic acid is taken as a raw material, triethanolamine is taken as a cross-linking regulating agent, and the composite hydrogel with stable mechanical properties, high drug loading efficiency and anti-inflammatory synergistic activity is prepared through a mild physical and chemical cross-linking reaction; the preparation process of the composite hydrogel does not need a toxic cross-linking agent, the reaction condition is mild, the raw materials are cheap and easy to obtain, and large-scale production can be realized; the composite hydrogel presents a multi-group ionic bond cross-linked structure, can be used as a carrier of a pH responsive drug, and has good practicability.

The invention discloses a method for preparing calcium hydroxide with high specific surface area and high pore volume by a semi-dry method, which comprises the following steps: S1, adding an alcohol reagent into water, and uniformly mixing to obtain a solution A; s2, adding a composite cationic surfactant into the solution A, and dissolving to obtain a solution B; s3, adding an iron salt solution into the solution B, and uniformly mixing to obtain a solution C; s4, adding triethanolamine into the solution C, and performing ultrasonic dissolution to obtain a solution D; and S5, spraying the solution D into calcium oxide powder, continuously stirring, and reacting to prepare calcium hydroxide with high specific surface area and high pore volume. The calcium hydroxide prepared by the method has a high specific surface area and a rich pore structure, is powdery after reaction, and is relatively low in water content.

The invention provides liquiritin gel as well as a preparation method and application thereof. The liquiritin gel is prepared from the following components in concentration: 0.1 weight percent to 2 weight percent of liquiritin, 0.1 weight percent to 4 weight percent of carbomer, 0.1 weight percent to 4 weight percent of water-soluble cellulose ether compounds and 1 to 10 mL / Kg of triethanolamine. Wherein liquiritin and the water-soluble cellulose ether compound are respectively used as a main thickening agent and an auxiliary thickening agent, a synergistic thickening system is more stable and more suitable for liquiritin compared with a single thickening system or other neutralization systems, and the liquiritin and the water-soluble cellulose ether compound can synergistically adjust viscosity; triethanolamine is used as a neutralizer to neutralize carboxyl of carbomer to form gel; carbomer and a water-soluble cellulose ether compound are cooperated according to a specific ratio and can be different from a single thickening system or different neutralization systems, so that the liquiritin gel with excellent film-forming property, proper flowability and high transdermal absorption efficiency is prepared.

The invention discloses a solid ultrasonic gel patch as well as a preparation method and application thereof, and belongs to the technical field of medical chemistry. The solid ultrasonic gel patch is prepared from an acrylamide monomer, polyvinyl alcohol, sodium polyacrylate, sodium carboxymethyl cellulose, nano silicon dioxide, propylene glycol, glycerol, acrylic acid, triethanolamine, a cross-linking agent, an initiator and water according to a specific ratio. The prepared solid ultrasonic gel patch is highly matched with human soft tissue in acoustic impedance (about 1.62-1.63 * 10 < 6 > Pa.s / m), low in acoustic attenuation coefficient (less than or equal to 0.034 dB / (cm.MHz)), moderate in skin adhesion, excellent in flexibility and moisture retention, capable of solving the problems that a traditional ultrasonic coupling agent is inconvenient to use, easy to dry, poor in experience and the like, and suitable for acoustic wave conduction in ultrasonic examination and treatment.

The invention relates to the technical field of concrete, and particularly discloses low-temperature-resistant self-repairing waterproof concrete for water conservancy and a preparation method of the low-temperature-resistant self-repairing waterproof concrete. The water conservancy low-temperature-resistant self-repairing waterproof concrete is specifically prepared from the following components in parts by weight: 70 to 80 parts of cement, 10 to 20 parts of fly ash, 8 to 12 parts of silica fume, 2.5 to 3.5 parts of a reinforcing material, 0.2 to 0.4 part of a crystallization inducer, 1.5 to 2.5 parts of a repairing agent and 20 to 40 parts of water, the reinforcing material is formed by mixing nano silica sol, bentonite, quartz sand and triethanolamine; the crystallization inducer is formed by mixing sodium silicate and aluminum hypophosphite; the repairing agent is obtained by loading calcium ions on an amino silane modified zeolite material and then mixing with a bacillus pasteurii bacterial solution. By utilizing the technical scheme provided by the invention, the prepared concrete has excellent mechanical properties, water resistance, impermeability, freezing resistance, crack resistance and good durability.

The invention relates to cream for repairing radiodermatitis and a preparation method of the cream, and belongs to the technical field of biomedical skin treatment. The cream consists of the following components in percentage by weight: 8% of glycerin monostearate, 6% of stearic acid, 5% of white vaseline, 4% of liquid wax, 1-2% of tea tree oil, 1-2% of eugenol, 1-2% of vitamin E, 3% of trehalose, 8% of polyethylene glycol (PEG-400), 10% of glycerol, 0.5% of methylparaben, 1% of triethanolamine and the balance of purified water. According to the cream disclosed by the invention, the natural traditional Chinese medicine component eugenol and the natural substance vitamin E are utilized to synergistically enhance the anti-oxidation and bacteriostatic effects, and the tea tree oil, the trehalose and other effective components are utilized to repair radiodermatitis from multiple aspects of anti-inflammation, bacteriostasis, antioxidation, promotion of skin barrier repair and the like. The cream is simple in component, good in treatment effect, high in safety and convenient to produce and process, and can be popularized and applied to treatment of radiodermatitis.

The invention discloses a quick-hardening early-strength concrete mineral additive and a preparation method thereof, and belongs to the technical field of building materials. The additive comprises the following components in parts by weight: 50-75 parts of a mineral active material (compounded by silica fume, slag powder and metakaolin), 15-30 parts of a composite activator (sodium silicate, lithium sulfate and triethanolamine synergistically), 5-10 parts of a sustained-release microcapsule (calcium sulphoaluminate coated with nano-silica) and 2-5 parts of an auxiliary thickening agent (compounded by HPMC and a water reducing agent). The preparation method comprises the steps of mineral activation, excitant reaction and mixing of the microcapsule and the thickening agent. After the additive is doped into concrete, the 3h compressive strength is greater than or equal to 15MPa, the initial setting time is less than or equal to 5min, and the additive has low resilience (less than or equal to 13%), high durability (impermeability is greater than or equal to P11) and environmental adaptability (-5 DEG C strength fluctuation ratio is less than or equal to 9%). And compared with the prior art, the cost is reduced by 40%, and the method has remarkable economic and social benefits.

The invention discloses a novel compound rapid surface anesthetic and a preparation method thereof, and belongs to the field of pharmaceutical preparations. According to the anesthetic, core anesthetic components of lidocaine and tetracaine are compounded with propylene glycol-laurocapram synergistic penetration enhancer, menthol auxiliary penetration enhancer, carbomer 980 gel matrix, triethanolamine pH regulator, glycerol humectant, panthenol soothing agent, purified water and the like, a surface smearing agent is prepared through a specific process, and the anesthetic can be administered in combination with an iontophoresis technology. Compared with the existing surface anesthetic for the cosmetic surgery, the surface anesthetic disclosed by the invention solves the problems of slow effect taking and poor effect, can realize rapid penetration of local skin, has short anesthesia effect taking time, long duration and good effect, has no obvious irritation to the skin, has good product stability, can effectively reduce the drug toxicity, and has a good application prospect. The device is suitable for surface anesthesia of non-surgical medical beauty items such as skin beauty, laser treatment and water-light micro-needles.

The invention discloses a modified nano hydrated calcium silicate chloride ion curing agent as well as a preparation method and application thereof, and belongs to the technical field of chemical materials. The curing agent is composed of 65-75 parts of synergistically modified nano calcium silicate hydrate, 10-20 parts of mesoporous silica with a high specific surface area, a composite dispersion stabilizer with a specific ratio, and an active activator compounded by triethanolamine and anhydrous sodium sulfate. The nano calcium silicate hydrate is synergistically modified by gamma-aminopropyltriethoxysilane and sodium dodecyl benzene sulfonate, so that the nano calcium silicate hydrate has the excellent performance that the zeta-potential absolute value is greater than or equal to 25 mV, the dispersity is high, and the chloride ion binding capacity is improved by greater than or equal to 40%. Through the synergistic effect of all the components, the technical problems that an existing chloride ion curing agent is low in adsorption capacity, poor in selectivity, prone to agglomeration in concrete and the like are solved, and the chloride ion curing agent is particularly suitable for improving the durability of the concrete in harsh chloride salt environments such as port engineering and maritime work structures.

The invention relates to the technical field of surface strengthening treatment and coating preparation, in particular to a micro-arc oxidation electrolyte, a preparation method of the micro-arc oxidation electrolyte and a preparation method of an oxide ceramic coating on the surface of a magnesium-copper dissimilar metal material component. The invention provides a micro-arc oxidation electrolyte. The micro-arc oxidation electrolyte comprises a main film-forming agent, an arcing aid, a pH regulator, a corrosion inhibitor and water, the main film-forming agent comprises ammonium fluozirconate and / or potassium fluozirconate; the arcing aid comprises one or more of disodium hydrogen phosphate, sodium dihydrogen phosphate, ammonium dihydrogen phosphate and diammonium hydrogen phosphate; the corrosion inhibitor comprises one or more of hexamethylenetetramine, ammonium bifluoride and triethanolamine. The micro-arc oxidation electrolyte breaks through the problem that valve metal and non-valve metal cannot be subjected to arc discharge at the same time for micro-arc oxidation treatment in the micro-arc oxidation process.

The invention relates to a fabric flavor enhancer containing ester-based quaternary ammonium salt and a preparation method thereof. The fabric flavor enhancer containing ester-based quaternary ammonium salt comprises the following components: polyethylene glycol, an ester-based quaternary ammonium salt solution, modified silicon dioxide, polyquaternary ammonium salt and the like. The modified silicon dioxide is prepared by the following steps: carrying out a blending reaction on hydroxylated silicon dioxide and KH570 to obtain an intermediate product, then carrying out a blending reaction on triethanolamine, acrylic acid, lauric acid and sodium bromoacetate to obtain an intermediate product 2, and finally polymerizing the intermediate product, the intermediate product 2 and hydroxyethyl methylacrylate. Long alkyl chains, quaternary ammonium cations and hydroxyl are introduced into the modified silicon dioxide, so that organic matters on the surface of the modified silicon dioxide form a net-shaped structure; wherein the long alkyl chain can improve the compatibility; quaternary ammonium cations can neutralize charges and make the fabric softer and more fluffy; hydroxyl can adsorb essence, the antistatic performance and the like can be improved, and in addition, silicon dioxide and a net-shaped structure can further enhance the fragrance of the fabric.

The invention discloses polyacrylate anti-deposition and cerium chloride synergistic composite corrosion inhibitor cooling liquid, relates to the field of cooling liquid, and is particularly suitable for a multi-metal cooling system. According to the method, polyacrylate, cerium chloride, benzotriazole, benzimidazole, ethylene glycol, deionized water and triethanolamine serve as core raw materials, during preparation, equipment and the raw materials are pretreated, then a base solution is prepared, the pH value is adjusted to be alkalescent, then polyacrylate and cerium chloride are dissolved and coordinated, an auxiliary corrosion inhibitor is added, and synergistic protection is formed. And defoaming, filtering and filling. The cooling liquid adapts to multi-metal material protection through the synergistic effect of deposition resistance of polyacrylate and corrosion inhibition and synergism of cerium chloride, the cooling liquid is diluted according to working conditions during application, waste cooling liquid is discharged after being subjected to combined treatment of biological contact oxidation and Fenton oxidation, a finished product needs to be stored in a proper environment in a sealed mode, and the protection performance, the environmental protection property and the storage stability are effectively considered.

The invention discloses a method for preparing nano calcium carbonate by efficiently removing iron impurities in nano calcium carbonate raw material ore, and belongs to the technical field of nano material preparation. The method comprises the steps of raw material pretreatment, digestion treatment, size mixing treatment, carbonization treatment, surface treatment and drying, in the size mixing treatment process, a whitening agent Na2SO3 is adopted for removing iron in raw material ore, Na2SO3 serves as a reducing agent, Fe < 3 + > is reduced into Fe < 2 + >, a proper amount of whitening auxiliary such as DTPA or triethanolamine forms colorless water-containing iron chelate ions with iron ions, and the iron chelate ions are subjected to surface treatment. And through a synergistic system of the whitening agent and the whitening auxiliary agent, efficient removal of iron is realized. The whiteness of the prepared nano calcium carbonate reaches up to 97.2%, the nano calcium carbonate has the remarkable advantages of being efficient, environmentally friendly, economical and the like, the iron content in the nano calcium carbonate can be remarkably reduced, the purity and whiteness of the product are effectively improved, and the high requirement of the high-end application field for the quality of the nano calcium carbonate is met. Meanwhile, the method is simple and convenient to operate and easy to industrially apply, and has wide market prospects and popularization value.

The invention belongs to the technical field of medical or hygiene materials, and particularly relates to a medical human body lubricant and a preparation method and application thereof.The medical human body lubricant is prepared from, by mass, 1%-20% of glycerin, 1%-20% of propylene glycol, 0.1%-1% of hydroxyethyl cellulose, 0.05%-0.5% of carbomer, 0.05%-0.5% of sodium polyacrylate, 0.05%-0.5% of triethanolamine, 0.2%-1% of preservative and the balance purified water. The medical human body lubricant prepared by the invention has high moisture retention, is mild and non-irritant, and is suitable for people sensitive to skin.

The invention discloses a preparation method of high-color-fastness woven body paper and the high-color-fastness woven body paper, and relates to the technical field of papermaking, and the preparation method of the high-color-fastness woven body paper comprises the steps of preparing a composite dyeing assistant and preparing the woven body paper. The preparation method comprises the following steps: stirring and mixing cationic microcrystalline cellulose, sodium carboxymethyl cellulose, triethanolamine myriceate, glucan hydroxypropyl trimethyl ammonium chloride, a water-based polycarbodiimide cross-linking agent and deionized water to obtain a composite dyeing assistant, then adding the composite dyeing assistant into slurry, adding a water-based dye, and carrying out a papermaking process to obtain the composite dyeing assistant. According to the method, the color fastness of the woven body paper can be improved. The sun-proof grade of the high-color-fastness woven body paper is greater than or equal to 4 grades.

The present application relates to a kind of carbon dioxide mineralization method and carbon dioxide mineralization device.The carbon dioxide mineralization method includes the following steps: mixing absorption liquid and industrial solid waste at room temperature, obtain mortar;Make mortar solid-liquid separation, obtain clear liquid and thick slurry;Carbon dioxide in flue gas is absorbed by clear liquid, obtain carbon-rich absorption liquid;Carbon-rich absorption liquid and thick slurry occur mineralization reaction at 180 DEG C-220 DEG C, obtain mineralized slurry;Make mineralized slurry solid-liquid separation, obtain mineralized ash and mineralized clear liquid;Wherein, absorption liquid includes inorganic base and organic base, organic base includes monoethanolamine, diethanolamine, triethanolamine, 3-methylaminopropylamine, N-methyl diethanolamine, piperazine, diethylene triamine, triethylene tetramine, tetraethylene pentamine and 2-amino-2-methyl-1-propanolamine at least two kinds.The method greatly improves CO2 capture rate and CO2 utilization rate, and organic base consumption is less, absorption liquid regeneration energy consumption is low, and overall economy is good.

This invention discloses a demulsifier for polymer flooding crude oil produced fluids, its preparation method, and its application, belonging to the field of chemical additives for petrochemicals. The technical solution includes a main agent, an auxiliary agent, a penetrant, and water; the main agent is a polyene-polyamine block polyether, the auxiliary agent is a triethanolamine block polyether quaternary ammonium salt, and the penetrant is selected from at least one of methanol, ethanol, ethylene glycol, and diethylene glycol butyl ether; in the demulsifier, the ratio of the main agent to the auxiliary agent is 4-9:1, the amount of penetrant is 30% of the total amount of the main agent and auxiliary agent, and the amount of water is 70% of the total amount of the main agent and auxiliary agent. This invention, applied to demulsification of polymer flooding crude oil produced fluids, features high demulsification efficiency and rapid demulsification effect.

The invention discloses easy-to-disperse diamond grinding fluid and a preparation method thereof, and relates to the technical field of grinding fluid. The easy-to-disperse diamond grinding fluid is prepared from the following raw materials in parts by weight: 1 to 20 parts of modified diamond micro powder, 40 to 80 parts of deionized water, 1 to 10 parts of polyethylene glycol 6000, 0.5 to 1.2 parts of sodium carboxymethyl cellulose, 1 to 20 parts of glycerol, 1 to 10 parts of triethanolamine, 0.3 to 0.7 part of sodium polyacrylate, 0.05 to 5 parts of 1, 2-benzisothiazolin-3-ketone and 1 to 10 parts of a modified silane coupling agent. According to the easy-to-disperse diamond grinding fluid, through the synergistic effect of the modified diamond micro powder and the modified silane coupling agent, the dispersity is excellent, and the stability is high; the formula is scientific, polyethylene glycol and other assistants are matched, precise process parameters and graded filtration are combined, the grinding efficiency is high, the surface smoothness of a workpiece is good, the antibacterial property and storage stability are good, and the application scene is wide.

This invention belongs to the field of pharmaceutical chemistry, and specifically relates to a compound antifungal cream containing the traditional Chinese medicine ingredient tryptamine ketone and its application. The invention comprises the following components, with the following percentage content: stearic acid 10%~16%, glyceryl monostearate 3%~7%, liquid paraffin 5%~9%, tryptamine 0.1%~0.01%, terbinafine hydrochloride 0.00625%~0.000625%, glycerin 4%, triethanolamine 2%~6%, ethylparaben 0.5%, and the balance being purified water or distilled water. This invention is highly effective, low in toxicity, and exhibits low drug resistance.

The invention discloses chlorinated polypropylene modified water-based acrylic resin with high adhesive force and water resistance and a preparation method of the chlorinated polypropylene modified water-based acrylic resin. The chlorinated polypropylene modified water-based acrylic resin is prepared from the following components in percentage by mass: 5-15% of chlorinated polypropylene, 20-30% of methyl methacrylate, 5-10% of isobornyl acrylate, 10-15% of methoxy polyethylene glycol monomethacrylate, 3-5% of acrylic acid, 0.5-1.5% of an initiator and 2-5% of hydroxyethyl acrylate. The cleaning agent is prepared from the following components in percentage by weight: 20-40% of triethanolamine, 3-8% of triethanolamine, 5-10% of acetone, 20-40% of sec-butyl acetate and 1-5% of deionized water. The optimal raw material composition and proportion are screened through a large number of experiments, the optimal synthesis process is preferably obtained through a large number of experiments, the conversion rate reaches up to 99%, and the solid content of the resin reaches 65% or above. The chlorinated polypropylene modified water-based acrylic resin with high adhesive force and water resistance has the advantages of excellent adhesive force, water resistance, storage stability and the like, and has a very good technical effect in comprehensive performance.

This invention relates to the field of pesticide technology, specifically to a fungicidal composition, its preparation method, and its uses. The invention provides a fungicidal composition comprising an active ingredient, a first functional component, a second functional component, and an adjuvant; the active ingredient comprises fluthiazopyrone and cyazofamid; the first functional component comprises at least one selected from silica, titanium dioxide, and zinc oxide; the second functional component comprises at least one selected from citric acid, acetic acid, benzoic acid, urea, and triethanolamine. By introducing specific first and second functional components, this invention synergistically works with the active ingredient, effectively overcoming the key defects of fluthiazopyrone's easy photodegradation and cyazofamid's easy hydrolysis, thus improving the stability of the compound formulation; while ensuring the excellent control efficacy and resistance management advantages of both against oomycete diseases such as grape downy mildew, it extends the duration of action and weather resistance of the agent, providing a more stable, efficient, and long-lasting solution for field application.

This invention relates to a rapid-setting high-strength concrete and its preparation method. The rapid-setting high-strength concrete comprises the following raw materials in parts by weight: 100-200 parts cement, 80-100 parts coarse aggregate, 40-60 parts fine aggregate, 10-20 parts rubber powder, 20-30 parts modified straw-based carbon powder, 0.3-0.5 parts coupling agent, and 0.6-0.8 parts water-reducing agent. The modified straw-based carbon powder is obtained by first adding straw powder to an activation solution containing aluminum sulfate, carboxymethyl starch, and triethanolamine, followed by activation, ball milling, and freeze-drying to obtain a precursor. The precursor is then mixed with flake aluminum powder and heated under an inert atmosphere to obtain the final product. The mass fraction of aluminum sulfate is 5-10%, the mass fraction of carboxymethyl starch is 5-10%, and the mass fraction of triethanolamine is 3-5%. This invention improves the rapid setting effect, compressive strength, flexural strength, and crack resistance of concrete by incorporating modified straw-based carbon powder into the concrete components. This is of great significance for improving the overall performance of concrete and developing infrastructure construction.

The invention discloses a composite thermal insulation material suitable for A-grade fire prevention and a preparation method thereof, relates to the technical field of building composite materials, and solves the problem that an existing building material is difficult to meet the comprehensive requirements of fire prevention, thermal insulation and freezing resistance in alpine regions. Comprising quick-hardening sulphoaluminate cement, silica powder, MDI-50, polyether polyol, silane coupling agent modified basalt fibers, silane coupling agent modified polyvinyl alcohol fibers, triethanolamine, a thickening foam stabilizer, fatty alcohol ether sodium sulfate and 1-1.5 parts of a calcium nitrite antifreezing agent. The thickening foam stabilizer is a compound of hydroxypropyl methyl cellulose and polyether modified silicone oil. The material can be prepared without special construction equipment, can be accurately adapted to construction scenes of traffic inconvenience and energy shortage in alpine regions, and has extremely high engineering application value and popularization prospect.

The invention discloses a flexible glass cutting fluid and a preparation method thereof, and the preparation method comprises the following steps: S1, adding cellobiose into DMF, then adding chloroacetic anhydride and pyridine, and carrying out a stirring reaction to obtain an intermediate; s2, adding the intermediate into DMF (Dimethyl Formamide), and then carrying out constant-temperature reaction on glycerol monocaprylate, 2-(2-hydroxyphenyl) benzothiazole and triethylamine to obtain a modifier; s3, uniformly mixing a modifier, sodium dioctyl sulfosuccinate and a polyoxyethylene polyoxypropylene block copolymer, so as to obtain a composite surfactant; s4, adding the composite surfactant, the propylene glycol, the defoaming agent, the sterilizing agent and the triethanolamine into the water, and uniformly stirring to obtain the cleaning agent. According to the prepared cutting fluid, the protection effect on a flexible glass base material and a surface functional layer of the flexible glass base material is remarkably improved while the excellent wettability is kept, microcrack generation and surface damage in the cutting process are reduced, and the cutting fluid is particularly suitable for precise glass processing of flexible display devices.

The invention relates to the technical field of petroleum and natural gas drilling engineering, in particular to a solid-free well killing fluid and a preparation method thereof, and the solid-free well killing fluid comprises the following raw materials in parts by weight: 80-100 parts of a base fluid, 25-35 parts of a composite additive, 8-12 parts of a soluble thickener, 6-10 parts of a liquid-phase anti-collapse agent and 3-5 parts of a lubricating aid. According to the high-density well killing fluid, a high-density system is constructed through the additive solution A of the composite additive, the specific gravity upper limit of a traditional salt weighting agent is broken through, the hydrotropy stabilizing effect of triethanolamine is combined, salting-out of high-concentration components is avoided, and the problem that specific gravity increase of traditional solid-free well killing fluid is limited is effectively solved; the system viscosity is increased, a liquid rubber plug can be formed, exchange dilution of the well killing fluid and residual sewage in a shaft is effectively blocked, performance degradation caused by dilution of the well killing fluid is avoided, and material waste caused by supplementing of the well killing fluid is also reduced.

The invention belongs to the technical field of refractory materials, and particularly relates to an environment-friendly high-temperature-resistant refractory brick and a preparation method thereof. The environment-friendly high-temperature-resistant refractory brick is prepared from the following raw materials in percentage by weight: 12 to 15 weight percent of crystalline flake graphite, 8 to 12 weight percent of modified fly ash, 1 to 3 weight percent of zirconium oxide, 5 to 8 weight percent of composite binder and the balance of magnesium oxide, the modified fly ash is prepared by the following preparation processes: adding fly ash into a nitric acid solution, stirring, filtering, washing and drying to obtain active fly ash; adding the active fly ash, a surfactant and scandium chloride into water, adjusting the pH value at 50-60 DEG C, standing, filtering, washing and drying to obtain scandium modified fly ash; ball-milling and mixing the scandium modified fly ash, lime slag and triethanolamine, and calcining to obtain the modified fly ash. The refractory brick disclosed by the invention has excellent compression strength, high-temperature fracture resistance and excellent oxidation resistance.

This application relates to the field of wastewater treatment, specifically disclosing a sulfur autotrophic denitrification process; including the following specific steps: S1: After adjusting the pH of calcium nitrate tetrahydrate solution and ammonium dihydrogen phosphate solution to alkaline, triethanolamine is added dropwise to the calcium nitrate solution, followed by the addition of ammonium dihydrogen phosphate solution to form a reaction solution. The pH of the reaction solution is maintained at alkaline, and the reaction is heated. After filtration, washing, and drying, hydroxyapatite powder is obtained. The hydroxyapatite powder is mixed with a foaming agent, foam stabilizer, and adhesive, pressed into shape, and sintered to obtain a porous ceramic carrier; S2: The porous ceramic carrier, ground inorganic energy material, and denitrifying bacteria are added to the wastewater to be treated, mixed, and subjected to aeration treatment. The inorganic energy material is replenished periodically to complete the process. The sulfur autotrophic denitrification process used in this application has high denitrification efficiency, and no replenishment of denitrifying bacteria is required during the process.

The invention relates to the technical field of coatings, and provides a high-solid-content solvent-free high-build epoxy resin coating as well as a preparation method and application thereof.The coating comprises a first component and a second component, the first component comprises modified epoxy resin, a reactive diluent, a filler and an auxiliary agent; the second component comprises a modified curing agent, a composite accelerant and a retarder; the composite accelerant is formed by compounding modified nano zinc oxide and a composite catalyst; the modified nano-zinc oxide is prepared by reacting KH560 with nano-zinc oxide and then reacting with 3-sulfonic acid propyl methacrylic acid potassium salt; the composite catalyst is formed by compounding imidazolium salt ionic liquid and triethanolamine. A flexible chain segment is introduced into the modified epoxy resin to reduce viscosity, the modified curing agent adopts cardanol and mixed amine to be compounded to regulate and control reaction, and the composite accelerant and the retarder cooperate to catalyze and control speed; the problems of incomplete curing and low performance caused by the fact that the diffusion of a curing agent in a thick coating of the high-solid-content solvent-free thick paste type epoxy resin coating is blocked are solved.

The invention discloses an efficient flame-retardant fire extinguishing agent for rapidly extinguishing a lithium battery fire and a preparation formula, and relates to the technical field of fire fighting. The fire extinguishing agent is composed of a liquid-phase component and a solid-phase component, wherein the liquid-phase component comprises ethylene glycol, triethanolamine, fluoroalkyl betaine, sodium dodecyl benzene sulfonate, a phosphate flame retardant, an orange peel extracting solution and purified water; the solid-phase component comprises dodecyl sulfate, ammonium phosphate, potassium perchlorate, sodium carboxymethyl cellulose, polyacrylamide, benzotriazole and the like. The method comprises the following steps: drying and activating solid-phase components after graded crushing, and stirring in a nitrogen atmosphere; carrying out segmented treatment on liquid-phase components, and carrying out ultrasonic emulsification on an orange peel extracting solution; and after solid-liquid mixing, carrying out vacuum defoaming, high-speed shearing dispersion and homogenization treatment. According to the lithium battery fire extinguishing agent, component particle sizes with different dissolution rates are matched through graded crushing, nanoscale dispersion is achieved through ultrasonic emulsification, the bubble residual rate is reduced through vacuum defoaming, and the problems that a traditional lithium battery fire extinguishing agent is low in insulativity, low in cooling efficiency and insufficient in flame retardant efficiency are solved.