The invention discloses a preparation and regeneration method of an iron-aluminum-
lanthanum-based composite
fluorine removal agent, relates to the technical field of
fluorine removal agent preparation, and aims to solve the problem that the performance of an existing
fluorine removal agent needs to be improved. The preparation method comprises the following steps: weighing raw materials according to a
molar ratio of iron ions to aluminum ions to
lanthanum ions of 1: 1: 1, fully stirring and dissolving the raw materials in deionized water at
room temperature, and making the volume constant to prepare a clear
mixed solution; adding excessive
triethanolamine into the
mixed solution, dropwise adding a
nitric acid solution, adjusting the pH value of the
mixed solution to 3.0-4.0, continuously stirring at
room temperature, and fully reacting to obtain a precursor solution; continuously heating and stirring the precursor liquid at 150 DEG C for
dehydration to obtain
organic group brown fluffy precursor
powder; fully
grinding the precursor
powder, and calcining to obtain a gray powdery iron-aluminum-
lanthanum-based composite fluorine removal agent; the method is simple, the prepared fluorine removal agent is large in adsorption capacity and short in reaction time, most of the adsorption capacity can be recovered through simple acid
pickling, operation is easy, the service life is long, and the regeneration cost is low.