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1075 results about "Triethanolamine" patented technology

Triethanolamine aka Trolamine (abbr. as TEOA or TELA to distinguish it from TEA which is for triethylamine) is a viscous organic compound that is both a tertiary amine and a triol. A triol is a molecule with three alcohol groups. Approximately 150,000 tonnes were produced in 1999. It is a colourless compound although samples may appear yellow because of impurities.

Preparation method of calcium hydroxide with high specific surface area

The invention belongs to the technical field of calcium hydroxide preparation, and particularly relates to a preparation method of calcium hydroxide with high specific surface area, which comprises the following steps: S1, adding triethanolamine and diethanolisopropanolamine into water, and uniformly mixing to obtain an active agent solution; s2, mixing quick lime with an active agent solution, and carrying out digestion reaction to generate a calcium hydroxide coarse material; and S3, sieving and drying the calcium hydroxide coarse material to obtain the calcium hydroxide with the high specific surface area. The specific surface area of calcium hydroxide can be remarkably increased through the active agent solution, meanwhile, the uniformity and sufficiency of the quick lime digestion reaction are optimized, the calcium hydroxide particle aggregation phenomenon is reduced, and finally the calcium hydroxide product with the high specific surface area and the high activity is prepared.
Owner:XINJIANG LONGXIN ENVIRONMENTAL PROTECTION TECH CO LTD

Ultralow-density foam concrete and preparation method thereof

The invention relates to the technical field of concrete, and particularly discloses ultralow-density foam concrete and a preparation method thereof. The ultralow-density foam concrete is prepared from the following raw materials in parts by weight: 35 to 60 parts of cement, 15 to 25 parts of steel slag, 8 to 15 parts of lightweight aggregate, 1 to 3 parts of reinforced fiber, 0.5 to 1 part of a foaming agent, 0.1 to 0.3 part of a stabilizer, 0.3 to 0.5 part of a foaming aid and 30 to 70 parts of water, the foaming aid is at least one of aluminum powder, silica fume, calcium stearate and triethanolamine, and the foaming agent is one of an animal protein foaming agent and a rosin foaming agent; the foaming agent and the foaming aid are combined, a stable foam structure is formed in a concrete system, meanwhile, the phenomena of foam merging and foam breaking are reduced, formation of communicating holes is reduced while the foam hole structure is refined, the stability of foam concrete bubbles is improved, and foam collapse is reduced.
Owner:HANGZHOU HANTE BUILDING MATERIALS CO LTD

WS2 / MXene / HBPSi synergistically enhanced epoxy resin composite material and preparation method thereof

PendingCN120484445APolymer scienceSilicic acid
The invention discloses a preparation method of a WS2 / MXene / HBPSi synergistically enhanced epoxy resin composite material. The preparation method specifically comprises the following steps: preparing a WS2 / MXene hybrid from few-layer MXene powder, WCl6 and a sulfur source precursor; the preparation method comprises the following steps: uniformly mixing tetraethoxysilane, neopentyl glycol and triethanolamine, and carrying out gradient heating reaction to obtain HBPSi; epoxy resin EP is used as a resin matrix, DDS is used as a curing agent, a WS2 / MXene hybrid is used as a lubricating additive, HBPSi is used as a toughening agent, and the epoxy resin composite material is prepared by combining a melt blending process with a staged heating curing method. According to the method, the toughness and the interface bonding strength of the material are remarkably improved by introducing HBPSi, the friction coefficient of the material is effectively reduced and the wear resistance is improved through the synergistic effect of WS2 and MXene, and cooperative regulation and control of structural strengthening and friction performance improvement are achieved.
Owner:XIAN UNIV OF TECH

Method for preparing calcium hydroxide slurry with high specific surface area and high pore volume

The invention discloses a method for preparing calcium hydroxide slurry with high specific surface area and high pore volume, which comprises the following steps: S1, adding an alcohol reagent into water to obtain a solution A; s2, adding an inorganic salt solution into the solution A, and uniformly mixing to obtain a solution B; s3, a reagent X is added into the solution B, ultrasonic mixing is performed to obtain a solution C, and the reagent X is a mixture of phenol or triethanolamine, ethidene diamine and ethylamine; and S4, adding calcium oxide powder into the solution C, continuously stirring, and reacting to obtain calcium hydroxide slurry. The invention provides a method for preparing calcium hydroxide slurry with high specific surface area and high pore volume, the calcium hydroxide slurry prepared by the method can form calcium hydroxide with high specific surface area and high pore volume when in use, and the method aims to solve the problems of low specific surface area and low pore volume of the existing calcium hydroxide. Therefore, the problem of desulfurization performance inactivation caused by blockage of calcium hydroxide (desulfurizer) pores by generated CaSO3 and CaSO4 in the desulfurization process is avoided.
Owner:CHANGZHOU INST OF TECH +1

Antifouling waterborne polyurethane coating for ships

The invention discloses an antifouling waterborne polyurethane coating for ships, and relates to the technical field of waterborne polyurethane coatings, and the antifouling waterborne polyurethane coating is prepared from the following raw materials in parts by weight: 5 to 8 parts of polytetrahydrofuran, 3 to 5 parts of diphenylmethane diisocyanate, 4 to 5.2 parts of chain extender and 0.45 to 0.7 part of functional filler. According to the antifouling waterborne polyurethane coating for the ship, the chain extender I tends to be distributed on a coating-water interface through the hydrophilicity of triethanolamine in the chain extender I, meanwhile, boric acid groups are preferentially in contact with seawater and are distributed on the surface layer of a coating, the water solubility is high, boric acid ions are rapidly released at the initial stage, and the antifouling waterborne polyurethane coating is good in antifouling property. The initial adhesion of marine microorganisms is inhibited through ion repulsion; an MDI fragment in the chain extender II provides an extra-NCO reaction site, and chemical crosslinking is generated between the MDI fragment and a network formed by the chain extender I, so that the overall crosslinking density is improved, and the toughness and weather resistance of a coating film are improved.
Owner:YANTAI HAIYU NEW MATERIAL CO LTD

Glycyrrhizic acid / glycyrrhetinic acid-triethanolamine composite hydrogel as well as preparation method and application thereof

The invention provides glycyrrhizic acid / glycyrrhetinic acid-triethanolamine composite hydrogel as well as a preparation method and application thereof, and belongs to the technical field of preparation of biological medicine carriers and composite materials. According to the invention, glycyrrhizic acid or glycyrrhetinic acid is taken as a raw material, triethanolamine is taken as a cross-linking regulating agent, and the composite hydrogel with stable mechanical properties, high drug loading efficiency and anti-inflammatory synergistic activity is prepared through a mild physical and chemical cross-linking reaction; the preparation process of the composite hydrogel does not need a toxic cross-linking agent, the reaction condition is mild, the raw materials are cheap and easy to obtain, and large-scale production can be realized; the composite hydrogel presents a multi-group ionic bond cross-linked structure, can be used as a carrier of a pH responsive drug, and has good practicability.
Owner:JIANGSU UNIV

Copper-nickel alloy foil and preparation method and application thereof

The invention provides a copper-nickel alloy foil and a preparation method and application thereof, and belongs to the technical field of lithium ion battery negative electrode current collectors, and the preparation method comprises the following steps: preparing a copper-nickel composite electrolyte, and adding a coordination agent, a pH buffer agent and an additive into the copper-nickel composite electrolyte to obtain a mixed electrolyte; the coordination agent comprises a main coordination agent and an auxiliary coordination agent, and the main coordination agent comprises at least one of trisodium citrate, potassium sodium tartrate and sodium pyrophosphate; the auxiliary coordination agent comprises at least one of ammonia water, glycine and triethanolamine; and a cathode and an anode are placed in the mixed electrolyte, the pH of the mixed electrolyte is controlled to be 6-10, direct current is applied for electrochemical deposition, and the copper-nickel alloy foil is obtained. According to the method, the alkalescence system is adopted, the main coordination agent and the auxiliary coordination agent are used, full coordination of free Cu < 2 + > and Ni < 2 + > is achieved, precipitation is avoided, the hydrogen evolution phenomenon is greatly reduced, and the alloy foil quality is improved.
Owner:HUBEI ZHONGYI TECH +1

Method for preparing calcium hydroxide with high specific surface area and high pore volume by semi-dry method

The invention discloses a method for preparing calcium hydroxide with high specific surface area and high pore volume by a semi-dry method, which comprises the following steps: S1, adding an alcohol reagent into water, and uniformly mixing to obtain a solution A; s2, adding a composite cationic surfactant into the solution A, and dissolving to obtain a solution B; s3, adding an iron salt solution into the solution B, and uniformly mixing to obtain a solution C; s4, adding triethanolamine into the solution C, and performing ultrasonic dissolution to obtain a solution D; and S5, spraying the solution D into calcium oxide powder, continuously stirring, and reacting to prepare calcium hydroxide with high specific surface area and high pore volume. The calcium hydroxide prepared by the method has a high specific surface area and a rich pore structure, is powdery after reaction, and is relatively low in water content.
Owner:CHANGZHOU INST OF TECH +1

Preparation method of modified steel slag powder applied to cold-mixed full-steel-slag asphalt mixture

The invention relates to the technical field of modified steel slag powder, and discloses a preparation method of modified steel slag powder applied to a cold-mixed full-steel-slag asphalt mixture, which comprises the following preparation steps: 1) stirring and mixing 80-90 parts by mass of steel slag, 10-20 parts by mass of waste slurry powder particles and 1-2 parts by mass of triethanolamine in a stirring drum to form a mixture; 2) grinding the mixture in a ball mill for a set time to form powder; 3) drying the powder in a dryer to obtain modified steel slag powder; through the preparation steps, the activity, the particle distribution uniformity, the compatibility with the emulsified asphalt and the chemical stability of the modified steel slag powder are remarkably improved, so that a higher-quality material choice is provided for the application of the cold-mixed full-steel-slag asphalt mixture.
Owner:SHENZHEN MUNICIPAL ENG CORP +1

Aqueous total-iron flow battery negative electrode electrolyte and aqueous total-iron flow battery

The invention discloses an aqueous all-iron flow battery negative electrode electrolyte and an aqueous all-iron flow battery, and belongs to the fields of an electrochemical energy storage technology and a flow battery. The aqueous total iron flow battery negative electrode electrolyte comprises an iron ion-containing active substance, a first complexing agent, a second complexing agent and hydrogen evolution inhibitor, a supporting electrolyte and water, and the first complexing agent and the second complexing agent and hydrogen evolution inhibitor are simultaneously combined to iron ions to form a stable chelate with a saturated six-coordinate structure. The first complexing agent is selected from triethanolamine or analogues thereof, and the second complexing agent and hydrogen evolution inhibitor is selected from organic acids having a chelation effect and salts thereof. According to the invention, two complexing agents are combined with the same iron ion at the same time to form a stable six-coordinate structure, so that the problems of capacity fading, low energy efficiency and poor cycling stability caused by iron separation and hydrogen separation due to dissociation of organic matters and ferrous ions in the operation process of the battery are effectively relieved.
Owner:SICHUAN SHENGKUN NEW ENERGY TECHNOLOGY CO LTD

Water-resistant silk leather and related materials, and methods of making and using the same

A host of new silk material formats are disclosed, all prepared from an initial liquid composition including both silk fibroin and a polysaccharide. In some cases, particularly preferred material properties are achieved by the addition of a plasticizer selected from the group consisting of a di(ethylene glycol), a tri(ethylene glycol), a di(propylene glycol), a tri(propylene glycol), triethanolamine, a vegetable oil, and combinations thereof. These various formats include liquids, whipped silk creams, silk meringues, and compressed / heat-compressed meringues. Among the useful end-uses for these materials is a silk leather, which mimics the feel of conventional leather. Other uses include thermal insulation, absorption / gas sensing, biological scaffolding, and the like. A material that has material properties unexpectedly similar to mycelium is also disclosed.
Owner:TRUSTEES OF TUFTS COLLEGE

Liquiritin gel as well as preparation method and application thereof

The invention provides liquiritin gel as well as a preparation method and application thereof. The liquiritin gel is prepared from the following components in concentration: 0.1 weight percent to 2 weight percent of liquiritin, 0.1 weight percent to 4 weight percent of carbomer, 0.1 weight percent to 4 weight percent of water-soluble cellulose ether compounds and 1 to 10 mL / Kg of triethanolamine. Wherein liquiritin and the water-soluble cellulose ether compound are respectively used as a main thickening agent and an auxiliary thickening agent, a synergistic thickening system is more stable and more suitable for liquiritin compared with a single thickening system or other neutralization systems, and the liquiritin and the water-soluble cellulose ether compound can synergistically adjust viscosity; triethanolamine is used as a neutralizer to neutralize carboxyl of carbomer to form gel; carbomer and a water-soluble cellulose ether compound are cooperated according to a specific ratio and can be different from a single thickening system or different neutralization systems, so that the liquiritin gel with excellent film-forming property, proper flowability and high transdermal absorption efficiency is prepared.
Owner:GUANGDONG PHARMA UNIV

Aloe extract-probiotic composite hydrogel for skin diseases of pets

The invention belongs to the technical field of medical preparations for pets, and particularly relates to an aloe extract-probiotic composite hydrogel for pet dermatosis, a preparation method comprises the following steps: under an aseptic condition, animal combined lactobacillus ZYpet-012 with the preservation number of CGMCC No.32008 is subjected to solid slant culture medium recovery and liquid culture, and then the animal combined lactobacillus ZYpet-012 with the preservation number of CGMCC No.32008 is subjected to freeze-drying to obtain the aloe extract-probiotic composite hydrogel for pet dermatosis. Centrifugally washing to obtain a probiotic suspension; the preparation method comprises the following steps: preparing blank hydrogel from carbomer 940, triethanolamine, zinc hyaluronate and the like; and mixing the aloe extract solution with the blank hydrogel, and then adding the probiotic suspension to prepare the composite hydrogel. According to the present invention, by using the anti-inflammatory, antibacterial and prebiotic characteristics of the aloe extract and combining the skin micro-ecology adjusting effect of the animal and the lactobacillus ZYpet-012, the prepared composite hydrogel can effectively treat the skin diseases of pets, and has advantages of nature, safety, accurate targeting and the like.
Owner:北京和益源生物技术有限公司

Herbal sleep-aiding gel and preparation process thereof

The invention belongs to the technical field of sleep-aiding gels, and discloses a herbal sleep-aiding gel and a preparation process thereof, the gel comprises the following components: deionized water, propylene glycol, glycerol, carbomer 980 and triethanolamine; the mask is prepared from, by weight, 1.8% of lavender essential oil, chamomile extract, bitter orange flower essential oil, gamma-aminobutyric acid, melatonin, spina date seed extract, xylaria nigripes extract and phospholipid wall materials. Sodium chloride and azone; camphor and borneol; eDTA (Ethylene Diamine Tetraacetic Acid) disodium, phenoxyethanol and ethylhexylglycerin. The traditional Chinese medicine composition is suitable for people with sleep disorders such as long-term insomnia, difficulty in falling asleep, insomnia and dreaminess, easy awakening due to light sleep, restlessness and depression and the like; through the high transdermal absorption rate of a nano micro-capsule technology, in combination with a colloid double-electrode-layer structure, capacitance-like micro-current is generated, in cooperation with lavender-chamomile-bitter orange flower and other herbal essence and GABA and melatonin active ingredients, the sleep center is adjusted in a multi-channel mode, and the physical sleep-aiding scheme is a new physical sleep-aiding scheme for safely replacing a sleeping drug.
Owner:HANYI VALLEY (HAINAN) HEALTH TECHNOLOGY GROUP CO LTD

Solid ultrasonic gel patch as well as preparation method and application thereof

The invention discloses a solid ultrasonic gel patch as well as a preparation method and application thereof, and belongs to the technical field of medical chemistry. The solid ultrasonic gel patch is prepared from an acrylamide monomer, polyvinyl alcohol, sodium polyacrylate, sodium carboxymethyl cellulose, nano silicon dioxide, propylene glycol, glycerol, acrylic acid, triethanolamine, a cross-linking agent, an initiator and water according to a specific ratio. The prepared solid ultrasonic gel patch is highly matched with human soft tissue in acoustic impedance (about 1.62-1.63 * 10 < 6 > Pa.s / m), low in acoustic attenuation coefficient (less than or equal to 0.034 dB / (cm.MHz)), moderate in skin adhesion, excellent in flexibility and moisture retention, capable of solving the problems that a traditional ultrasonic coupling agent is inconvenient to use, easy to dry, poor in experience and the like, and suitable for acoustic wave conduction in ultrasonic examination and treatment.
Owner:SICHUAN TAIYOU TECH CO LTD

Gynecological gel with repairing effect

PendingCN120285160AOrganic active ingredientsAntibacterial agentsSodium methylparabenPharmacology
The invention is suitable for the technical field of gynecological gels, and provides a gynecological gel with a repairing effect. Comprising the following components in percentage by weight: 0.1%-0.5% of recombinant III type human collagen, 0.05%-0.2% of mussel mucin, 1%-3% of chitosan, 0.2%-1% of sodium hyaluronate, 2%-5% of lactobacillus fermentation product filtrate, 0.05%-0.2% of tea tree essential oil, 0.2%-0.5% of carbomer, 0.1%-0.4% of triethanolamine, 0.1%-0.2% of sodium methylparaben and the balance of purified water. The gynecological gel with the repairing effect has the excellent repairing effect, integrates multiple effects of effectively resisting bacteria and diminishing inflammation, promoting repairing of damaged vaginal mucosa, adjusting vaginal micro-ecological balance and the like, not only can efficiently inhibit growth of various pathogens, but also can remarkably promote proliferation and repairing of vaginal mucosa cells, and has the advantages that the repairing effect is good, and the repairing effect is good. The vaginal micro-ecological balance can be accurately adjusted, no stimulation is caused to vaginal mucosa, safety and reliability are achieved, and long-term use can be achieved.
Owner:BEIJING LIANSHENG TRANSDERMAL MEDICAL TECHNOLOGY CO LTD

Low-temperature-resistant self-repairing waterproof concrete for water conservancy and preparation method thereof

The invention relates to the technical field of concrete, and particularly discloses low-temperature-resistant self-repairing waterproof concrete for water conservancy and a preparation method of the low-temperature-resistant self-repairing waterproof concrete. The water conservancy low-temperature-resistant self-repairing waterproof concrete is specifically prepared from the following components in parts by weight: 70 to 80 parts of cement, 10 to 20 parts of fly ash, 8 to 12 parts of silica fume, 2.5 to 3.5 parts of a reinforcing material, 0.2 to 0.4 part of a crystallization inducer, 1.5 to 2.5 parts of a repairing agent and 20 to 40 parts of water, the reinforcing material is formed by mixing nano silica sol, bentonite, quartz sand and triethanolamine; the crystallization inducer is formed by mixing sodium silicate and aluminum hypophosphite; the repairing agent is obtained by loading calcium ions on an amino silane modified zeolite material and then mixing with a bacillus pasteurii bacterial solution. By utilizing the technical scheme provided by the invention, the prepared concrete has excellent mechanical properties, water resistance, impermeability, freezing resistance, crack resistance and good durability.
Owner:BEIJING FENGHUI HUAQI TECH DEV

Ardealite modified catalyst and application thereof, ardealite-based low-carbon cementing material and preparation method of ardealite-based low-carbon cementing material

The invention discloses an ardealite modified catalyst and application thereof, an ardealite-based low-carbon cementing material and a preparation method of the ardealite-based low-carbon cementing material. The modified catalyst comprises triethanolamine, a calcium-based compound, aluminum salt, glycerin, polyethylene glycol, zeolite powder and P.042.5 cement. The modified ardealite is prepared by mixing ardealite and the modified catalyst; the modified phosphogypsum is mixed with S95-grade mineral powder, I-grade or II-grade fly ash, an ultrafine admixture and limestone powder to prepare the phosphogypsum-based low-carbon cementing material. The preparation method has the beneficial effects that the modified catalyst adopts an organic-inorganic-mineral ternary composite catalytic system for the first time, impurity passivation, crystal reconstruction and in-situ reaction can be synchronously realized, a micro-nano crystal nucleus material is generated, and the modified phosphogypsum-based low-carbon cementing material can completely replace cement for use; according to the present invention, the strength of the cementing material can be adjusted, the carbon emission is reduced by more than 75% compared with the traditional cement, and the maximum consumption of the phosphogypsum in each ton of the cementing material product can be up to 300 kg.
Owner:SINOCHEM CHONGQING FULING CHEM IND CO LTD

Preparation and application of cyclodextrin-coated azelaic acid oil-control skin-care product

The invention relates to the technical field of cosmetics, in particular to preparation and application of a cyclodextrin-coated azelaic acid oil-control skin-care product. Comprising the following steps: S1, adding deionized water into a mixer, adding a cyclodextrin-azelaic acid inclusion compound, nicotinamide and allantoin, mixing to obtain a water phase, mixing glycerol, caprylic / capric triglyceride, polydimethylsiloxane, polysorbate-80 and tocopheryl acetate to obtain an oil phase, slowly adding the oil phase into the water phase, and shearing and emulsifying to obtain a nanoemulsion; and S2, cooling the nano-emulsion, adding carbomer while stirring, continuously cooling to room temperature, sequentially adding phenoxyethanol, ferulic acid, menthol and essence, adjusting the pH value of the emulsion with triethanolamine, homogenizing, defoaming, disinfecting and filling. By adjusting the proportion of the components in the formula, the skin feeling of the product can be further optimized, so that the product is more comfortable and not greasy, and a lasting oil control effect is provided.
Owner:GUANGZHOU SENYE BIOMEDICAL TECH CO LTD

Method for measuring content of calcium fluoride in dolomite-containing fluorite mine

The invention discloses a method for measuring the content of calcium fluoride in dolomite-containing fluorite mine. The method comprises an acetic acid solution, a hydrochloric acid solution, a triethanolamine solution, a potassium hydroxide solution and boric acid. The method for measuring the content of calcium fluoride in the dolomite-containing fluorite mine comprises the following steps: S1, reagent proportioning; s2, preparing a calcium standard solution; s3, preparing an EDTA standard titration solution; s4, selecting an instrument; s5, preparing a sample; s6, step analysis; s7, content correction and determination; and S8, calculating a result. The invention belongs to the technical field of calcium fluoride content determination, and particularly relates to a method for measuring the content of calcium fluoride in dolomite-containing fluorite mine, compared with the prior art, the method solves the problem of dolomite dissolution when calcium carbonate is leached by acetic acid, and the content of calcium fluoride in the fluorite mine can be measured by accurately calculating the dissolution amount of dolomite. The measured calcium fluoride content is clearer, more reasonable and more reliable and approaches to a true value, and the process operation is simple and rapid, and is suitable for the requirements in the fields of mine production, assay detection and the like.
Owner:王聪玲

Method for preparing calcium hydroxide with high specific surface area by digesting calcium oxide

The invention discloses a method for preparing calcium hydroxide with a high specific surface area by digesting calcium oxide, and relates to the technical field of preparation of calcium hydroxide with a high specific surface area. The method is characterized in that diethylene glycol / triethanolamine / magnesium chloride is adopted as a compound digestion aid through two processes of wet digestion and dry digestion; and calcium hydroxide with high specific surface area can be controllably prepared. The specific surface area of the calcium hydroxide prepared through wet digestion can reach 70 m < 2 >. G <-1 > or above, the specific surface area of the calcium hydroxide prepared through dry digestion is 45 m < 2 >. G <-1 > or above, the reaction activity of the calcium hydroxide is effectively improved, and the novel controllable method for preparing the calcium hydroxide with the high specific surface area is provided.
Owner:GUANGXI FUWEI TECHNOLOGY DEVELOPMENT CO LTD +1

Cream for repairing radiodermatitis and preparation method thereof

The invention relates to cream for repairing radiodermatitis and a preparation method of the cream, and belongs to the technical field of biomedical skin treatment. The cream consists of the following components in percentage by weight: 8% of glycerin monostearate, 6% of stearic acid, 5% of white vaseline, 4% of liquid wax, 1-2% of tea tree oil, 1-2% of eugenol, 1-2% of vitamin E, 3% of trehalose, 8% of polyethylene glycol (PEG-400), 10% of glycerol, 0.5% of methylparaben, 1% of triethanolamine and the balance of purified water. According to the cream disclosed by the invention, the natural traditional Chinese medicine component eugenol and the natural substance vitamin E are utilized to synergistically enhance the anti-oxidation and bacteriostatic effects, and the tea tree oil, the trehalose and other effective components are utilized to repair radiodermatitis from multiple aspects of anti-inflammation, bacteriostasis, antioxidation, promotion of skin barrier repair and the like. The cream is simple in component, good in treatment effect, high in safety and convenient to produce and process, and can be popularized and applied to treatment of radiodermatitis.
Owner:CHONGQING UNIV

Quick-hardening early-strength concrete mineral additive and preparation method thereof

The invention discloses a quick-hardening early-strength concrete mineral additive and a preparation method thereof, and belongs to the technical field of building materials. The additive comprises the following components in parts by weight: 50-75 parts of a mineral active material (compounded by silica fume, slag powder and metakaolin), 15-30 parts of a composite activator (sodium silicate, lithium sulfate and triethanolamine synergistically), 5-10 parts of a sustained-release microcapsule (calcium sulphoaluminate coated with nano-silica) and 2-5 parts of an auxiliary thickening agent (compounded by HPMC and a water reducing agent). The preparation method comprises the steps of mineral activation, excitant reaction and mixing of the microcapsule and the thickening agent. After the additive is doped into concrete, the 3h compressive strength is greater than or equal to 15MPa, the initial setting time is less than or equal to 5min, and the additive has low resilience (less than or equal to 13%), high durability (impermeability is greater than or equal to P11) and environmental adaptability (-5 DEG C strength fluctuation ratio is less than or equal to 9%). And compared with the prior art, the cost is reduced by 40%, and the method has remarkable economic and social benefits.
Owner:GUILIN UNIVERSITY OF TECHNOLOGY

Low-corrosivity halogen-free soldering flux for aluminum-based part brazing and preparation method of low-corrosivity halogen-free soldering flux

The invention discloses a low-corrosion halogen-free soldering flux for aluminum-based part brazing and a preparation method of the low-corrosion halogen-free soldering flux, and belongs to the technical field of halogen-free welding materials.The low-corrosion halogen-free soldering flux comprises, by mass, 4-6 parts of oxalic acid, 1-2 parts of triethanolamine, 0.8-1.5 parts of Tween-80, 4-6 parts of polyvinylpyrrolidone, 0.3-1 part of compound nano cerium oxide, 0.5-1.5 parts of chitosan oligomer and the balance deionized water. And the welding spot oxidation resistance and the interface self-repairing capability are further improved. Through the synergistic effect of four mechanisms of complexing, oxidation prevention, wetting and film forming, the flux achieves efficient film removal, excellent wetting, no corrosion residue and stable film forming protection, is high in shear strength, low in welding spot porosity and clean in surface after welding, and is suitable for electronic packaging, heat exchanger manufacturing and high-reliability aluminum welding occasions.
Owner:SUZHOU KUNTENGWEI NEW MATERIAL TECH CO LTD

Preparation method of epoxy resin adhesive

The invention relates to the technical field of adhesives, and discloses a preparation method of an epoxy resin adhesive, which comprises the following steps: reacting p-aminophenol with diphenyl dichlorosilane under the catalysis of triethanolamine to obtain di (p-aminophenoxy) diphenyl silane; the preparation method comprises the following steps: carrying out Mannich reaction on amino in di (p-aminophenoxy) diphenyl silane, amino in polyether amine, formaldehyde and phenol to obtain the silane-containing polyether amine type benzoxazine intermediate. And finally, uniformly mixing the silane-containing polyether amine type benzoxazine intermediate and epoxy resin, and curing to obtain the epoxy resin adhesive. The prepared silane-containing polyether amine benzoxazine intermediate contains a silane structure and a benzoxazine structure, both the silane structure and the benzoxazine structure have excellent heat resistance, and the epoxy resin adhesive prepared by adding the silane-containing polyether amine benzoxazine intermediate into epoxy resin has excellent heat resistance.
Owner:NANTONG BAOLILAI COATINGS CO LTD

Novel compound rapid surface anesthetic and preparation method thereof

The invention discloses a novel compound rapid surface anesthetic and a preparation method thereof, and belongs to the field of pharmaceutical preparations. According to the anesthetic, core anesthetic components of lidocaine and tetracaine are compounded with propylene glycol-laurocapram synergistic penetration enhancer, menthol auxiliary penetration enhancer, carbomer 980 gel matrix, triethanolamine pH regulator, glycerol humectant, panthenol soothing agent, purified water and the like, a surface smearing agent is prepared through a specific process, and the anesthetic can be administered in combination with an iontophoresis technology. Compared with the existing surface anesthetic for the cosmetic surgery, the surface anesthetic disclosed by the invention solves the problems of slow effect taking and poor effect, can realize rapid penetration of local skin, has short anesthesia effect taking time, long duration and good effect, has no obvious irritation to the skin, has good product stability, can effectively reduce the drug toxicity, and has a good application prospect. The device is suitable for surface anesthesia of non-surgical medical beauty items such as skin beauty, laser treatment and water-light micro-needles.
Owner:AFFILIATED RENHE HOSPITAL OF CHINA THREE GORGES UNIV

Modified nano hydrated calcium silicate chloride ion curing agent as well as preparation method and application thereof

PendingCN121426454ACalcium silicateChloride ion binding
The invention discloses a modified nano hydrated calcium silicate chloride ion curing agent as well as a preparation method and application thereof, and belongs to the technical field of chemical materials. The curing agent is composed of 65-75 parts of synergistically modified nano calcium silicate hydrate, 10-20 parts of mesoporous silica with a high specific surface area, a composite dispersion stabilizer with a specific ratio, and an active activator compounded by triethanolamine and anhydrous sodium sulfate. The nano calcium silicate hydrate is synergistically modified by gamma-aminopropyltriethoxysilane and sodium dodecyl benzene sulfonate, so that the nano calcium silicate hydrate has the excellent performance that the zeta-potential absolute value is greater than or equal to 25 mV, the dispersity is high, and the chloride ion binding capacity is improved by greater than or equal to 40%. Through the synergistic effect of all the components, the technical problems that an existing chloride ion curing agent is low in adsorption capacity, poor in selectivity, prone to agglomeration in concrete and the like are solved, and the chloride ion curing agent is particularly suitable for improving the durability of the concrete in harsh chloride salt environments such as port engineering and maritime work structures.
Owner:WANJIANG INST OF TECH

High-performance compound bentonite for drilling mud and preparation method of high-performance compound bentonite

The invention discloses high-performance compound bentonite for drilling mud and a preparation method of the high-performance compound bentonite, and relates to the technical field of bentonite, and the high-performance compound bentonite comprises the following raw materials in parts by weight: 80-100 parts of mixed bentonite, 4-6 parts of sodium carbonate, 0.3-0.5 part of sodium humate, 0.2-0.4 part of triethanolamine and 0.2-0.4 part of a surfactant. Through the synergistic effect of the bentonite A with the high montmorillonite content, the bentonite B with the high expansion multiple and the bentonite C with the medium water absorption rate, in cooperation with sodium modification and assistant regulation and control, the product viscosity is stable, the requirement for the sand-carrying capacity of the drilling fluid is met, the filter loss is far lower than that of a traditional product, the filter cake thickness is smaller than or equal to 1.2 mm, the structure is compact, water permeation can be effectively controlled, the well wall can be stabilized, and the drilling fluid can be used for well drilling. The problem that single raw ore is insufficient in viscosity or too high in filter loss is solved.
Owner:WUHU FEISHANG NONMETAL MATERIAL

Preparation method and application of endothelium corneum gigeriae galli and angelica sinensis ointment

The invention discloses a preparation method and application of an endothelium corneum gigeriae galli and angelica sinensis ointment, and relates to the technical field of traditional Chinese medicine, the endothelium corneum gigeriae galli and angelica sinensis ointment comprises the following raw materials in parts by weight: a medicine solution: 1-3g of angelica sinensis extract and 30-35 parts of endothelium corneum gigeriae An oil phase: 1-5 g of white vaseline, 1-5 g of glycerin monostearate, 10-14 g of stearic acid, 5-8 g of liquid paraffin and 3-6 g of wool fat; a water phase: 0.2 to 0.5 g of triethanolamine, 0.5 to 1 g of glycerin, and 0.1 to 0.5 g of ethylparaben; according to the endothelium corneum gigeriae galli and angelica sinensis ointment, endothelium corneum gigeriae galli and angelica sinensis materials are adopted, endothelium corneum gigeriae galli has the effects of healing sore, promoting tissue regeneration, removing blood stasis and the like, angelica sinensis has the effects of replenishing qi, enriching blood and promoting blood circulation to remove blood stasis, and skin wound healing and capillary regeneration can be effectively promoted, local blood circulation is improved, and inflammatory response is inhibited; meanwhile, the ointment is soft in texture and can absorb percolate and inhibit microbial infection; the method is convenient, economical, practical, good in stability and suitable for application and popularization.
Owner:庞晓军

Bio-based sulfur-phosphorus-free nitrogen-containing borate organic molybdenum antifriction agent as well as preparation method and application of bio-based sulfur-phosphorus-free nitrogen-containing borate organic molybdenum antifriction agent

The invention relates to a bio-based sulfur-phosphorus-free nitrogen-containing borate organic molybdenum antifriction agent and a preparation method and application thereof.The preparation method comprises the following steps that A1, monoglyceride and boric acid are dissolved in methylbenzene and subjected to a heating reaction, triethanolamine is added, the reaction continues, and OBN is obtained; a2, OBN and MoO3 obtained in the step A1 are dissolved in methylbenzene, a heating reaction is conducted in the inert atmosphere, and OBN-Mo is obtained; or B1, dissolving monoglyceride and boric acid in toluene, carrying out a heating reaction, adding triethanolamine, and continuing the reaction to obtain OBN; b2, the OBN obtained in the step B1 and molybdenum acetylacetonate are subjected to a heating reaction in ethyl alcohol, and OBN-Mo-OBN is obtained. Compared with the prior art, the two bio-based sulfur and phosphorus-free nitrogen-containing borate organic molybdenum antifriction agents OBN-Mo and OBN-Mo-OBN can be compounded with ZDDP to prepare lubricating oil, so that the wear resistance of the lubricating oil has a synergistic interaction effect.
Owner:SHANGHAI INST OF TECH