The application discloses a kind of high-efficiency
silicon nitride slurry based on light-cured forming and its
ceramic low-temperature
sintering forming method, comprising,
beta phase silicon nitride powder, high-temperature binder,
sintering aid is dispersed in
ethanol solution by ball milling,
ceramic mixed
powder is obtained after
drying and
grinding;Add photo-initiator and
oxygen barrier in photosensitive resin, stir uniformly to obtain premix liquid;
Ceramic mixed
powder and premix liquid are mixed, add dispersing agent, thixotropic agent, stir uniformly and vacuum defoaming to obtain
silicon nitride ceramic slurry.The application effectively solves the technical defects of low single-layer curing thickness of traditional
silicon nitride ceramic
slurry light-cured forming, realizes high-precision, defect-free sample of 50 μm
layer thickness printing of single layer, effectively improves the printing efficiency.High-temperature binder aluminum dihydrogen
phosphate is introduced at the same time, and the problem of more and larger gaps between powders after debinding is solved by using
metasilicate generated by its
decomposition to bond
silicon nitride particles, so as to realize the preparation of dense
silicon nitride ceramics.