7839 results about "Silica fume" patented technology

An anode structure for lithium batteries includes nanofeatured silicon particulates dispersed in a conductive network. The particulates are preferably made from metallurgical grade silicon powder via HF/HNO₃ acid treatment, yielding crystallite sizes from about 1 to 20 nm and pore sizes from about 1 to 100 nm. Surfaces of the particles may be terminated with selected chemical species to further modify the anode performance characteristics. The conductive network is preferably a carbonaceous material or composite, but it may alternatively contain conductive ceramics such as TiN or B₄C. The anode structure may further contain a current collector of copper or nickel mesh or foil.

A highly durable and easy to use prefabricated construction product is disclosed having a cellular concrete component sandwiched between two cement boards, wherein the cellular concrete component comprises cement, fly ash, an activating agent and water, and the cement boards comprise cement, fly ash, an activating agent, sand, silica fume, a water reducer agent, a reinforcing fiber, and water.

Dental bleaching compositions that include sucralose. The bleaching agent is dispersed within a carrier, which is optimally sticky and viscous such as a mixture of propylene glycol and silica fume. Anhydrous propylene glycol and/or anhydrous glycerin are especially useful in order to maintain the desired degree of hydration of the perborate being used. Flavorants may be added to enhance the taste of the dental compositions, since they will be used within a person's mouth. For best results, a flexible, thin-walled, comfortable-fitting, custom dental tray is used with the dental bleaching compositions. The dental compositions are sufficiently sticky and viscous so as to adhere and retain a dental tray against a person's teeth which is designed so as to not exert significant mechanical pressure onto the person's teeth.

The invention discloses a preparation method for a fiber reinforced carbon-silicon carbide-zirconium carbide-based (C/C-SiC-ZrC) composite material. The preparation method comprises the following steps of: (a) evenly dispersing ZrC nanopowder in absolute ethyl alcohol; (b) mixing phenolic resin and ZrC dispersion liquid to form slurry; (c) immersing a two-dimensional carbon fiber sheet into the slurry for dipping and drying, then carrying out continuous superposition paving on the two-dimensional carbon fiber sheet, and carrying out curing and post-curing treatment to prepare a fiber-reinforced sintered body; (d) cracking the fiber-reinforced sintered body to obtain a porous C/C prefabricate; (e) placing silicon powder into a graphite crucible, burying the porous C/C prefabricate into the silicon powder, heating to 1,500-1,650 DEG C, and preserving heat for preset time so as to carry out liquid silicon permeation. The method can be used for improving the high-temperature oxidizing property and ablation property of the carbon fiber reinforced ceramic (C/C-SiC) composite material.

The invention provides high-strength and high-toughness reactive powder concrete of a carbon doped nano-tube. The high-strength and high-toughness reactive powder concrete is prepared by taking cement, a carbon nano-tube, silica fume, a water reducing agent, silica sand, coal ash, quartz powder, steel fiber and water as raw materials, wherein all the components in the mixture are calculated in parts by mass: 1000-1200 parts of cement, 250-350 parts of silica fume, 250-350 parts of slag powder, 40-50 parts of water reducing agent, 1200-1400 parts of silica sand, 180-230 parts of water, 190-230 parts of steel fiber, 180-250 parts of coal ash, 80-120 parts of quartz powder, 0.1-5 parts of carbon-nano-tube dispersing agent and 1-10 parts of carbon nano-tube powder. The invention also provides a preparation method of the high-strength and high-toughness reactive powder concrete. The reactive powder concrete obtained by the invention has the high compression strength of 250-300MPa and breaking strength of 45-60MPa, which are higher than the 200-level related performances of the traditional RPC (Reactive Powder Concrete). Meanwhile, the initial cracking strength of the reactive powder concrete material prepared by using the carbon nano-tube is greatly improved and is up to 10MPa in a direct stretching state, and the tensile strain corresponding to peak stress is up to more than 0.5%, so that the toughness and strength of the traditional RPC material are greatly improved.

The invention relates to a method for preparing a composite material for a cathode of a lithium ion battery, and the cathode and the battery which comprise the cathode material. The preparation method comprises: uniformly mixing silicon powder, graphite, pyrolytic carbon precursor and a solvent to prepare slurry, wherein the silicon powder comprises micro-silicon powder and nano-silicon powder, and the weight ratio of the micro-silicon powder and the nano-silicon powder is 2-20:1; and removing the solvent in the slurry, performing primary sintering under the protection of inert gas, performing primary ball grinding, performing secondary sintering under the protection of the inert gas, and performing secondary ball grinding, wherein the temperature of the secondary sintering is higher than that of the primary sintering. The battery made from the composite material for the cathode of the lithium ion battery obtained by the method has good cycling performance and charge and discharge capacity.

The invention discloses a silicon-carbon negative electrode material of a lithium ion battery and a preparation method thereof, and solves the technological problem of improving the charge and discharge cycling stability of the electrode material. The silicon-carbon negative electrode material is prepared by mixing a silicon-carbon composite material and a natural graphite material, wherein the weight of the silicon-carbon composite material is 7-20% and the silicon-carbon composite material is prepared by depositing carbon nanotube and/or carbon nanofiber on the surface of nanometer silica fume and/or embedding into the nanometer silica fume to form core, the surface of which is covered with 3-15wt% of a carbon layer. The preparation method provided by the invention comprises steps of: precursor silicon powder preparation; chemical vapor deposition; liquid-coating roasting; crushing; and mixing. In comparison with the prior art, the reversible specific capacity of the silicon-carbon composite negative electrode material is greater than 500mAh/g; the coulombic efficiency for a first cycle is greater than 80%; the capacity conservation rate of cycling for 50 weeks is greater than 95%. The preparation method is simple, is easy to operate, requires low cost and is suitable for a high-volume negative electrode material of lithium ion batteries used for various portable devices.

The invention discloses crack self-remediation regenerated concrete based on urease production microorganism mineralization deposition and a preparation method. The crack self-remediation regenerated concrete comprises components, namely, expanded perlite carried with urease production microorganisms, cement, stone, sand, silica fume, water, urea, calcium chloride, a urease production microorganism suspension and a water reducing agent. The urease production microorganisms are adopted as a concrete crack remediation agent, urease can be generated through metabolism through the urease production microorganisms, and the urea can be decomposed into NH4<+> and CO3<2+>, and furthermore the calcium carbonate can be mineralized and deposited to remedy cracks. In the preparation process, a part of the crack remediation agent is directly mixed with the concrete, then cracks and holes in regenerated crude aggregate self and weak adhesion areas between regenerated aggregate and a new cement stone base can be remedied, and thus the mechanical property of the regenerated concrete can be improved; meanwhile, the other part of the crack remediation agent is firstly adsorbed into an expanded perlite carrier and is further mixed into the concrete, then the crack self-remediation property of the regenerated concrete in the service period can be improved, and thus the anti-penetrability performance and the durability of the regenerated concrete can be improved.

A cement mix suitable for blocking or plugging an abandoned pipeline or back filling a mine shaft, tunnel or excavations contains Portland cement or a cement blend of two components selected from Portland cement, fly ash, pozzolan, slag, silica fume and gypsum; diatomaceous earth; zeolite and an inorganic salt accelerator. The cement mix may further contain an alkali metasilicate and/or alkali silicate. A cementitious slurry, formulated from the cement mix, may have a density less than or equal to 1500 kg/m³, and exhibits good compressive strength.

The invention discloses a silicon-carbon composite material, a lithium ion battery, and a preparation method and application of the silicon-carbon composite material. The preparation method of the silicon-carbon composite material comprises the steps: uniformly mixing silicon powder and silicon monoxide powder, then mixing with a solution containing an organic carbon source dispersant, and performing wet-process ball milling to obtain a slurry; uniformly mixing the slurry, graphite and a conductive agent, and performing spray drying to obtain spherical-like particles, wherein graphite is synthetic graphite and/or intermediate-phase graphite; mixing the spherical-like particles and asphalt, performing cladding processing under the inert atmosphere to obtain a cladded material; and then performing carbonizing processing to obtain the silicon-carbon composite material, wherein silicon powder, silicon monoxide powder, graphite and asphalt respectively accounts for 5-15%, 3-10%, 45-75% and 5-40% by weight of the sum of the above materials, and the organic carbon source dispersant and the conductive agent both accounts for 0.1-2% by weight of the sum of silicon powder, silicon monoxide powder and graphite. The silicon-carbon composite material has relatively good cycle performance, and can be directly used as a cathode material of the lithium ion battery. The preparation method is simple in technology, low in cost and applicable to industrial production.

The invention provides a silicon-carbon composite cathode material for preparing a lithium-ion battery at the room temperature and a preparation method thereof. The composite cathode material is a material with a nuclear shell structure and comprises the following proportional elements: 0.01-10% of simple substance silicon and 90-99.9% of carbon. With regard to the preparation method, silicon powder and graphite are mixed for ball grinding and then added with bitumen or polymer cladding material for ball grinding again, after the treatment of carbonization, the mixture is crushed and sieved to obtain the material containing 0.01-10wt% of silicon and 10-99.9% of carbon. The capacity of the material is more than 350mAh/g, the cycle efficiency of the material is larger than 90% for the first time, and keeps larger than 80% after 200 cycles, and the material has good charging and discharging property.

The invention discloses a high performance cement-base self-leveling mortar. The mortar is characterized by comprising cement, an auxiliary gel material, fine aggregate, a filling material, an additive, and water; wherein the cement is common silicate cement and sulphoaluminate-silicate cement, the auxiliary gel material comprises mineral slag, fly ash, silica fume, and gypsum, and the ratio of common silicate cement to sulphoaluminate-silicate cement to gypsum is equal to 1:0.2-0.6:0.1-0.4. The mortar has a self-leveling function without vibration, so the surface flatness is very high. The curing speed of the mortar is very quick, and after two hours, the strength of the mortar can meet the requirements of subsequent construction. Moreover the mortar has the advantages of low contraction rate, good volume stability, good surface wear resistance, and high compression strength.

The invention provides a cement slurry with long-term-integrity cement sheath for a heavy-oil thermal-recovery well. The cement slurry comprises, by weight, 100 parts of thermally responsive cement, 25 to 65 parts of water and 0.2 to 8 parts of a cement slurry aid. The thermally responsive cement comprises 30 to 60 parts of oil well cement, 10 to 20 parts of active silicon powder, 0 to 10 parts of hollow glass beads and 10 to 50 parts of a thermally responsive composite material. The thermally responsive composite material comprises 20 to 30 parts of clay mineral, 10 to 20 parts of fly ash and/or vulcanic ash, 5 to 20 parts of rubber powder and/or latex powder, 3 to 10 parts of carbon fiber, 10 to 15 parts of nanometer silicon dioxide, 5 to 10 parts of calcined magnesia, 10 to 20 parts of ultrafine superfine slag powder and 5 to 10 parts of inorganic whiskers. The cement slurry provided by the invention can solidify at normal temperature; and set cement can resist long-term high temperature, and the mechanical properties and thermal properties of the set cement in a high temperature environment are integrally adaptive to strata and casing pipes.

The invention relates to a 3D printing cement-based material used for underwater construction and a preparation method of the 3D printing cement-based material. The 3D printing cement-based material is prepared from the following components and raw materials by weight: 100 parts of cement, 0-60 parts of mineral powder, 0-30 parts of fly ash, 0-20 parts of silica fume, 0.1-3 parts of a water reducing agent, 0.1-5 parts of an anti-dispersion agent, 0.2-5 parts of a binder, 0.005-0.5 part of an air entraining agent, 0.01-25 parts of a plastic retaining agent, 0-0.5 part of starch ether, 0.01-0.5 part of a thickening time control agent, 0.1-10 parts of an expanding agent, 0.1-10 parts of an early strength agent, 0.01-0.5 part of fiber, 50-300 parts of fine aggregate, and 0-400 parts of coarse aggregate. Compared with the prior art, the 3D printing cement-based material, when used in the underwater printing construction, has the excellent advantages of constructability, dispersion resistance and durability and has an excellent bulk property in water, a printed building does not collapse, and the mechanical property is excellent.

The invention discloses a fibre reinforced coal ash based geopolymer foam material and a preparation method thereof. The fibre reinforced coal ash based geopolymer foam material disclosed by the invention comprises the following components in percentage by weight: 50-70% of aluminium silicon raw material, 5-15% of slag, 3-8% of inorganic fibre, 15-30% of liquid alkaline exciting agent, 0.2-2% of foaming agent, and 2.5-3.5% of foam stabilizer. The preparation method disclosed by the invention comprises the step of also adding the foam stabilizer while adding the foaming agent by adopting the liquid alkaline exciting agent by taking the inorganic fibre as the reinforcing agent, the slag as the Ca adjusting agent and other solid raw materials (such as coal ash, metakaolin and silica fume) as powder for providing aluminium silicon. The light foam material prepared by the invention has the characteristics of being high in intensity, small in size change rate, low in water absorption and the like in the event of having same volume weight and heat conductivity of the similar materials, and is applied to various applications.

The invention relates to a recovery processing method of silicon slice cut waste mortar, comprising the following steps: (1) separating solid-liquid components in the silicon slice cut waste mortar; (2) further recovering the remained cutting liquid component in a solid; (3) separating silicon powder and silicon carbide through water flow flotation; (4) recovering the silicon powder; (5) recovering the silicon carbide; (6) coarsely filtering, finely filtering, decoloring, vacuum distilling and dehydrating the recovered cutting liquid, and adding component with corresponding amount for secondary filter. The method can get various recovered products, such as silicon carbide micro powder, cutting liquid and silicon powder, has high recovery rate and recovery profit and can save the cost of the mortar by at least 40 percent; meanwhile, the invention effectively solves the problem of possible secondary pollution caused by single recovery; the cutting function of recovered and treated silicon carbide micro powder is recovered again, thereby changing waste into wealth, realizing the resource reutilization in true sense, and promoting the development of recycling economy; and the method basically realizes the zero emission of waste liquid by reutilizing the treated waste water after combining a sewage treatment process, thereby being beneficial to environment protection.

The invention discloses an ultrahigh-toughness concrete and a preparation method thereof. The ultrahigh-toughness concrete mainly comprises cement, silica fume, mineral slag, fly ash, quartz powder, quartz sand, steel fiber, nano calcium carbonate, water and a water reducing agent. The weight ratio of the silica fume to the cement is (10-20):100; the weight ratio of the mineral slag to the cement is (1-20):100; the weight ratio of the fly ash to the cement is (5-20):100; the weight ratio of the quartz powder to the cement is (30-38):100; the weight ratio of the quartz sand to the cement is (80-150):100; the steel fiber accounts for 2.0-4 vol% of the concrete; the weight ratio of the calcium carbonate to the cement is (0.1-5):100; the water-binder ratio is 0.16-0.22; and the weight ratio of the water reducing agent to the cement is (0.5-4):100. The concrete has the advantages of high strength, high toughness and favorable workability; the slump is greater than or equal to 180mm; and the concrete is pumpable and can be cast in place.

Process for production of acid and high temperature resistant cement composites, where the matrix is alkali activated F fly ash alone, F Fly ash combined with ground slag or ground slag alone. F-fly ash produces lower quality alkali activated cement systems. On the other hand the lack of calcium oxide results in very high resistance to medium and highly concentrated inorganic or organic acids. The high strength and low permeability of pure F-fly ash cement systems is achieved by using in the composition un-densified silica fume, the amorphous silicone dioxide obtained as by products in production of ferro-silicones. Precipitated nano-particle silica made from soluble silicates and nano-particle silica fume produced by burning silicon tetra chloride in the hydrogen stream.

The invention relates to a concrete commonly used in building materials, and especially relates to a thermal-insulation loading recycled concrete. A technical problem to be solved is to provide a recycled concrete which is an integration of thermal insulation, loading, quake resisting, and energy saving and emission reduction. A technical scheme adopted is characterized in that a weight ratio (kg/m<3>) of a composite lightweight aggregate admixture: cement: recycled fine aggregate: sand: recycled coarse aggregate: cobblestone: ceramsite: coal ash: water: additives is (5-250):(200-800):(20-500):(5-800):(30-600):(5-1400):(50-800):(10-600):(50-500):(0.1-200); the composite lightweight aggregate admixture is a mixture of glazed hollow beads and an aerogel, and the weight part ratio of the glazed hollow beads to the aerogel is 1:(0.7-1.5); and the additives comprise the following components, by weight, 10-150 parts of silica fume, 4-40 parts of an air entraining agent, 5-30 parts of a foaming agent, 3-30 parts of a water reducing agent, 1-30 parts of a polypropylene fiber, and 10-150 parts of waste slag. The technical scheme is used for making the recycled concrete.

The invention provides a preparation method for a carbon-coated silicon negative electrode material for a lithium ion battery. The negative electrode material for the lithium ion battery with excellent performance is obtained from silicon powder by two times of carbon coating; the preparation method comprises the following steps of carrying out liquid phase dispersion on the silicon powder, then carrying out dispersion on the silicon powder, the first carbon coating layer and a dispersing agent; removing the solvent, and carrying out high-temperature carbonization treatment on the obtained solid material to obtain primary carbon-coated silicon negative electrode material; preparing a dispersion solution of a second carbon-coated material, dispersing the primary carbon-coated silicon material to the dispersion solution of the second carbon-coated material, and then removing the solvent and carrying out secondary roasting to obtain the secondary carbon-coated silicon negative electrode material. According to the preparation method, the raw materials are low in cost and easily available; the ratio of silicon to carbon can be optionally regulated and controlled; and the preparation method is simple in equipment, easy to implement the technological process, and suitable for scale production.