Recovery processing method of silicon slice cut waste mortar
A silicon wafer cutting and recycling technology, applied in the direction of lubricating compositions, etc., can solve the waste mortar recycling process is not very mature and perfect, the waste mortar cannot be processed in a timely and effective manner, and the deep processing technology of silicon carbide micropowder is not mastered. Achieve the effect of being conducive to environmental protection, saving mortar cost, and high recovery rate
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Embodiment 1
[0031] Example 1 The applicant was entrusted to recycle waste mortar for a silicon wafer cutting company in Hebei, and the contract was signed with a recovery rate of 40% for the liquid and 35% for the recovered sand. The recycling process is as follows:
[0032] ① Solid-liquid separation The waste mortar is heated to 60°C after being stirred, and a horizontal screw centrifuge (800r / min) is used for solid-liquid separation; ② The residual cutting fluid in the solid is recovered and separated, and the mass concentration of the solid slurry is 40%. Use a scraper centrifuge to separate, and filter the obtained liquid. Use a first-stage vacuum distillation equipment to reduce the water content in the liquid to 20%. After filtering, use a second-stage vacuum distillation equipment to reduce the water content in the cutting fluid to about 5%. Filter Afterwards, the liquid separated from step 1 is treated in the same way; 3. Separation of silicon carbide and silicon powder Add water ...
Embodiment 2
[0034] Example 2 The applicant was entrusted to recycle waste mortar for a silicon chip cutting enterprise in Jiangxi, and the contract was signed with a recovery rate of 40% for the liquid and 35% for the recovered sand. The recycling process is as follows:
[0035] ① Solid-liquid separation The waste mortar is heated to 80°C after being stirred, and a horizontal screw centrifuge (1000r / min) is used for solid-liquid separation; ② The residual cutting fluid in the solid is recovered and separated. Separation by a scraper centrifuge, filtering the obtained liquid, using a first-stage vacuum distillation equipment to reduce the water content in the liquid to 20%, and using a second-stage vacuum distillation equipment to reduce the water content in the liquid to 10% after filtration, and after filtration and step ①The separated liquid is treated in the same way; ③Separation of silicon carbide and silicon powder Add water to the solid material separated in the previous step to mak...
Embodiment 3
[0036] Embodiment 3 A method for recycling waste mortar from cutting silicon wafers, the steps are as follows:
[0037] ① Solid-liquid separation Adjust the temperature of the silicon wafer cutting waste mortar to 30°C, reduce its viscosity, and separate the waste mortar with a sedimentation centrifuge (centrifugal speed 600r / min); ②Recover the residual cutting fluid in the solid Add water to make slurry (concentration: 20%) of the solid obtained in the first step of separation, and then use a scraper centrifuge to separate, filter the liquid, use a first-stage vacuum distillation equipment to concentrate, reduce the moisture content in the liquid to 20%, and use a second-stage vacuum distillation equipment after filtration Moisture content in the liquid is reduced to below 10%; 3. silicon carbide and silicon powder are separated and the solid material separated in the previous step is added with water to make a slurry (concentration is 25), and 0.02% of the solid mass is added...
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