The invention belongs to the field of
inorganic materials. The invention provides a rapid preparation method and a preparation device of SiC
whiskers, and the preparation method comprises the following steps: placing a
silicon-containing material and a carbon-containing material in the device, then enabling the device to be in a
closed state, vacuumizing the device, then filling
inert gas for pressurizing, preheating the raw materials through a
Joule heating system, heating to 300-500 DEG C, stopping heating, and cooling to
room temperature to obtain the SiC
whiskers. A self-propagating
ignition system is used for ignition, the
reaction temperature is controlled to range from 1500 DEG C to 1750 DEG C, the reaction pressure is controlled to range from 0.5 MPa to 5 MPa, materials are cooled after the reaction is finished, the materials are taken out after the temperature of the device is cooled to 400 DEG C or below, the SiC
whiskers are obtained, the device comprises a kettle body, a
Joule heating system is arranged in the kettle body, and the device is further provided with the self-propagating
ignition system. According to the preparation method and device disclosed by the invention, the reaction activity of the material is increased by utilizing a
Joule heat
auxiliary heating mode, the smooth proceeding of the self-propagating reaction is promoted, the
reaction energy consumption is obviously reduced, the reaction time is shortened, no catalyst is used, and the rapid and large-scale preparation of the high-purity SiC
whisker is realized.