5446 results about "Boron nitride" patented technology

The invention discloses a high temperature and high pressure resistant electric power tube and a preparation method thereof, the electric power tube comprises the following raw materials by weight: 100-120 parts of polyethylene master batch, 5-10 parts of a modifier, 0.5-1 part of benzoyl peroxide and 20-30 parts of a modified filler, in a melt extrusion process of the raw materials, a maleimide structure on a molecular side chain of the modifier can be grafted with a polyethylene molecular chain, and the molecular chain of the modifier can be grafted with the polyethylene molecular chain. Meanwhile, an organic silicon chain segment and a benzene ring structure are added in a polymer molecule, the high-temperature-resistant effect of the material is improved, after reflux treatment in water, a siloxane structure in the modified filler and a siloxane structure in a modifier molecule can be subjected to hydrolytic condensation, and therefore the high-temperature-resistant and high-pressure-resistant effects of the material are improved. According to the invention, polyhedral oligomeric silsesquioxane is taken as a core, boron nitride is taken as a shell to form a core-shell structure, and the three-dimensional grid structure of the polymer can greatly improve the high-temperature-resistant and high-pressure-resistant effects of the polymer.

The invention discloses a preparation method and application of a vertically-oriented boron nitride / epoxy resin heat-conducting composite material under a magnetic field, and belongs to the field of composite materials. The invention aims to solve the problems of high cost, complex process and narrow application range of the existing filler directional arrangement method. The method comprises the following steps: 1, preparing a mixed solution of boron nitride and ferroferric oxide; 2, preparing a boron nitride nanosheet solution with ferroferric oxide attached to the surface; (3) preparing BNNS coated Fe3O4; and 4, preparing the vertically-oriented boron nitride / epoxy resin heat-conducting composite material under the magnetic field. The invention relates to application of a vertically-oriented boron nitride / epoxy resin heat-conducting composite material in electronic packaging under a magnetic field. The heat conductivity of the epoxy resin can be effectively improved, the process is simple and reliable, the efficiency is high, the cost is low, the heat conductivity coefficient is high, and the method can be applied to electronic packaging.

The invention discloses a high-temperature-resistant epoxy insulating material for a transformer and a preparation method thereof, and belongs to the technical field of insulating materials. The high-temperature-resistant epoxy insulating material for the transformer is prepared from the following components in parts by weight: 50 to 60 parts of bisphenol A epoxy resin, 20 to 50 parts of anhydride curing agent, 10 to 20 parts of modified composite filler and 5 to 10 parts of epoxidized hydroxyl-terminated liquid polybutadiene, wherein the modified composite filler is a mixture of first boron nitride, second boron nitride and silicon nitride grafted with a silane coupling agent and dopamine, and the mass ratio of the first boron nitride to the second boron nitride to the silicon nitride is (1-2): (2-4): 1. The high-temperature-resistant epoxy insulating material for the transformer has excellent mechanical property, insulating property, heat-conducting property and high-temperature aging resistance.

The invention relates to the technical field of low-dielectric heat-conducting functional materials, in particular to a nano silicone rubber composite material as well as a preparation method and application thereof. According to the preparation method, a modified vinyl silsesquioxane coupling agent is taken as a bridge, and boron nitride nanosheets, silicon carbide nanowires and the modified vinyl silsesquioxane coupling agent are covalently connected through hydrolysis reaction, so that a heterostructure is constructed, and the nano heat-conducting filler is obtained; the preparation method comprises the following steps: dispersing a nano heat-conducting filler in vinyl silicone oil, and constructing a covalent cross-linked network through addition cross-linking reaction and curing treatment to obtain the nano composite silicone rubber material. According to the processing method, the filling amount, the dielectric constant and the dielectric loss can be reduced, meanwhile, the heat conduction capacity is improved, and the problems that in the prior art, the dielectric constant and the dielectric loss are low due to simple mixing of the boron nitride nanosheets and the silicon carbide nanowires are solved.

Systems and methods for forming an oxidation protection system on a composite structure are provided. In various embodiments, the oxidation protection system comprises a boron-glass layer formed on the composite substrate and a silicon-glass layer formed over the boron-glass layer. Each of the boron-glass layer and the silicon-glass layer include a glass former and a glass modifier. The boron-glass layer includes a boron compound comprising a mixture of boron carbide (B4C) powder and cubic boron nitride (BN) powder.

The invention relates to the technical field of capacitor films, in particular to a high-temperature-resistant polypropylene capacitor film and a preparation method thereof.The high-temperature-resistant polypropylene capacitor film is prepared from, by weight, 94-98 parts of polypropylene resin, 1-3 parts of filler-doped modified balance adjusting agent, 0.5-2 parts of boron nitride-glass fiber combined agent, 0.05-0.4 part of nucleating agent, 0.2-0.4 part of antioxidant and 0.1-0.4 part of silane coupling agent; the high-temperature-resistant polypropylene capacitor film is obtained through the processes of melting extrusion molding, cooling shaping, preheating, two-way stretching, heat shaping, rolling and the like of the raw material composition. The polypropylene resin, the nucleating agent, the antioxidant and the silane coupling agent are blended, the filler-doped modified balance adjusting agent and the boron nitride-glass fiber coupling agent are added, and the raw materials are blended and coordinated, so that high feasibility of a two-way stretching process is guaranteed, breakdown resistance, mechanical strength and dielectric loss performance of the product are optimized, and the product has good mechanical properties. And meanwhile, the high-temperature-resistant and corrosion-resistant stability effects are remarkable.

The invention relates to the technical field of textiles, and discloses a cool and washable bio-based nylon 56 fabric and a preparation method thereof. The preparation method of the cool and washable bio-based nylon 56 fabric comprises the following steps: loading modified nano aluminum oxide on modified aluminum nitride microchips to obtain a composite cool material; nylon 56, an ethylene-methyl acrylate-glycidyl methacrylate terpolymer, polypentamethylene guanidine hydrochloride and a composite cool feeling material are subjected to blending extrusion and melt spinning, and then the bio-based nylon 56 fabric is woven. Mixing the composite modified boron nitride and ethanol to obtain finishing liquid; spraying the finishing liquid on one side of the bio-based nylon 56 fabric, and drying to obtain the cool washable bio-based nylon 56 fabric. The cool and washable bio-based nylon 56 fabric disclosed by the invention has excellent cool feeling, antibacterial property, washable property, moisture absorption property and unidirectional perspiration property.

The invention relates to an insulating weather-resistant powder coating and a preparation method thereof, and belongs to the technical field of coatings, and the powder coating comprises composite modified resin, a dual curing agent, a functional filler, a polyacrylate leveling agent, fumed silica, a benzotriazole ultraviolet light absorber, polytetrafluoroethylene wax powder and the like. A core-shell structure of the composite modified resin is designed, high insulativity is kept through a silane modified epoxy core layer, a weather-proof barrier is provided through an acrylic acid shell layer, and the phase separation problem is solved through interface chemical bonding; a dual-curing mechanism is designed, and isocyanate and acrylic hydroxyl react to form an interpenetrating network while an epoxy core layer is cured by anhydride; a filler synergistic effect is designed, silane coupling agent modified nano boron nitride forms a three-dimensional heat-conducting insulating network, and rutile type titanium dioxide is coated with silicon dioxide, so that ultraviolet aging is resisted. All the components cooperate with one another, so that the coating has excellent insulativity, weather resistance, adhesiveness and the like at the same time.

To provide a cubic boron nitride sintered body and a coated cubic boron nitride sintered body that can extend a tool life by having excellent wear resistance and chipping resistance.SOLUTION: In a cubic boron nitride sintered body including cubic boron nitride and a bonding phase, a content ratio of the cubic boron nitride and the bonding phase is within a specific range, the bonding phase comprises a Ti compound phase, an Al compound phase, and a phase containing an element W, a content ratio of the Ti compound phase, the Al compound phase, and the phase containing the element W is within a specific range, the phase containing the element W includes at least one kind selected from the group consisting of W2B and WB, and a ratio I2 / I1 is in a specific range, where I1 is the X-ray diffraction peak intensity of a (111) plane of cubic boron nitride and I2 is the sum of the X-ray diffraction peak intensities of a (211) plane of the W2B and a (110) plane of the WB in the bonding phase.SELECTED DRAWING: None

The invention relates to the field of cable materials, and provides a flexible flame-retardant polyolefin insulating material for a high-flexibility drag chain cable and a preparation method thereof.The flexible flame-retardant polyolefin insulating material comprises phosphorus-containing flame retardant surface modified boron nitride, polyphosphazene modified magnesium hydroxide nanowires, polyolefin matrix resin and the like. The phosphorus-containing flame retardant surface modified boron nitride is prepared by carrying out surface modification on hydroxyl modified hexagonal boron nitride through 10-dihydro-9-oxa-10-phosphaphenanthrene-10-oxide and vinyl trimethoxy silane, and shows excellent flame retardant property and flexibility. The polyphosphazene modified magnesium hydroxide nanowire is prepared through silane coupling agent functionalization and polyphosphazene cross-linking polymerization, and has flame retardance and a reinforcing effect. The preparation method of the material comprises the steps of raw material premixing, melt blending, cooling granulation and extrusion molding. The material has the characteristics of flame retardance, high flexibility and the like, and is widely applied to dynamic high-flexibility cables in the fields of industrial automation equipment, robots, machine tool manufacturing, logistics conveying systems and the like.

The invention relates to a cool master batch and a preparation method thereof, a cool polyester fiber and a cool polyester fiber fabric, the cool master batch is prepared from the following components in parts by mass: 70-90 parts of polyester and 10-30 parts of a cool agent, and the cool agent is prepared by hybridizing boron nitride and a carbon material according to a mass ratio of (98-99.9): (0.1-1) to obtain carbon hybridized boron nitride and adding a modifier for modification. According to the cool master batch, boron nitride is hybridized by adopting a small amount of carbon materials such as graphene and carbon nanotubes, so that the heat conductivity of the boron nitride material is improved, and meanwhile, the absorption of visible light, near-infrared rays and even ultraviolet rays by the graphene and the carbon nanotubes is eliminated, namely, the light absorption and heating effects are achieved; meanwhile, graphene and a carbon nano tube layer are inserted into boron nitride through ultrasonic hybridization, and then grinding is performed until the particle size is proper, so that compared with a processing mode of directly adding a dispersing agent, the boron nitride has a better dispersing effect and a more perfect heat-conducting network, and the dispersing effect of the cooling agent in the cooling master batch and the fiber is greatly improved.

The invention relates to the technical field of woven ceramic materials, in particular to a high-toughness woven ceramic material and a preparation method thereof, and the high-toughness woven ceramic material comprises the following raw materials in parts by weight: 30-40 parts of diopside, 20-30 parts of quartz, 10-15 parts of silicon carbide, 7-11 parts of boron nitride, 6-10 parts of a modified carbon nanotube reblended admixture, 5-7 parts of an intercalated synergistic supplement, 4-6 parts of aluminum oxide, 10-15 parts of water and 3-5 parts of a sodium dodecyl benzene sulfonate solution. According to the high-toughness woven ceramic material, the diopside is matched with the quartz, the silicon carbide, the boron nitride and the aluminum oxide raw materials, the blending and matching effects of the raw materials are optimized by improving the interfacial activity of the sodium dodecyl benzene sulfonate solution, and meanwhile, the added modified carbon nanotube reblended admixture and the intercalated synergistic supplement are used for carrying out coordination and synergistic effects, so that the high-toughness woven ceramic material is prepared. The durable usability of the product is enhanced, the fracture toughness of the product is excellent, the scrubbing-resistant and corrosion-resistant stability effects are remarkable, and the performance improvement effect of the product is remarkable.

The invention provides a diaphragm and a preparation method thereof and a lithium ion battery, the diaphragm comprises a porous support layer and a gradient functional layer, the porous support layer comprises a base membrane with the porosity of 45-60% and active groups modified on the surface of the base membrane, and the gradient functional layer comprises a heat conduction strengthening layer and an ion channel layer, the heat conduction strengthening layer comprises a first polymer and a modified boron nitride nanosheet, and the ion channel layer comprises a second polymer and a solid electrolyte nanowire. The porous supporting layer and the gradient functional layer are overlapped to form the composite diaphragm, so that high thermal stability, high wettability and high ion conductivity are synergistically realized, and formation of lithium dendrites can be inhibited.

The invention discloses a scratch repair coating and a preparation method thereof, and relates to the technical field of high polymer materials. When the scratch repair coating is prepared, hydroxylated boron nitride reacts with 1-(3-triethoxysilylpropyl)-2-imidazoline to prepare pre-modified boron nitride, and then the pre-modified boron nitride and 4-chloro-1-butene are subjected to quaternization to prepare modified boron nitride; the preparation method comprises the following steps: reacting styryl phosphonic dichloride with 4, 4, 5, 5, 6, 6, 7, 7, 7-nonafluoro-1, 2-heptanediol to prepare a hydroxyl-terminated phosphorus-fluorine-containing polymer; the preparation method comprises the following steps: reacting isophorone diisocyanate with a hydroxyl-terminated phosphorus and fluorine-containing polymer to prepare a polyurethane prepolymer; reacting the polyurethane prepolymer with hydroxyl-terminated coumarin to generate modified polyurethane; and uniformly mixing the modified polyurethane, the modified boron nitride and a photoinitiator to prepare the scratch repair coating. The scratch repairing coating prepared by the invention has good self-repairing performance, flame retardant property, corrosion resistance and mechanical property.

The invention relates to the technical field of ceramic materials, in particular to a ceramic composite material and a preparation method thereof.The ceramic composite material is prepared from, by weight, 30-35 parts of silicon carbide, 15-20 parts of boron nitride, 10-15 parts of silicon dioxide, 8-11 parts of additive based on modified filler and 7-10 parts of ball milling agent based on sodium alginate reconditioning modification. According to the ceramic composite material, silicon carbide and boron nitride are matched with silicon dioxide, the additive based on the modified filler and the ball-milling agent based on sodium alginate reconditioning modification are blended and coordinated, and through coordination and synergism of the raw materials, the obtained product can achieve coordinated improvement of strength, wear resistance and thermal conductivity; and the product has remarkable heat-resistant and corrosion-resistant stability effects.

The invention provides a robot joint dynamic cable made of a self-repairing polyurethane material and a preparation method of the robot joint dynamic cable, and belongs to the field of cables. Polytetrahydrofuran glycol and hexamethylene diisocyanate react to form a soft and hard segment structure, 1, 4-butanediol is added for chain extension, dopamine hydrochloride is introduced, the hard segment structure is enhanced, and a self-repairing hydrogen bond network is formed; carbon nanotubes are introduced, and through plasma treatment and silane coupling agent modification, the tensile resistance, fatigue resistance and electrical properties of the material are improved; montmorillonite is compounded with polyethyleneimine through organic treatment, so that the cracking resistance and wear resistance of the material are enhanced; epoxy groups are introduced to the surface of boron nitride, and dopamine hydrochloride is self-polymerized, so that excellent heat dissipation capability and dimensional stability are provided. Through the synergistic effect of the components, the composite material has excellent mechanical properties, electrical properties, heat dissipation, wear resistance and the like, is especially suitable for a dynamic cable of a robot, and can stably work in a complex environment for a long time.

The invention relates to the technical field of coatings, in particular to a high-performance environment-friendly coating and a galvanized sheet prepared from the same. The high-performance environment-friendly coating is prepared from the following components in parts by weight: 120 to 150 parts of waterborne polyurethane dispersion liquid, 10 to 15 parts of graphene oxide nanosheets, 4 to 10 parts of boron nitride nanosheets, 2 to 6 parts of inorganic nanoparticles, 0.5 to 2 parts of anti-settling agent, 0.5 to 2 parts of defoaming agent, 0.2 to 2 parts of wetting dispersant and 50 to 100 parts of deionized water. By selecting inorganic nanoparticles with specific particle sizes, the inorganic nanoparticles can be dispersed between the boron nitride nanosheets and the graphene oxide nanosheets, the dispersion and lubrication effects similar to those of bearings are achieved, the isolation and shielding effects of the nanosheet material are improved, and the stability of the coating is improved.

The invention belongs to the technical field of polymer heat conduction, and particularly relates to a preparation method of a high-heat-conductivity polymer with modified boron nitride as filler, which comprises the following steps: (1) dissolving boron nitride nanosheets into tetrahydrofuran, ultrasonically dispersing uniformly, adding a modifier for reaction, then removing tetrahydrofuran by using a rotary evaporator, transferring into deionized water, and drying to obtain a boron nitride nano-sheet; drying to obtain a modified boron nitride nanosheet; (2) dispersing carbon nanotubes in deionized water, stirring and carrying out ultrasonic treatment, adding the modified boron nitride nanosheets, and then carrying out freeze orientation treatment and freeze drying treatment to obtain a porous foamed composite heat-conducting filler; and (3) carrying out melt blending on the composite heat-conducting filler and polyethylene glycol terephthalate, and carrying out hot press molding to finally prepare the modified high-heat-conductivity polymer. According to the invention, the composite heat-conducting filler improves the interfacial compatibility and dispersity with a polymer matrix, and reduces the interfacial thermal resistance of the composite material, so that the modified polymer has good application in the aspect of heat dissipation of electronic equipment.

The invention discloses a self-adaptive anti-sticking cable and a preparation method and application thereof. The self-adaptive anti-sticking cable comprises a superconducting core wire, a self-adaptive anti-sticking layer, a self-repairing insulating layer and a multifunctional outer sheath which are sequentially arranged from inside to outside. According to the scheme, the problems of debonding, breakdown, energy consumption and failure of a traditional cable in an extreme environment are comprehensively solved through gradient piezoelectric-phase change synergistic dynamic stress compensation, vertical boron nitride insulation network directional blocking, thermoelectric-super-hydrophobic multifunctional outer sheath integration and an extreme environment adaptive self-repairing system.

The invention relates to the technical field of heavy anti-corrosion coatings, in particular to a graphene enhanced epoxy modified organic silicon resin heavy anti-corrosion powder coating. The coating is prepared from the following components in parts by weight: 42 to 58 parts of epoxidized epoxy modified organic silicon resin, 0.8 to 2.5 parts of hydroxylated graphene, 6 to 11 parts of nano zirconium dioxide coated boron nitride, 2.5 to 5.5 parts of lanthanum iso-octoate-titanate composite coupling agent, 1.5 to 3.5 parts of bis (3-triethoxysilylpropyl) disulfide, 4 to 7 parts of polyhedral oligomeric silsesquioxane, 5 to 8 parts of curing agent, 0.8 to 1.8 parts of flatting agent and 0.4 to 0.9 part of defoaming agent. 2.5 to 4.5 parts of polyether-ether-ketone micro powder and 1.2 to 2.8 parts of fluorine-containing phosphate ester. According to the invention, the resin is modified through chemical bridging, the modified graphene and the nano-coated powder are matched to construct a synergistic enhancement system, and the interface bonding is optimized by the composite coupling agent. The coating is excellent in adhesive force, corrosion resistance and mechanical property, good in processing fluidity and high in aging resistance and thermal stability, solves the problem that a traditional product is short in performance, and meets the industrial requirement.

The invention relates to the field of quantum dot ink, and discloses diffusion plate printing quantum dot ink and a preparation method thereof.The diffusion plate printing quantum dot ink comprises acrylic resin, hyperbranched polyester resin, a quantum dot material, modified boron nitride, a reactive diluent, a photoinitiator, a wetting agent and a defoaming agent; the hyperbranched polyester resin is prepared by reacting hyperbranched polyester acrylate and a sulfydryl-terminated silicon-containing reaction monomer, wherein the hyperbranched polyester acrylate is prepared by reacting pentaerythritol with 2, 2-dimethylolpropionic acid and then carrying out esterification reaction with acrylic acid; the sulfydryl-terminated silicon-containing reaction monomer is prepared by reacting eugenol with 1, 1, 3, 3-tetramethyldisiloxane and then carrying out esterification reaction with 3-mercaptopropionic acid; the modified boron nitride is prepared by modifying a cationic polymer which is prepared by carrying out a Mannich reaction on triethylene tetramine, formaldehyde and acetone and then carrying out a condensation polymerization reaction with formaldehyde. After the ink prepared by the invention is cured, a coating film is high in hardness, adhesive force and heat conductivity coefficient, and good in flexibility, heat resistance and migration barrier property.

The invention provides a preparation method of an h-BN / PI high-temperature-resistant anticorrosive coating, and relates to the technical field of polymer composites.The preparation method of the h-BN / PI high-temperature-resistant anticorrosive coating comprises the steps that under the protection of inert atmosphere, aromatic diamine containing impurity element five-membered rings and aromatic dianhydride containing ether bonds are taken and subjected to a polymerization reaction in a polar aprotic solvent, and the h-BN / PI high-temperature-resistant anticorrosive coating is obtained. A polyamide acid solution is obtained; performing ultrasonic-assisted liquid phase stripping on the micron-sized hexagonal boron nitride to obtain single-layer hexagonal boron nitride; adding the single-layer hexagonal boron nitride into the polyamide acid solution for multiple times, and uniformly stirring to obtain a hexagonal boron nitride / polyimide composite solution; and coating the hexagonal boron nitride / polyimide composite liquid on a to-be-coated surface, and carrying out gradient heating curing to obtain the h-BN / PI high-temperature-resistant anticorrosive coating. The h-BN / PI high-temperature-resistant anticorrosive coating based on interaction of multiple hydrogen bonds has relatively good high temperature resistance, relatively good resistance mechanical property and excellent corrosion resistance.

The invention relates to the field of aluminum materials, and provides an automobile corrosion-resistant aluminum material and a preparation method thereof.The automobile corrosion-resistant aluminum material is prepared from cerium oxide loaded aluminum oxide nanorods, scandium / boron nitride nanotubes, zirconium powder, magnesium powder, copper powder, manganese powder, silicon carbide nanoparticles, TiB2 nanoparticles, aluminum powder and stearic acid. Wherein the cerium oxide loaded aluminum oxide nanorod is composed of an aluminum oxide nanorod and cerium oxide nanoparticles loaded on the surface of the aluminum oxide nanorod, and the scandium / boron nitride nanotube is composed of a boron nitride nanotube and a scandium nanolayer uniformly coated on the surface of the boron nitride nanotube. The material is prepared through mechanical ball milling, cold isostatic pressing forming, vacuum sintering and aging treatment, and finally the aluminum-based composite material containing the Al3Sc nano precipitated phase and the boron nitride nanotube reinforced phase is formed. And an Al3Sc precipitated phase and an aluminum matrix form a coherent interface, so that the strength, the corrosion resistance and the wear resistance of the material are improved. Through nanostructure optimization, high performance of the aluminum alloy is achieved, and the aluminum alloy is suitable for the fields of automobiles, aerospace and the like.

The invention relates to the technical field of coatings, and discloses a modified hexagonal boron nitride and organic silicon double-component doped high-flame-retardant epoxy resin powder coating as well as a preparation method and application thereof. Comprising the following raw materials in parts by weight: 25-50 parts of modified hexagonal boron nitride, 90-110 parts of organic silicon resin, 120-150 parts of epoxy resin, 5-8 parts of dicyandiamide, 100-120 parts of silica powder, 8-12 parts of other auxiliaries and 80-100 parts of filler. The flame-retardant epoxy resin powder coating is prepared by uniformly mixing the components, melting, extruding a sheet material, grinding and sieving. The flame-retardant and fireproof performance of the epoxy resin powder coating is greatly improved in a modified hexagonal boron nitride and organic silicon double-component doping mode.

The invention relates to the technical field of TPU (thermoplastic polyurethane) protective films, in particular to a fluoride-free antibacterial TPU protective film and a preparation method thereof. The fluoride-free antibacterial TPU protective film comprises the following raw materials in parts by weight: 35-40 parts of TPU particles, 10-15 parts of a balance regulator, 8-12 parts of an antibacterial agent, 3-6 parts of an antioxidant, 3-5 parts of a heat stabilizer and 2-3 parts of a lubricant. According to the TPU protective film disclosed by the invention, TPU particles are matched with the antibacterial agent, the antioxidant, the heat stabilizer and the lubricant to serve as functional aids, and the balance regulator and the filling agent doped with flaky boron nitride are added to coordinate, cooperate and jointly achieve synergistic effects, so that the product is excellent in raw material interfacial compatibility, and the antibacterial property, barrier property and mechanical property of the product are improved in a coordinated and balanced manner; and the product has remarkable weather-resistant and acid-corrosion-resistant stability effects.

The preparation method comprises the following steps: firstly, uniformly stirring and mixing synthetic fluorophlogopite, silica, polymethylsilsesquioxane, boron nitride, bismuth oxychloride, zinc stearate, aluminum starch octenylsuccinate, mica, aluminum oxide, hydrolyzed sodium hyaluronate and toner in a stirring homogenizer; then uniformly mixing polydimethylsiloxane, octyldodecanol stearoyloxy stearate, isoamyl laurate, diisostearyl malate, phenoxyethanol and caprylyl glycol, and heating to 45 + / -5 DEG C; pouring the mixture into an oil spraying barrel of a stirring homogenizer, uniformly stirring and mixing while spraying oil, crushing, then carrying out airflow crushing, sieving the material, putting the sieved material into a mold plate, and carrying out compression molding, so as to obtain a pressed powder block; and putting the mixture into a packing material powder box to obtain the make-up fixing and brightening pressed powder. The pressed powder is prepared by adding an airflow crushing process, the particle size of the powder is smaller, the powder is dispersed more uniformly, the powder is pressed into the solid pressed powder, and the phenomenon of powder flying is well reduced while makeup fixing and brightening effects are achieved.

The invention discloses a lithium ion battery composite diaphragm, a preparation method and a lithium ion battery, and relates to the technical field of lithium ion batteries. The lithium ion battery composite diaphragm comprises a base membrane and a functional coating arranged on the negative electrode side of the base membrane, the functional coating sequentially comprises an ion conducting layer, a thermal barrier layer and a self-repairing layer from the position close to the base film to the position far away from the base film; wherein the base membrane is a polyimide and aramid nanofiber blended electrostatic spinning membrane; the ion conducting layer comprises a compound of a modified fast ion conductor and polyvinylidene fluoride-hexafluoropropylene; the thermal barrier layer comprises a cross-linked network of boron nitride nanosheets and polybenzimidazole; the self-repairing layer comprises polyurethane microspheres loaded with dynamic disulfide bonds. The composite diaphragm provided by the invention can remarkably inhibit a purple area on the surface of a negative electrode, and enhance high-temperature self-protection and interface self-repairing of the lithium ion battery, so that the cycle and safety performance of the lithium ion battery are remarkably improved.

The invention discloses high-thermal-conductivity carbon black and a preparation method and application thereof, and relates to the technical field of carbon black modification.The preparation method of the high-thermal-conductivity carbon black comprises the following steps that carbon black is subjected to oxidation treatment, silanization treatment and tannic acid coating treatment, and modified carbon black is obtained; preparing a graphene / boron nitride / modified carbon black multi-dimensional filler; carrying out primary modification on the graphene / boron nitride / modified carbon black multi-dimensional filler by adopting lignin, polyvinylpyrrolidone and samarium chloride, and then carrying out secondary modification by adopting 6-aminocaproic acid to obtain the high-thermal-conductivity carbon black. The high-thermal-conductivity carbon black prepared by the invention not only has good dispersity, but also can well improve the thermal conductivity and mechanical properties of a rubber matrix.

The invention discloses a micron-resolution boron nitride neutron scintillation screen and a preparation method thereof, and the preparation method comprises the following steps: taking an inch-level sapphire single crystal as a substrate, and selecting an aluminum polar surface as a growth surface; fixing the substrate by using a graphite clamp, putting the substrate and the chemical vapor deposition furnace into a chemical vapor deposition furnace, vacuumizing, and heating the furnace body to a reaction temperature by using a graphite heater; then raw material gas and carrier gas N2 are introduced into the furnace, meanwhile, the graphite clamp and the graphite heater are decomposed at high temperature so as to provide a proper amount of carbon source, and the gas is mixed and reacts to deposit a crystalline boron nitride film on the substrate; and soaking with alcohol to separate the boron nitride film from the substrate, cutting, and fixing on an aluminum plate to prepare the neutron scintillation screen. The boron nitride film is compact and transparent, shows a strong blue light emission characteristic due to carbon defects, and can be used as a micron-resolution neutron scintillation screen. The micron-resolution boron nitride neutron scintillation screen is successfully realized, and the potential of the micron-resolution boron nitride neutron scintillation screen in the aspect of high-resolution neutron imaging is proved.

The invention provides an aerogel-based heat-preservation, heat-insulation and waterproof composite coating material for a building outer wall and a preparation method thereof, and belongs to the field of building materials. Through hydrophobic modified silicon dioxide aerogel, a lightweight heat insulation frame is provided, and the waterproofness and compatibility are improved; the mechanical property and the crack resistance are enhanced through the modified potassium titanate nanofibers, and self-adaptive heat insulation is achieved; the thermoelectric effect, the wear resistance and the thermal regulation performance are optimized through plasma treatment and polyaniline coated tungsten carbide nanoparticles; the heat management performance, the crack resistance and the comprehensive heat insulation and waterproof capacity are improved through graphene oxide composite modified boron nitride; the flexibility, the hydrophobicity and the interfacial compatibility are improved through organic silicon modified bisphenol A epoxy resin; and the performance of the coating is optimized through the synergistic effect of the components.