6861 results about "Heat treated" patented technology

The invention relates to a hot-rolled wire rod for a 2230 MPa grade stranded wire and a manufacturing method of the hot-rolled wire rod, after a Cr-Nb-Al high-carbon component design is rolled and spun into a wire rod, the wire rod is subjected to online molten salt isothermal toughening treatment, so that the wire rod is firstly subjected to front-section molten salt treatment and enters a sorbite phase region from an austenite state to form a structure taking a sorbite structure as a main structure; and then carrying out rear-section molten salt treatment, reducing the circulation volume of molten salt, promoting the unconverted retained austenite to be continuously converted into sorbite, carrying out isothermal tempering, promoting fusing of a part of sorbite lamellar layers, and finally carrying out slow cooling through a roller way, so as to prepare the hot-rolled wire rod of which the microscopic structure comprises a mixed structure consisting of tempered sorbite, ferrite and fused sorbite, the material cost can be controlled, the tensile strength is 1513-1563 MPa, the percentage reduction of area is 31%-36%, and the structure uniformity and the production efficiency are both considered, so that off-line heat treatment is avoided during stranded wire manufacturing, and the drawing pass and the cracking risk are reduced.

The invention discloses an integrated preparation method of a SiC-based composite material environment barrier coating in the technical field of aviation thermal structure materials, which comprises the following steps: cleaning a substrate, carrying out vacuum impregnation of phenolic resin and curing, coating Si slurry to form a bonding layer, coating rare earth silicate slurry to form a barrier layer, and drying to obtain the SiC-based composite material environment barrier coating. And finally carrying out high-temperature heat treatment in an inert atmosphere. According to the method, through an integrated slurry coating and gradient curing process, the performance of a base body is protected, and meanwhile efficient preparation of the coating is achieved; by adopting an integrated slurry coating and gradient curing technology and combining with an optimized medium-temperature sintering process, the matrix performance is effectively protected while the compactness of the coating is ensured, the bonding strength and interface stability of the coating are improved through the design of the phenolic resin transition layer and the silicon bonding layer in cooperation with the rare earth silicate barrier layer, and the bonding strength of the coating is improved. And the coating shows excellent protection performance in a high-temperature corrosion environment.

The invention discloses a multi-element low-alloying high-speed extrusion flame-retardant magnesium alloy and a preparation method thereof. The alloy comprises the following components in percentage by mass: 0.5 to 2.0 percent of Al, 0.2 to 1.0 percent of Zn, 0.1 to 1.0 percent of Mn, 0.2 to 0.8 percent of Ca, 0.2 to 1.0 percent of heavy rare earth element Y, Er or Gd and the balance of Mg and inevitable impurities. Through the synergistic effect of non-rare earth elements Al, Zn, Mn and Ca and trace heavy rare earth elements, matching of low cost, good mechanical property and flame retardant property is realized. After the alloy is subjected to optimized bipolar homogenization heat treatment, the alloy can be subjected to extrusion production at the extrusion rate of 10-30 m / min. The room-temperature ultimate tensile strength is larger than or equal to 270 MPa, the yield strength is larger than or equal to 240 MPa, the ductility is larger than or equal to 12%, and the ignition point is larger than or equal to 850 DEG C. Important support is provided for propelling the magnesium alloy extrusion material to achieve equipment lightweight and low-carbon manufacturing in the fields of rail transit, aerospace and the like.

The invention relates to a hot-rolled wire rod for a 2200MPa-grade stranded wire and a manufacturing method of the hot-rolled wire rod, after Nb-Al high-carbon component is rolled and spun into a wire rod, the wire rod is subjected to online molten salt strong isothermal treatment, so that the wire rod is firstly subjected to front-section molten salt treatment and enters a sorbite phase region from an austenite state to form a structure taking a sorbite structure as a main structure, and then is subjected to rear-section molten salt treatment to form the hot-rolled wire rod for the 2200MPa-grade stranded wire. The molten salt temperature is increased, the molten salt circulation amount is reduced, unconverted retained austenite is promoted to be continuously converted into sorbite, isothermal tempering is carried out, part of sorbite lamellas are promoted to be fused, and finally slow cooling is carried out through a roller way, so that the hot-rolled wire rod with the microscopic structure comprising a mixed structure composed of tempered sorbite, ferrite and fused sorbite is prepared. According to the method, abnormal structures can be inhibited, the strength of a hot-rolled wire rod can be improved, plasticity and production efficiency are both considered, the tensile strength is 1490-1540 MPa, the percentage reduction of area is 34%-39%, downstream users can avoid off-line heat treatment, and stable production of stranded wires is promoted.

The invention relates to the technical field of aluminum alloy materials, in particular to a high-temperature-resistant and high-strength aluminum alloy material and a preparation method thereof. The problems that an existing aluminum alloy material is insufficient in mechanical property and poor in high temperature resistance are solved. A plurality of strengthening elements with synergistic effects, including copper, magnesium, scandium, zirconium, nickel, manganese and titanium, are introduced into an aluminum alloy matrix, meanwhile, multiple layers of graphene nanosheets are added for step-by-step smelting, and under argon protection, hexachloroethane refining and lithium salt complexing agent grain refinement are performed to prepare a smelted alloy; and by combining the multi-stage refined smelting, the staged heat treatment process, the three-stage aging treatment and the surface modification process, the microstructure is optimized, and meanwhile the surface performance is improved. According to the prepared aluminum alloy material, through multi-element cooperation and multi-process optimization, the mechanical property, the high temperature resistance and the surface oxidation resistance of aluminum alloy are remarkably improved, and the aluminum alloy material is suitable for the field of aerospace.

The invention discloses a 1500MPa-grade titanium alloy bar and a preparation method thereof, and belongs to the field of titanium alloy preparation. The 1500MPa-grade titanium alloy bar comprises the following chemical components in percentage by mass: 5.5 to 6.5 percent of V, 4.5 to 5.5 percent of Mo, 3.0 to 4.0 percent of Al, 2.5 to 3.5 percent of Zr, 1.5 to 2.5 percent of Cr, 1.5 to 2.5 percent of Nb, 0.9 to 1.1 percent of Fe and the balance of Ti and impurities. The preparation method comprises the following steps: preparing raw materials according to the components, pressing the raw materials into electrode blocks, welding to obtain consumable electrodes, and performing multi-vacuum consumable smelting to obtain cast ingots; the cast ingot is subjected to cogging forging in a beta area, multi-heating-number upsetting and drawing deformation in the beta area and forged into a bar in a two-phase area; and through multi-pass rolling and multiple solid solution aging heat treatment, the 1500MPa-grade titanium alloy bar is obtained, meanwhile, the ductility is kept to be 6% or above, and the requirement of future aerospace for high-performance titanium alloy is met.

The invention relates to the technical field of non-ferrous metal processing, and particularly provides a preparation method of a high-strength beryllium-containing Al-Mg-Zn-Cu series aluminum alloy profile. The preparation method of the high-strength beryllium-containing Al-Mg-Zn-Cu series aluminum alloy profile comprises the following steps that S1, after alloy raw materials are subjected to smelting treatment and refining treatment, an ingot blank is obtained through casting treatment or spray forming treatment; s2, the ingot blank is subjected to homogenization treatment and extrusion treatment, and an extruded profile is obtained; and S3, the extruded profile is subjected to solid solution quenching treatment and two-stage aging treatment, and the high-strength beryllium-containing Al-Mg-Zn-Cu series aluminum alloy profile is obtained. According to the invention, specific extrusion process parameters are adopted and a two-stage aging heat treatment system is combined, so that the preparation of the low-cost, low-density, high-strength and corrosion-resistant aluminum alloy profile is successfully realized.

The invention discloses a heat treatment method of an iron-nickel-based high-temperature alloy, which solves the contradiction between stress relief annealing and performance maintenance through four-step temperature coordinated regulation and control: in the first step, MC type carbide is dissolved through solid solution, segregation is eliminated, and excessive growth of crystal grains is avoided; in the second step, roughening of M23C6 type carbides is inhibited through solid solution, and formation of fine and uniform carbides on grain boundaries is promoted so as to strengthen the grain boundaries; in the third step, the residual stress is reduced through stress relief annealing, and meanwhile grain boundary carbide growth and abnormal grain growth are avoided; and in the fourth step, uniform and stable precipitation of a gamma'phase is promoted through aging, the nanometer size and the high volume fraction are maintained, and coarsening is avoided. Through precise temperature connection, the residual stress is effectively reduced, grain growth, structure nonuniformity or performance degradation caused by traditional annealing are avoided, and finally the application requirement of the superhigh-temperature steam environment at the temperature of 650 DEG C or above is met on the premise that the mechanical property and the corrosion resistance are guaranteed.

The invention relates to the technical field of manufacturing of engineering machinery parts, and discloses an engineering machinery driving wheel made of a medium carbon alloy cast steel material. The invention also discloses a preparation process of the engineering machinery driving wheel material, which comprises the following steps: S1, casting treatment: melting the medium carbon alloy steel material, and casting into a driving wheel blank; s2, normalizing heat treatment: carrying out normalizing heat treatment on the driving wheel blank; s3, rough machining treatment; s4, quenching treatment: carrying out induction quenching treatment; and S5, finish machining treatment. The synergistic effect of alloy elements in a medium carbon alloy cast steel material is combined with an optimized air cooling process, so that the cast steel is normalized to obtain a uniform structure which mainly contains superfine pearlite and contains extremely little ferrite, the matrix hardness is stable, and the requirement of a high-performance driving wheel is completely met; after the process route is improved, tempering and shot blasting and flaw detection procedures after tempering are canceled; the technological process is greatly shortened, material turnover is reduced, and the production efficiency is improved.

The invention relates to the technical field of crossing of artificial intelligence and intelligent manufacturing, discloses a position self-adaptive AI regulation and control method and system for continuous heat treatment of a fastener, and aims to solve the problems of non-uniform temperature field, high hardness dispersion, increase of quenching cracking rate and the like caused by lack of position perception and dynamic compensation lag in the prior art. According to the method, in-furnace coordinates of fasteners are tracked in real time through a high-speed visual positioning device, a thermal demand prediction neural network model with space-time convolution mixed with a gating circulation unit is constructed in combination with the conveying speed, thermal environment parameters and material characteristics, and an instantaneous thermal power instruction is output; the system comprises a high-speed visual positioning module, a motion state monitoring module, a thermal environment sensing module, a thermal demand prediction module and the like, and drives a high-density partitioned infrared heating array to realize millisecond-level local thermal compensation. According to the method, the temperature deviation of the junction of the temperature zones can be controlled within + / -8 DEG C, the hardness dispersion and the cracking rate are remarkably reduced, and the heat treatment consistency and the finished product yield are improved.

The invention relates to the technical field of high polymer material processing, in particular to a blow molding method of a composite toughened film, which comprises the following steps: step 1, preheating matrix resin in preheating equipment; 2, feeding the mixed raw materials into a double-screw extruder for melt blending; 3, feeding the dried composite particles into a hopper of a single-screw blow molding extruder; 4, adjusting the air volume and the air pressure of the cooling system according to the monitoring result; and 5, the formed film pipe is folded into a flat shape through a guide component and led out through a traction roller, the traction speed and the extrusion speed are coordinated to control the traction ratio, corona treatment is conducted on the surface of the thin film to improve the surface energy, then rolling tension is controlled for rolling, and the rolling tension is controlled according to the elasticity and thickness of the thin film to prevent excessive stretching or loosening. The uniform distribution and proper compatibility of the composite toughening component improve the toughness of the film, and maintain the strength and barrier property of the film.

The invention relates to a high-strength complex-phase hot-rolled wire rod for a 2260MPa-grade stranded wire and a manufacturing method of the high-strength complex-phase hot-rolled wire rod, after the high-carbon component design of C-Si-Mn-Cr-V-Nb-V is rolled and spun into a wire rod, the wire rod is subjected to online molten salt mixed quenching isothermal treatment, so that the wire rod is subjected to front-section molten salt treatment to be quickly cooled, enters a bainite and pearlite mixed phase region from an austenite state, and is subjected to hot rolling and hot rolling to form the high-strength complex-phase hot-rolled wire rod. The method comprises the following steps: carrying out first-stage molten salt treatment on austenite to promote transformation of part of austenite to bainite and sorbite, then carrying out later-stage molten salt treatment to increase the molten salt temperature, promoting decomposition and transformation of untransformed retained austenite into sorbite, carrying out isothermal tempering, and finally carrying out slow cooling through a roller way, a hot-rolled wire rod with a microscopic structure comprising a complex-phase structure composed of tempered bainite, tempered sorbite and ferrite is manufactured, the tensile strength is 1547-1597 MPa, and the percentage reduction of area is 27%-32%, so that when a high-strength stranded wire is manufactured, off-line heat treatment is not needed, the drawing pass number is reduced, and the wire breaking risk is reduced.

The invention relates to the technical field of preparation of aluminum alloy conductor materials, and particularly discloses a preparation method of an Al-Mg-Si-RE-based aluminum alloy conductor for a 10-35kV middle and low voltage cable, which comprises the following steps: adding a microalloyed intermediate alloy into an aluminum melt by adopting an addition method, stirring, smelting, refining, and casting to form, thereby obtaining the Al-Mg-Si-RE-based aluminum alloy conductor for the 10-35kV middle and low voltage cable. And performing annealing, rolling, wire drawing and aging heat treatment to obtain a final product. Wherein in the smelting stage, raw materials are completely melted at 700-750 DEG C; hexachloroethane is used as a refining agent for refining; annealing at 330-350 DEG C and preserving heat for 4-8 hours; and aging at 300 DEG C for 10 hours after deformation. In the preparation of a wire of a 10-35kV medium and low voltage power cable, the aluminum alloy wire has high conductivity of 62.1-62.5% IACS (International Annealed Copper Standard) and tensile strength of 101-117MPa by simplifying the process steps and optimizing the element ratio on the premise of ensuring the controllable raw material cost, and the mechanical property and electrical property requirements of the medium and low voltage wire are balanced.

The invention provides an asphalt-based hard carbon negative electrode material as well as a preparation method and application thereof, belongs to the technical field of battery materials, and is used for solving the technical problems that a template is non-uniformly distributed in a carbon source and the size is difficult to control in hard carbon preparation. The preparation method of the asphalt-based hard carbon negative electrode material comprises the following steps: mixing asphalt and organic zinc salt, and then carrying out heat treatment to obtain high-softening-point asphalt; and pre-oxidizing and carbonizing the high-softening-point asphalt to obtain the asphalt-based hard carbon negative electrode material. Organic zinc salt and asphalt form a metal template in situ at a high temperature, the metal template can be uniformly distributed in the asphalt, meanwhile, the particle size of the template is controlled through process change, and the prepared asphalt-based hard carbon negative electrode material has high reversible specific capacity, high initial coulombic efficiency and good rate capability.

In the case of forming a fine resist pattern, it is desired to further reduce the roughness of the resist pattern.SOLUTION: A substrate processing apparatus comprising: a heat treatment unit configured to bake a resist film; an exposure unit configured to irradiate the resist film having a portion irradiated with a first radioactive ray with a second radioactive ray; a development unit configured to form a resist pattern by development for removing a part of the resist film; and a control unit configured to control the exposure unit such that the second radioactive ray is collectively irradiated to an entire region of the resist film including the portion irradiated with the first radioactive ray and a portion other than the portion irradiated with the first radioactive ray. The first radiation is ionizing radiation or non-ionizing radiation, and the second radiation is non-ionizing radiation. When the first radiation is non-ionizing radiation, the second radiation is non-ionizing radiation having a wavelength longer than the wavelength of the first radiation. The resist film includes a metal oxide photoresist material.SELECTED DRAWING: Figure 1

This invention provides a method for high-strength aluminum-lithium alloy friction stir deposition additive manufacturing and multi-stage heat treatment, relating to the technical field of aluminum alloy friction stir deposition additive manufacturing. The method includes: fixing a substrate and placing a stirring head in the area to be added to the substrate; loading a base material into the stirring head; starting the program, with a push rod slowly pushing the aluminum-lithium alloy base material to the area to be added; when the aluminum-lithium alloy base material reaches a thermoplastic state, the stirring head advances to complete deposition; lifting the stirring head and adjusting the height of the end face of the stirring head relative to the deposited layer to perform reverse-direction additive manufacturing to complete deposition; repeating the deposition steps layer by layer upwards until the height of the deposited layer reaches the target height to obtain a friction stir deposition additive component; subjecting the friction stir deposition additive component to low-temperature solution treatment and a first aging treatment, followed by high-temperature solution treatment and a second aging treatment to obtain a high-strength aluminum-lithium alloy, effectively solving the problems of difficult forming and easy cracking of ultra-large and moderately complex aluminum-lithium alloy structural parts.

The invention discloses a regulation and control method and a preparation method of in-situ ceramic particles of a copper-based composite material. The method comprises the following steps: weighing according to a reaction equation and a reaction molar ratio; the molar ratio coefficient is changed, trace alloy is added, and the size and morphology of in-situ particles are regulated and controlled; the copper-based pre-dispersed in-situ ceramic intermediate alloy reinforcer is prepared through powder mixing, cold pressing and sintering; crushing the reinforcer, remelting, stirring and casting; and after the cast alloy is subjected to heat treatment, the high-performance in-situ particle reinforced copper-based composite material is prepared. According to the obtained in-situ ceramic intermediate alloy reinforcer, pre-dispersion of ceramic particles in a copper matrix can be achieved, and good combination of the particles and the matrix is achieved by adding the copper-based pre-dispersion in-situ ceramic intermediate alloy reinforcer into a molten matrix alloy; interface pores caused by sharp corners, surface pollution and the like of the heterogeneous particles in an external addition method are avoided, and the strengthening effect of the heterogeneous particles is weakened.

The invention provides a Fe-containing Ti-Al-Mo series high-strength, high-plasticity and low-cost titanium alloy. The titanium alloy comprises the following components in percentage by mass: 6.0%-7.5% of Al, 0.5%-2.5% of Fe, 1.0%-2.5% of Mo, 0.5%-2.0% of V, 1.5%-3.5% of Zr and 0%-2.0% of Sn. And the balance of Ti and inevitable impurities. The microscopic structure of the titanium alloy is a first tissue structure or a second tissue structure, the first tissue structure comprises an equiaxed primary alpha phase and a secondary alpha phase, and the second tissue structure comprises an equiaxed primary alpha phase, a lamellar primary alpha phase and a secondary alpha phase; wherein the equiaxial primary alpha phase is uniformly distributed in the beta matrix, the lamellar primary alpha phase is distributed in the beta matrix along the deformation direction, and the secondary alpha phase is uniformly dispersed and distributed in the beta matrix. A performance foundation is laid through component design and element matching, directional regulation and control of an alloy microstructure are achieved by combining precise forging and heat treatment processes, excellent matching of high strength and high plasticity is finally obtained, and meanwhile the production cost is remarkably reduced.

The invention belongs to the field of negative electrode materials, and particularly relates to a silicon-graphite composite material, a preparation method and application thereof and a lithium ion battery, the preparation method comprises the following steps: mixing and slurrying silicon powder, graphite and a composite functional additive, and then carrying out ball milling modification to obtain primary composite particles; the composite functional auxiliary agent comprises an auxiliary agent A, an auxiliary agent B and an auxiliary agent C; the primary composite particles and a carbon source liquid phase are compounded and then subjected to spray drying and heat treatment, or spray pyrolysis is directly carried out, and secondary composite particles are prepared; and carrying out modification treatment on the secondary composite particles prepared in the step 2 in a surface modification liquid, and then carrying out low-temperature annealing at 150-300 DEG C to prepare the silicon-graphite composite material. The surface modification liquid is an organic solution in which conductive lithium salt and an auxiliary agent D are dissolved. Based on the combined control of the preparation process and the structure, the silicon-based negative electrode material with ultra-long cycle life and excellent low-temperature fast charging performance can be obtained.

The invention discloses a preparation method of a high-strength, high-hardness and ablation-resistant CuWTaTeAl gradient nano composite material. The method comprises the following steps: 1, mechanically mixing Cu80Al20 spherical coated powder, Cu90W10 spherical coated powder, WTe2 alloy powder, Ta powder and Cu powder, and then carrying out ball milling and mixing; 2, performing SPS (spark plasma sintering); thirdly, after soaking treatment, multi-pass hot rolling deformation is carried out, and then quenching treatment is carried out; and 4, annealing heat treatment. The binary spherical coating powder, the alloy powder and the elementary substance powder are subjected to ball milling and mixing to achieve uniform distribution of all elements, high-melting-point W and Ta are added to improve the ablation-resistant temperature of the composite material, large-scale copper dendrite powder is added to form gradient distribution nanocrystals, the proportion of all the elements is controlled, the lattice distortion degree is increased, and the ablation-resistant temperature of the composite material is improved. The high-strength, high-hardness and ablation-resistant CuWTaTeAl gradient nano composite material is suitable for the fields of contacts, switches, electrical connectors, resistance welding electrodes and the like.

The application relates to a continuous macro-preparation device and method of a soft and elastic ceramic superfine fiber material, which sequentially comprises a feeding and liquid preparation system, a multi-jet uniform electrostatic spinning system, a low-temperature calcination system and a winding system. Raw materials are mixed, low-temperature dispersed and vacuum concentrated to obtain a sol; the sol and a polymer flow into a polymer mixing device to be mixed and bubble removed; the mixed sol flows into an inorganic component content control device to be pumped by negative pressure to obtain a spinning solution; the spinning solution flows into a multi-jet electrostatic spinning module to adjust and control the temperature, humidity and multi-directional differential speed during spinning to obtain a fiber membrane material or a fiber flake material; the fiber material is sequentially transmitted to a drying area, a microwave pretreatment area, a polymer removal area, an oxygen-poor atmosphere heat treatment area and a cooling area to be calcined in multiple temperature zones to obtain the soft and elastic ceramic superfine fiber material; and winding and packaging are realized to realize the continuous macro-manufacture of the soft and elastic ceramic superfine fiber material.

The invention relates to the technical field of corrosion-resistant coatings, in particular to a post-treatment method for improving the corrosion resistance of a chemical nickel-plated layer in a plasma environment. Comprising the following steps: preparing composite sol, coating a workpiece, carrying out plasma-assisted curing, and then carrying out heat treatment on an inorganic-organic hybrid coating framework; an inorganic-organic hybrid coating framework firmly combined with a nickel-plated layer is formed on the surface of a chemical nickel-plated workpiece under a low-temperature condition by preparing composite sol and matching with plasma-assisted curing, and rare earth elements are immobilized in situ; the inorganic-organic hybrid coating framework is further condensed through subsequent heat treatment, pore collapse and structural densification are achieved, and therefore the final compact corrosion-resistant coating is formed, and rare earth elements are fixed in the compact corrosion-resistant coating in a chemical bonding mode; therefore, thermal stress and interface stripping risks caused by a thermocuring process are eliminated, and long-acting, stable and reliable protection on a matrix under extremely harsh working conditions is realized.

The invention discloses a preparation process of a high-performance Cu-Ni-Fe alloy calculated and designed based on a first principle, and relates to the technical field of alloy material preparation. According to the process, a precise Cu-Ni-Fe ternary alloy thermodynamic database is constructed by combining a first principle with a CALPHAD method, a multivariate phase diagram is calculated based on the database to determine a component range, then optimized components of a work function, an elastic constant and a thermal expansion coefficient are calculated through the first principle, and a finished product is obtained through smelting, heat treatment and forming machining. The final alloy is composed of, by atomic percent, 30%-75% of Cu, 10%-30% of Ni and 10%-30% of Fe, the tensile strength is larger than or equal to 816.4 MPa, the total elongation at break is larger than or equal to 34.27%, the thermal expansion coefficient is smaller than 20 * 10 <-6 > / K, the excellent mechanical property and thermal stability are achieved, the problems that component design is blind and performance fluctuation is large in a traditional process are solved, and the alloy is suitable for the fields of ocean engineering, electronic packaging and the like.

The invention relates to the technical field of intelligent scheduling, in particular to a steel structure weld fatigue cracking real-time monitoring system based on machine vision, which is characterized in that an image acquisition module acquires a high-stability image sequence in a strong vibration environment; the displacement field reconstruction module adopts a frequency domain-space domain combined decomposition technology to isolate environmental noise and material non-uniformity interference in a breakthrough manner, and an anti-noise deformation field and a stress distribution diagram are synchronously output through dual-channel parallel processing; a damage response module accurately locks sub-pixel-level crack initiation coordinates based on strain energy accumulation rate mutation, and dynamically predicts a yield risk area in combination with a displacement gradient diffusion model; the early warning module intelligently triggers graded response according to the crack position and the space coupling state of the risk area, performs positioning maintenance in a low risk area and automatic strengthening in a high risk area, and outputs heat treatment scheme coordinates when no crack exists; the system solves the problems of false detection caused by vibration noise and lagging response of single-parameter monitoring, and active protection from damage initiation to failure blocking is realized.

The invention discloses a high-strength heat-insulation aerogel structure with a dual multi-scale design and a preparation method thereof, relates to the technical field of thermal protection of spacecrafts, and in particular relates to the high-strength heat-insulation aerogel structure with the dual multi-scale design and the preparation method thereof. The invention aims to solve the problems of insufficient structural rigidity and poorer thermal protection property and thermal stability of the traditional spacecraft surface aerogel structure under the conditions of extreme high temperature and mechanical load. The structure is composed of an upper carbon-carbon composite material plate, a lower carbon-carbon composite material plate, an alloy skeleton and a filler. The method comprises the following steps: 1, preparing a multi-scale C / C composite material; 2, designing and preparing a titanium alloy honeycomb framework; 3, proportioning the multi-scale aerogel; 4, in-mold in-situ gelation; 5, drying and heat treatment; and 6, assembling and solidifying. The porosity of the aerogel is 85-98%, the structure has high rigidity and thermal protection performance, and the aerogel is applied to the field of aerospace thermal protection.

The invention provides an optimization method and an optimization device for electrical performance of a ZnO piezoresistor based on O2 heat treatment. According to the method, O2 is introduced into the ZnO varistor under the condition of heat treatment, and oxygen vacancies in the ZnO varistor are reduced under the oxygen atmosphere, so that the donor concentration is reduced, the carrier concentration is reduced, and the electrical performance of the ZnO varistor is remarkably improved. Besides, the optimization device provided by the invention is used for the heat treatment step in the electrical performance improvement process of the ZnO varistor, and the front and back surfaces of the ZnO varistor can be in full contact with gas in the heat treatment process, so that the electrical performance is uniformly and effectively improved.

The application discloses a MnFe2O4 / GO wave-absorbing aerogel with a directional aperture structure and a preparation method thereof, belongs to the technical field of wave-absorbing material preparation, and is characterized in that manganese ferrite (MnFe2O4) magnetic particles are uniformly loaded on the surface of graphene to obtain a graphene aerogel with a three-dimensional loose porous structure and magnetic particle assembly; the MnFe2O4 is prepared by using a low-temperature co-precipitation method, and the MnFe2O4 / GO wave-absorbing aerogel is prepared by combining directional freezing and heat treatment, and the method is mild and simple. The application improves the impedance mismatch problem of the graphene material, enhances the magnetic loss of the material, and obtains a novel porous aerogel wave-absorbing material which has both dielectric loss and magnetic loss by introducing the manganese ferrite.

The invention discloses an annular furnace heat-resistant supporting forged chassis and an additive manufacturing process and a fixing device thereof, and belongs to the technical field of plating of metal materials, and the annular furnace heat-resistant supporting forged chassis comprises the steps that heat-resistant alloy steel base metal with specific components is prepared; carrying out laser texturing and nickel-based alloy bottom layer pretreatment on the surface of the steel plate; performing laser cladding on high-silicon high-temperature alloy powder containing niobium and rare earth elements to form a functional cladding layer, and performing gradient cladding on the edge of the atmosphere guide hole; and finally, carrying out heat treatment and assembling with a fan-shaped refractory brick fixing device. A composite oxide film and a multi-scale strengthening system are constructed, hydrogen resistance and brittleness resistance are effectively achieved, interface thermal stress is relieved, cracking and stripping of a cladding layer are avoided, a fixing device adapts to thermal expansion, the atmosphere is dredged, and the annealing uniformity of a steel coil is improved; the problems of creep deformation, hydrogen embrittlement, cladding layer stripping and thermal stress cracking of a traditional supporting component under the conditions of high temperature, heavy load and nitrogen and hydrogen atmosphere are solved.

The invention relates to the technical field of powder metallurgy materials, and discloses rare earth microalloyed ultrahigh-strength high-toughness hot work die steel and a preparation method thereof.The die steel is prepared from 4Cr5MoSiV1 pre-alloyed powder, rare earth hydride, boron carbide and porous amorphous carbon powder loaded with a nickel catalyst. The preparation method comprises the steps of material mixing, sheath packaging, graded dynamic reaction thermal devolatilization, hot isostatic pressing densification and heat treatment, in the graded dynamic reaction thermal devolatilization, active hydrogen generated by decomposition of rare earth hydride is used for reducing oxide on the surface of powder, and nickel catalyzed carbon powder is used for capturing water vapor at low temperature to generate CO to be discharged. An oxide film on the surface of the powder is thoroughly removed through in-situ chemical reaction, original particle boundaries are eliminated, meanwhile, a nano strengthening phase with high thermal stability is generated in situ, and the high-temperature strength, impact toughness and tissue compactness of the die steel are remarkably improved.

The invention relates to the technical field of metal smelting, and particularly discloses a preparation method of a high-purity IN718 alloy material. According to the method, on the premise that the mechanical property result redundancy of the IN718 alloy material is large, the content of inclusions and formation of carbides in the steelmaking process are reduced by optimizing the content of C, N and Nb elements in the vacuum induction melting process, reducing the refining temperature and reducing the melting speed of vacuum self-consuming remelting; and in cooperation with two-heating-number upsetting and drawing deformation in the forging process, the situation that carbides in the IN718 alloy material are dispersed unevenly due to segregation is avoided. According to the high-purity IN718 alloy material and the preparation method thereof, the content of carbides in steel ingots is remarkably reduced by controlling all parameters in the duplex process, the overall level of the carbides in the high-purity IN718 alloy material is smaller than or equal to 2.0 level after homogenizing diffusion annealing, forging, machining and heat treatment, the purity of the existing IN718 alloy material is improved, and the use requirements of special equipment such as deep sea equipment and nuclear power equipment can be met.