13584 results about "Heat treating" patented technology

The invention relates to the technical field of welding deformation control, and discloses a multi-stage adjusting method and system for steel structure welding deformation control. The method comprises the steps that steel member parameters are measured, a welding deformation prediction model is established, and pre-deformation data are obtained; performing accurate pre-deformation processing according to the data; executing segmented welding and recording a temperature field and a deformation amount; performing local heat treatment on the high-stress area to obtain stress distribution; correcting a deformation area by using multi-point force; and performing precision detection and quality evaluation according to the corrected data to form a control file. According to the method, high-precision control over welding deformation of the complex steel structure is achieved through data transmission and feedback adjustment of all stages.

The invention relates to the technical field of process optimization, and discloses a hot work die steel heat treatment process optimization method and system.The method comprises the steps that hot work die steel samples are collected under multiple sets of different process conditions, and a performance basic data set is obtained; constructing a multi-target coordination optimization model based on the performance basic data set; performing phase change detection on the hot work die steel sample to obtain phase change monitoring data; performing prediction in combination with the phase change monitoring data to obtain a performance prediction result; and solving an optimal process parameter combination based on the performance prediction result and the multi-target coordinated optimization model, and realizing simultaneous optimization and coordinated balance of a plurality of performance indexes in the heat treatment process of the hot work die steel by making full use of associated information among different performance indexes.

The invention discloses a processing method of a fusion device, and belongs to the technical field of nuclear fusion. The processing method comprises the following steps: carrying out at least one time of vacuum heat treatment on a Dewar embedded part blank; carrying out cleaning anti-corrosion treatment and physical correction treatment on the surface of the dewar embedded part blank subjected to heat treatment; carrying out grinding and polishing treatment on the surface of the Dewar embedded part blank subjected to the cleaning and antiseptic treatment and the physical correction treatment to obtain the Dewar embedded part; the Dewar embedded part is transported to the installation position of the window to be installed, and the Dewar embedded part located at the installation position is temporarily fixed; performing concrete pouring on the mounting position of the Dewar embedded part; and after the concrete is solidified, a cast-in-place concrete structural body is formed in the area below the Dewar embedded part, and a part of the Dewar embedded part is embedded into the cast-in-place concrete structural body. By means of the method, the magnetic conductivity of the Dewar embedded part is reduced, and the risk that elements are activated to form isotopes with the long decay period and the high irradiation dose rate or isotopes with the short decay period and the high irradiation dose rate is reduced.

The invention relates to a high-strength complex-phase hot-rolled wire rod for a 2100MPa-grade stranded wire and a manufacturing method of the high-strength complex-phase hot-rolled wire rod, after a C-Si-Mn-Cr-Mo high-carbon component system is rolled and spun into a wire rod, the wire rod is subjected to online molten salt strong quenching isothermal treatment, so that the wire rod is firstly subjected to front-section molten salt treatment and is cooled at a cooling speed of greater than or equal to 33 DEG C / s, and enters a bainite phase region from an austenite state; the method comprises the following steps: firstly, carrying out first-stage molten salt treatment to promote transformation of austenite into bainite, then carrying out later-stage molten salt treatment to form a structure mainly comprising bainite, carrying out isothermal tempering on the structure, reserving part of untransformed retained austenite, and finally, carrying out roller way slow cooling to promote transformation of the untransformed retained austenite into martensite, and carrying out tempering, the microstructure of the hot-rolled wire rod comprises a complex-phase structure composed of tempered bainite and tempered martensite, the tensile strength of the hot-rolled wire rod can reach 1435-1485 MPa, the percentage reduction of area of the hot-rolled wire rod is 31%-36%, off-line heat treatment of follow-up machining is avoided, and the risk of wire breakage is reduced.

Disclosed is a robot welding assembly mechanism and an application in annular welding seam detection and postweld heat treatment. The robot welding assembly mechanism comprises a rotatable column. A plurality of transverse clamping portions are disposed at intervals on the column. A height-adjustable first V-shaped support portion is disposed at a periphery of the column. The first V-shaped support portion is mounted on a radial track. An annular track is disposed on an outer side of the radial track. A plurality of height-adjustable second V-shaped support portions are disposed on the annular track. The first V-shaped support portion and the second V-shaped support portions are capable of supporting a non-welded portion of the welded workpiece. A first driving mechanism of the rotation base, a second driving mechanism of the transverse clamping portions, and a third driving mechanism of each of the second V-shaped support portions are connected with a control system.

The invention relates to a hot-rolled wire rod for a 2260MPa-grade stranded wire and a manufacturing method of the hot-rolled wire rod, after the high-carbon component design of C-Si-Mn-Cr-Mo-Nb-Al is adopted for rolling and spinning to form the wire rod, online molten salt isothermal toughening treatment is carried out, so that the wire rod is firstly subjected to front-section molten salt treatment and is rapidly cooled, and enters a sorbite phase region from an austenite state to form a structure taking a sorbite structure as a main structure; and then carrying out rear-section molten salt treatment, reducing the circulation volume of molten salt, promoting the unconverted retained austenite to be continuously converted into sorbite, carrying out isothermal tempering, promoting fusing of a part of sorbite lamellar layers, and finally carrying out slow cooling through a roller way, so as to prepare the hot-rolled wire rod of which the microscopic structure comprises a mixed structure consisting of tempered sorbite, ferrite and fused sorbite, the tensile strength can reach 1534-1584 MPa, the percentage reduction of area can reach 33%-38%, and the alloy can be used in the application fields of manufacturing 2260 MPa grade stranded wires and the like without additional heat treatment procedures.

The present application relates to the technical field of glass-ceramics, in particular to a lithium-free transparent spinel glass-ceramics, a preparation method and application thereof. The lithium-free transparent spinel glass-ceramics is obtained by heat treatment of a base glass, and spinel crystal is the main crystal phase. The composition of the glass-ceramics contains the following oxides in mol%: SiO2 38.00-48.00%, Al2O3 25.50-30.00%, ZrO2 3.00-5.00%, MgO 5.00-8.00%, ZnO 8.00-14.00%, Na2O 7.20-14.00%, B2O3 3.00-8.00%, K2O 0-2.00%, and Y2O3 0-1.00%, and basically no Li2O. The glass-ceramics of the present application does not use high-cost lithium, and can obtain excellent surface and deep stress characteristics and excellent drop impact resistance through chemical strengthening.

The invention discloses a wafer composite film and a preparation method thereof, and belongs to the technical field of semiconductor preparation. The method comprises the following steps: (1) performing hydrogen ion or hydrogen-helium mixed ion implantation on a piezoelectric wafer to obtain an implanted wafer, wherein the implanted wafer sequentially comprises a thin film layer, an implanted layer and a residual layer; (2) sequentially forming a defect layer and an isolation layer on the supporting substrate; (3) bonding the isolation layer and the thin film layer of the injected wafer to obtain a bonding body; and (4) laser is adopted to heat the injection layer, then annealing heat treatment is carried out on the bonding body to achieve complete stripping, polishing and cleaning of the film, then the wafer composite film is obtained, the wavelength of the laser is 100-700 nm, the power of the laser is 50 mw to 100 w, and the scanning speed of the laser is 10-50 mm / s. According to the method, complete stripping of the composite film and combination of laser and thermal annealing processes can be effectively achieved, the method has high process stability, the yield of the composite film can be greatly improved, and the processing time cost of the composite film is shortened.

The present invention relates to the technical field of steel plate production, and particularly to a thick steel plate for high-strength storage tanks with a low ductile-brittle transition temperature and a preparation method thereof. The chemical components in the steel are as follows: C: 0.22% - 0.26%, Si: 0.13% - 0.144%, Mn: 0.73% - 0.92%, P≤0.015%, S≤0.01%, Cr: 0.03% - 0.049%, V: 0.01% - 0.019%, Nd: 0.00016% - 0.00047%, and the balance is Fe and impurities. Microalloying is used to ensure the excellent internal structure and service performance of the steel plate; the purity of the molten steel is improved by optimizing the smelting process; the internal structure of the steel plate is optimized and the plate shape is improved by adopting a four-stage slab heating process and a three-stage controlled rolling process; the simulated post-weld heat treatment process is used to improve the strength-ductility matching and adjust the microstructure of the material, ensuring the low-temperature service performance of the steel plate in the full thickness direction.

The invention relates to the technical field of additive manufacturing, and particularly provides a heat treatment method of a nickel-based superalloy for additive manufacturing. The heat treatment method comprises the following steps: S1, preparing a nickel-based high-temperature alloy forming part by adopting a selective laser melting process; s2, the formed part is subjected to homogenizing annealing treatment at the temperature ranging from 1000 DEG C to 1200 DEG C; s3, the formed part subjected to homogenizing annealing treatment is subjected to water quenching treatment and cooled to the room temperature; and S4, the formed part subjected to water quenching treatment is subjected to primary aging treatment at the temperature of 700-800 DEG C, then cooled to 600-700 DEG C, subjected to secondary aging treatment and then air-cooled to the room temperature. According to the method, the effect of simultaneously regulating and controlling the grain structure and the precipitated phase of the SLM-GH4169 alloy is achieved by increasing the homogenizing annealing heat treatment time, combining a water quenching cooling mode and cooperating with two-stage aging, and the strength and plasticity of the alloy are successfully and synergistically improved. According to the prepared SLM-GH4169 alloy, not only can the tensile strength reach 1400 MPa, but also the elongation at break can reach 22% or above.

The invention relates to a high-strength complex-phase hot-rolled wire rod for a 2230 MPa grade stranded wire and a manufacturing method of the high-strength complex-phase hot-rolled wire rod. After a Nb-containing high-carbon component is used for rolling and spinning at a spinning temperature to form a wire rod, online molten salt mixing quenching isothermal treatment is carried out, so that the wire rod is firstly subjected to front-section molten salt treatment and is cooled at a cooling speed of more than or equal to 35 DEG C / s, and enters a bainite and pearlite mixed phase region from an austenite state; the method comprises the following steps: firstly, carrying out heat treatment on austenite to promote part of austenite to be converted into bainite and sorbite, then carrying out later-section molten salt treatment, increasing the molten salt temperature, promoting unconverted retained austenite to be decomposed and converted into sorbite, carrying out isothermal tempering, and finally, carrying out roller way slow cooling, so as to prepare the hot-rolled wire rod of which the microscopic structure comprises a complex-phase structure consisting of tempered bainite and tempered sorbite, the drawing and hardening capacity can be improved, the production efficiency is considered, the tensile strength is 1522-1572 MPa, and the percentage reduction of area is 29%-34%, so that off-line heat treatment is avoided, and the wire breaking risk and cost of stranded wire manufacturing are reduced.

The invention provides a multi-step aging treatment method for improving the toughness of an ultrahigh-strength steel ingot, and belongs to the technical field of steel heat treatment. The treatment method comprises the following steps: carrying out solution treatment on the ultrahigh-strength steel at the temperature above AC3, carrying out water cooling or oil cooling to the room temperature, then carrying out subzero treatment, taking out and recovering to the room temperature; the multi-step aging treatment comprises the first step of single-time or multi-time low-temperature aging at the temperature of 400-550 DEG C and the second step of high-temperature aging at the temperature of 550-650 DEG C, and the ultrahigh-strength steel ingot is obtained. According to the method, the content of reversed austenite is increased, especially film-shaped austenite with stable mechanics is increased, meanwhile, it is guaranteed that a precipitated phase is not obviously coarsened, and good obdurability matching is achieved.

The invention discloses a neodymium-iron-boron magnet with double main phases and light rare earth diffusion based on asymmetric cerium distribution and a preparation method, and relates to the technical field of neodymium-iron-boron magnets. The method comprises the steps that a diffusion matrix is prepared through a double-main-phase technology, in the double-main-phase technology, the components of a main-phase alloy and an auxiliary-phase alloy are RaCebFe100-a-b-c-dMcBd, R is PrNd alloy or Nd metal, M is at least one of Cu, Al, Zr, Co and Ga, the content of Ce in the main-phase alloy is larger than that of Ce in the auxiliary-phase alloy, then the upper surface and the lower surface of the diffusion matrix are coated with a diffusion source solution, and the diffusion matrix is obtained through heat treatment. Carrying out heat treatment and aging treatment to obtain a neodymium-iron-boron magnet; the diffusion source solution is formed by mixing a diffusion source and a solvent, and the diffusion source is (PrmNdn) aAlbCucZrdCoeMgf. The neodymium-iron-boron magnet obtained through the method has high residual magnetism and high coercive force at the same time, the diffusion efficiency of the diffusion source is high, and the rare earth utilization rate is increased.

The invention relates to the technical field of digital management, in particular to a digital management system for cold heading and heat treatment processing of fasteners, which comprises a phase deviation identification module, a load regulation and control parameter generation module, a heat treatment efficiency regulation and control module, a defect type association control module and an early warning instruction output module. According to the method, a load change node is positioned through a main shaft angle value, synchronous offset between a main shaft and a slave shaft is identified by combining multi-shaft displacement and load data, an angular displacement point in an impact rhythm, a corresponding speed and a holding time length set value are extracted, and targeted impact regulation and control parameters are formed; in the heat treatment stage, the fluctuation trend of heat conduction efficiency is recognized by combining the surface area and temperature rise data of the fastener, process response establishment of multiple types of defects is achieved by combining the crack size, the hardness value and the surface atlas label in the machining period, and shutdown and feeding interruption signals are issued to the control terminal according to the machining beat continuous triggering condition. Defect closed-loop linkage control in the fastener cold heading and heat treatment process is achieved.

The invention relates to the technical field of magnesium-aluminum alloy heat treatment, and discloses a high-strength and high-conductivity magnesium-aluminum alloy heat treatment method which comprises the following steps: step 1, surface cleaning treatment: carrying out surface cleaning treatment on a magnesium-aluminum alloy workpiece to remove oil stains, impurities and an oxide layer on the surface; secondly, preheating treatment is conducted, specifically, the cleaned magnesium-aluminum alloy workpiece is put into a heating furnace, the temperature is slowly increased to 200 DEG C at the temperature increasing speed of 10 DEG C / min, and heat preservation is conducted for 1-2 hours at the temperature; thirdly, the temperature is rapidly increased to the solid solution temperature, and after preheating treatment is completed. Precipitated phase distribution is optimized through two-stage aging treatment, a precipitated phase is preliminarily formed through low-temperature short-time aging, then the precipitated phase is uniformly grown through high-temperature long-time aging, local aggregation is avoided, meanwhile, solution treatment and quenching cooling are optimized, uniform dissolution of solute atoms is ensured, the alloy strength and hardness are improved, and the service life of the alloy is prolonged. And the fatigue resistance and the crack propagation resistance are remarkably improved through uniform precipitated phase distribution.

The invention relates to the field of control, in particular to a zone control method and system for a temperature field of a copper material heat treatment furnace. In the off-line stage, a strategy library containing various high-efficiency affine control laws is calculated in advance by solving a multi-parameter planning problem, the furnace temperature state space is divided into a plurality of explicit control subareas according to the coupling strength of all temperature areas in the furnace, and a set of alternative control laws are assigned for each subarea; during on-line operation, the partition to which the current furnace temperature belongs is determined according to the current furnace temperature, the partition with the minimum performance cost is quickly selected from the alternative control laws of the partition through short-time domain prediction to serve as the current optimal law, and when the predicted furnace temperature enters the boundary of the partition, the optimal control laws of the current partition and the adjacent partition are weighted and mixed; otherwise, directly adopting the current optimal law to generate a control instruction and applying the control instruction to the heater.

The invention relates to the field of pipeline welding. The invention discloses a pipeline welding robot, and aims to solve the problems that a small-diameter pipe, a large-diameter pipe and a conical pipe are not located on the same axis during splicing operation, so that deviation occurs in the welding process, and when a plurality of clamps are used for clamping a pipeline, when the pipeline is subjected to preheating treatment during welding, the pipeline cannot be damaged, and the welding efficiency is greatly improved. And the butt joint time is influenced when mutual rapid butt joint needs to be carried out, so that butt joint is carried out after pretreatment, and the welding part of the pipeline is influenced. The driving rod rotates to synchronously control the two expansion clamps to clamp a small-diameter pipe and a large-diameter pipe, it can be ensured that the axes of the two pipes are located on the same straight line and are consistent with the axis of the driving rod, and the problem of misalignment or eccentricity of the pipes is avoided.

The invention belongs to the technical field of seamless steel pipe manufacturing, and particularly relates to a preparation method of an ultra-large-specification 9Cr series ferrite heat-resistant seamless steel pipe and a product thereof. The preparation method of the ultra-large 9Cr series ferrite heat-resistant seamless steel pipe sequentially comprises the following working procedures of continuous casting, forging and pipe manufacturing. According to the continuous casting process, blast furnace molten iron and scrap steel serve as raw materials, and a continuous casting pipe blank is produced through an electric furnace, LF refining, VD vacuum treatment and round blank continuous casting machine pouring; the forging process comprises the steps of blanking, forging, annealing, perforating and the like to produce a pipe blank; the seamless steel pipe is produced through the procedures of heating, perforating, pipe rolling, pipe expanding, heat treatment, turning and the like in the pipe manufacturing procedure. And the prepared 9Cr series seamless steel tube is uniform in component and high in purity, so that the 9Cr series seamless steel tube has relatively high high-temperature strength, and the problems of unqualified flaw detection, non-uniform wall thickness, eccentricity and the like caused by alloy segregation in the prior art are solved.

A method to achieve a yield ratio of 0.60 or more in a component from non-heat-treated steel having bainitic microstructure. The component includes a predetermined chemical composition, in mass %, in amounts such that a value of F1 obtained by Formula (1) is 0.65% or more, with the balance as Fe and inevitable impurity. Bainitic microstructure area fraction is 85% or more and Retained austenite area fraction is 5% or less. Crystal grains of the bainitic microstructure have an average diameter of 10 μm or more and 25 μm or less, an average aspect ratio of 0.5 or more, and an average ratio of crystal grain boundary length to crystal grain circumference of 60 or less.F⁢1=C+Si / 24+Mn / 6+Ni / 40+Cr / 5+Mo / 4+V / 14(1)

The invention discloses an ultrahigh-strength collision energy absorption aluminum-magnesium-silicon-copper alloy profile and a preparation method thereof. The ultrahigh-strength collision energy absorption aluminum-magnesium-silicon-copper alloy profile is prepared from, by mass, 1.2%-1.4% of Si, smaller than or equal to 0.2% of Fe, 0.50%-0.80% of Cu, 0.50%-0.8% of Mn, 1.0%-1.3% of Mg, 0.15%-0.20% of Cr, smaller than or equal to 0.20% of Zn, 0.01%-0.05% of Ti, smaller than or equal to 0.20% of V, 0.10%-0.20% of Zr, smaller than or equal to 0.05% of other single impurities, smaller than or equal to 0.10% of total impurities and the balance Al. Through strict limitation of chemical components, impurity and gas contents and homogenization, extrusion and heat treatment systems, the aluminum alloy has excellent transverse and longitudinal collision energy absorption performance under the condition of sufficient strengthening, the yield strength of the aluminum alloy is larger than 360 MPa, the tensile strength is 390-430 MPa, the transverse bending angle is larger than or equal to 75 degrees, the longitudinal bending angle is larger than or equal to 65 degrees, and the tensile strength is larger than or equal to 390 MPa. After 60% of axial compression, no through crack larger than 10 mm occurs; and meanwhile, the dual requirements of light weight and safety of the automobile are met.

The invention relates to a high-strength complex-phase hot-rolled wire rod for a 2200MPa-grade stranded wire and a manufacturing method of the high-strength complex-phase hot-rolled wire rod, and the manufacturing method comprises the following steps: rolling and spinning to form a wire rod by adopting a high-hardenability component design, and then carrying out online molten salt mixed phase region quenching isothermal treatment, so that the wire rod is firstly subjected to front-section molten salt treatment and enters a bainite and pearlite phase region from an austenite state; the method comprises the following steps: carrying out high-temperature treatment on austenite to promote part of austenite to be converted into bainite and sorbite, carrying out later-section molten salt treatment, increasing the molten salt temperature, reducing the molten salt circulation amount, promoting unconverted retained austenite to be decomposed and converted into bainite and sorbite, carrying out isothermal tempering, and finally carrying out slow cooling through a roller way, the hot-rolled wire rod with a microscopic structure comprising a complex phase structure composed of tempered bainite and tempered sorbite is prepared, the material cost can be reduced, the complex phase structure and the structure toughness can be regulated and controlled on line, the tensile strength is 1505-1555 MPa, the percentage reduction of area is 32%-37%, efficiency and energy consumption are both considered, off-line heat treatment is avoided, and high-efficiency production of stranded wires is promoted.

The invention relates to a high-strength complex-phase hot-rolled wire rod for a 2360MPa-grade stranded wire and a manufacturing method of the high-strength complex-phase hot-rolled wire rod. After a Mo-V high-carbon component system is rolled and spun into a wire rod, the wire rod is subjected to on-line molten salt weak quenching toughening treatment, so that the wire rod is subjected to front-section molten salt treatment to be quickly cooled, enters a bainite and sorbite mixed phase region from an austenite state, and is subjected to high-temperature heat treatment to form a high-strength complex-phase hot-rolled wire rod; the method comprises the following steps: firstly, carrying out heat treatment on residual austenite to form a structure mainly comprising bainite and sorbite, then carrying out later-section molten salt treatment, increasing the temperature of molten salt, promoting decomposition and conversion of unconverted residual austenite into sorbite, carrying out isothermal tempering, and finally, carrying out roller way slow cooling to prepare a hot-rolled wire rod of which the microscopic structure comprises a complex-phase structure consisting of tempered bainite and tempered sorbite, the method has the advantages that the structure toughness can be regulated and controlled on line, the tensile strength is 1574-1627 MPa, the percentage reduction of area is 28-33%, the mechanical property fluctuation is reduced, the material cost and the production efficiency are both considered, the ultra-high-strength stranded wire can be produced without off-line heat treatment, and the wire breaking risk is reduced.

The present application relates to the field of metal material manufacturing, and in particular to a GH4151 alloy bar and a preparation method therefor and a use thereof. The method comprises the following steps: (1) carrying out homogenization heat treatment on a GH4151 alloy cast ingot to obtain a heat treated bar; (2) forging the heat treated bar to obtain a forged bar; (3) carrying out hot rolling treatment on the forged bar to obtain a hot rolled bar; (4) carrying out solution treatment on the hot rolled bar to obtain a solid solution bar; (5) carrying out cold drawing treatment on the solid solution bar to obtain a cold drawn bar; and (6) carrying out aging treatment on the cold drawn bar to obtain a GH4151 alloy bar. According to the GH4151 alloy bar prepared in the present application, grains can be effectively refined, the surface dimensional precision is improved, and the tensile strength of the prepared GH4151 alloy bar is improved, so that the GH4151 alloy bar has excellent mechanical properties.

The invention discloses an automatic feeding and discharging device of a continuous heating furnace, and relates to the technical field of industrial heat treatment equipment. An automatic feeding and discharging device of a continuous heating furnace comprises two first transmission rollers rotationally connected to a feeding port and a discharging port of a furnace body, and further comprises a conveying mesh belt connected to the two first transmission rollers in a sleeving mode; the first motor is fixedly connected to one side of the furnace body; through cooperative operation of the conveying net belt and the conveying belt with the jacking columns, dynamic adjustment of the jacking frequency and precise synchronous control are combined, the contact area of a workpiece and the conveying belt is effectively reduced, bottom thermal compensation is achieved through the heat conduction jacking columns, and meanwhile through integrated control of an automatic adjustment system and the waste heat recovery device, the waste heat recovery efficiency is improved. The problems that traditional equipment is uneven in heating, high in energy consumption and frequent in maintenance are solved, and the device has the advantages that the workpiece heating uniformity is improved, the service life of the device is prolonged, energy consumption is reduced, and intelligent dynamic regulation and control are achieved.

The invention belongs to the technical field of sodium-ion batteries, and particularly relates to a preparation method of a coal-based hard carbon material and application of the coal-based hard carbon material in a sodium-ion battery negative electrode. The preparation method of the hard carbon material comprises the following steps: carrying out acid-base chemical heat treatment on a coal-based material to obtain an ash-removed and dried precursor material, and activating the material by water vapor to obtain a target sample with etched micropore inner gaps, and in the subsequent carbonization process, the carbon layer is twisted to form a closed pore structure to obtain the electrode material. According to the invention, the application of the rich-resource coal precursor and the high carbon conversion rate in the sodium ion battery is realized, and the storage capacity of sodium and the cycling stability of the material are effectively improved. The coal-based hard carbon material can be used for preparing a sodium ion battery and has important application value.

The invention relates to an ultrahigh-strength low-temperature maritime work wide thin steel plate with good cold working performance and a manufacturing method of the ultrahigh-strength low-temperature maritime work wide thin steel plate. The steel plate comprises the following chemical components in percentage by weight: 0.04% to 0.08% of C, 0.1% to 0.4% of Si, 1.0% to 1.6% of Mn, 5.0% to 8.0% of Ni, 0.4% to 0.7% of Cr, 0.8% to 1.2% of Mo, 1.0% to 1.5% of Cu, 0.2% to 0.3% of V, 0.025% to 0.045% of Ti, 0.025% to 0.040% of Zr, 0.03% to 0.06% of Als, 0.002% to 0.005% of B, less than or equal to 0.005% of P, less than or equal to 0.001% of S and the balance of Fe and inevitable impurities. A low-carbon component design is adopted, elements such as V and Ti are added, and elements such as Ni, Cr, Mo, B and Zr are compositely added; a high-cleanliness smelting control technology, an electroslag remelting technology and a composite ply rolling technology are adopted, a two-stage rolling process, a transverse-longitudinal rolling process and a heat treatment process of quenching, two-phase region quenching and critical temperature tempering are matched, and the finally obtained wide and thin steel plate has excellent comprehensive mechanical properties.

The invention relates to the technical field of new energy, in particular to a nickel-free lithium-rich manganese-based positive electrode material and a preparation method thereof. The preparation method comprises the following steps: (1) preparing a precursor: mixing a lithium source, a sodium source and a manganese source according to a stoichiometric ratio of a chemical formula # imgabs0 #, grinding, and calcining in an oxidizing atmosphere to form a P3 type layered precursor; (2) ion exchange: mixing the P3 type layered precursor obtained in the step (1) with a lithium salt, and carrying out sodium-lithium ion exchange through a solid-phase reaction to form a sodium-deficient intermediate; and (3) annealing treatment: carrying out heat treatment on the material subjected to ion exchange to obtain the lithium-rich manganese-based positive electrode material with the O3 type layered structure. According to the invention, only substances composed of three elements of Li, Mn and O are used for synthesizing the positive electrode material, so that the use of materials containing cobalt and nickel is avoided.

The invention relates to a high-permeability ultralow-coercive-force soft magnetic stainless steel heat treatment process which comprises the following steps: in a nitrogen atmosphere, firstly heating a hot-rolled wire rod to 900-950 DEG C at a heating rate of 30-50 DEG C / h, preserving heat for 4-6 hours to obtain a fine grain structure of equiaxial recrystallization ferrite, then cooling to room temperature at a cooling rate of less than or equal to 15 DEG C / h to homogenize the ferrite structure, and finally cooling to room temperature at a cooling rate of less than or equal to 15 DEG C / h to obtain the high-permeability ultralow-coercive-force soft magnetic stainless steel. The soft magnetic stainless steel is obtained. The method has the advantages that the maximum magnetic conductivity of the soft magnetic stainless steel is improved, the coercive force of the soft magnetic stainless steel is reduced, and the plasticity index of the soft magnetic stainless steel is improved.

The invention discloses a production method of 900 MPa-grade high-strength sucker rod round steel based on rare earth microalloying, and belongs to the technical field of steel and iron material production. A proper amount of rare earth elements are added into the steel, and the purification, modification and alloying effects of the rare earth elements are utilized, so that the inclusion form and distribution of the steel are improved, grains are refined, and the strength, toughness and corrosion resistance of the steel are improved; meanwhile, by reasonably controlling production process parameters of smelting, continuous casting, rolling, heat treatment and the like, the structure uniformity and the mechanical property stability of the steel are ensured. Compared with a traditional production method, the 900 MPa-grade high-strength sucker rod round steel produced through the method has higher strength and better toughness and corrosion resistance, and the requirement of the oil exploitation industry for high-end sucker rod materials can be met.

The invention discloses a purification method for removing quartz inclusion, which comprises the following steps: calcining a quartz sand raw material at high temperature for a certain time, then taking out and quickly putting into cold water for cold quenching; dehydrating quartz sand, feeding into a microwave reactor, heating to a set temperature, and keeping for a period of time; after the reaction is finished, cleaning the quartz sand with ultrapure water; filling the quartz sand into a high-temperature and high-pressure reactor, introducing supercritical carbon dioxide and hydrogen fluoride mixed gas, and keeping the temperature and the pressure for a period of time; and after the reaction is finished, discharging gas to obtain the high-purity quartz. Through two-stage heat treatment, a channel between gas-liquid inclusions in quartz particles and the outside can be efficiently opened, and meanwhile, the supercritical method ensures that impurities in the inclusions can be effectively dissolved out; the treatment time is short, the required temperature is low, the acid consumption is less than 10%, and the method has the advantages of high efficiency and low cost.