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1082 results about "Micron scale" patented technology

Cleaning control method and system based on electronic cleaning agent

The invention discloses a cleaning control method and system based on an electronic cleaning agent, and the method comprises the steps: obtaining the distribution characteristics of pollutants and a material sensitivity judgment result through obtaining the micron-sized particle distribution data, chemical residue concentration data and surface roughness parameters of the pollutants on the surface of an electronic workpiece; according to the pollutant distribution characteristics and the material sensitivity judgment result, matching a candidate formula from a preset cleaning agent formula database, calculating pollutant removal rate predicted values of different concentration and time combinations through a linear regression algorithm, and determining optimized cleaning agent formula parameters and cleaning strength control parameters; and in the cleaning process, the residual quantity of pollutants and the surface damage degree are collected in real time, if the residual quantity of the pollutants exceeds a preset threshold value T1 or the surface damage degree exceeds a preset threshold value T2, cleaning agent injection pressure and cleaning time parameters are dynamically adjusted, and updated cleaning execution parameters are generated. Accurate and efficient cleaning of the surface of the electronic workpiece is achieved.
Owner:SHANLIXINYE NEW MATERIALS (GUANGDONG) CO LTD

Film coating processing technology simulation and optimization system based on digital twinning

The invention belongs to the technical field, and discloses a film coating processing technology simulation and optimization system based on digital twinning. The system is composed of a data acquisition module, a feature recognition and analysis module, a behavioral digital twinborn simulation module, a coating uniformity evaluation module, a process parameter optimization module and a coating distribution prediction module. The method comprises the following steps: acquiring a three-dimensional roughness digital model of a base material, accurately identifying a micron-sized local rough region and extracting geometrical characteristic parameters of the micron-sized local rough region; constructing a coating growth behavior digital twinborn model based on the geometrical characteristic parameters and the process parameters, and accurately simulating the coating growth process of the local rough area; and establishing a global coating uniformity quantitative evaluation system, and optimizing a process parameter combination by applying machine learning and a genetic algorithm. The system breaks through the limitation of traditional static shadow hypothesis, real-time tracking and accurate simulation of microstructure evolution in the deposition process are achieved, and the coating growth prediction accuracy is remarkably improved.
Owner:GUANGDONG INST OF SCI & TECH

Double-PHA (polyhydroxyalkanoate) barrier system for paper-based containers and paperboards and preparation method and application of double-PHA barrier system

The invention discloses a double-PHA barrier system for a paper-based container and a paperboard as well as a preparation method and application of the double-PHA barrier system, and belongs to the technical field of paper-based material surface engineering and green packaging. The system sequentially comprises a paper base material, a water-based PHA dispersion hole sealing layer and a PHA extrusion compact layer from inside to outside. According to the invention, the micron-sized PHA dispersoid without cell debris is utilized, so that an efficient hole sealing effect which is difficult to achieve by a high coating amount in a traditional process can be achieved by only needing an extremely low coating amount, and the pinhole defect of an extrusion layer is eliminated from the source. And in cooperation with the modified PHA extrusion layer with the specific crystallinity, the problem of micro-cracking of a single coating during edge rolling forming is cooperatively solved. According to the system, excellent barrier performance is achieved through a thinner bio-based structure, and meanwhile the system has a wide heat sealing window and excellent repulp recycling performance. Compared with the prior art, on the premise that high performance is guaranteed, the consumption amount of packaging materials and the environmental burden are remarkably reduced.
Owner:DU BAI CHENG NEW MATERIAL TECH (SHANGHAI) CO LTD +3

Multi-tooth micro-blade milling cutter and manufacturing method and application thereof

The invention relates to the technical field of milling cutters, in particular to a multi-tooth micro-blade milling cutter and a manufacturing method and application thereof. The multi-tooth micro-blade milling cutter comprises a cutter handle and a cutter head body, wherein the cutter head body is fixedly connected to one end of the cutter handle; the multiple cutter teeth are arranged on the outer side face of the cutter head body, and each cutter tooth extends to the tail end, close to the cutter handle, of the cutter head body from the top end, away from the cutter handle, of the cutter head body; each cutter tooth comprises a front cutter face, a rear cutter face and a cutting edge, the cutting edge is provided with a plurality of continuously-distributed micron-sized protruding micro-blades, the micro-blades form an arc-shaped sawtooth structure, the micro-blades extend to the front cutter faces and form micro grooves in the front cutter faces, the micro-blades extend to the front cutter faces and form micro grooves in the front cutter faces, and the micro-blades extend to the rear cutter faces and form micro grooves in the front cutter faces. The multi-tooth micro-blade milling cutter has the structure of the front angle of the front cutter face of the milling cutter tooth and the rear angle of the rear cutter face of the milling cutter tooth, the linear cutting blade of the traditional cutter tooth is dispersed into micro blades, the stress concentration of the cutter is reduced, a plurality of convex micro blades are in grinding motion on the machining face in the milling process, and the milling and grinding combined machining effect is formed. Unification of machining efficiency and machining precision is achieved.
Owner:GUANGDONG UNIV OF TECH

Micro-fluidic chip and micro-fluidic system

The utility model provides a micro-fluidic chip and a micro-fluidic system, a micron-sized main channel is arranged in the micro-fluidic chip, and a sample to be detected is introduced into a generation area of the main channel to form a large number of micro-droplets. The micro-droplets serve as a reaction container to react with tyrosine and tyrosinase which are guided into the reaction area of the main channel, and finally absorbance testing can be conducted on the micro-droplets in the detection area of the main channel. The micro-droplets are small in volume, have high surface area to volume ratio, and can form a reaction container for efficient reaction. The microfluidic system can rapidly and accurately measure to-be-detected samples with different concentrations, and has the advantages of low reagent consumption, energy conservation, environmental protection, small required detection space, large-scale parallel operation and the like.
Owner:SHENZHEN 863 NEW MATERIAL & TECH CO LTD

Composite regulation and control method for improving performance of laser additive manufacturing high-strength aluminum alloy

The invention discloses a composite regulation and control method for improving the performance of a laser additive manufacturing high-strength aluminum alloy, and relates to the technical field of laser additive manufacturing high-strength aluminum alloy materials, micron-sized ceramic particles and micron-sized AlMgScZr alloy powder are mixed, and ceramic particle reinforced aluminum-based composite powder is prepared. According to the composite material powder, the solidification structure is regulated and controlled through the characteristics of ceramic particles, stress concentration is reduced, and meanwhile the reinforcing phase particle aggregation phenomenon is avoided. The obtained composite material is excellent in quality and few in metallurgical defects in laser forming, and the density reaches up to 99.8% or above. By combining the optimized selective laser melting and heat treatment process, the room-temperature mechanical property of the prepared composite material part is remarkably improved, the tensile strength exceeds 540 MPa, the yield strength exceeds 490 MPa, and the elongation at break exceeds 10%.
Owner:BEIJING UNIV OF TECH +1

High-strength and high-conductivity copper alloy with fine grain structure and preparation method of high-strength and high-conductivity copper alloy

The invention provides a high-strength and high-conductivity copper alloy with a fine grain structure and a preparation method of the high-strength and high-conductivity copper alloy, and belongs to the technical field of copper alloy preparation. The copper alloy comprises the following elements in percentage by mass: 2.0-12.0 wt.% of Ni, 0.4-3.0 wt.% of Si, less than or equal to 1.0 wt.% of Zn, less than or equal to 5.0 wt.% of Ti, less than or equal to 1.0 wt.% of B and the balance of Cu and inevitable impurities. According to the method, the heat treatment process is adjusted, generation of Ni16Ti6Si7 and TiB2 phases is promoted through introduction of Ti and B elements, micron-sized particles can serve as nucleation sites and pinning grain boundaries in the heat deformation process, and grain refinement is promoted. The high-strength and high-conductivity copper alloy with a fine grain structure is obtained by changing the content of Ti and B elements in the copper alloy and regulating and controlling the proportion of Ni16Ti6Si7, a TiB2 micron phase and a Ni2Si nano phase.
Owner:NORTH CHINA ELECTRIC POWER UNIV +1

Manufacturing method of glass through hole

The embodiment of the invention provides a manufacturing method of a glass through hole, which is used for solving the technical problem that a glass through hole with an ultrahigh depth-diameter ratio cannot be manufactured according to a pre-designed scheme in an existing manufacturing method of the glass through hole. According to the manufacturing method of the glass through hole, before laser-induced modification, exposed prefabricated through hole graphical areas are formed on the front face and the back face of a glass substrate through the micron-order photoresist mask technology, and meanwhile a photoresist layer with the thickness not smaller than 5 micrometers is formed on the surface, outside the prefabricated through hole graphical areas, of the glass substrate. In the laser-induced modification stage, laser with higher irradiation power can be used for deeply modifying the glass material in the prefabricated through hole patterned area to form a prefabricated through hole modified area. In the chemical etching stage, the surface of the glass substrate outside the prefabricated through hole modified area is covered with the anti-corrosion photoresist layer, and etching liquid only acts on the prefabricated through hole modified area, so that the phenomenon that the thickness of the glass substrate is reduced in the etching process is effectively prevented.
Owner:CHENGDU MAIKE TECH CO LTD

High-stability porous hydroxyapatite microspheres as well as preparation method and application thereof

The invention relates to the technical field of biomedical materials, and discloses a high-stability porous hydroxyapatite microsphere as well as a preparation method and application thereof, and the porous hydroxyapatite microsphere is formed by self-assembling nano-scale hydroxyapatite particles under the driving of a thermodynamic behavior of reducing excess surface free energy; the porous hydroxyapatite microspheres are nano-scale to micron-scale microspheres with rough surfaces; the porous hydroxyapatite microspheres have a nano-scale pore channel structure; the mineralization is improved under the assistance of the porous hydroxyapatite microspheres; the defects that hydroxyapatite microspheres in the prior art are sharp in microstructure, poor in histocompatibility, free of a porous structure and the like are overcome, the preparation method is simple, the safety coefficient of the production process is high, the obtained porous microspheres are stable in structure, various parameters can be adjusted according to requirements, and the method is suitable for industrial large-scale production.
Owner:SHANGHAI MOYANG BIOTECHNOLOGY CO LTD

High-temperature-resistant, bending-resistant and high-flexibility polyimide film for flexible display and preparation method of high-temperature-resistant, bending-resistant and high-flexibility polyimide film

The invention discloses a high-temperature-resistant, bending-resistant and high-flexibility polyimide film for flexible display and a preparation method of the high-temperature-resistant, bending-resistant and high-flexibility polyimide film. According to the polyimide film, by introducing the nano silicon dioxide particles and constructing the porous structure design, the problems that a traditional polyimide film is insufficient in stability in a high-temperature environment, cracks are likely to be generated after bending, and the flexibility is poor are effectively solved. The polyimide film disclosed by the invention is prepared by adopting a diamine monomer and a dianhydride monomer as main raw materials, adding nano silicon dioxide particles, and carrying out solution polymerization, gelation, pore regulation and control and thermal imidization processes. The obtained polyimide film has a micron-sized porous structure, keeps stable at a high temperature of 400 DEG C, does not generate cracks after being bent for 100,000 times, has tensile strength of more than or equal to 150MPa, elongation at break of more than or equal to 25% and light transmittance of more than or equal to 85%, and is suitable for a substrate material of a flexible display device.
Owner:SAINT MAINT NEW MATERIALS TECHNOLOGY (SHENZHEN) CO LTD +2

Sample preparation and characterization method for angle-rotating crystal interface

The invention discloses a sample preparation and characterization method of a rotation angle crystal interface, which is suitable for a sample with dislocation at the interface of two crystals, and comprises the steps of sample preparation and measurement of the relative rotation angle theta of the two crystals. A certain angle is formed between the cutting direction and the interface for sample preparation, a slice is taken out, and the obtained slice has three thin areas including a top material A crystal, a top material A / bottom material B crystal mixing area and a bottom material B crystal; measurement of the rotation angle theta: the electron beam direction is parallel to the rotation axis of the top sample during testing, and the rotation angle theta is directly measured by analyzing crystallographic information of the three thin areas. According to the method, the rotation angle of the top crystal relative to the bottom crystal can be accurately measured through TEM analysis of the three thin regions, and the error-tolerant rate of TEM sample preparation and analysis experiments is improved. In addition, the sample preparation technology can be used for monitoring the change of the physical properties of the sample in mechanics, thermotics, optics, electricity and the like along with the reduction of the size of the sample from the micron level to the nano level.
Owner:HUBEI JIUFENGSHAN LAB

Micron-sized speckle preparation method for quasi-in-situ OIM-DIC mesoscopic strain field analysis

A micron-sized speckle preparation method for quasi-in-situ OIM-DIC mesoscopic strain field analysis comprises the following steps: (1) polishing the surface of a sample to be detected to obtain a bright and scratch-free mirror surface; (2) preparing Si powder turbid liquid; (3) dipping speckles of a sample to be detected in the Si powder turbid liquid to obtain micron-sized speckles; and (4) observing and shooting speckle morphology, and if Si particles are uniformly distributed and dispersed, applying the Si particles to quasi-in-situ OIM-DIC mesoscopic strain field analysis. The method is simple, convenient and rapid, low in operation and construction cost, high in practicability, good in particle dispersity, high in precision, more suitable for calculation of a quasi-in-situ OIM-DIC mesoscopic strain field, controllable in preparation process, low in cost and free of damage to the surface of a sample, the definition and stability of speckle characteristics are remarkably improved, DIC mesoscopic micron-scale operation under a quasi-in-situ OIM mechanical test can be effectively achieved, and the method is suitable for large-scale industrial production. And the grain and mesoscopic strain field information is successfully coupled.
Owner:SHANDONG UNIV

Microcrystal texture glass cover plate and preparation method thereof

The invention discloses a microcrystalline texture glass cover plate and a preparation method thereof. The microcrystalline texture glass cover plate comprises a glass body; a series of surface microstructures are arranged on the surface of the glass body, the section of each surface microstructure is in a wave shape, compared with a common glass cover plate, the glass cover plate is endowed with more excellent optical and mechanical performance due to the special structure of the microcrystalline glass, and the requirements of high-end markets are better met when the glass cover plate is applied to consumer electronics cover plates. The diversification of the MASK design provides diversification of the texture effect of the microcrystalline glass, and specific requirements are met. And the surface of the microcrystalline glass is processed more accurately by the yellow light development technology and reaches the micron level. Pyramid morphology of particles on the surface of the microcrystalline glass is regulated and controlled through a wet etching process, uniform etching is carried out, the texture effect is brighter, and the hand feeling is finer and smoother.
Owner:WUHU TOKEN SCI

Photoelectric wafer defect detection method

The invention discloses a photoelectric wafer defect detection method, and belongs to the technical field of semiconductors. The detection method comprises the steps that the surface of a photoelectric wafer is covered with a quantum dot precursor solution, annealing is carried out, after a quantum dot film is formed, irradiation is carried out under ultraviolet light, a displayed fluorescence signal can mark defects on the surface of the photoelectric wafer, and the purpose of detecting the defects of the photoelectric wafer is achieved. The quantum dots used in the invention have excellent fluorescence efficiency and stability, and can provide a high-contrast marking effect in an SEM image. Therefore, the detection of micron-scale and nano-scale defects is more accurate, and the details are clearer. A traditional fluorescence labeling solution is limited in infiltration capacity in nanoscale defects and can only cover the surface. The quantum dots can penetrate into the defect to form a mark with the depth ratio as high as 1: 3. The depth marking capability is helpful for comprehensively knowing the internal structure of the defect and the defect extension condition. In addition, the quantum dots have excellent adaptability and multifunctionality, and show good stability and coupling effect under different types of wafer conditions.
Owner:BEIJING INST OF TECH

Optical microscopy method, system and device for positioning magnetic nanoparticles

The invention discloses an optical microscopy method, system and device for positioning magnetic nanoparticles, and the method comprises the steps: obtaining an interference pattern generated when laser passes through a to-be-detected sample, and distributing the magnetic nanoparticles in the to-be-detected sample; the interference pattern is formed by interference of incident laser and scattered light of the magnetic nanoparticles; determining a distribution function of the interference pattern, and determining the central position of the magnetic nanoparticle according to the interference pattern and the distribution function; the device comprises a laser, an amplification objective lens, a focusing lens, an imaging unit and a processor, light emitted by the laser passes through a to-be-detected sample to generate an interference pattern, the interference pattern is amplified by the amplification objective lens and focused by the focusing lens to be imaged in the imaging unit, and magnetic nanoparticles are distributed in the to-be-detected sample. According to the embodiment of the invention, micron-sized space positioning of the magnetic nanoparticles can be realized, and the method can be widely applied to the technical field of optical positioning.
Owner:HUAZHONG UNIV OF SCI & TECH +1

Indented pattern color scraping decorative film and preparation method thereof

The invention relates to the field of decorative films, in particular to an indented pattern color scraping decorative film and a preparation method thereof.The indented pattern color scraping decorative film comprises a skin feeling functional layer, a pattern developing layer, a supporting strengthening layer and a coloring strengthening layer, the skin feeling functional layer, the pattern developing layer and the supporting strengthening layer are composited into an integrated structure through hot pressing, and micron-sized air guide grooves are formed in the bonding faces of all the layers; the air guide grooves are arranged in parallel along the extending direction of the dimpled grains, the 60-degree glossiness of the surface of the decorative film is less than 3GU, the pencil hardness is greater than 1H, and the texture spacing difference between the outline edge of the dimpled grains and the printed pattern layer is 0.1-0.5 mm, so that the decorative film is endowed with excellent stereoscopic visual effect and physical property. The dimpled grain structure in the skin-touch functional layer is directly formed on the surface of the skin-touch coating, the problem of interlayer dislocation caused by traditional composite embossing is avoided, it is ensured that the dimpled grain outline is clear, the peeling strength between layers is high, bonding is tighter, and no bubble is left on the bonding face between the layers.
Owner:广东瀚泰装饰材料有限公司

Foot-wheel matching type multi-degree-of-freedom piezoelectric robot with foot and leg integrated design and excitation method thereof

The invention discloses a foot and leg integrated design foot and wheel matched type multi-degree-of-freedom piezoelectric robot and an excitation method thereof, and belongs to the field of centimeter-level small robots. According to the robot, piezoelectric ceramics are pasted on an integrated base body, and the piezoelectric ceramics are divided into two pieces of Y-direction piezoelectric ceramics and two pieces of Z-direction piezoelectric ceramics; when two paths of sine excitation signals with the phase difference of 90 degrees are applied to the Y-direction piezoelectric ceramic and the Z-direction piezoelectric ceramic respectively, the base body beam bends and vibrates in the horizontal (Y-direction) direction and the vertical (Z-direction) direction, the foot bottom end is driven to synthesize an elliptic track in the YOZ plane, and rotation motion is achieved through friction between the foot end and the ground. Similarly, an elliptical track can be synthesized in an XOZ plane under excitation of different signals, and linear motion is achieved through friction between the foot end and the ground; when a pulse signal is applied to the piezoelectric ceramic, the robot moves at a micron-order micro step pitch. The robot has the advantages of being simple in structure, high in response speed, capable of giving consideration to fast macro motion and precise micro motion and the like, and faces scenes such as large-range precise detection.
Owner:HARBIN INST OF TECH

Method for ultrasonic-assisted laser additive manufacturing of multi-scale structure coupling high-toughness aluminum alloy and application

The invention discloses a method and application for ultrasonic-assisted laser additive manufacturing of a multi-scale structure coupling high-toughness aluminum alloy, and the method comprises the steps that high-Ni-content alloy steel powder is refined through high-energy ball milling, and then the refined alloy steel powder is dispersed and distributed in Al-Mg-Sc-Er-Zr alloy powder; an ultrasonic energy field is introduced to assist selective laser melting to form mixed powder, the ultrasonic energy field assists in generating nonlinear effects such as cavitation, acoustic streaming and heat effect, defects such as air holes and cracks are overcome to eliminate residual stress, and the Marlangoni effect is accelerated to increase the solidification speed; and finally, the high-strength and high-toughness aluminum alloy which has high density and is composed of micron-scale, submicron-scale and nano-scale multi-scale phase structures is prepared. The production cost is low, and the room-temperature tensile properties of the prepared high-strength and high-toughness aluminum alloy are as follows: the strength is greater than 850 MPa, and the fracture strain is greater than 6%.
Owner:GUANGDONG POLYTECHNIC NORMAL UNIV +1

Two-phase cold plate with three-stage porous heat dissipation and processing method thereof

The invention relates to the technical field of heat dissipation of semiconductor devices, in particular to a two-phase cold plate with three-stage porous heat dissipation and a processing method of the two-phase cold plate. The invention discloses a two-phase cold plate with three-stage porous heat dissipation, which comprises a substrate, and a micro-channel is arranged in the substrate. On one hand, flow distribution is regulated and controlled based on the micro-channel of topological optimization, and on the other hand, the surface liquid storage capacity during two-phase boiling is improved and the separation diameter of bubbles is regulated and controlled by machining the micron-sized blind holes in the inner bottom of the micro-channel; on the other hand, nanoscale blind holes are formed in the inner bottom and the inner wall of the micro-channel and in the micron-sized blind holes to improve the gasification core density and strengthen the liquid wicking performance; and the three are combined to form three-stage heat dissipation, so that the heat dissipation performance of the cold plate can be remarkably improved. The problems that an existing conventional two-phase cold plate is unreasonable in design, physical damage is prone to occurring, and the heat dissipation performance of the two-phase cold plate is affected are solved.
Owner:NANJING UNIV OF SCI & TECH

High-precision manufacturing process and quality control method of aluminum alloy guide rail for rail transit

The invention relates to the technical field of aluminum alloy guide rail machining processes, in particular to a high-precision manufacturing process of an aluminum alloy guide rail for rail transit, and the high-precision manufacturing process of the aluminum alloy guide rail specifically comprises the following steps: step 1, designing and smelting an alloy material, and utilizing component optimization to design an alloy formula to inhibit grain coarsening; impurity control: Fe < = 0.25%, and Mn < = 0.15%; the tensile strength is greater than or equal to 275MPa, and the ductility is greater than or equal to 12%, which is superior to that of similar products (conventionally less than or equal to 10%); micron-order precision control: the cross section dimensional tolerance is less than or equal to + / -0.15 mm (improved by 50% compared with the traditional process); 12 key parameters from smelting to finished products are monitored in real time, and the yield is increased to 99.8% from 92%.
Owner:ZHEJIANG LEXIANG ALUMINUM

Method for improving medium-temperature strength of additive manufacturing Al-Si alloy

The invention discloses a method for improving the medium-temperature strength of an additive manufacturing Al-Si alloy, and belongs to the field of metal materials. According to the method, the Al-Si alloy serves as a base body, micron-sized AlB2 and Ti powder are added, laser irradiation energy in the additive manufacturing process is used for enabling the micron-sized AlB2 and Ti powder to react, and nanoscale TiB2 and D022-Al3Ti strengthening phases are synthesized in situ so that the medium-temperature strength of the material can be improved. By optimizing the content of the components, the adding proportion of the AlB2 powder and the adding proportion of the Ti powder are controlled to be 1.20-1.60 wt.% and 1.80-2.40 wt.% respectively, and the mass ratio of the AlB2 powder to the Ti powder is 2: 3. Through the synergistic effect of the two nanoscale second phases, the alloy can have high strength in a medium-temperature environment without post-heat treatment, and meanwhile, the high percentage elongation after fracture is kept. The yield strength of the alloy in the environment of 300 DEG C reaches 190 MPa, the tensile strength reaches 200 MPa, the ductility reaches 10%, and the strength upper limit of the selective laser melting near-eutectic Al-Si alloy in the working environment of 300 DEG C is broken through. The mechanical property of the aluminum alloy is comparable with that of Al-Ni, Al-Ce and other heat-resistant aluminum alloys prepared through selective laser melting, and the aluminum alloy is lower in cost and lighter in density.
Owner:UNIV OF SCI & TECH BEIJING

Double-layer stacking hole type SiO2-coated SiO2 core-shell microsphere as well as preparation method and application of double-layer stacking hole type SiO2-coated SiO2 core-shell microsphere

The invention belongs to the technical field of chromatographic packing, and particularly relates to a double-layer stacking hole type SiO2-coated SiO2 core-shell microsphere as well as a preparation method and application thereof. The core-shell microsphere takes micron-sized non-porous SiO2 as a core and takes a SiO2 nanoparticle stacking layer as a porous shell layer, the porous shell layer sequentially comprises a first SiO2 mesoporous shell layer and a second SiO2 mesoporous shell layer from inside to outside, SiO2 nanoparticles in the first SiO2 mesoporous shell layer are stacked to form a first gap pore channel, and SiO2 nanoparticles in the second SiO2 mesoporous shell layer are stacked to form a second gap pore channel. According to the invention, a porous shell structure with dual or multiple pore size distribution is constructed on the surface of a SiO2 core, and by integrating more than two pore sizes with obvious size difference, exclusive mass transfer paths are provided for solute molecules with different sizes, exclusive mass transfer channels can be provided for small-molecular compounds and macromolecular substances at the same time, and the pore size difference is greatly reduced. Therefore, the selectivity and column efficiency of chromatographic separation are remarkably improved.
Owner:NORTHWEST UNIV

Method for refining grains on surface of tungsten material based on friction induction and application

The invention relates to the technical field of tungsten metal surface refinement, in particular to a method for refining grains on the surface of a tungsten material based on friction induction and application, and the method achieves grain refinement on the surface of refractory metal through the shear friction force and the thermal-mechanical coupling effect. Firstly, a tungsten material sample is in contact with a friction pair of a friction instrument, then a certain pressure is applied to the surface of the tungsten material through the friction pair, the material is heated to a preset temperature through a temperature control module, then rotary friction is conducted at a certain rotating speed, and after a period of time, a nanoscale gradient structure layer can be formed on the surface of the sample. By means of the method, the grain size can be refined to the nanometer level from the initial micrometer level, and the surface hardness of the material is greatly improved. The method is simple in process, low in cost and obvious in grain refinement effect, and has important engineering application value.
Owner:HEFEI INSTITUTE OF PHYSICAL SCIENCE CHINESE ACADEMY OF SCIENCES

Nano-silver-loaded porous cyclodextrin microspheres as well as preparation method and application thereof

The invention discloses porous cyclodextrin microspheres loaded with nano-silver as well as a preparation method and application of the porous cyclodextrin microspheres. The porous cyclodextrin microspheres are obtained by loading nano-silver on oligomeric cyclodextrin with the molecular weight of 8000-14000, then blending the oligomeric cyclodextrin with poly (methyl vinyl ether-alt-maleic acid) to obtain microspheres and then cross-linking the microspheres. The porous cyclodextrin microspheres are selected as the carrier of AgNP, and cyclodextrin has a hydrophobic cavity, so that specific hydrophobic molecules and pollutants can be included in the cavity, and contact and catalysis processes of reactants and silver particles are promoted synergistically. Moreover, the cyclodextrin microspheres have micron-scale and even millimeter-scale porous structures, the abundant porous structures can ensure that reactants quickly enter the microspheres to be in full contact with silver, the catalytic reaction is efficiently carried out, and meanwhile, the larger size of the microspheres ensures that fluid can pass through the microspheres at a high speed in a fixed bed reactor, so that the catalytic efficiency is improved. And the contradiction between the catalyst efficiency and the large particle size in practical application is solved.
Owner:SICHUAN UNIV

Laser processing method of ceramic substrate

The invention relates to the technical field of laser processing, and discloses a laser processing method of a ceramic substrate, which adopts an ultrashort pulse laser and nanosecond laser dual-laser system process, integrates the advantages of precise surface modification of ultrashort pulse laser and efficient processing of nanosecond laser, and forms a micron-sized porous sacrificial layer on the surface of a ceramic material. Micropores and microcracks on the micron-sized porous sacrificial layer destroy the continuous heat conduction path of the original compact ceramic, and heat is gathered on the micron-sized porous sacrificial layer formed on the surface, so that when subsequent nanosecond laser acts, compared with the original smooth ceramic substrate, the generated cracks are easy to block, two-dimensional cracks are not easy to generate on the surface of the ceramic substrate, and the surface of the ceramic substrate is not easy to crack. And low-power and high-efficiency processing can be carried out on the ceramic material without coating an auxiliary material, and high-absorption and low-heat-influence processing is realized.
Owner:杭州银湖激光科技有限公司

Tilt angle sensor and preparation method and application thereof

The invention belongs to the technical field of angle sensors, and particularly relates to a tilt angle sensor and a preparation method and application thereof. The tilt angle sensor provided by the invention comprises a base body and a micro-channel communicated with any two points in the base body, the micro-channel is filled with gallium-based alloy liquid, the surface of the micro-channel contains a plurality of bulges, and the average height of the bulges is 50-200 microns; the two ends of the micro-channel are sealed by conductive adhesive; the conductive adhesive is connected with the electrode; the matrix is prepared from polydimethylsiloxane. The micro-channel containing the micron-sized bulge structure is arranged in the base body, so that local capillary force gradient can be generated, and the body response speed of the gallium-based alloy liquid is accelerated; and meanwhile, the special structure of the micro-channel has directional textures, so that asymmetric flow resistance and multi-path conductive paths can be generated, and differential resistance changes are generated during inclination to realize multi-directional inclination angle detection. The detection sensitivity and the anti-noise capability of the tilt angle sensor are remarkably improved by inducing a nonlinear flow control effect through the bulges in the micro-channel.
Owner:BEIJING FORESTRY UNIVERSITY

Micron-sized Cu powder and preparation method thereof

The invention discloses micron-sized Cu powder and a preparation method thereof.The method comprises the steps that raw materials are placed in a heating chamber, the heating chamber is vacuumized so that the vacuum degree can reach 80-150 KPa, and inert gas is introduced; the raw materials are subjected to heating treatment, the heating treatment temperature ranges from 1300 DEG C to 1700 DEG C, and the heat preservation time ranges from 10 min to 20 min; and cooling treatment is conducted on the Cu steam, the cooling treatment comprises the steps that the Cu steam and inert gas are mixed and then supplied into a closed space with a condenser, the flowing speed of the Cu steam and the inert gas supplied into the closed space is not lower than 500 ml / s, and the temperature difference of a cooling medium in the condenser before and after cooling treatment is not larger than 30 DEG C. According to the method, the micron-sized Cu powder which is uniform in size distribution and good in roundness can be obtained through simple operation.
Owner:HANGZHOU XINCHUAN ELECTRONIC MATERIALS CO LTD

Dry pattern transfer method for AMB copper-clad ceramic substrate

The invention discloses a dry pattern transfer method for an AMB copper-clad ceramic substrate in the technical field of ceramic substrate sintering, and the method comprises the following steps: S1, manufacturing a positioning hole, and forming a process reference; s2, prefabricating a circuit pattern through a stamping process; s3, brazing material layers are printed on the two faces of the ceramic substrate; S4, the copper layer pattern and the ceramic substrate are assembled in an aligned mode; s5, carrying out high-temperature sintering on the copper layer and the ceramic substrate, and carrying out metallurgical bonding; and S6, the sintered substrate is subjected to cleaning, surface treatment and laser precision cutting. According to the method, laser positioning and micron-sized reaming are adopted, an accurate alignment reference is established, mechanical assembly errors are fundamentally eliminated, a copper circuit directly forms a preset pattern on a substrate through cooperation of a copper block pre-forming structure and an accurate brazing process, the lateral corrosion problem of a traditional etching process is avoided, and the production efficiency is improved. The size error of the product graph is reduced, and the product graph accuracy and the machine graph size consistency are improved.
Owner:JIANGSU TOBO OPTOELECTRONICS TECH CO LTD

Waterproof printing process for paper printed matter

The invention relates to the technical field of paper printing, in particular to a waterproof printing process of a paper printed matter. The method overcomes the problems of poor waterproof effect and poor adhesive force of printed matters caused by imperfect traditional printing processes. According to the method, the printed matter is obtained by pretreating the base material, coating the bottom layer, coating the surface layer and calendering the mirror surface roller; parameters of corona treatment and micron-sized embossing treatment in pretreatment are changed; acrylic resin is modified and then mixed with nano silicon dioxide, and bottom layer coating liquid is prepared; a transition layer is arranged between the bottom layer coating and the surface layer coating; specially-treated hydrophobic nano-alumina is introduced into a surface coating liquid and has a synergistic effect with modified polyurethane, so that the waterproof effect and adhesive force of the printed matter are improved.
Owner:HUBEI GUANGCAI PRINTING CO LTD

Joint analysis method for organic matter types and micropore development characteristics in rock

The invention relates to the technical field of energy exploration analysis, in particular to a conjoint analysis method for organic matter types and micropore development characteristics in rocks, which comprises the following steps: step 1, drying a blocky or granular rock sample, and performing cold inlaying by using epoxy resin mixed with conductive powder to prepare a cylindrical sample; 2, after the cylindrical sample is demolded, first-time mechanical polishing is carried out; 3, marking the surface of the sample by using an etching objective lens when the sample is observed by a microscope; 4, performing secondary mechanical polishing and argon ion polishing on the sample obtained in the step 3; and 5, carrying out rapid positioning observation by using the scanning electron microscope navigation photo and the marked sample photo. The mark etching method is applied to organic matter microscopic observation marking, after the secondary treatment process is completed, various scanning electron microscope analysis can be carried out on the sample, and multi-scale and multi-characteristic analysis technology combination from the micron level to the nanometer level is achieved.
Owner:NAT RESERACH CENT OF GEOANALYSIS