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2051 results about "Micron scale" patented technology

A preparation method of high-performance sintered NdFeB with low dysprosium content

The invention discloses a method for preparing sintered NdFeB with low dysprosium (Dy) content and high performance; the method comprises the following steps of: sputtering and plating the Dy element on the surface of jet mill powder by using the powder plate technology based on magnetron sputtering on the basis of preparing NdFeB powder, and then sufficiently dispersing the Dy element to micron-sized NdFeB crystal particles by dispersing the Dy element at high temperature in the sintering and tempering process, thereby achieving the effect of improving magnetic performance of the sintered NdFeB. Compared with the introduction of the Dy element in the proportioning process of the prior art, the method disclosed by the invention has the advantages: the low dysprosium content and high performance is limited in the nano-size by adopting the physical gas-phase deposition, the consumption quantity of the Dy element during the production process is controlled effectively and the preparationof sintered NdFeB with low dysprosium content and high performance is realized. Compared with the sintered NdFeB of the same components prepared by the traditional casting and powder metallurgy process, both the intrinsic coercivity and the maximum magnetic energy product of the sintered NdFeB rare-earth permanent magnetic material obtained according to the invention are improved obviously; compared with the sintered NdFeB with the same performance prepared by the traditional casting and powder metallurgy process, the dosage of the dysprosium element is reduced remarkably. The method can be widely applicable to producing and manufacturing sintered NdFeB with high performance.
Owner:NANJING UNIV OF SCI & TECH +1

Emulsion deep profile/displacement control agent and preparation method of emulsion deep profile/displacement control agent containing gel microspheres of core shell structure

The invention relates to a preparation method of an emulsion deep profile/displacement control agent containing gel microspheres of a core shell structure. According to the method, materials are fed many times to carryout inverse emulsion low-temperature oxidation and reduction to initiate free radical polymerization so that water-solubility monomers (including acrylamide, ionic monomer I, the ionic monomer II and the third monomer) react with a cross-linking agent to generate the emulsion deep profile/displacement control agent containing gel microspheres of a core shell structure. The invention also relates to the emulsion deep profile/displacement control agent containing gel microspheres of a core shell structure, which is prepared by using the method. The profile/displacement control agent is a water-solubility microgel oil displacement material containing gel microspheres from nano scale to micron scale; with small initial grain size, the profile/displacement control agent can enter into the deep part of stratum; in addition, the profile/displacement control agent has high emulsion active component content and good flowability, can have volume expansion and mutual cementation under the actions of formation water and temperature according to the condition whether charges carried by the ionic monomers at a core layer and a shell layer are same or not; therefore the profile/displacement control requirements of different geological oil deposits of oil fields can be met.
Owner:TECHNICAL INST OF PHYSICS & CHEMISTRY - CHINESE ACAD OF SCI

Silicon MEMS based two-phase heat transfer device

The present invention is a MEMS-based two-phase LHP (loop heat pipe) and CPL (capillary pumped loop) using semiconductor grade silicon and microlithographic/anisotrophic etching techniques to achieve a planar configuration. The principal working material is silicon (and compatible borosilicate glass where necessary), particularly compatible with the cooling needs for electronic and computer chips and package cooling. The microloop heat pipes (μLHP™) utilize cutting edge microfabrication techniques. The device has no pump or moving parts, and is capable of moving heat at high power densities, using revolutionary coherent porous silicon (CPS) wicks. The CPS wicks minimize packaging thermal mismatch stress and improves strength-to-weight ratio. Also burst-through pressures can be controlled as the diameter of the coherent pores can be controlled on a sub-micron scale. The two phase planar operation provides extremely low specific thermal resistance (20-60W/cm2). The operation is dependent upon a unique micropatterened CPS wick which contains up to millions per square centimeter of stacked uniform micro-through-capillaries in semiconductor-grade silicon, which serve as the capillary “engine,” as opposed to the stochastic distribution of pores in the typical heat pipe wick. As with all heat pipes, cooling occurs by virtue of the extraction of heat by the latent heat of phase change of the operating fluid into vapor. In the cooling of a laptop computer processor the device could be attached to the processor during laptop assembly. Consistent with efforts to miniaturize electronics components, the current invention can be directly integrated with a unpackaged chip. For applications requiring larger cooling surface areas, the planar evaporators can be spread out in a matrix and integrally connected through properly sized manifold systems.
Owner:UNIVERSITY OF CINCINNATI

Preparation method of pre-dispersed carbon nano-tube rubber masterbatches

The invention belongs to the field of materials and specifically relates to a preparation method of pre-dispersed carbon nano-tube rubber masterbatches. The method is characterized in that the rubber masterbatches comprise the following ingredients, by weight, 5-100 parts of carbon nano-tube, 5-100 parts of rubber, 5-100 parts of wax, 0.5-50 parts of a dispersing aid, 0.5-5 parts of an anti-aging agent and 0.1-10 parts of an activator. The preparation method of the rubber masterbatches comprises the following specific steps: carrying out high-speed shearing on the above ingredients, mixing, carrying out in situ activated modification on carbon nano-tube such that carbon nano-tube is uniformly dispersed and has no micron-scale aggregate, and pelleting so as to obtain the pre-dispersed high-concentration carbon nano-tube rubber masterbatches. By the use of the pre-dispersed carbon nano-tube rubber masterbatches prepared by the above formula and method, tear strength of tire tread rubber can be raised by about 5-10% and even more, wear volume of Akron is reduced by about 30% and even more, volume resistivity is minimized by two orders of magnitudes, and mechanical properties such as tensile strength, elongation at break and the like are basically unchanged or increased a little.
Owner:SHANDONG DAZHAN NANO MATERIALS

Soft chemical preparation method for hollow glass micro-balloon, prepared hollow glass micro-balloon and application thereof

The invention belongs to the technical field of a soft chemical method. According to the invention, the method is used for overcoming the defects that the traditional solid-phase glass powder method for preparing a hollow glass micro-balloon is high in energy consumption, long in technical process and difficult in controlling grain size distribution and the hollow glass micro-balloon prepared according to a liquid-phase atomizing method is high in alkalinity, easy to absorb water, high in strength and easy to break, and the like. A liquid material system is compounded through a chemical reaction; after the system is homogenized, the system is quickly atomized, dewatered and dried, thereby obtaining approximate spherical precursor powder with required grain size and corresponding distribution; and the powder is treated under high temperature at 600-1100 DEG C, thereby obtaining a micron-scale hollow glass micro-balloon with the volume floating rate being above 90%, the SiO2 content (weight) being 55-88%, the true density being 0.1-0.7g/cm<3> and the compression strength being 1-50MPa. The method is low in energy consumption, free from fusion and sintering, and high in yield. The prepared hollow glass micro-balloon is high in compression strength, light in weight, low-alkali, waterproof, excellent in fluidity and dispersibility, and suitable for various high-performance light compound materials.
Owner:TECHNICAL INST OF PHYSICS & CHEMISTRY - CHINESE ACAD OF SCI

Silicon carbide reinforced aluminum-based composite material and its preparation method

The invention relates to a silicon carbide reinforced aluminum-based composite material and its preparation method. The composite material is characterized by being composited by micron-scale and nano-scale beta-phase silicon carbide spherical particles and an aluminum substrate, with the beta-phase silicon carbide spherical particles distributed in the aluminum substrate to form a synergistic reinforced phase. The preparation method is summarized to be mainly composed of: pre-preparing beta-phase silicon carbide spherical particles, adding aluminum substrate powder and the beta-phase silicon carbide spherical particles accounting for 0-25wt% of the composite material into a ball mill for ball milling treatment, and conducting cold press molding, sintering, as well as air hot pressing sequentially, and finally carrying out hot extrusion molding to obtain a molded product of the composite material. Specifically, the particle size of the aluminum substrate powder is 1micrometer to 100micrometers. The technical scheme of the invention innovatively uses spherical particulate beta-phase silicon carbide and makes use of the synergistic reinforcement effect of the micron and nano-silicon carbide particles, substantially improves the strength, toughness, abrasion resistance and others of the aluminum-based composite material. The preparation process is simple, and the cost input is effectively reduced.
Owner:SUZHOU INST OF NANO TECH & NANO BIONICS CHINESE ACEDEMY OF SCI +1
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