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1960results about How to "Improve magnetism" patented technology

A preparation method of high-performance sintered NdFeB with low dysprosium content

The invention discloses a method for preparing sintered NdFeB with low dysprosium (Dy) content and high performance; the method comprises the following steps of: sputtering and plating the Dy element on the surface of jet mill powder by using the powder plate technology based on magnetron sputtering on the basis of preparing NdFeB powder, and then sufficiently dispersing the Dy element to micron-sized NdFeB crystal particles by dispersing the Dy element at high temperature in the sintering and tempering process, thereby achieving the effect of improving magnetic performance of the sintered NdFeB. Compared with the introduction of the Dy element in the proportioning process of the prior art, the method disclosed by the invention has the advantages: the low dysprosium content and high performance is limited in the nano-size by adopting the physical gas-phase deposition, the consumption quantity of the Dy element during the production process is controlled effectively and the preparationof sintered NdFeB with low dysprosium content and high performance is realized. Compared with the sintered NdFeB of the same components prepared by the traditional casting and powder metallurgy process, both the intrinsic coercivity and the maximum magnetic energy product of the sintered NdFeB rare-earth permanent magnetic material obtained according to the invention are improved obviously; compared with the sintered NdFeB with the same performance prepared by the traditional casting and powder metallurgy process, the dosage of the dysprosium element is reduced remarkably. The method can be widely applicable to producing and manufacturing sintered NdFeB with high performance.
Owner:NANJING UNIV OF SCI & TECH +1

Method for preparing heavy rare earth hydride nano-particle doped sintered NdFeB permanent magnet

The invention discloses a method for preparing a heavy rare earth hydride nano-particle doped sintered NdFeB permanent magnet, which belongs to the technical field of magnetic materials. The prior preparation method improves the coercive force and the temperature stability of magnets by adding heavy rare earth elements, namely terbium or dysprosium into master alloy, but the method can cause the residual magnetism of the magnets, the reduction of magnetic energy product and the increase of manufacturing cost. The method adopts heavy rare earth terbium hydride and dysprosium hydride nano-powder doping technology to prepare the sintered NdFeB permanent magnet with high coercive force and excellent magnetic property. The method comprises the following steps: preparing NdFeB powder by a rapidly solidified flake process and a hydrogen decrepitation process; preparing the terbium hydride or the dysprosium hydride nano-powder by physical vapor deposition technology; mixing the two powders, and performing magnetic field orientation and press forming; and performing dehydrogenation treatment, sintering and heat treatment on a green compact at different temperatures, and obtaining the sintered magnet. The coercive force of the magnet prepared by the method is higher than that of the prior sintered magnet with the same ingredients; and compared with the sintered magnet with the equivalent coercive force, the proportion of the terbium and dysprosium needed by the magnet prepared by the method is remarkably reduced.
Owner:BEIJING UNIV OF TECH

Preparation method of flexible anisotropy bonding rare earth permanent magnet material

The invention discloses a preparation method of flexible anisotropy bonding rare earth permanent magnet material, belonging to the field of magnetic materials. The material is prepared by combining the two-step approach accompanying temperature magnetic field orientation technology of which the calendaring process and the accompanying temperature magnetic field orientation process are separated. A certain quantity of anisotropy magnetic powder which is performed with surface treatment by the processing agent in advance, binder and processing agent are evenly mixed; the mixed material is calendered into flaky flexible bonding magnetic body by the calendaring technology; then, the flaky flexible bonding magnetic body is cut into parts which are heated at certain temperature under the condition of heat preservation for certain time, after that, the obtained product is put into an orientation magnetic field for accompanying temperature magnetic field orientation; and the direction of the orientation magnetic field is parallel to the plane normal direction of the flaky flexible bonding magnetic body. In the preparation technology, magnetic powder can overcome the constraint of a bonding system and rotates under the action of magnetic field force to ensure that the direction of easy magnetization of the magnetic powder generally points to the orientation direction, and the magnetic property of prepared flexible anisotropy bonding rare earth permanent magnet material can be greatly improved.
Owner:UNIV OF SCI & TECH BEIJING

Method for preparing rare-earth iron series biphase nanocrystalline composite permanent-magnet material

The invention belongs to the field of magnetic material. At present much of the permanent magnet material is thin belt or powder, and since the custom sintering process for preparing block material will make the crystal grow, the magnetic property drops significantly. The steps of said invention comprises: the alloy whose component is RxFeyBz, in which R stands for rare-earth Nd or Pr element and the content of x is 4-10, y is 78-88, z is 6-18, is smelted for mother alloy in induction furnace in vacuum; Then preparing the quenched alloy in amorphous, nanometer crystalline state or amorphous-nanometer mixed state by smelting quick-quench method; the linear speed of smelting quick-quench is arranged between 10-50 m / s; under the protection of inertance gas, abrading the alloy into powder whose coarseness is lower than 80 items; encasing the powder into module to precompression and shaping, while range of pressure is 10-1000MPa; carrying the process of discharging plasma sintering, while the sintering temperature is 550Deg C.-700Deg C., the pressure is 30-1000MPa, the elevated temperature speed is 50-500Deg C. / min, the time of heat preservation is 0-10 min, the elevated temperature speed is 50-200Deg C. / min, Said invention can realize high magnetic property material with high degree of compactness, whose crystal grain is smaller than 100 nanometers, and it can be used in high temperature.
Owner:BEIJING UNIV OF TECH

Preparing method of metal magnetic powder core

The invention discloses a preparing method of a metal magnetic powder core. The preparing method includes the following steps that (1) master alloy is melt through a vacuum induction furnace, and an alloy thin belt is obtained through a quick quenching device; (2) ball milling is conducted on the thin belt; (3) annealing is conducted on powder; (4) particle size distribution is conducted on the annealed powder; (5) passivant is added into the distributed powder to conduct passivating on the powder, and then a binding agent and an insulating agent are added into the powder to conduct insulating bonding and wrapping on the powder; (6) a lubricating release agent is then added, the mixture is mixed, and compression moulding is conducted; (7) annealing is conducted on a sample obtained through compression moulding, and the sample is cooled along with the furnace, and spraying and coating are conducted to obtain the target product. According to the preparing method, the master alloy contains an appropriate number of alloy elements, so that the alloy processing performance is improved; the alloy powder and an insulating medium are mixed and pressed to be the magnetic powder core, so that eddy-current loss under a high frequency can be greatly reduced; meanwhile, the problem that alloy materials are limited in use due to single shapes is solved through shape diversity of the magnetic powder core.
Owner:ZHEJIANG MINGHE STEEL PIPE CO LTD +1

Fe-Si-Al magnetic core preparation method and inorganic composite insulation coating material for magnetic core

The invention discloses a Fe-Si-Al magnetic core preparation method and an inorganic composite insulation coating material for a magnetic core, belonging to the field of Fe-Si-Al magnetic material and used for solving the high eddy-current loss problem of existing magnetic cores and such problems caused by the fact that the existing magnetic cores usually use organic coating materials as stress is difficult to eliminate in a forming process, the insulation property of the material is poor, and the volatilization quantity of organics is large in heating processes such as heat treatment. The Fe-Si-Al magnetic core preparation method disclosed by the invention comprises the following steps: cast ingot smelting, powder making, surface phosphorization, insulation coating, compression moulding, annealing treatment and surface coating; the prepared Fe-Si-Al magnetic core has the advantages of low eddy-current loss, small magnetic conductivity temperature coefficient, good temperature stability, high direct current superposition characteristic, high saturation flux density and good high-frequency characteristic and meets the requirements for high frequency, small size, high power and electromagnetic interference resistance of electronic devices.
Owner:临沂银凤新材料技术服务有限公司

Nano-silver dispersion liquid and preparation method of nano-silver dispersion liquid as well as preparation method of nano-silver antibacterial coating

The embodiment of the invention discloses a preparation method of nano-silver dispersion liquid. The preparation method comprises the following steps that thickening agents and dispersing agents are added into pure water or deionized water, then, soluble silver salt is dissolved in solution, and the silver salt solution is obtained; and under the stirring effect, silver complexing agents are firstly added into the silver salt solution, then, reducing agents are added, or silver complexing reduction agents are directly added, the reaction is carried out for at least 12 hours under the condition of room temperature to 90 DEG C, silver ions in the silver salt solution are reduced into metal silver, the nano-silver dispersion liquid is obtained, the silver complexing agents and the silver complexing reduction agents can form the chemical bonding with the nano-silver particle surface, and in addition, functional groups with the cross linking effect are reserved. The invention correspondingly provides the nano-silver dispersion liquid prepared by the method. The process of the preparation method is simple, the stability of the prepared nano-silver dispersion liquid is good, nano-silver particles are uniform, the application is convenient, and the bonding force of the nano-silver and substrates is high. In addition, the invention also provides a preparation method of a nano-silver antibacterial coating.
Owner:ENVIROCHEM TECH

Preenrichment-three segment suspension roasting-magnetic separation treatment method of complex refractory iron ores

The invention discloses a preenrichment-three segment suspension roasting-magnetic separation treatment method of complex refractory iron ores, and belongs to the technical field of mineral processing. The method comprises the following steps: 1, levigating the complex refractory iron ores, carrying out weak magnetic separation, and carrying out strong magnetic separation on mine tailings; 2, putting concentrate obtained after strong magnetic separation in a suspension roasting furnace, and heating to 450-800DEG C in a suspension state in order to carry out pre-oxidation roasting; 3, introducing nitrogen to displace air, and introducing a reducing gas to carry out reduction in a suspension loose state; 4, introducing air when the temperature decreases to 250-400DEG C in order to oxidize, taking out the obtained material when the temperature decreases to below 100DEG C, and carrying out ore milling; and 5, carrying out third segment magnetic separation, and mixing concentrate obtained after three segment magnetic separation with concrete obtained after the weak magnetic separation to obtain finial concentrate. The method has the advantages of simple process, improvement of the recovery rate of the complex refractory iron ores, strong adaptability, safe and reliable process, uniform and stable product quality, energy saving and consumption reduction.
Owner:上海逢石科技有限公司

Flexible rare earth bonded magnet with roll anisotropy and manufacturing method thereof

The invention discloses a flexible rare earth bonded magnet with roll anisotropy and a manufacturing method thereof. The magnet comprises the following components in part by mass: 94 to 97 parts of anisotropic rare earth composite permanent magnet powder, 2.8 to 5.5 parts of binder and 0.2 to 0.5 part of processing aid, wherein the anisotropic rare earth composite permanent magnet powder comprises anisotropic ferrite permanent magnet powder, anisotropic samarium-iron-nitrogen permanent magnet powder, anisotropic neodymium-iron-nitrogen permanent magnet powder and neodymium-iron-boron permanent magnet powder with roll anisotropy. The anisotropic rare earth composite permanent magnet powder is subjected to surface treatment by using a surface treatment agent. A permanent magnet product with the thickness of 0.35 to 8mm and the maximum width of 1,000mm can be manufactured by processing the components by a calendering method; the disadvantages of various conventional permanent magnet materials are overcome; and a magnetic material which has a thin wall, large length-diameter ratio, high flexibility and higher magnetic performance can be manufactured under the condition that an oriented magnetic field is not required to be applied.
Owner:BEIKUANG MAGNETS FUYANG CO LTD

Double-hard magnetic main phase mixed rare-earth permanent magnet and preparation method thereof

The invention relates to a double-hard magnetic main phase mixed rare-earth permanent magnet and a preparation method thereof. The permanent magnet comprises double hard magnetic main phases and a rear-earth-rich phase, wherein the double hard magnetic main phases are MM<2>Fe<14>B and (PrNd)<2>Fe<14>B respectively; the permanent magnet is prepared from the following chemical component in percentage by mass: [MM<x1>(PrNd)<1-x1>]<x>Fe<100-x-y-z>B<y>TM<z>; x is smaller than or equal to 31 and greater than or equal to 27; x1 is smaller than or equal to 1 and greater than or equal to 0; y is smaller than or equal to 1 and greater than or equal to 0.9; z is smaller than or equal to 1.5 and greater than 0; TM is a composition of more of the elements Al, Cu, Co, Nb, Ga, Tb and Zr; and MM is a mixed rare-earth alloy which is directly separated from raw ore and contains La, Ce, Pr and Nd. The anisotropic sintered mixed rare-earth permanent magnet with high cost performance within a range of 10-48MGOe can be prepared by adjusting the content of PrNd. A basic rare-earth raw material used by the permanent magnet is cheap mixed rare earth, so that a separation and purification technology for the rare earth can be reduced, efficient utilization of lanthanum-cerium rare earth is achieved and the double-hard magnetic main phase mixed rare-earth permanent magnet meets the requirements of low carbon economy on green production technology innovation of a rare-earth permanent magnet product.
Owner:CENT IRON & STEEL RES INST

Nano toughening NdFeB magnetic material and preparation method thereof

The invention discloses a nano toughening NdFeB magnetic material and a preparation method of the nano toughening NdFeB magnetic material. The main mechanism is that a nano composite crystal boundary phase is formed on an NdFeB main phase crystal boundary, an H-grade rare earth permanent magnetic material with high coercive force M is prepared without doping any heavy rare earth, and then, a SH-grade rare earth permanent magnetic material is prepared by adding a little heavy rare earth. The nano material is prepared by a plasma arc method, has a grain size of 5-80nm and mainly contains metallic elements, such as Al, Cu, Cr, Co, Fe, Zn and the like, and all kinds of rare earth elements. A NdFeB main phase having a rare earth content of Pr-Nd is prepared by a SC-HD process; after smelting and hydrogen breaking, the product grain size is milled to be about 3.5 microns by an air-current mill, and in the argon protection atmosphere, a nano additive is added in a manner of jetting composite, so the nano additive is uniformly attached to the NdFeB main phase. In the sintering process, the nano powder and the main phase form the crystal boundary, the coercive force of NdFeB is greatly increased, and since the product has uniform crystal components, the machining property is also elevated well, the NdFeB magnetic material can be applied to the wider field. At the same time, the technical process is simple, low-cost and suitable for the batch production.
Owner:辽宁恒德磁业有限公司

Non-oriented high-silicon electrical steel ribbon and its making method

InactiveCN103060701ASolve the characteristics of poor processing performanceImprove magnetismElectrical steelUltimate tensile strength
The invention relates to a non-oriented high-silicon electrical steel ribbon and its making method, and belongs to the fields of the metallurgical technology and the material science. The chemical components of the ribbon comprise 4.5-7.0wt% of Si, 2.0-5.0wt% of Cr, 0.06-1.0wt% of Al, 0.3-0.8wt% of Mn, 0.005wt% or less of N, 0.004wt% or less of S, 0.02wt% or less of P, 0.003wt% or less of O, 0.005wt% or less of C, and the balance Fe, and the thickness of the ribbon is 0.35-0.5mm. The making method comprises the following steps: smelting non-oriented high-silicon steel in a vacuum smelting furnace; carrying out double-roller ribbon roll-casting at a casting temperature of 1420-1460DEG C to the ribbon thickness of 1.0-1.5mm; carrying out hot rolling of the ribbon at 800-1100DEG C to the hot rolled ribbon thickness of 0.8-1.0mm; pickling, and preheating the ribbon, and carrying out warm rolling at 400-700DEG C; and annealing. The addition of the Cr element in the high-silicon electrical steel ribbon obviously improves the processing performance of the high-silicon steel ribbon, the iron loss value is same to the iron losses of present high-silicon steel products, and the magnetic induction intensity is above 0.03T higher than that of the present products. The making method has the advantages of simple technology, low energy consumption, high yield, and excellent product magnetic property.
Owner:NORTHEASTERN UNIV
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