The invention belongs to the field of magnetic material. At present much of the permanent
magnet material is thin belt or
powder, and since the custom
sintering process for preparing block material will make the
crystal grow, the magnetic property drops significantly. The steps of said invention comprises: the
alloy whose component is RxFeyBz, in which R stands for rare-earth Nd or Pr element and the content of x is 4-10, y is 78-88, z is 6-18, is smelted for mother
alloy in
induction furnace in vacuum; Then preparing the quenched
alloy in amorphous, nanometer crystalline state or amorphous-nanometer mixed state by
smelting quick-quench method; the linear speed of
smelting quick-quench is arranged between 10-50 m / s; under the protection of
inertance gas, abrading the alloy into
powder whose coarseness is lower than 80 items; encasing the
powder into module to precompression and shaping, while range of pressure is 10-1000MPa; carrying the process of discharging
plasma sintering, while the
sintering temperature is 550Deg C.-700Deg C., the pressure is 30-1000MPa, the elevated temperature speed is 50-500Deg C. / min, the time of heat preservation is 0-10 min, the elevated temperature speed is 50-200Deg C. / min, Said invention can realize high magnetic property material with high degree of compactness, whose
crystal grain is smaller than 100 nanometers, and it can be used in high temperature.