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1976results about How to "Improve coercive force" patented technology

Method for improving performance of sintered Nd-Fe-B permanent magnetic material

ActiveCN101615459AEvenly distributed and orderlySolve bad problems such as α-Fe segregationInorganic material magnetismHigh energyPositive pressure
The invention relates to a method for improving performance of sintered Nd-Fe-B permanent magnetic property by a rapid-hardening flake grain boundary diffusion heavy rare earth compound in rare earth material technical field, which comprises the following steps: 1) rapid-hardening technology is adopted to prepare an Nd-Fe-B alloy rapid-hardening flake; 2) a high-energy ball mill is used to prepare the heavy rare earth compound into powder particles with diameter being smaller than 1mu m; 3) the rapid-hardening flake is put into heavy rare earth compound turbid liquid to carry out ultrasonic coating; 4) the coated rapid-hardening flake is put into a sintered furnace filled with Ar2 to carry out positive pressure thermal diffusion; 5) ball milling, powder processing, orientation shaping, isostatic pressing and vacuum sintering are adopted to prepare the strip-casting flake after the heat treatment into a magnet. The chemical formula of the Nd-Fe-B permanent magnetic material is NdxFe(100-x-y-z-xl)ByCozCuxl, and the mass percent is as follows: x is 30-31.5, y is 0.95-1, z is 1-1.2, and xl is 0-0.06. The magnet prepared by the invention improves the intrinsic coercivity on the basis of keeping the current magnetic energy product.
Owner:NINGBO INST OF MATERIALS TECH & ENG CHINESE ACADEMY OF SCI

Method for preparing heavy rare earth hydride nano-particle doped sintered NdFeB permanent magnet

The invention discloses a method for preparing a heavy rare earth hydride nano-particle doped sintered NdFeB permanent magnet, which belongs to the technical field of magnetic materials. The prior preparation method improves the coercive force and the temperature stability of magnets by adding heavy rare earth elements, namely terbium or dysprosium into master alloy, but the method can cause the residual magnetism of the magnets, the reduction of magnetic energy product and the increase of manufacturing cost. The method adopts heavy rare earth terbium hydride and dysprosium hydride nano-powder doping technology to prepare the sintered NdFeB permanent magnet with high coercive force and excellent magnetic property. The method comprises the following steps: preparing NdFeB powder by a rapidly solidified flake process and a hydrogen decrepitation process; preparing the terbium hydride or the dysprosium hydride nano-powder by physical vapor deposition technology; mixing the two powders, and performing magnetic field orientation and press forming; and performing dehydrogenation treatment, sintering and heat treatment on a green compact at different temperatures, and obtaining the sintered magnet. The coercive force of the magnet prepared by the method is higher than that of the prior sintered magnet with the same ingredients; and compared with the sintered magnet with the equivalent coercive force, the proportion of the terbium and dysprosium needed by the magnet prepared by the method is remarkably reduced.
Owner:BEIJING UNIV OF TECH

Preparation method of neodymium iron boron magnet

A preparation method of neodymium iron boron magnet is disclosed. The composition general formula of the magnet provided by the invention is R1R2FeMB, wherein R1 is at least one element selected from the group consisting of Nd, Pr, La, Ce, Sm, Sc, Y and Eu, having a content of 23 to 35 wt%; R2 is at least one element selected from the group consisting of Tb, Dy, Gd, and Ho, having a content of 0.1 to 5 wt%; M represents transition group metal with the exception of Fe, having the content of 0.01 to 5 wt%; B represents simple substance boron, having the content of 0.8 to 1.2 wt%; the balance isFe and the other inevitable impurities. The preparation method of neodymium iron boron magnet provided by the invention works in such a manner that: one or more elements in the R2 are plated to the surface of the magnet, the metal R2 is diffused into the interior of the magnet by primary high temperature heat treatment, and imbalance organization and internal stress brought by the high temperature treatment are eliminated through secondary low temperature tempering. Low temperature molten salt electrodeposition method is employed to plate films. The present invention is advantageous in greatly improving the production efficiency, reducing the dosage of the heavy rare earth during preparation process of magnet, saving rare earth resource, and obtaining high coercivity without reducing remanent magnetism and magnetic energy product of a magnet.
Owner:GRIREM ADVANCED MATERIALS CO LTD

Method and System for Manufacturing Sintered Rare-Earth Magnet Having Magnetic Anisotropy

To improve the performance of a rare-earth magnet, it is effective to use a low-oxidized powder having a small grain size. One objective of the present invention is to provide a method for manufacturing a sintered rare-earth magnet having a magnetic anisotropy, in which a very active powder having a small grain size can be safely used in a low-oxidized state. Another objective is to provide a method capable of efficiently manufacturing products having various shapes. In a weighing and loading section 41 and a high-density loading section 42, a fine powder as a material of the sintered rare-earth magnet having a magnetic anisotropy is loaded into a mold until its density reaches a predetermined level. Then, in a magnetic orientation section 43, the fine powder is oriented by a pulsed magnetic field. Subsequently, the fine powder is not compressed but immediately sintered in a sintering furnace 44. The present method enables the mass-producing machine to be simple in its operation and its housing to be accordingly smaller, so that it will be possible to eliminate the danger of oxidization or burning of the powder, which has been a serious problem for a conventional method that uses a large-scale die-pressing machine. Furthermore, the manufacturing efficiency can be improved by using a multi-cavity mold for manufacturing a sintered rare-earth magnet having an industrially important shape, such as a plate magnet or an arched plate magnet.
Owner:DAIDO STEEL CO LTD

Preparation method of flexible anisotropy bonding rare earth permanent magnet material

The invention discloses a preparation method of flexible anisotropy bonding rare earth permanent magnet material, belonging to the field of magnetic materials. The material is prepared by combining the two-step approach accompanying temperature magnetic field orientation technology of which the calendaring process and the accompanying temperature magnetic field orientation process are separated. A certain quantity of anisotropy magnetic powder which is performed with surface treatment by the processing agent in advance, binder and processing agent are evenly mixed; the mixed material is calendered into flaky flexible bonding magnetic body by the calendaring technology; then, the flaky flexible bonding magnetic body is cut into parts which are heated at certain temperature under the condition of heat preservation for certain time, after that, the obtained product is put into an orientation magnetic field for accompanying temperature magnetic field orientation; and the direction of the orientation magnetic field is parallel to the plane normal direction of the flaky flexible bonding magnetic body. In the preparation technology, magnetic powder can overcome the constraint of a bonding system and rotates under the action of magnetic field force to ensure that the direction of easy magnetization of the magnetic powder generally points to the orientation direction, and the magnetic property of prepared flexible anisotropy bonding rare earth permanent magnet material can be greatly improved.
Owner:UNIV OF SCI & TECH BEIJING

Grain boundary diffusion method for improving properties of sintered NdFeB magnets

The invention relates to a grain boundary diffusion method for improving properties of sintered NdFeB magnets. The grain boundary diffusion method comprises the following steps of stacking sintered NdFeB magnets and diffusion alloy sheets together and placing in a hot-pressing furnace; vacuumizing the hot-pressing furnace until the vacuum degree reaches a set value, heating the hot-pressing furnace, and when the temperature of the hot-pressing furnace reaches a set value, beginning to exert a pressure and maintaining the pressure and putting the diffused sample into a high-vacuum furnace for annealing, wherein the diffusion alloy sheets are low-melting-point eutectic diffusion alloys and are represented by R-TM, R is one or more of Sc, Y, La, Ce, Pr or Nd and TM is one or more of Ti, V, Cr, Mn, Fe, Co, Ni, Cu and Zn. Compared with the prior art, the sintered NdFeB magnets modified by the pressure diffusion method, which is provided by the invention, have the advantages of large diffusion depth of a diffusion agent, uniform distribution of grain boundary phases, high coercivity and the like, especially, low-melting-point diffusion alloys designed by the invention are free of expensive heavy rare earth element dysprosium and thus the cost of the raw materials is relatively low, the diffusion temperature is low and the energy consumption in the diffusion process is small.
Owner:SHANGHAI JIAO TONG UNIV

High switching speed digital faraday rotator device and optical switches containing the same

In all-optical networks, high speed optical switching and routing becomes one of the most important issues for interconnecting the transport network layers. This invention describes novel polarization-independent high speed optical switches using a digital Faraday rotator, which can also be used for various other optical switching devices. The basic digital Faraday rotator device is composed of (a) a semi-hard or hard iron garnet based magneto-optic crystal having bi-stable magnetization states at zero external magnetic field. (b) a wire winding around the crystal for changing the magnetization states by pulsed current having both fast rise time and short duration. (c) a circuit generating the required current pulses with both polarities. After a driving current pulse excitation to set the magnetization direction, the high coercive force and high remnant squareness in the garnet-based crystal will maintain the saturation magnetization state in the crystal without the need of any external current or magnetic field to sustain the remnant state. The apparatus and the method disclosed in this invention effectively reduces the overall power consumption. By using this digital Faraday rotator device, the polarization independent 1x2 and 2x2 optical switches are designed and fabricated.
Owner:SUI ZHIFENG
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