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2802results about How to "Not easily oxidized" patented technology

Method for preparing heavy rare earth hydride nano-particle doped sintered NdFeB permanent magnet

The invention discloses a method for preparing a heavy rare earth hydride nano-particle doped sintered NdFeB permanent magnet, which belongs to the technical field of magnetic materials. The prior preparation method improves the coercive force and the temperature stability of magnets by adding heavy rare earth elements, namely terbium or dysprosium into master alloy, but the method can cause the residual magnetism of the magnets, the reduction of magnetic energy product and the increase of manufacturing cost. The method adopts heavy rare earth terbium hydride and dysprosium hydride nano-powder doping technology to prepare the sintered NdFeB permanent magnet with high coercive force and excellent magnetic property. The method comprises the following steps: preparing NdFeB powder by a rapidly solidified flake process and a hydrogen decrepitation process; preparing the terbium hydride or the dysprosium hydride nano-powder by physical vapor deposition technology; mixing the two powders, and performing magnetic field orientation and press forming; and performing dehydrogenation treatment, sintering and heat treatment on a green compact at different temperatures, and obtaining the sintered magnet. The coercive force of the magnet prepared by the method is higher than that of the prior sintered magnet with the same ingredients; and compared with the sintered magnet with the equivalent coercive force, the proportion of the terbium and dysprosium needed by the magnet prepared by the method is remarkably reduced.
Owner:BEIJING UNIV OF TECH

Preparation method of core-shell magnetic/gold nano particles

The invention discloses a preparation method of magnetic/gold nano particles. The preparation method comprises the following steps: firstly adopting a co-precipitation method to prepare the magnetic Fe3O4 nano particles; polymerizing the dopamine in-situ on the surfaces of the magnetic particles to obtain Fe3O4 nano particles modified by the poly dopamine; introducing polyphenol and amino groups to the surfaces of the Fe3O4 nano particles; absorbing the nano gold seeds on the surfaces of the modified magnetic particles through the static action; adopting the nano gold which is absorbed on the surfaces of the magnetic particles as the seed, adopting the polyphenol on the surfaces of the magnetic particles as a reducing agent, gradually adding the chloroauric acid liquid to gradually produce the gold layers on the surfaces of the magnetic particles to obtain the core-shell magnetic/gold nano particles. The nano particles have good water dispersion and strong magnetic respond performance. The diameters of the nano particles are 30-100 nanometers, the saturation magnetization is 30.1-38.7emu/g, and the nano particles are superparamagnetic. The nano particles have wide application prospect on the fields of targeted drug controlled release, thermal therapy, separation of protein and enzyme, etc.
Owner:SOUTHWEST UNIVERSITY FOR NATIONALITIES

Vitamin D3 microcapsule and preparation method thereof

The invention relates to a microcapsule and a preparation method thereof, aiming at providing a vitamin D3 microcapsule and a preparation method thereof. The vitamin D3 microcapsule comprises core material vitamin D3, oil fat, an oil-soluble emulsifier and a wall material. The preparation method comprises the following steps of: (1) adopting the core material vitamin D3, the oil fat, the oil-soluble emulsifier as oil phase for dissolving and mixing evenly; (2) adding deionized water in the wall material, stirring and dissolving as water phase; (3) adding the oil phase into the water phase, mixing, stirring evenly, then carrying out homogenization and emulsifying the obtained mixture into microcapsule; (4) carrying out spray drying to the microcapsule to form the vitamin D3 microcapsule; and (5) screening, mixing, inspecting and packing to obtain the finished product. The microcapsule and the preparation method thereof have the advantages of high embedding rate, good flowability, hard photolysis, oxidation, high heat stability, even dispersion in water and the like. The microcapsule can be widely added into food or feedstuff, is easy to be absorbed by the human body or animals, also can be used as original drug of rat poison to strengthen the stability thereof greatly.
Owner:ZHEJIANG GARDEN BIOCHEM HIGH TECH +1

Magnalium composite board and method for producing the same

The invention discloses a magnesium-aluminum composite board and a method for manufacturing the same. The magnesium-aluminum composite board comprises at least one layer of magnesium or magnesium alloy plate and at least one layer of aluminum or aluminum alloy plate which are cast together by vacuum die-casting, and at least one two-layer joint surface which is provided with a mutually occlusive zigzag structure, namely the magnesium-aluminum composite board consists of a magnesium plate and an aluminum plate, or the magnesium alloy plate and the aluminum plate, or the magnesium plate and the aluminum alloy plate, or the magnesium alloy plate and the aluminum alloy plate by vacuum die-casting, and can be a structure with two layers, three layers or more than three layers. The method for manufacturing the composite board comprises the following steps: preheating a manufactured aluminum or aluminum alloy plate finished product as an insert of a die to certain temperature, and then putting the insert into a magnesium or magnesium alloy vacuumized die; matching the die in a vacuum pressure casting machine; pouring the molten magnesium or magnesium alloy molten; performing vacuumizing injection; and finally forming the magnesium-aluminum composite board. The joint surface of the composite board is provided with the mutually occlusive zigzag structure so that the layers are closely connected with each other sequentially and the combined strength is higher.
Owner:青岛地恩地材料科技有限公司

Preparation method and application of nitrogen-doped porous carbon nano sheet composite material

The invention discloses a preparation method of a nitrogen-doped porous carbon nano sheet composite material. The preparation method comprises the steps of performing high-temperature carbonization treatment on a mixture which consists of melamine and adjacent phenanthroline iron and serves as a precursor in a tubular furnace under an inert gas environment, and then removing dissolved iron compounds from an acidic solution to obtain a porous carbon nano sheet layer with carbon-coated iron carbide nano particles. The preparation method has the advantages that the technology is simple, the raw materials are cheap, and operation is easy to implement; in the prepared composite material, iron carbide is uniformly dispersed in the carbon nano sheet layer, so that the composite material is high in specific surface area and pore volume; iron carbide nano particles are completely coated by graphitized carbon, so that oxidization and corrosion are hardly caused; the composite material is stable in acidic electrolyte, and the battery activity can be effectively improved; when used as an electrocatalyst, the composite material is relatively high in electrocatalysis efficiency; the preparation method has an important value and significance in the field of preparation of doped carbon nano composite materials and electrocatalysis of proton membrane fuel batteries.
Owner:NANKAI UNIV

Method for preparing colorful film for protecting solar cell thin grid line metal electrode by adopting mask

The invention relates to a method for preparing a colorful film for protecting a solar cell thin grid line metal electrode by adopting a mask. In the method, after a solar cell is prepared, a mask is utilized to cover a main grid line metal electrode on the front surface of the solar cell, a film is coated on the area which is not covered by the mask for the second time, and a dielectric layer for protecting the thin grid line metal electrode is prepared to form a structure comprising the dielectric layer, the thin grid line metal electrode and a passivation layer. The method can protect the thin grid line metal electrode against easy oxidation, and the main grid line metal electrode can be normally connected by welding rods. The passivation effect of the front surface can be enhanced through optimizing the passivation layer; the reflectivity of the front surface of the solar cell can be reduced and color regulation can be realized through regulating the dielectric layer; and characters, figures, graphics and the like can be displayed on the front surface of the solar cell through changing a mask pattern. In addition, the secondary film coating method is convenient to be in butt joint with the traditional crystalline silicon solar cell preparation process and is easy for industrialization.
Owner:SUN YAT SEN UNIV

Internal combustion engine variable geometry turbine supercharger nozzle ring components

The invention discloses an internal-combustion engine variable geometry turbocharger nozzle ring component, comprising forks(1), a mounting plate(2) and a blade(3), wherein the side surface of the mounting plate(2) is provided with a plurality of groups of blades(3) which are evenly spaced and arranged on the same circumference and are in the same direction, each group of blades which consists of at least three blades(3) and can be mutually opened and folded simultaneously; the other side of the mounting plate is provided with forks(1) which are connected with corresponding blades; because the blades are the three dimensional curved surface, air inlet passages for blades are continuously changed, the air input of the turbocharger is also continuously changed according to the working condition of the engine, thereby the engine can get proper amount of pressurized air under all conditions, which makes that the engine always runs under a reasonable condition, thereby realizing that the turbocharger increases the output power of the engine by 30 to 100 percent, reducing the emission of harmful gas by more than 10 percent, realizing that the fume emission reaches the emission standard of the European IV, lowering oil consumption by 5 to 10 percent and improving the economical efficiency of the automobile.
Owner:PINGXIANG DEBO TECH CO LTD

Preparation method of anionic aqueous polyurethane dispersoid for fabric coating and decoration

The invention relates to a preparation method of an anionic aqueous polyurethane dispersoid for fabric coating and decoration. The preparation method is operated according to the following steps that: (a) polyether polyol, polyester polyol and diisocyanate are subjected to polymerization reaction for 2 to 4 hours at 70 to 90 DEG C under the effect of catalysts; (b) acetone solvents and diamine hydrophilic chain extenders containing picolinic acid structures are added for taking reaction for 5 to 30 minutes at 40 to 65 DEG C, and polyurethane prepolymers are prepared; (c) the temperature is lowered to 20 to 40 DEG C, low-molecular-weight chain extenders and water are added and are emulsified through being stirred at high speed; (d) the acetone solvents are removed through reduced pressure distillation, and the anionic aqueous polyurethane dispersoid for fabric coating and decoration is obtained. Because diamine containing the picolinic acid structures is used as hydrophilic chain extenders, the regular pyridine ring structure is contained, the crystallization performance and the initial bonding intensity can be improved, meanwhile, a pyridine ring is an electron deficiency system, the color deepening caused by oxidation cannot easily occur, and the product has the yellowing resistance performance.
Owner:JIAXING UNIV +1
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