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1562 results about "Dysprosium" patented technology

Dysprosium is a chemical element with the symbol Dy and atomic number 66. It is a rare earth element with a metallic silver luster. Dysprosium is never found in nature as a free element, though it is found in various minerals, such as xenotime. Naturally occurring dysprosium is composed of seven isotopes, the most abundant of which is ¹⁶⁴Dy.

A preparation method of high-performance sintered NdFeB with low dysprosium content

The invention discloses a method for preparing sintered NdFeB with low dysprosium (Dy) content and high performance; the method comprises the following steps of: sputtering and plating the Dy element on the surface of jet mill powder by using the powder plate technology based on magnetron sputtering on the basis of preparing NdFeB powder, and then sufficiently dispersing the Dy element to micron-sized NdFeB crystal particles by dispersing the Dy element at high temperature in the sintering and tempering process, thereby achieving the effect of improving magnetic performance of the sintered NdFeB. Compared with the introduction of the Dy element in the proportioning process of the prior art, the method disclosed by the invention has the advantages: the low dysprosium content and high performance is limited in the nano-size by adopting the physical gas-phase deposition, the consumption quantity of the Dy element during the production process is controlled effectively and the preparationof sintered NdFeB with low dysprosium content and high performance is realized. Compared with the sintered NdFeB of the same components prepared by the traditional casting and powder metallurgy process, both the intrinsic coercivity and the maximum magnetic energy product of the sintered NdFeB rare-earth permanent magnetic material obtained according to the invention are improved obviously; compared with the sintered NdFeB with the same performance prepared by the traditional casting and powder metallurgy process, the dosage of the dysprosium element is reduced remarkably. The method can be widely applicable to producing and manufacturing sintered NdFeB with high performance.
Owner:NANJING UNIV OF SCI & TECH +1

Method for preparing heavy rare earth hydride nano-particle doped sintered NdFeB permanent magnet

The invention discloses a method for preparing a heavy rare earth hydride nano-particle doped sintered NdFeB permanent magnet, which belongs to the technical field of magnetic materials. The prior preparation method improves the coercive force and the temperature stability of magnets by adding heavy rare earth elements, namely terbium or dysprosium into master alloy, but the method can cause the residual magnetism of the magnets, the reduction of magnetic energy product and the increase of manufacturing cost. The method adopts heavy rare earth terbium hydride and dysprosium hydride nano-powder doping technology to prepare the sintered NdFeB permanent magnet with high coercive force and excellent magnetic property. The method comprises the following steps: preparing NdFeB powder by a rapidly solidified flake process and a hydrogen decrepitation process; preparing the terbium hydride or the dysprosium hydride nano-powder by physical vapor deposition technology; mixing the two powders, and performing magnetic field orientation and press forming; and performing dehydrogenation treatment, sintering and heat treatment on a green compact at different temperatures, and obtaining the sintered magnet. The coercive force of the magnet prepared by the method is higher than that of the prior sintered magnet with the same ingredients; and compared with the sintered magnet with the equivalent coercive force, the proportion of the terbium and dysprosium needed by the magnet prepared by the method is remarkably reduced.
Owner:BEIJING UNIV OF TECH

Rare earth permanent magnet produced by applying abundant rare earth cerium (Ce) and preparation method thereof

ActiveCN103123839AReduce production and sales balancePromote the balance of production and salesInductances/transformers/magnets manufactureMagnetic materialsRare-earth elementCost Controls
The invention discloses a rare earth permanent magnet produced by applying abundant rare earth cerium (Ce) and a preparation method of the rare earth permanent magnet produced by applying abundant rare earth Ce. Based on a double-alloy process, main phase alloy formula uses Ce to partly replace neodymium (Nd), an optimized composition design enables a main alloy to form Ce2Fe14B phase and Nd2Fe14B phase to a greatest extent, and therefore high intrinsic magnetic property is guaranteed. A brand new crystal boundary phase is prepared by a crystal boundary reconstitution technology, and high integral magnetic property and corrosion resistant property are guaranteed, and meanwhile a nanometer powder crystal modification method is supplemented, a micro organization structure of a magnet is optimized, crystal boundary distribution is improved, and the magnetic property and the corrosion resistant property are further improved. By applying abundant rare earth cerium, cost is effectively reduced, and meanwhile balance between production and marketing is promoted. Praseodymium (Pr), Nd, and the like are chosen to form a hard magnetic shell layer of a main phase boundary in a composition design of crystal phase auxiliary alloy at the same time, compared high price heavy rare earth elements of dysprosium (Dy) and terbium (Tb) with the elements, and cost control can be further achieved.
Owner:ZHEJIANG UNIV +1

Rare earth aluminum alloy, and method and device for preparing same

The invention discloses a rare earth aluminum alloy, and a method and a device for preparing the same. The alloy contains at least one rare earth metal of lanthanum, cerium, praseodymium, neodymium, gadolinium, terbium, dysprosium, holmium, erbium, thulium, lutetium, scandium and yttrium, the content of raw earth is 5 to 98 weight percent, and the balance is aluminum and inevitable impurities. The device for preparing the rare earth aluminum alloy is characterized in that: a) graphite serves as an electrolysis bath, a graphite plate is an anode, a tungsten bar is a cathode and a molybdenum crucible serves as a rare earth aluminum alloy receiver; b) the diameter of the tungsten bar is 30 to 55 mm; and c) the anode of the graphite consists of a plurality of graphite plates. The rare earth aluminum alloy, and the method and the device for preparing the same have the advantages that: the alloy has uniform components, little segregation and low impurity content; technology for preparing the rare earth aluminum alloy through fusion electrolysis can maximally replace a process for preparing single medium-heavy metal through metallothermic reduction, greatly reduce energy consumption and the emission of fluorine-containing tail gas and solid waste residue, improve current efficiency and metal yield and reduce the consumption of auxiliary materials and the energy consumption; and the rare earth aluminum alloys with different rare earth contents can be obtained by controlling different electrolytic temperatures and different cathode current densities.
Owner:GRIREM ADVANCED MATERIALS CO LTD

Grain boundary diffusion method for improving properties of sintered NdFeB magnets

The invention relates to a grain boundary diffusion method for improving properties of sintered NdFeB magnets. The grain boundary diffusion method comprises the following steps of stacking sintered NdFeB magnets and diffusion alloy sheets together and placing in a hot-pressing furnace; vacuumizing the hot-pressing furnace until the vacuum degree reaches a set value, heating the hot-pressing furnace, and when the temperature of the hot-pressing furnace reaches a set value, beginning to exert a pressure and maintaining the pressure and putting the diffused sample into a high-vacuum furnace for annealing, wherein the diffusion alloy sheets are low-melting-point eutectic diffusion alloys and are represented by R-TM, R is one or more of Sc, Y, La, Ce, Pr or Nd and TM is one or more of Ti, V, Cr, Mn, Fe, Co, Ni, Cu and Zn. Compared with the prior art, the sintered NdFeB magnets modified by the pressure diffusion method, which is provided by the invention, have the advantages of large diffusion depth of a diffusion agent, uniform distribution of grain boundary phases, high coercivity and the like, especially, low-melting-point diffusion alloys designed by the invention are free of expensive heavy rare earth element dysprosium and thus the cost of the raw materials is relatively low, the diffusion temperature is low and the energy consumption in the diffusion process is small.
Owner:SHANGHAI JIAO TONG UNIV

Method for preparing rare-earth permanent magnets by infiltration process and graphite box utilized in method

Disclosed are a method for preparing rare-earth permanent magnets by the infiltration process and a graphite box utilized in the method. The method includes: preparing base materials of R (rare earth)-Fe (ferrum)-B (boron) rear earth magnets by prepared raw materials which are subjected to smelting, hydrogen decrepitation, magnetic field forming, sintering and the like; cutting the base material into slices with the thickness ranging from 2mm to 10mm; placing the slices into a specially-made graphite box and placing heavy rare earth type metal fluoride and a few of metal calcium particles into the bottom of the graphite box; sintering the graphite box in a sintering furnace, inflating air into the sintering furnace to cool the temperature to be lower than 60 DEG C, finally ageing magnets, then inflating Ar gas into the sintering furnace to cool the temperature to be lower than 60 DEG C after ageing, and finally obtaining the rare-earth permanent magnets. Elements including Dy (dysprosium), Tb (terbium), Ho (holmium) and the like are infiltrated into the crystal boundary of the R-Fe-B to prepare high-coercivity rare-earth permanent magnets by means of infiltration process, usage of heavy rare earth metal can be greatly reduced, and production cost of magnets can be effectively reduced. Additionally, the method for preparing rare-earth permanent magnets by the infiltration process is simple in operation and suitable for batch production.
Owner:BAOTOU TIANHE MAGNETICS TECH CO LTD

High-performance sintered neodymium-iron-boron (Nd-Fe-B) rare-earth permanent magnet material and manufacturing method thereof

The invention discloses a high-performance sintered neodymium-iron-boron (Nd-Fe-B) rare-earth permanent magnet material and a manufacturing method thereof. The manufacturing method comprises the following steps: firstly, casting R-iron-boron-aluminum (R-Fe-B-Al) into a rapidly solidified alloy plate (R represents one and/or several of rare-earth elements containing Nd) by adopting a vacuum rapid solidifying process, then, coating a metal penetrant comprising the component Ra-Al or Ra-Al-X [the Ra represents dysprosium (Dy) and/or terbium (Tb), and the X represents one or several of cobalt, copper, gallium and zirconium (Co, Cu, Ga and Zr) elements] to the surface of the alloy plate, and heating to enable the metal penetrant to penetrate into the crystal boundary of the rapidly solidified alloy plate. A replacement reaction happens between the Ra in the penetrant entering the crystal boundary of the rapidly solidified alloy plate and the Nd and/or praseodymium (Pr) in the main phase of the alloy plate to form an Rh2(Fe, Al)14B phase with high content of the Dy and/or the Tb (the Rh represents that the content of the Dy and/or the Tb is higher than that of the Dy and/or the Tb in the R), and the positions of part of Fe atoms are replaced by Al atoms to encircle the double-main phase structure of an R2Fe14B phase. The high-performance sintered neodymium-iron-boron (Nd-Fe-B) rare-earth permanent magnet material disclosed by the invention is capable of effectively improving a coercive force and obviously reducing the use level of rare earth, and simultaneously, is also capable of improving the corrosion resistance of a magnet.
Owner:SHENYANG GENERAL MAGNETIC

Coating Method and Apparatus, a Permanent Magnet, and Manufacturing Method Thereof

A film is formed at a high rate on the surface of an iron-boron-rare-earth-metal magnet having a given shape, while effectively using dysprosium or terbium as a film-forming material. Thus, productivity is improved and a permanent magnet can be produced at low cost. A permanent magnet is produced through a film formation step in which a film of dysprosium is formed on the surface of an iron-boron-rare-earth-metal magnet of a given shape and a diffusion step in which the magnet coated is subjected to a heat treatment at a given temperature to cause the dysprosium deposited on the surface to diffuse into the grain boundary phase of the magnet. The film formation step comprises: a first step in which a treating chamber where this film formation is performed is heated to vaporize dysprosium which has been disposed in this treating chamber and thereby form a dysprosium vapor atmosphere having a given vapor pressure in the treating chamber; and a second step in which a magnet kept at a temperature lower than the internal temperature of the treating chamber is introduced into this treating chamber and the dysprosium is selectively deposited on the magnet surface based on a temperature difference between the treating chamber and the magnet until the magnet temperature reaches a given value.
Owner:ULVAC INC
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