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1353 results about "Neodymium" patented technology

Neodymium is a chemical element with the symbol Nd and atomic number 60. Neodymium belongs to the lanthanide series and is a rare-earth element. It is a hard, slightly malleable silvery metal, that quickly tarnishes in air and moisture. When oxidized, neodymium reacts quickly to produce pink, purple/blue and yellow compounds in the +2, +3 and +4 oxidation states. Neodymium was discovered in 1885 by the Austrian chemist Carl Auer von Welsbach. It is present in significant quantities in the ore minerals monazite and bastnäsite. Neodymium is not found naturally in metallic form or unmixed with other lanthanides, and it is usually refined for general use. Although neodymium is classed as a rare-earth element, it is fairly common, no rarer than cobalt, nickel, or copper, and is widely distributed in the Earth's crust. Most of the world's commercial neodymium is mined in China.

Neodymium-iron-boron magnet with double main phases and light rare earth diffusion based on asymmetric cerium distribution and preparation method of neodymium-iron-boron magnet

The invention discloses a neodymium-iron-boron magnet with double main phases and light rare earth diffusion based on asymmetric cerium distribution and a preparation method, and relates to the technical field of neodymium-iron-boron magnets. The method comprises the steps that a diffusion matrix is prepared through a double-main-phase technology, in the double-main-phase technology, the components of a main-phase alloy and an auxiliary-phase alloy are RaCebFe100-a-b-c-dMcBd, R is PrNd alloy or Nd metal, M is at least one of Cu, Al, Zr, Co and Ga, the content of Ce in the main-phase alloy is larger than that of Ce in the auxiliary-phase alloy, then the upper surface and the lower surface of the diffusion matrix are coated with a diffusion source solution, and the diffusion matrix is obtained through heat treatment. Carrying out heat treatment and aging treatment to obtain a neodymium-iron-boron magnet; the diffusion source solution is formed by mixing a diffusion source and a solvent, and the diffusion source is (PrmNdn) aAlbCucZrdCoeMgf. The neodymium-iron-boron magnet obtained through the method has high residual magnetism and high coercive force at the same time, the diffusion efficiency of the diffusion source is high, and the rare earth utilization rate is increased.
Owner:MIANYANG JUXING PERMANENT MAGNET MATERIAL CO LTD

Rare-earth metal arylamine group compound as well as preparation method and application thereof

The invention discloses a rare-earth metal arylamine group compound as well as preparation method and application thereof. The invention discloses the rare-earth metal arylamine group compound which is characterized in that a general formula of the rare-earth metal arylamine group compound is (2,6-R12PhNH)5LnLi2(THF)2, wherein Ln is a rear-earth metal selected from one of neodymium, samarium, ytterbium or yttrium; R1 is selected from one of hydrogen, methyl or isopropyl. The rare-earth metal arylamine group compound has the advantages that the rare-earth metal arylamine group compound has a definite structure; raw materials used in the preparation method are simple, easily obtained and cheap; the reaction process is simple and easily operated; the rare-earth metal arylamine group compound product is conveniently purified and the yield of the product is high; the rare-earth metal arylamine group compound has a high activity when acting as a single component catalyst to catalyze a hydrogen phosphine reaction of aldehyde or ketone and phosphite ester; the use amount of the catalyst is less; the yield is high; a substrate has wide universality; a new and simple method is provided for synthesis of a-hydroxyphosphonate.
Owner:SUZHOU UNIV

A medium-high performance neodymium iron boron magnet and preparation method thereof

The present invention discloses a medium-high performance neodymium iron boron and a preparation method thereof. Through the master-slave phase double alloy process, the master phase alloy is cerium iron boron with a low total rare earth content, and the slave phase is a neodymium iron boron alloy with a high total rare earth content, avoiding the entry of light rare earths in the master phase into the grain boundaries, while the surplus rare earths in the slave phase enter the grain boundaries and are recombined into rare earth-rich phases. The prepared magnet is processed into a thin magnetic sheet, and a low-melting-point HReM alloy is magnetron sputtered, realizing low-temperature grain boundary diffusion. This alloy improves the grain boundary wettability and also improves the fluidity of the rare earth-rich phase, enabling the cerium-containing neodymium iron boron master and slave phase grains to be quickly isolated during grain boundary diffusion. The low-temperature diffusion avoids the replacement of the diffused heavy rare earths by praseodymium, neodymium, and cerium elements, inhibits the exchange coupling between cerium iron boron grains, and makes the heavy rare earths free in the grain boundaries or interact with the rare earth-rich phase to form a core-shell structure on the surface layer of the master phase grains, enabling the rare earth-rich phase to be continuously and uniformly distributed, effectively enhancing the effectiveness of the grain boundary diffusion of heavy rare earth elements in improving the intrinsic coercivity of the cerium-containing magnet.
Owner:ZHEJIANG KAIVEN MAGNETICS CO LTD

Yttrium-rich neodymium-iron-boron magnet and preparation method thereof

The invention discloses an yttrium-rich neodymium-iron-boron magnet and a preparation method thereof, and belongs to the technical field of rare earth permanent magnet material preparation. The preparation method comprises the following steps: mixing yttrium-rich neodymium-iron-boron matrix alloy powder with grain boundary doped alloy powder containing Gd and / or Ho, and carrying out compression molding and sintering tempering treatment to obtain a first yttrium-rich neodymium-iron-boron magnet. According to the invention, the grain boundary doped alloy powder containing Gd and / or Ho is added into the yttrium-rich neodymium iron boron matrix alloy powder and then is sintered, so that a continuous and uniform non-magnetic thin-wall grain boundary phase structure is formed in the grain boundary, and the coercive force of the magnet is enhanced. Dy and / or Tb heavy rare earth element grain boundary diffusion is carried out based on the first yttrium-rich neodymium-iron-boron magnet after grain boundary modification, a second yttrium-rich neodymium-iron-boron magnet is obtained, the diffusion depth of Dy and / or Tb in the magnet can be increased, the utilization rate can be increased, the cost can be reduced, the coercivity of the magnet can be improved, and the adverse effect of Dy and / or Tb on residual magnetism can be reduced.
Owner:NINGBO INST OF MATERIALS TECH & ENG CHINESE ACAD OF SCI

Neodymium-iron-boron magnet material and preparation method therefor and use thereof, and motor

Disclosed are a neodymium-iron-boron magnet material, a preparation method, use thereof and a motor. The neodymium-iron-boron magnet material has an amorphous RE-rich phase located in a grain boundary phase. The amorphous RE-rich phase, containing elements TM, RE, Cu and Ga at an atom ratio of TM:RE:Cu:Ga=(15-30):(40-60):(10-25):(10-30), accounts for 3-8% by volume of the grain boundary phase. TM is Fe and Co. RE is a rare earth element. The neodymium-iron-boron magnet material increases the coercivity using none or a small amount of heavy rare earth elements, while maintaining high remanence and magnetic energy.
Owner:FUJIAN CHANGTING GOLDEN DRAGON RARE EARTH CO LTD

Tungsten alloy wire, preparation method therefor, and use thereof in cutting of semiconductor material

The present application relates to the technical field of tungsten alloy materials, and in particular to a tungsten alloy wire, a preparation method therefor, and a use thereof in cutting of a semiconductor material. The tungsten alloy is composed of the following elements in percentage by mass: 0.4-1.1 wt% of L, 0.001-0.25 wt% of Z, and the balance of tungsten and inevitable impurities, wherein L is one or more than two of lanthanum, cerium, praseodymium, neodymium, gadolinium and erbium, and Z comprises oxygen and carbon. The wire diameter of the wire is 20-60 μm, the wire contains linear L or a compound of L along the wire axis direction, and the radial average width D of L or the compound of L is smaller than or equal to 5 nm. According to the present application, the linear L element is doped between tungsten base bodies, and the radial average width of L is controlled to be smaller than or equal to 5 nm, so that the wire has the tensile strength of 5000 MPa or above under the wire diameter of 20-60 μm, and the machining performance of the tungsten alloy wire is enhanced.
Owner:XIAMEN HONGLU TUNGSTEN MOLYBDENUM IND CO LTD

Tungsten alloy wire, and preparation method therefor and use thereof

The present invention relates to the technical field of tungsten alloy materials, and in particular to a tungsten alloy wire, and a preparation method therefor and a use thereof. The tungsten alloy is composed of the following elements in percentage by mass: 0.45-0.9 wt% of L, 0.05-0.2 wt% of oxygen, and the balance being tungsten and inevitable impurities, wherein L is one or more of lanthanum, cerium, praseodymium, neodymium, gadolinium, and samarium, the wire has a wire diameter of 20-60 μm, in the wire, L or compounds of L exist in the axial direction of the wire in a linear shape, and the average width D of L or the compounds of L in the radial direction is less than or equal to 5 nm. The element L is controlled to be doped between the tungsten base materials in a linear shape, and the average width D of L in the radial direction to be less than or equal to 5 nm, so that cracks and wire breakage caused by second-phase particles in the subsequent pressure machining process are greatly reduced, thereby guaranteeing the mechanical strength of the tungsten alloy wire, and thus the wire has a tensile strength of 5000 MPa or above under a wire diameter of 20-60 μm, and the machining performance of the tungsten alloy wire is enhanced.
Owner:XIAMEN HONGLU TUNGSTEN MOLYBDENUM IND CO LTD

Neodymium-zirconium co-substituted M-type strontium ferrite wave-absorbing material and preparation method thereof

The invention discloses a neodymium-zirconium co-substituted M-type strontium ferrite wave-absorbing material and a preparation method thereof, the chemical formula of the neodymium-zirconium co-substituted M-type strontium ferrite wave-absorbing material is Sr1-xNdxZr0. 2Fe11.8 O19, and x is more than or equal to 0.1 and less than or equal to 0.4. The method comprises the following steps: (1) mixing strontium nitrate, ferric nitrate nonahydrate, neodymium nitrate hexahydrate, zirconium nitrate pentahydrate, citric acid monohydrate and deionized water, stirring and dissolving to obtain sol; (2) adjusting the pH value of the sol to 6.5-7.5, and then heating to carry out sol-gel reaction to obtain wet gel; (3) drying and grinding the wet gel to obtain precursor powder; and (4) performing heat treatment on the precursor powder in a box-type furnace, cooling and grinding to obtain the neodymium-zirconium co-substituted M-type strontium ferrite wave-absorbing material. According to the material, effective wave-absorbing frequency band broadening is achieved, the matching thickness corresponding to the effective wave-absorbing bandwidth is as thin as 0.55-0.7 mm, and meanwhile, the performance requirements of thinness, width and strength in the field of electromagnetic compatibility are met.
Owner:HEFEI UNIV OF TECH

Grinding equipment for sintered neodymium-iron-boron magnet

The invention discloses sintered neodymium-iron-boron magnet grinding machining equipment, and relates to the technical field of neodymium-iron-boron magnet machining, the sintered neodymium-iron-boron magnet grinding machining equipment comprises a machining table, the machining table is provided with a grinding assembly, a clamping assembly, a steering adjusting assembly and a cooling assembly, and the clamping assembly is used for clamping a magnet body; the grinding assembly is used for achieving grinding machining of a magnet body, the steering adjusting assembly is used for achieving rotation of the magnet body and achieving multi-directional machining of the magnet body in a matched mode, and the cooling assembly is used for cooling treatment when the magnet body is machined, so that machining is more stable. A plurality of through grooves are formed in the machining table, and a waste collecting assembly is arranged in the machining table and used for collecting machined waste. The problems that in the prior art, a grinding mechanism is directly driven by a feeding mechanism to conduct grinding, the microstructure of a magnet is easily damaged, and the magnetic performance is reduced are solved.
Owner:ANHUI ONE MAGNET ELECTRONIC CO LTD

High-flux district dispersing agent and application thereof

The invention relates to a high-flux selective diffusion agent and application thereof. The high-flux selective diffusion agent is obtained by mixing heavy rare earth-containing spherical powder and a solid organic binder and then melting and processing; the particle size of the heavy rare earth-containing spherical powder is 10-60 [mu] m, and the sphericity is greater than 85%. According to the method, the heavy rare earth-containing spherical powder with high sphericity degree and good fluidity and the raw material suitable for additive manufacturing are adopted, and the comprehensive magnetic performance of the subsequently prepared magnet can be remarkably improved by strictly controlling the morphology of the heavy rare earth-containing spherical powder. According to the method, the high-flux selected area dispersion technology is combined with the additive manufacturing means, selected area diffusion is conducted on the surface of the neodymium-iron-boron magnet, and the coercive force and high-temperature stability of the neodymium-iron-boron magnet can be greatly improved under the condition that the use amount of heavy rare earth is small. The method is suitable for multi-batch and small-batch production exploration and has the advantages of being high in technological process automation process and short in research and development period.
Owner:SHENZHEN INST OF ADVANCED TECH CHINESE ACAD OF SCI

Method for coating slurry on surface of sintered neodymium-iron-boron substrate, preparation method of sintered neodymium-iron-boron magnet and slurry

The invention provides a method for coating slurry on the surface of a sintered neodymium-iron-boron matrix, a preparation method of a sintered neodymium-iron-boron magnet and the slurry. The method for coating the surface of the sintered neodymium-iron-boron substrate with the slurry comprises the steps that the slurry is prepared; wherein the slurry comprises powder containing heavy rare earth elements, an organic solvent and a binder, and the viscosity of the slurry is 2000-5000 mPa.s; and coating the surface of the sintered neodymium-iron-boron substrate with the slurry by adopting a roller coater to form a coating layer. The slurry provided by the invention is low in viscosity, good in flowability, low in thixotropy, low in shear viscosity mutation rate and low in temperature sensitivity, the weight gain uniformity of magnets in each batch and between batches is good, and the coercive force is obviously improved.
Owner:BEIJING ZHONG KE SAN HUAN HI TECH

Entropy-regulated composite dielectric thin film and preparation method thereof

The present application provides an entropy-regulated composite dielectric film, which comprises a polymer matrix; and fillers dispersed in the polymer matrix, wherein the fillers comprise Bi 4‑a M 1a Ti (3‑3b) M 2b O 12 , wherein M1 comprises at least one of lanthanum, neodymium, samarium and praseodymium, M2 comprises at least one of zirconium, hafnium and tin, 0 The entropy-regulated composite dielectric film has high temperature resistance, high breakdown strength, high polarization strength, high energy storage density and good stability.
Owner:TSINGHUA UNIVERSITY

Diffusion source for neodymium-iron-boron magnet as well as preparation method and application of diffusion source

The invention relates to a diffusion source for a neodymium-iron-boron magnet and a preparation method and application of the diffusion source. The invention discloses a rare-earth metal catalyst which comprises the following components in percentage by mass: 46%-49% of an organic solvent, 0.1%-2% of an adhesive, 0.1%-5% of a metal oxide and 46%-49% of rare-earth metal, and the melting point of the metal oxide is higher than that of the neodymium-iron-boron magnet. The specific organic solvent, the adhesive, the metal oxide and the rare earth metal are matched for use according to a specific matching relation, so that the diffusion source is more stable, the diffusion effect is improved, and when the magnet attached with the diffusion source is subjected to thermal diffusion treatment, the rare earth metal can be diffused into the magnet so as to improve the coercive force and other properties of the magnet. In the process, the high-melting-point metal oxide is adhered to the surface of the magnet and then serves as a spacer, the adhesion phenomenon of the magnet in the high-temperature sintering diffusion process is reduced or avoided, grain boundary diffusion is further promoted, and the performance of the magnet is improved.
Owner:HUNAN RARE EARTH NEW ENERGY MATERIALS CO LTD

Grain boundary diffusion method of sintered neodymium-iron-boron magnet

The invention discloses a grain boundary diffusion method of a sintered neodymium-iron-boron magnet. The grain boundary diffusion method comprises the following steps: providing a magnet to be diffused; coating the surface of the magnet to be diffused with coating slurry containing heavy rare earth metal powder, and performing grain boundary diffusion after vacuum heat preservation and dehydrogenation; the vacuum heat preservation dehydrogenation process comprises the steps that under the vacuum condition, the temperature is increased to 220-250 DEG C from the normal temperature after 1-1.5 h, heat preservation is conducted for 2-3 h, then the temperature is increased to 520-560 DEG C after 1-2 h, and heat preservation is conducted for 1-2 h; the grain boundary diffusion process comprises the following steps: heating to 650-750 DEG C after 1-1.5 hours, and preserving heat for 24-30 hours for permeation; and finally, the temperature is increased to 970-1000 DEG C after 1-1.5 h, and heat preservation is conducted for 2-3 h. According to the grain boundary diffusion method, the coercive force of the center part of the sintered neodymium-iron-boron magnet with the high permeation thickness can be remarkably improved, and the intrinsic coercive force gradient difference of the surface layer and the center part of the magnet is reduced.
Owner:EARTH PANDA ADVANCE MAGNETIC MATERIAL +1

Continuous cutting equipment for machining neodymium-iron-boron magnet of magnetic coupler

The invention relates to the technical field of neodymium-iron-boron magnet machining, and discloses continuous cutting equipment for magnetic coupler neodymium-iron-boron magnet machining, which comprises a laser cutting machine body and a material guide mechanism mounted below a blanking groove in the laser cutting machine body, the slide way is obliquely and fixedly installed below the blanking groove in the workbench through a support and used for assisting the cut neodymium-iron-boron magnet in falling, a bearing assembly and a separating mechanism which assist the neodymium-iron-boron magnet in falling onto the slide way are installed in the blanking groove, the separating mechanism comprises an installation plate, and the installation plate is fixedly connected between baffles on the two sides of the slide way. According to the continuous cutting equipment for machining the neodymium-iron-boron magnet of the magnetic coupler, the problems that in the prior art, residual magnetism is left after laser cutting of the neodymium-iron-boron magnet, and due to magnetic interference, cut finished products and waste materials are still adhered due to magnetic force adsorption and are not prone to separation can be effectively solved.
Owner:DONGGUAN SANEN MAGNETIC IND CO LTD

Low-temperature-resistant organic silicon elastic damping body and preparation method thereof

The invention discloses a low-temperature-resistant organic silicon elastic damping body and a preparation method thereof, and belongs to the field of synthesis of organic polymer materials. The invention relates to a high-efficiency photoinitiator, which is prepared from the following ingredients in parts by weight: 95 to 110 parts of fluorosiloxane-phenylsiloxane segmented copolymers, 25 to 35 parts of boric acid ester end-capped polyurethane prepolymers, 10 to 15 parts of neodymium-containing metal organic frameworks, 20 to 40 parts of azobenzene modified CNT / TiO2, 2 to 4 parts of photoinitiators 1173 and 2 to 3 parts of neodymium acetylacetonate. Ultralow-temperature adaptability, self-repairing and high-modulus coexistence and wide-temperature-range damping stability are achieved through fluorosilicone / phenyl block copolymer molecular design, a borate-neodymium coordination double-dynamic network, stress response filler and a light-heat gradient curing process. The low-temperature-resistant organic silicon elastic damping body prepared by the invention provides a new solution idea for an extreme environment damping material, and has a wide application prospect.
Owner:BENGBU AIYOU NEW MATERIALS CO LTD

Sintered neodymium-iron-boron magnet performance prediction method based on data driving

The invention discloses a sintered neodymium-iron-boron magnet performance prediction method based on data driving, which is used for gradually capturing the influence of process parameters in the production process and gradually predicting the middle and final magnet performance. In the first stage, technological parameters are used as input, the characteristics of powder are predicted through the combined prediction model, and intermediate output characteristics of the first stage are obtained. And in the second stage, training and prediction are carried out again in combination with the process parameters and the powder performance parameters obtained through prediction in the first stage, so that the final performance of the magnet is obtained. Through the multi-stage mode, the model can gradually accumulate and extract the influence of each process link, which is beneficial to reveal the complex mass transfer mechanism of the process. The stage training not only improves the prediction precision, but also enhances the interpretability of the model, so that the key process links can be better identified in the production process, thereby improving the consistency of the product quality and the optimization efficiency of the process flow.
Owner:AUTOMATION RES & DESIGN INST OF METALLURGICAL IND

High-coercivity and high-stability cerium-containing neodymium-iron-boron magnet and preparation method thereof

The invention belongs to the technical field of neodymium iron boron rare earth permanent magnets, and relates to a cerium-containing neodymium iron boron magnet with high coercivity and high stability and a preparation method thereof. According to the preparation method, the cerium-containing copper auxiliary alloy and the neodymium iron boron magnetic powder are ingeniously combined, the whole preparation process is optimized, and remarkable technical progress and economic benefits are achieved. Firstly, in the aspect of magnetic performance, Ce in a specific proportion is added into the cerium-containing copper auxiliary alloy, the cerium-containing copper auxiliary alloy is used, the coercive force of a magnet is effectively improved, high residual magnetism is kept to a certain degree, and introduction of Cu is beneficial to refining of grains and improvement of a grain boundary phase structure; therefore, the reverse magnetization resistance in the magnet is enhanced, and the magnet can maintain stable performance in a wider temperature range.
Owner:NINGBO JINJI STRONG MAGNETIC MATERIAL CO LTD +1

Dual-rare earth metal catalytic nano material, diaphragm and preparation method and application of dual-rare earth metal catalytic nano material

The invention relates to a dual-rare earth metal catalytic nano material, a diaphragm and a preparation method and application thereof. The preparation method comprises the following steps: carrying out hydrothermal reaction on an aqueous solution containing a carbon source, a hard template, a graphene oxide dispersion liquid, a nitrogen source, a phosphorus source, cerium salt and neodymium salt; then carrying out centrifugal separation to obtain a precipitate, and generating a precursor containing Ce and Nd rare earth bimetallic modified nitrogen and phosphorus doped graphene coated microspheres; and carrying out chemical etching on the precipitate after heat treatment to obtain the dual-rare earth metal catalytic nano material (HCS-coated NPrGO / CeNd). The HCS-coated NPrGO / CeNd can be used as a modification material of a lithium-sulfur battery diaphragm, not only can catalyze the conversion of polysulfide, but also can inhibit the shuttle effect of the polysulfide, so that the lithium-sulfur battery has relatively high capacity under high-rate charge and discharge, and has relatively low capacity fading rate in a high-rate long-cycle test.
Owner:SUZHOU UNIV

Neodymium-iron-boron magnet detection system for neodymium-iron-boron waste recovery

The invention discloses a neodymium-iron-boron magnet detection system for neodymium-iron-boron waste recovery. The neodymium-iron-boron magnet detection system comprises a detection main body and a detection mechanism. A mounting seat, a first rotating part, a second rotating part and a limiting part are arranged in the detection assembly. After the electromagnetic part is electrified, the electromagnetic part is kept to attract neodymium iron boron waste in the bearing seat, so that the limiting part pulls the upper end of the first rotating part to rotate towards the bearing seat, the lower end of the first rotating part is kept to drive the upper end of the second rotating part to reversely rotate, and the second rotating part applies pressure to the pressure applying part; the pressure applying piece transmits pressure to the pressure sensor. According to the neodymium-iron-boron magnet detection system for neodymium-iron-boron waste recovery, the neodymium-iron-boron waste loaded into the bearing seat is clamped through the mechanical arm and is in automatic butt joint with the detection assembly, automatic operation is achieved, and magnetic force detection is conducted on the neodymium-iron-boron waste. Compared with an existing manual detection mode, personal danger of detection personnel is avoided, meanwhile, the labor intensity is reduced, and the detection precision is improved.
Owner:CIXI XINHONG IND CO LTD

Sintered neodymium-iron-boron magnet and preparation method and application thereof

The invention discloses a sintered neodymium-iron-boron magnet and a preparation method and application thereof. The magnet comprises main phase crystal particles with RE2Fe14B structures and a grain boundary phase. The grain boundary phase comprises a two-particle grain boundary phase between two main phase crystal particles and a grain boundary triple-phase point composed of more than three main phase crystal particle gaps; the ratio of the number of the main phase crystal particles to the number of grain boundary triphase points is smaller than or equal to 3. According to the sintered neodymium-iron-boron magnet, through proper component design, reasonable control over the (Cu + Ga) / X ratio and control over the thickness of an alloy sheet and the ratio relation between the average width of columnar crystals in the alloy sheet and the granularity of magnetic powder, concentrated distribution of grain boundary three-phase points can be effectively restrained, the grain boundary phase proportion can be increased, grain boundary phase distribution can be optimized, and the performance of the sintered neodymium-iron-boron magnet can be improved. Therefore, both high magnetic performance and high impact toughness are achieved. The sum of the magnetic energy product and the coercive force of the sintered neodymium-iron-boron magnet is larger than or equal to 75, the impact toughness of the sintered neodymium-iron-boron magnet is larger than or equal to 20 kJ / m < 2 >, and the sintered neodymium-iron-boron magnet can be applied to new energy automobile motors, energy-saving
Owner:YANTAI ZHENGHAI MAGNETIC MATERIAL CO LTD

High-temperature-resistant high-performance neodymium-iron-boron permanent magnet material and preparation method thereof

The invention discloses a high-temperature-resistant high-performance neodymium-iron-boron permanent magnet material and a preparation method thereof, and belongs to the technical field of neodymium-iron-boron permanent magnet materials. The material is prepared from neodymium iron boron magnetic powder, auxiliary metal, hyperbranched polyimide polymer modified nano zirconium oxide and a silane coupling agent through mixing, smelting, crushing, sintering, tempering, coating and curing. The hyperbranched polyimide polymer modified nano-zirconia is introduced into the components, so that the permanent magnet material has excellent thermal stability, the permanent magnet material can still keep stable magnetic performance and mechanical performance at high temperature, the attenuation resistance is good, the thermal demagnetization is low, and the interface bonding strength is improved after the nano-zirconia is modified by hyperbranched polyimide. The interfacial compatibility between the nano zirconium oxide and the polyimide is enhanced through click chemical reaction, and the interfacial bonding strength of the nano zirconium oxide on a neodymium iron boron matrix is improved. The three-dimensional branched structure of the hyperbranched polyimide can form physical crosslinking points in the material, so that the mechanical strength of the material is enhanced.
Owner:INNER MONGOLIA QIANSHAN HEAVY IND CO LTD

MIM injection molded high-performance neodymium-iron-boron magnet and preparation process thereof

The invention provides a high-performance neodymium-iron-boron magnet formed by MIM (metal injection molding), which comprises the following components in percentage by weight: 28 to 38 weight percent of Re, 4 to 5 weight percent of FeB, 0.05 to 0.2 weight percent of Cu, 0 to 0.15 weight percent of Al, 0.15 to 0.3 weight percent of Ga, 0.2 to 1.5 weight percent of Co, 0.15 to 0.2 weight percent of Zr and the balance of iron and other inevitable impurities, the MIM injection molding process is carried out under the protection of nitrogen, the position of an extrusion material rod opening and the interior of a mold cavity are both under the protection of inert gas, and the extrusion material rod opening and the mold cavity are sealed. Meanwhile, a mold core is in a pulsed magnetic field environment in the injection molding process, it is guaranteed that the magnet has a proper neodymium-rich phase by regulating the rare earth content to be 28-38%, and therefore the coercive force of the magnet is improved, the compactness of the magnet is improved, the production cost is reduced, and through the optimized jet milling technology, the particle size and particle size distribution of neodymium-iron-boron powder are controlled, so that the yield of neodymium-iron-boron powder is improved. And meanwhile, the proportions of the magnetic powder with different particle sizes are adjusted through the sorting wheel, so that gap coating of the pre-coating solute is facilitated, and the injection molding density of the MIM neodymium iron boron is improved.
Owner:동관 화옌 뉴 매터리얼 테크놀로지 씨오 엘티디 +2

Permanent magnet alloy powder, preparation method thereof, prepared permanent magnet and method

The invention relates to the technical field of rare earth permanent magnet materials, in particular to permanent magnet alloy powder, a preparation method thereof, a prepared permanent magnet and a method. Wherein the permanent magnet alloy powder and the permanent magnet alloy comprise the following components: REa (La1-mCems) b-Feba-Mc-Tn-Bd, and RE is at least one of Pr, Nd, Sm, Y, Gd, Tb, Dy, Ho and Yb; m is at least one of Zr, Nb, Mo, Hf, Mn, Ta and W; t is at least one of Cr, V, Si and Ti; wherein 0 < a < = 2.0, 11 < = b < = 13.5, 0 < = c < = 1.5, 6 < = d < = 8.1, 0 < = m < = 1, and 0 < n < = 3.0. According to the permanent magnet alloy powder, lanthanum and cerium are adopted to replace part of precious rare earth elements to prepare the permanent magnet alloy powder, the cost can be greatly reduced, the oxidation resistance is improved and the flammability is reduced through a small amount of refractory metal M and antioxidant reinforced metal T matched elements, and the problem that a pure praseodymium neodymium-lanthanum cerium / cerium-based iron boron material is poor in temperature resistance and oxidation resistance is solved.
Owner:CHENGDU GALAXY MAGNETAB +1

Method for improving performance of rare earth permanent magnet sintered neodymium iron boron grain boundary diffusion

The invention discloses a method for improving performance of rare earth permanent magnet sintered neodymium iron boron grain boundary diffusion, and belongs to the technical field of rare earth permanent magnet materials. The method comprises the steps that a low-melting-point metal layer and a diffusion layer containing heavy rare earth elements are sequentially formed on the surface of a clean sintered neodymium-iron-boron magnet, and then vacuum diffusion heat treatment and tempering treatment are conducted. Wherein the low-melting-point metal layer comprises at least one of copper, aluminum, gallium and tin or an alloy of the copper, the aluminum, the gallium and the tin; the heavy rare earth element comprises at least one of dysprosium, terbium, holmium and gadolinium. The low-melting-point metal layer is preferentially diffused and wets the grain boundary in the heat treatment process, heavy rare earth elements are promoted to be deeply and uniformly diffused towards the interior of the magnet along the grain boundary, so that a heavy rare earth-rich shell layer is formed outside main phase grains of the magnet, and the intrinsic coercive force is improved; meanwhile, the low-melting-point metal forms a strengthening phase at the grain boundary, the brittleness of the magnet after diffusion is improved, the surface corrosion phenomenon is restrained, and collaborative optimization of the comprehensive performance of the magnet is achieved.
Owner:NINGBO LIANDE PERMANENT MAGNET TECHNOLOGY CO LTD

Linear Halbach array based on non-uniform permanent magnet and preparation method thereof

The invention provides a linear Halbach array based on a non-uniform permanent magnet and a preparation method of the linear Halbach array, and belongs to the field of permanent magnets. The method comprises the steps that the interior of a mold is divided into an area A1, an area A2 and an area B, wherein the area A1 and the area A2 are symmetrical on the two sides and concave in an arc shape; the B area is loosely filled with low-grade magnetic powder, and the A1 area and the A2 area are loosely filled with high-grade magnetic powder; carrying out compression molding and magnetization orientation to obtain a neodymium iron boron pressed blank; the neodymium-iron-boron pressed blank is subjected to heat treatment after being demolded to obtain the non-uniform permanent magnet, and the heat treatment comprises preheating, gradient sintering of first heating and then cooling, and tempering treatment; and (2n + 3) groups of non-uniform permanent magnets are adhered and fixed by using magnet glue to obtain the linear Halbach array. According to the non-uniform permanent magnet, the non-uniform permanent magnet is manufactured by adopting different marks of magnetic powder partition mold pressing, region strengthening is carried out on the edge, the demagnetization effect of the magnet at the corner angle under the extreme condition is reduced, the local intrinsic coercive force is improved, the service performance of the magnet is enhanced, and the performance of a Halbach array assembled by the non-uniform permanent magnet is promoted to be more excellent.
Owner:JIANGXI UNIV OF SCI & TECH +1

High-temperature-resistant neodymium-iron-boron magnet and preparation method thereof

The invention relates to the technical field of magnet materials, and discloses a high-temperature-resistant neodymium-iron-boron magnet and a preparation method of the high-temperature-resistant neodymium-iron-boron magnet. The high-temperature-resistant neodymium-iron-boron magnet comprises the following components in parts by weight: 25-30 parts of neodymium, 60-65 parts of iron, 1.0-2.0 parts of boron, 3.0-5.0 parts of lanthanum, 0.5-2.0 parts of zirconium, 0.5-1.0 part of molybdenum and 0.1-0.5 part of nano ceramic particles, and the invention further provides a preparation method of the high-temperature-resistant neodymium-iron-boron magnet. S1, preparing and mixing alloy raw materials; s2, nano ceramic coating treatment is carried out; s3, magnetic field assisted pressing forming; and S4, rapid induction sintering. Through the magnetic field assisted directional pressing process, effective control over grain orientation in the pressing forming stage is achieved, magnetic domain arrangement is more ordered, and the residual magnetism and the energy product are improved. Different from a forming mode with disordered grain directions and poor magnetic anisotropy in an existing common cold pressing process, the technical defect that the utilization rate of magnetic performance is low due to poor orientation is overcome.
Owner:YUYAO HONGWEI MAGNETIC MATERIAL TECH CO LTD

Microwave neodymium lamp

The microwave neodymium lamp is composed of a magnetron, a rectangular waveguide, a resonant cavity and a quartz lamp tube, the magnetron is powered by a transformer to generate 2.45 GHz microwaves, and the 2.45 GHz microwaves are transmitted to the rectangular waveguide through a transmitting antenna. The Nd I < 3->-Na system neodymium compound in the quartz lamp tube is excited to emit light by coupling a cone resonant cavity through a slit with a specific size. The ideal microwave light source with the lighting effect larger than 150 Lm / W and the color rendering index higher than 95 can be provided.
Owner:HEBEI XIANGRUIXIN PHOTOELECTRIC TECH CO LTD

A magnetic elastomer and method of preparing the same

A magnetic elastomer and a method of preparing the same are provided. The magnetic elastomer includes the following components based on the total weight of the magnetic elastomer, 50 wt %-85 wt % of a magnet powder, 5 wt %-30 wt % of a binder, and 1 wt %-30 wt % of a processing aid. The magnet powder includes samarium iron nitrogen magnet powder and / or neodymium iron nitrogen magnet powder. When present, the samarium iron nitrogen magnet powder has an x50 particle size of less than or equal to 2.4 μm; when present, the neodymium iron nitrogen magnet powder has an x50 particle size of less than or equal to 2.0 μm.
Owner:NINGXIA MAGVALLEY NOVEL MATERIALS TECH CO LTD