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2605 results about "Organic dye" patented technology

Graphene/silver phosphate composite visible light photocatalyst and preparation method thereof

The invention discloses a high-efficiency graphene/silver phosphate composite visible light photocatalyst and a preparation method thereof, belonging to the technical field of composite materials and environmental management photocatalysis. The preparation method comprises the following steps: dissolving graphene oxide in water, and carrying out ultrasonic treatment to obtain a graphene oxide dispersed liquid; dissolving silver nitrate in deionized water, gradually and dropwisely adding into the graphene oxide dispersed liquid while stirring to obtain a mixed solution, uniformly stirring, and aging; dropwisely adding a prepared disodium hydrogen phosphate or sodium dihydrogen phosphate solution into the graphene oxide-silver nitrate mixed solution, continuing stirring, transferring into a hydrothermal reaction kettle, carrying out hydrothermal reaction, and cooling to room temperature; and washing the reaction product, and carrying out vacuum drying to obtain the visible light photocatalyst. The invention has the advantages of wide material sources and simple preparation process; and the obtained composite material has the advantages of controllable structure and regular pattern, and has high-efficiency degradation effect on organic dyes rhodamine B and methylene blue with certain concentration under the visible light irradiation.
Owner:JIANGSU UNIV

Preparation method and application method of titanium dioxide nanosheet supported MIL-100 (Fe) composite photocatalysis material

The invention relates to a preparation method and application method of a titanium dioxide nanosheet supported MIL-100 (Fe) composite photocatalysis material, belongs to the field of titanium dioxide photocatalysis, and especially relates to the field of titanium dioxide nanosheet supported porous metal organic skeleton (MOFs) composite materials. The preparation method comprises the following steps: 1, uniformly stirring tetrabutyl titanate and hydrofluoric acid at normal temperature, putting the obtained mixture in a hydrothermal reaction kettle, carrying out a reaction, separating the obtained material, washing the separated material, and drying the washed material to obtain titanium dioxide nanosheets; and 2, uniformly dispersing the titanium dioxide nanosheets in an anhydrous ethanol solution of iron trichloride, carrying out magnetic stirring at normal temperature for 15 min, carrying out suction filtration separation to obtain a product, dispersing the product in an anhydrous ethanol solution of trimesic acid, carrying out a 50-80 DEG C water bath reaction for 20-50 min, carrying out suction filtration separation to obtain a product, and repeating above processes in step 2 2-50 times to obtain the titanium dioxide nanosheet supported MIL-100 (Fe) composite photocatalysis material. The catalyst prepared through the method is especially suitable for catalytic degradation of high-concentration organic dyes (such as methylene blue) under visible light irritation) to reach a very high degradation rate.
Owner:UNIV OF SCI & TECH BEIJING

Preparation method of graphene-based composite separation membrane device

The invention discloses a preparation method of a graphene-based composite separation membrane device. The preparation method comprises the following steps of (1) dissolving a graphene oxide raw material in deionized water to be processed in ultrasonic bath to obtain the graphene oxide solution; (2) mixing and blending the graphene oxide solution with alkali under a given temperature, and then washing the mixture with deionized water to obtain the reduced graphene oxide dispersion liquid; (3) pouring the graphene dispersion liquid into a suction filtering flask to be filtered, and drying the graphene dispersion liquid in a vacuum drying box to obtain a graphene-based composite separation membrane; and (4) placing the graphene-based composite separation membrane inside a filtering device to obtain the graphene-based composite separation membrane device. The preparation method is simple and convenient, low in cost and environment-friendly, is suitable for industrialized mass production, has high separation efficiency, large water flux and good flexibility, is resistant to acid, alkali and high temperature and can be used in the fields of water treatment, solvent separation, nano-particle screening and the like. The separation membrane device can realize high-efficient separation of nano particles, organic dye, biological hormenes and metal salt.
Owner:ZHEJIANG UNIV
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