The invention relates to a preparation method and application method of a 
titanium dioxide 
nanosheet supported MIL-100 (Fe) composite 
photocatalysis material, belongs to the field of 
titanium dioxide 
photocatalysis, and especially relates to the field of 
titanium dioxide 
nanosheet supported 
porous metal organic skeleton (MOFs) composite materials. The preparation method comprises the following steps: 1, uniformly stirring tetrabutyl 
titanate and 
hydrofluoric acid at normal temperature, putting the obtained mixture in a 
hydrothermal reaction kettle, carrying out a reaction, separating the obtained material, washing the separated material, and 
drying the washed material to obtain 
titanium dioxide nanosheets; and 2, uniformly dispersing the 
titanium dioxide nanosheets in an 
anhydrous ethanol solution of iron trichloride, carrying out magnetic stirring at normal temperature for 15 min, carrying out suction 
filtration separation to obtain a product, dispersing the product in an 
anhydrous ethanol solution of 
trimesic acid, carrying out a 50-80 DEG C water bath reaction for 20-50 min, carrying out suction 
filtration separation to obtain a product, and repeating above processes in step 2 2-50 times to obtain the 
titanium dioxide nanosheet supported MIL-100 (Fe) composite 
photocatalysis material. The catalyst prepared through the method is especially suitable for 
catalytic degradation of high-concentration organic dyes (such as 
methylene blue) under visible light 
irritation) to reach a very high degradation rate.