364 results about "Organic dye" patented technology

The invention belongs to the technical field of organic dye synthesis and application, and discloses a conjugated compound containing a benzothiophenazine structure as well as a preparation method and application thereof, and the conjugated compound containing the benzothiophenazine structure has excellent photophysical properties, singlet oxygen yield and superoxide anion generation capacity. The novel conjugated compounds ENBO-NI and ENBS-NI containing benzothiophenazine structures are successfully prepared by replacing a benzene ring of Nile blue with a cycloalkane structure and adjusting the electron donating ability of an R1 group. The two compounds have near infrared fluorescence emission, good solubility and relatively high ROS yield. Compared with a classical photosensitizer NB, the singlet oxygen yield of ENBO-NI is increased by about 117.65%, and the singlet oxygen yield of ENBS-NI is as high as 70%. The absorption wavelength of the conjugated compound is in a red light wave band. The preparation process is simple and efficient, large-scale production is easy, and the preparation method has a wide clinical application prospect.

The embodiment of the invention relates to the field of photomasks, and provides a photomask protective film frame and a preparation method thereof, the photomask protective film frame comprises a frame main body made of a metal material and a coating formed on the surface of the frame main body, and the photomask protective film frame is characterized in that the coating is at least composed of carbon black, silicon dioxide particles and organic dye. The nanoscale carbon black in the coating has a high light absorption coefficient, fills gaps of dye molecules and forms a continuous light absorption network, the organic dye enhances absorption of light with specific wavelength through a molecular structure conjugated system, and the nanoscale carbon black and the organic dye form a composite function of broad-spectrum absorption and accurate waveband adjustment, so that more than 95% of light is absorbed in a broad-waveband range, light reflection on the surface of the frame is reduced, and the light absorption efficiency is improved. Pattern distortion caused by reflected light in the photoetching process is avoided, silicon dioxide is embedded into an organic dye matrix, silicon dioxide gaps are filled with carbon black particles, the porosity of the coating is reduced, the wear resistance of the coating is improved, and the cracking risk of the coating is reduced. Optical absorption, wear resistance and weather resistance are synchronously improved.

The invention discloses an MOF-loaded tobacco cellulose aerogel material as well as a preparation method and application thereof, and relates to the technical field of composite materials. Wherein the MOF-loaded tobacco cellulose aerogel material presents a loose and porous appearance, and comprises tobacco cellulose aerogel and an MOF material coated on the surface of the tobacco cellulose aerogel. According to the preparation method, the MOF material is generated on the surface of the tobacco cellulose aerogel in situ, so that a large amount of MOF material is exposed on the surface of the tobacco cellulose aerogel. Through specific adsorption of the MOF material, the effect of efficiently removing the organic dye Congo red by the MOF-loaded tobacco cellulose aerogel material is achieved.

The invention belongs to the technical field of near-infrared organic dye synthesis, and particularly discloses a cyanine dye with J aggregation characteristic, J aggregation nanoparticles, and preparation methods and applications of the cyanine dye and the J aggregation nanoparticles. The cyanine dye is 1-ethyl-2-(2-(2-(-3-(2-(1-ethyl-3, 3-dimethyl-1, 3-dihydro-2H-benzo [g] indole-2-subunit) ethylidene)-2-(2, 2, 2-trifluoro-N-(2-methylbenzyl) acetamide) cyclopent-1-ene-1-yl) vinyl)-3, 3-dimethyl-3H-benzo [g] indoleiodised salt, and the structural formula of the cyanine dye is shown in the description. The preparation method is simple, the J aggregation nanoparticles can be prepared by utilizing the unique property of J aggregation, the J aggregation nanoparticles have high light stability and have strong fluorescence emission in a near-infrared second region, and the material prepared by the invention can be used as a contrast agent and is applied to the field of near-infrared second region fluorescence imaging.

The invention provides a dye / ion separation membrane with pore diameter and charge coordinated regulation and control as well as a preparation method and application thereof, and belongs to the field of preparation of a double-layer ionic covalent organic framework (COFs) composite membrane. An aromatic polyamide ultrafiltration membrane is used as a base membrane, and a double-layer COFs membrane is constructed on the surface of the aromatic polyamide ultrafiltration membrane through a multi-time interfacial polymerization method. The first layer is a positive charge COFs layer formed by reacting a guanidyl monomer with 1, 3, 5-triformyl phloroglucinol (Tp); and the second layer is a negative charge COFs layer formed by reacting ionic aromatic diamine with Tp. By adjusting the type and concentration of the monomers, the pore diameter and charge distribution of the film layer can be synergistically regulated and controlled, and the double-layer composite film which is stable in structure and orderly stacked is constructed. The obtained membrane has molecular sieve separation and electrostatic regulation functions, can efficiently intercept organic dye molecules in high-salt printing and dyeing wastewater, and has high flux, high selectivity and good chemical stability.

The invention discloses an asymmetric magnetic mesoporous carbon superstructure material as well as a preparation method and application thereof. The preparation method comprises the following steps: (1) preparing Fe3O4amp; a SiO2 alcohol dispersion liquid; (2) preparing Fe3O4 < 4 > amp; the preparation method comprises the following steps: preparing a SiO2 (at) micro single micelle superstructure alcohol solution; (3) preparing Fe3O4 < 4 > amp; a SiO2 (at) C superstructure material; the specific surface area of the material is 87-116 m < 2 > / g, the aperture is 22.8-50 nm, and the length is 330-400 nm. The material is applied to catalytic degradation of organic dyes. The method has the beneficial effects that the surface chemical property is more active, the hydrophilicity and the catalytic degradation capability are stronger, the method is suitable for chemical catalytic degradation, the whole synthesis process is simple and convenient to operate, and intermediate byproducts cannot be generated to cause secondary pollution; in addition, in the dopamine carbonization process, high-temperature carbonization is carried out in nitrogen (inert atmosphere), and the operation is safe; by adjusting the type of the PS-PVP-PEO single micelle, accurate control of the mesoporous size can be realized, so that the PS-PVP-PEO single micelle is suitable for catalytic degradation of organic pollutants with different molecular weights, and selective catalytic degradation is realized.

The invention relates to the technical field of organic dyes, in particular to a novel xanthene dye for blue photoresist color paste and a synthesis method of the novel xanthene dye. The invention relates to a synthesis method of a novel xanthene dye for blue photoresist color paste, which comprises the following steps: 1) taking rigid cyclic amine as a nucleophilic reagent, and carrying out aromatic nucleophilic substitution reaction on a chlorinated xanthene compound to obtain a xanthene intermediate; 2) performing chlorination reaction on the xanthene intermediate by using a chlorination reagent to obtain a chlorinated xanthene intermediate; 3) mixing active amine and the chlorinated xanthene intermediate, and performing substitution reaction under the action of alkali to obtain the novel xanthene dye for the blue photoresist color paste.The novel xanthene dye for the blue photoresist color paste.The novel xanthene dye for the blue photoresist color paste.The novel xanthene dye for the blue photoresist color paste.The novel xanthene dye for the blue photoresist color paste has the advantages of being high in solubility, good in thermal stability and high in contrast ratio.

To provide an optical filter advantageous for exhibiting desired transmissivity characteristics even without comprising a near infrared ray reflection film.SOLUTION: An optical filter 1a comprises a first light absorber 11 and a second light absorber 12. The first light absorber 11 contains an organic dye. The second light absorber 12 contains a copper component, and absorbs at least part of infrared rays. The optical filter exhibits a first transmission spectrum satisfying the following conditions: (I) an average value TA450-600 of a transmissivity in a wavelength range of 450 nm to 600 nm is 76% or more; (II) a first cutoff wavelength λF falls in a range of 360 nm to 450 nm; (III) a second cutoff wavelength λS falls in a range of 600 nm to 700 nm; and (IV) a maximum value TM700-750 of a transmissivity in a wavelength range of 700 nm to 750 nm is 5% or less.SELECTED DRAWING: Figure 1

The invention discloses a colored aluminum pigment and a preparation method and application thereof.The colored aluminum pigment comprises aluminum paste, a first polymer resin layer, an organic dye layer and a second polymer resin layer, the surface of the aluminum paste is coated with the first polymer resin layer, and the surface of the first polymer resin layer is subjected to acid group modification; the colored aluminum pigment is prepared by the following preparation method: preparing aluminum powder coated with a first polymer resin layer; performing surface modification on the aluminum powder coated with the first polymer resin layer to obtain surface modified aluminum powder; performing air impact coating on organic dye and the surface modified aluminum powder to obtain a colored aluminum pigment substrate; and coating a second polymer resin layer on the surface of the colored aluminum pigment substrate. The aluminum pigment is subjected to multi-layer coating, organic dye and the surface modified aluminum powder are subjected to air impact coating, and the aluminum pigment has excellent aging resistance, is bright in color and is not prone to falling off.

The present invention discloses a magnetic yak hair-based biomass activated carbon, as well as its preparation method and application. The magnetic yak hair-based activated carbon is prepared by a two-step process of mixing Fenton iron mud with yak hair activated carbon, based on the carbonization and activation of yak hair. The activated carbon has a maximum specific surface area of ​​2632 m² / g and can be separated from a solution using magnetism. It can be used for the efficient adsorption of water pollutants such as organic dyes and antibiotics.

The invention provides a fluorescence sensor 4-MU (at) ZIF-8 (at) PLA-PEG as well as a preparation method and application thereof, and belongs to the technical field of visual food safety monitoring materials. The fluorescence sensor comprises a zeolite imidazate framework ZIF-8, an organic dye molecule 4-MU and a polymeric macromolecule PLA-PEG (Polylactic Acid-Polyethylene Glycol), the organic dye molecule 4-MU is coated with the zeolite imidazate framework ZIF-8 to form 4-MU (ZIF-8 nano particles with a core-shell structure, and the 4-MU (ZIF-8 nano particles with the core-shell structure are doped into a polymeric macromolecule PLA-PEG (Polylactic Acid-Polyethylene Glycol). The ZIF-8, 4-MU and PLA-PEG in the fluorescence sensor provided by the invention can cooperate with each other, can visually detect TCs with high response speed and low detection limit, and has certain mechanical properties and antibacterial properties, thereby providing a new thought for the field of intelligent packaging for detecting TCs in food at present.

The invention relates to the related technical field of costume fabrics, in particular to a high-antibacterial anti-sunshine costume fabric not prone to fading and a preparation technology, the high-antibacterial anti-sunshine costume fabric comprises a base fiber layer, and an antibacterial finishing layer, an anti-ultraviolet layer and a color fastness enhancing layer are arranged on the base fiber layer. According to the high-antibacterial anti-sunshine clothing fabric not prone to fading and the preparation process, a nano-silver and chitosan composite system is adopted, nano-silver releases silver ions to destroy the physiological structure of bacteria, chitosan inhibits the activity of the bacteria through the amino effect, the nano-silver and the chitosan cooperate with each other, the antibacterial effect of clothing is improved, nano-zinc oxide and titanium dioxide composite sol improve the antibacterial effect of the clothing, and the antibacterial effect of the clothing is improved. Through multiple mechanisms of reflecting, scattering and absorbing ultraviolet rays, broadband protection is formed, the ultraviolet rays can be effectively blocked, the high-grade sunscreen requirement is met, the skin is protected from being damaged by the ultraviolet rays, the sulfonic-group-containing organic dye fixing agent, dye molecules and fibers form chemical bond combination, a stable color fixing network is constructed, and the appearance color and luster are kept lasting.

A three-dimensional printing kit can include a polymeric build material including from about (80) wt % to (100) wt % polymer particles having an average particle size from about (10) μm to about (150) μm, and can also include a fusing agent including an aqueous liquid vehicle and from about (2) wt % to about (20) wt % of a mixture of organic dye radiation absorbers. The mixture of organic dye radiation absorbers can include a charged yellow water-soluble organic dye and a cyan water-soluble organic dye. The mixture of the organic dye radiation absorbers can be from about (1) wt % to about (40) wt % soluble in water.

The invention discloses a layered nano-porous copper loaded cuprous oxide / copper oxide nanowire composite material as well as a preparation method and application thereof. The material is a thin strip and comprises an amorphous substrate thin strip, multiple layers of nano-porous copper covering an amorphous substrate and a cuprous oxide / copper oxide two-component heterojunction nanowire loaded on the surface of the nano-porous copper. The preparation method comprises the following steps: firstly, freely dealloying an amorphous ribbon, and adding PVP (Polyvinyl Pyrrolidone) into dealloying corrosive liquid to generate layered nano-porous copper; then, copper hydroxide nanowires grow on the surface of each layer of nano-porous copper in situ through the anodic oxidation technology; and finally, converting the copper hydroxide into cuprous oxide / copper oxide nanowires with different component proportions by regulating and controlling the temperature by adopting a heat treatment process. The prepared composite material has a larger specific surface area and more active sites, and has unique structure and performance advantages in the field of photocatalytic degradation of organic dyes.

The application relates to the field of graphene preparation, and particularly provides a method for preparing reduced graphene oxide (rGO) by visible light in an aqueous solution, which uses an LED lamp simulating the visible light section of sunlight as a light source under normal temperature and pressure, and reduces industrial-grade graphene oxide (GO) to prepare rGO in a homogeneous aqueous solution system in the presence of an organic dye molecule eosin Y (water-soluble) as a photosensitizer and triethylamine as an electron sacrificial agent. The method overcomes the shortcomings of a low yield, the need for a strong reducing agent and high pollution in a traditional preparation process, and has the advantages of simple process, easy separation, high yield, low energy consumption, low cost and no pollution, and the prepared rGO has a smooth structure, a thin thickness and a perfect graphitization degree.

The invention discloses an adsorption and recovery device and process based on organic dye in a water body, and relates to the technical field of wastewater treatment. The recycling pool is arranged on the upper end face of the workbench; the collecting box is arranged on the upper end face of the supporting frame; the discharging assembly is arranged on the left side of the recycling pool and used for adding a reactant into the printing and dyeing wastewater; the recycling assembly is arranged on the upper side of the recycling pool and is used for recycling organic dye in the printing and dyeing wastewater; when an electric sliding block moves to the right arc surface part of a guide frame, a second motor controls an elastic adsorption plate to eccentrically rotate through an eccentric shaft, and the elastic adsorption plate can fully adsorb organic dye on the surface of an arc-shaped adsorption plate under the superposition of elastic release acting force generated by limiting of a fixed scraping plate and eccentric rotating force of the eccentric shaft; and then the organic dye moves into the matching frame and is limited by the fixed scraping plate to scrape out the adsorbed organic dye, so that efficient collection of the organic dye is realized.

Fe—Co core-shell nanospheres and a method for producing the Fe—Co core-shell nanospheres are disclosed. Further disclosed is a method of reducing an organic contaminant in a solution by mixing the Fe—Co core-shell nanospheres with the solution. The Fe—Co core-shell nanosphere includes a shell made of a material having a formula CoxFeyO(x+1.5y) and a hollow core. The Fe—Co core-shell nanospheres are produced by mixing cobalt nitrate and iron nitrate in a solvent mixture to form a first mixture and mixing urea with the first mixture to form a second mixture. The solvent mixture is removed from the second mixture to form a powder. The powder is ground to form the Fe—Co core-shell nanospheres.

The invention discloses a preparation method of a sodium alginate / polyphenol Pickering emulsion gel bead adsorbent and an adsorption application of the sodium alginate / polyphenol Pickering emulsion gel bead adsorbent. According to the adsorbent, polyphenol particles serve as a stabilizer, light oil serves as an oil phase, sodium alginate serves as a water phase to construct a low-density Pickering emulsion, then the obtained emulsion is dropwise added into a calcium chloride solution to be cured to form gel beads, and the obtained gel beads serve as the adsorbent with the self-suspension property. The self-suspension gel bead adsorbent designed by the invention is regular and controllable in shape, simple and rapid in preparation process, low in cost and easy for industrial production, has excellent adsorption capacity on various pollutants such as organic dyes, heavy metal ions and antibiotics, is simple and convenient to recycle after adsorption, and has a good application prospect in the field of water treatment.

The invention belongs to the technical field of organic dyes, and particularly relates to an anti-ultraviolet dye taking tannic acid as a coupling component as well as a preparation method and application of the anti-ultraviolet dye. Under a stirring condition, adding a diazonium salt solution of an arylamine derivative into the mixed solution for reaction, and continuously stirring for reaction after the diazonium salt solution is added, so as to obtain a reaction solution; adjusting the pH value of the reaction liquid, evaporating, filtering and drying to obtain the anti-ultraviolet dye taking tannic acid as the coupling component. The uvioresistant dye taking tannic acid as a coupling component can endow real silk with color and uvioresistant function during dyeing; the dyeing process is simple and short in time, damage to real silk is small, dye liquor composition is simple, follow-up wastewater is easy to treat, and the whole dyeing process is low-carbon and environment-friendly.

The invention relates to a preparation method of a perovskite type ferroelectric material photo-piezoelectric catalyst (MBA2-XDFCBAX) CuCl4 nanocrystal, which comprises the following steps: (1) preparing an organic phase solution, and dissolving 0.4 (2-X) mmol of MBA-Cl powder and 0.4 X mmol of DFCBA-Cl powder in 1ml of DMF (Dimethyl Formamide); (2) preparing an inorganic phase solution, taking 1ml of DMF (Dimethyl Formamide), dissolving 0.4 mmol of CuCl2. 2H2O powder, and adding 250ml of oleic acid; (3) mixing and reacting the two-phase solution for 10 minutes, injecting into 40 milliliters of vigorously stirred ethyl acetate, centrifuging, washing for three times, and drying to obtain synthesized substance powder; and (4) carrying out photo-piezoelectric catalytic degradation on the organic dye Sudan red (III) by using the catalyst. The synthesis method can be operated at room temperature and is low in cost. The catalyst does not contain heavy metal elements harmful to the environment, and is an environment-friendly green catalyst.

The invention provides spherical lignin-phenolic resin, a preparation method thereof and application of the spherical lignin-phenolic resin in adsorption of N-containing organic dye, and belongs to the technical field of adsorption materials. The lignin-phenolic resin with the regular spherical morphology can be prepared through a one-step condensation polymerization reaction by taking lignin, hydroquinone and trioxymethylene as raw materials under an acidic catalysis condition and adopting a reversed-phase suspension polymerization method, the lignin belongs to a renewable resource and has the characteristics of low cost and environmental friendliness, and the lignin-phenolic resin can be used for preparing the lignin-phenolic resin with the regular spherical morphology. The phenolic resin can replace phenols to become a main phenol source, the substitution rate can reach 75%, and the yield of the synthesized phenolic resin reaches up to 60-80%. Besides, abundant phenolic hydroxyl groups, sulfonic acid groups and other oxygen-containing groups can be introduced into the resin by selecting the types of monomers, the cross-linked structure of the resin is changed by regulating and controlling the proportion of the monomers, the adsorption capacity of N-containing organic dyes is effectively improved, and efficient adsorption of rhodamine B and methylene blue can be achieved.

The display device according to this disclosure includes: a substrate including a display area and a non-display area; a plurality of light-emitting diodes (LEDs) disposed on the substrate; an encapsulation layer disposed over the plurality of LEDs; a touch sensing unit disposed on the encapsulation layer and including a plurality of touch electrodes; a plurality of organic dye patterns disposed on the touch sensing unit overlapping the light-emitting areas of the plurality of LEDs, and having a lower surface larger than the upper surface; and a black matrix exposing the upper surface of the plurality of organic dye patterns. Therefore, light is refracted from the side surfaces of the plurality of organic dye patterns to the upper surface of the plurality of organic dye patterns, thereby improving luminous efficiency.

This invention discloses a Sn3O4-Ag-Ag2O photoelectric material based on TiO2 nanotubes and its preparation method, belonging to the field of photoelectric materials technology. The invention uses a hydrothermal Sn3O4-Ag-Ag2O nanoparticle method on a TiO2 nanotube array to construct an indirect Z-type heterojunction. The material exhibits high photocatalytic activity in dye degradation and water decomposition to produce hydrogen. The prepared sample showed strong photocatalytic ability and stability in organic dye degradation and Cr(VI) removal, with a visible light-driven photocatalytic hydrogen production rate of 55.79 μmol·cm ‑2 ·h ‑1 Photoelectrocatalytic data and electron spin resonance (ESR) signal results indicate that the composite photoelectrode forms an indirect Z-type electron transfer pathway, providing guidance for the preparation of composite photoelectrode materials with high optical and photocatalytic properties. The Z-type heterojunction structure will show broad application prospects in the design and application of photocatalysts.

The application relates to the technical field of organic dyes, in particular to a double-active-group cationic modified anthraquinone reactive dye as well as a preparation method and application thereof. The preparation method of the double-active-group cationic modified anthraquinone reactive dye comprises the following steps: S1: dissolving 1-amino-4-sulfonic acid-1'-(N,N-dimethylpropylaminomethyl) anthraquinone in ice water, then adding melamine dropwise to carry out reaction, and obtaining an intermediate solution; S2: the intermediate solution is warmed to 20-25 DEG C, and hydroxyethyl sulfone sulfonate is added to carry out reaction; after the reaction is completed, salting-out is carried out, and the double-active-group cationic modified anthraquinone reactive dye is obtained, as shown in formula (1). The reactive dye is synergized through the cooperation of "double active groups + cationic adjustment + precise water-solubility design", can guarantee water-solubility and dyeing fastness, and can completely get rid of the dependence on a large amount of salt.

The invention discloses a plant-based water filtering material and a preparation method thereof, and relates to the technical field of filtering materials. When the plant-based water body filtering material is prepared, 4-(10, 15, 20-triphenyl porphyrin-5-yl) aniline sequentially reacts with acrylic acid-2, 3-epoxypropyl ester and zinc acetate to obtain an alkenyl porphyrin zinc complex; the preparation method comprises the following steps: reacting chitosan with an alkenyl porphyrin zinc complex to obtain modified chitosan; reacting the oxidized reed carbon with butyl trimethyl ammonium chloride to obtain modified reed carbon; preparing a spinning solution from polybutylene terephthalate, the modified chitosan and the modified reed carbon, and performing electrostatic spinning to obtain a fiber membrane; itaconic acid and alkenyl benzisothiazolinone are prepared into a finishing solution; and finishing the fiber membrane with the finishing liquid to obtain the plant-based water filtering material. The plant-based water filtering material prepared by the invention can adsorb and catalytically degrade organic dyes in wastewater and adsorb heavy metals, and also has an antibacterial effect.

The invention discloses a preparation method of a BiOBr / LaNiO3 nanofiber composite photocatalyst, which is characterized in that a perovskite material LaNiO3 prepared by electrostatic spinning is used as a carrier, and BiOBr is loaded on the fiber surface by a solvothermal method to form a heterojunction structure. According to the composite material, separation of photon-generated carriers is promoted through heterojunction of BiOBr and LaNiO3 nanofibers, and the catalytic activity under visible light is remarkably improved. The invention further discloses application of the prepared BiOBr / LaNiO3 nanofiber composite photocatalyst in degradation of rhodamine B. The degradation efficiency of the BiOBr / LaNiO3 nanofiber composite photocatalyst on rhodamine B can reach 93% within 90 min, and after four times of circulation, the composite material shows good circulation stability. The method has the advantages of being low in cost, high in stability, environmentally friendly and the like, and a green solution is provided for organic dye pollution control.

This invention discloses a cross-linked cyclodextrin polymer, its preparation method, and its applications, belonging to the field of compound synthesis and separation enrichment technology. This invention employs a Sonogashira coupling reaction to react α, β, and γ cyclodextrins with 2-, 3-, or 6-position fully iodine-substituted cyclodextrins with polyalkynyl groups, respectively, to obtain cross-linked cyclodextrin polymers with large specific surface areas and numerous cyclodextrin cavities. These polymers exhibit good separation effects for organic dyes, small organic molecule pollutants, and harmful components in cigarette smoke.

The application discloses a preparation method of nanocellulose / polyethyleneimine / MIL-101(Cr) composite porous material for efficiently capturing dyes and heavy metal ions in wastewater. First, Cr(NO3)3.9H2O is selected as a metal ion source, H2BDC is selected as an organic ligand, and water is selected as a solvent, and MIL-101(Cr) powder without fluorine is prepared through a hydrothermal synthesis method; then, CNF is selected as a green polymer matrix, PEI is selected as a functional reagent, and MIL-101(Cr) nano-filler is simply complexed with a crosslinking agent to prepare a series of new nanocellulose / polyethyleneimine / MIL-101(Cr) aerogels which are uniform and low in density, can efficiently absorb organic dyes and heavy metal ions in wastewater, and have a synergistic effect on simultaneously absorbing dyes and heavy metal ions in a binary system. The raw materials in the application are derived from biomass, have the advantages of biodegradability and good biocompatibility, and have the characteristics of easy availability, simple preparation method, short operation process, recyclability, environmental protection and economy. The application has a good application prospect in wastewater treatment and other industries.

The invention discloses an oil absorption type 3D photocatalytic degradation device, a preparation method and a seawater desalination system, and belongs to the technical field of seawater desalination, the oil absorption type 3D photocatalytic degradation device is used for carrying out photocatalytic degradation on organic dye in water and adsorbing oily pollutants in the water, the shape of the oil absorption type 3D photocatalytic degradation device is a 3D porous foam structure, and the aperture is 15-45 microns. The oil absorption type 3D photocatalytic degradation device disclosed by the invention not only is helpful for improving the evaporation rate of seawater, but also has adsorption and enrichment capabilities on oil stains and organic pollutants. The oil absorption type 3D photocatalytic degradation device has high evaporation efficiency, also has an efficient degradation effect on organic dyes such as methylene blue and the like, and meanwhile, the oil retention rate on various oils is 95% or above. The oil absorption type 3D photocatalytic degradation device disclosed by the invention has the advantages that the oil absorption type 3D photocatalytic degradation device can be used for purifying a water body containing organic dyes such as methylene blue while continuously and efficiently desalting seawater, and a new scheme with an application prospect is provided for the technical field of environment-friendly, low-cost and multifunctional solar seawater desalination.

The present invention relates to the field of organic dyes, and particularly to an azo disperse dye and a preparation method thereof. The method includes: 1. After the initial reaction of cyanoacetate and organic amine, continue to react with acetoacetate to prepare a pyridone compound; 2. Add an aromatic amine compound to an acid solution and carry out a diazotization reaction with a diazotizing reagent to obtain an aromatic amine diazonium salt solution; 3. Add the pyridone compound to the aromatic amine diazonium salt solution for a coupling reaction to obtain the product. The molecular structure of the azo disperse dye of the present invention has an alkyl chain segment with a "lipophilic-hydrophilic" structure, which is similar to the chain segment structure of polyester fiber and has high affinity, so it has good dyeing performance on fiber materials. At the same time, this alkyl chain segment can make the dye have good dispersibility in water, has the ability to wash off the floating color on the fiber surface, and has excellent wet treatment fastness performance on fiber materials.