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95 results about "Magnetic carbon" patented technology

Magnetic carbon. From organic matter to pencil lead, carbon is a versatile element. Now, another use has been found: magnets. One would not expect pure carbon to be magnetic, but for more than ten years scientists have suspected that carbon can be made to be magnetic by doping it with nonmagnetic materials, changing its order ever so slightly.

Magnetic carbon-loaded slow-release microbial agent as well as preparation method and application thereof

The invention discloses a magnetic carbon-loaded slow-release microbial agent which comprises an activated carbon carrier containing ferroferric oxide nanoparticles and a compound microbial bacterium composed of bacillus megatherium, bacillus mucilaginosus, white-rot fungi and pseudomonas, and the mass ratio of the compound microbial bacterium to the activated carbon carrier is (3-4): 30. The invention further discloses a preparation method and application of the magnetic carbon-loaded slow-release microbial agent. According to the magnetic carbon-loaded slow-release microbial agent disclosed by the invention, the activated carbon containing the ferroferric oxide nano-particles is used as a carrier to load the compound bacteria, so that the stability of the microbial bacteria is improved, the microbial bacteria can better resist the impact of the environment, the service life of the microbial bacteria is prolonged, and the slow-release effect of the microbial agent in the remediation of vegetable planting soil is achieved; the nutrient absorption of the vegetables is promoted.
Owner:NINGXIA UNIVERSITY

Quantitative nuclear magnetic carbon spectrum valuing method for azido polyether branching degree standard substance

The invention provides a quantitative NMR (nuclear magnetic resonance) carbon spectrum valuing method of an azide polyether branching degree standard substance, which is based on quantitative NMR and directly values the branching degree of the azide polyether branching degree standard substance under the condition of not using an internal standard substance. Compared with the existing branching degree valuing method, such as a differential scanning calorimetry and a gel chromatography, the valuing method disclosed by the invention does not need an internal standard or an external standard, does not need to establish a calibration measurement curve, is simple and convenient in data processing and calculation, high in detection sensitivity and good in valuing accuracy, can realize unattended operation and stable operation in the testing process, and is suitable for large-scale popularization and application. The method is suitable for valuing the azide polyether branching degree standard substance.
Owner:XIAN MODERN CHEM RES INST

Magnetic carbon material for efficiently removing degradable micro-plastics in sewage and preparation of magnetic carbon material

The invention relates to the technical field of sewage treatment, in particular to a magnetic carbon material for efficiently removing degradable micro-plastics in sewage and a preparation method thereof.The magnetic carbon material is characterized in that S1, FeCl2. 4H2O and FeCl3. 6H2O are evenly mixed according to the mass percent of (3-7): (2-6), and the obtained mixture is marked as A; s2, preparing a premix B; s3, obtaining a mixture C; s4, obtaining a mixture D; s5, obtaining a powder substance E; s6, completing preparation of the magnetic biochar adsorbent which has high adsorption removal performance and is easy to separate and recycle the micro-plastics. According to the magnetic carbon material for efficiently removing the degradable micro-plastics in the sewage and the preparation method of the magnetic carbon material, the biochar prepared from the waste straws in the agricultural production process is used as the raw material, and compared with adsorbents such as organic silicon materials and polyamide fibers, the used raw materials are low in cost and easy to obtain, the process is simple, and the requirements for a production line and equipment are low; meanwhile, the invention also has the effect of recycling wastes.
Owner:ZHENGZHOU UNIV

Magnetic toner

A magnetic toner comprising a toner particle comprising a binder resin and a magnetic body, wherein the binder resin comprises a styrene-acrylic resin, the styrene-acrylic resin comprises a monomer unit represented by Formula (1):where, in Formula (1), R1 represents a hydrogen atom or a methyl group; and R2 represents a linear alkyl group having CB carbon atoms, CB being an integer from 10 to 15; the magnetic body comprises an alkyl group having CM carbon atoms, on a surface of the magnetic body, CM being an integer from 4 to 20; CB and CM satisfy Formula (3):|CM−CB|≤10  (3), andin a cross-sectional observation of the magnetic toner using a transmission electron microscope, a coefficient of variation of an occupied area ratio of the magnetic body in a specific square grid, is 80.0% or lower.
Owner:CANON KK

Development method of magnetic sludge carbon, functional equipment for enhancing biological efficient treatment of wastewater and application of functional equipment

The invention belongs to the technical field of wastewater treatment, and discloses a development method of magnetic sludge carbon, functional equipment for strengthening efficient biological treatment of wastewater and application of the functional equipment. On one hand, a nitrogen-doped carbon precursor is prepared by co-fermentation of excess sludge and agricultural and forestry wastes, and an LDH structure is formed through iron-nickel bimetal loading, so that the magnetism and catalytic performance of the material are improved, and the biological treatment effect of wastewater is enhanced. On the other hand, periodic deformation of the gel filler is induced through the rotating magnetic field, and the mass transfer limitation of a traditional biological membrane is broken through; and in combination with dissolved oxygen gradient regulation and control and Fenton-like catalytic activity of magnetic carbon, an anoxic nitrification-micro-aerobic oxidation stage treatment system is constructed. The electromagnetic separation and ultrasonic regeneration system realizes dynamic recovery of magnetic carbon and regeneration of surface active sites, and ensures the long-term operation stability of the system.
Owner:SHUIYI HLDG GRP CO LTD

Preparation method of magnetic carbon quantum dots with high relaxation rate

The present invention relates to a preparation method of magnetic carbon quantum dots with high relaxation rate, comprising the following steps: (1) dissolving sp<supgt;3< / supgt> precursor and sp<supgt;2< / supgt> precursor in a solvent for solvothermal reaction to obtain a first mixed system; (2) redispersing the reaction product in water, performing suction filtration, and then adding gadolinium ions for hydrothermal reaction to obtain a second mixed system; (3) performing dialysis on the second mixed system to obtain magnetic carbon quantum dots with high relaxation rate. During the preparation process of the present invention, the reaction conditions are controllable and the product purification is simple. The obtained carbon quantum dots not only have the paramagnetism of gadolinium ions but also have the fluorescence characteristics of carbon quantum dots, and can be used as a probe for nuclear magnetic resonance relaxation-fluorescence dual-mode in vitro diagnostic technology to improve the accuracy of in vitro diagnostic technology.
Owner:SHANGHAI INST OF MICROSYSTEM & INFORMATION TECH CHINESE ACAD OF SCI

Confined range assembly method of superstructure magnetic material and product

The invention discloses a confinement assembly method of a superstructure magnetic material and a product, the method comprises the following steps: mixing natural plant saccharides, long-chain charged supermolecules and an HCl solution for reaction, and calcining to obtain carbon cluster particles; then under the action of long-chain charged supramolecules, Fe < 3 + > covers the surfaces of carbon cluster particles, a spherical upper-layer structure, namely a carbon material containing Fe < 3 + >, is assembled, and the carbon material containing Fe < 3 + > is subjected to secondary calcination to obtain a magnetic carbon spherical upper-layer structure, namely a superstructure magnetic material; the superstructure magnetic material prepared by the confinement assembly method has the characteristics of high reflection loss, low dielectric constant and good uniformity and dispersity, has excellent microwave absorption capability and radar cross section attenuation capability, and can be used as a wave-absorbing material.
Owner:XI AN JIAOTONG UNIV

Preparation method and application of coupling agent modified sludge-based magnetic carbon material

The invention discloses a preparation method and application of a coupling agent modified sludge-based magnetic carbon material, and the method comprises the following operation steps: (1) pyrolyzing a Fenton sludge raw material in a nitrogen protective atmosphere to obtain sludge-based magnetic charcoal; (2) placing the sludge-based magnetic biochar in a sodium hydroxide solution for oxidation hydroxylation, filtering, and drying to obtain oxidized magnetic biochar; and (3) preparing a 3-aminopropyltriethoxysilane (APTES) solution with the concentration of 0.1 g / L, dispersing the oxidized magnetic biochar obtained in the step (2) in the APTES solution according to the solid-to-liquid ratio of 1: 100 (g: mL), reacting for 24 hours at the temperature of 50 DEG C under the acidic condition, filtering and drying to obtain the coupling agent modified sludge-based magnetic carbon material. According to the method, the Fenton sludge solid waste is used as a carbon material precursor, meanwhile, an endogenous iron element is provided, synchronous carbonization and magnetization are achieved through pyrolysis, and therefore the micro-plastics in the water body can be efficiently removed.
Owner:GUANGXI UNIV

An oil displacement demulsifier and a preparation method thereof

The application relates to an oil-displacing demulsifier and a preparation method thereof. First, magnetic carbon nanotubes are prepared by depositing ferric chloride hexahydrate and copper sulfate pentahydrate on the surface of carbon nanotubes; second, hyperbranched polymers with terminal double bonds are prepared; then, the two are mixed to obtain hyperbranched grafted magnetic carbon nanotubes; finally, allyl polyoxyethylene ether is continuously polymerized in situ to obtain the oil-displacing demulsifier. The oil-displacing demulsifier prepared by the application is suitable for oil-displacing demulsification treatment of coking wastewater in the early stage. The coking wastewater is complex in composition, contains little oil, but contains a lot of organic components. The polyether with multiple branched chains can form a net trapping effect in the water body, so that oil and water can be quickly gathered and separated in an emulsified state, and the oil removal rate can reach more than 97%. Meanwhile, the demulsifier has magnetism, can be recycled through magnetic separation, and the oil removal rate can still reach more than 92% after ten cycles of demulsification. The oil removal effect is good with a small amount of addition, and the coking wastewater treatment process is simplified.
Owner:JIANGSU JIANLIN ENVIRONMENTAL PROTECTION TECH CO LTD

Magnetic carbon nanobelt wave-absorbing agent and preparation method thereof

The invention relates to the field of radar wave-absorbing materials, in particular to a magnetic carbon nanobelt wave-absorbing agent and a preparation method thereof. The magnetic carbon nanobelt wave-absorbing agent comprises nitrogen-doped carbon converted by polyimidazolium salt and magnetic nanoparticles carbonized and converted by ferric iron salt; the average particle size of the magnetic nanoparticles is 5nm-20nm, and the mass loading capacity of the magnetic nanoparticles is 20%-50%. The magnetic carbon nanobelt wave-absorbing agent provided by the embodiment of the invention can give consideration to dielectric loss and magnetic loss, and the wave-absorbing performance of the material is improved.
Owner:BAIMTEC MATERIAL CO LTD +1

Oxygen-rich vacancy manganese dioxide magnetic carbon-based composite catalyst, preparation method thereof and application thereof in activated peroxymonosulfate degradation of bisphenol s

The application discloses an oxygen-vacancy-rich manganese dioxide magnetic carbon-based composite catalyst and a preparation method and application thereof in activating peroxymonosulfate to degrade bisphenol S. Wheat straw is used as a biochar raw material to prepare magnetic biochar, which is dispersed into a MnSO4*H2O solution and stirred, KMnO4 solution is added and stirred, the obtained material is transferred into a hydrothermal high-pressure kettle with a quartz liner, the high-pressure kettle is then transferred to a set temperature, after the reaction is completed, the material in the high-pressure kettle is cooled to room temperature, the reacted material is then filtered, the filtered solid is separated through a magnetic field, the solid with magnetism is washed and dried to obtain a catalyst precursor, and the catalyst precursor is aged through an NH4Cl solution to obtain the composite catalyst MBMN rich in OVs. The MBMN composite catalyst prepared by the application has low raw material cost, simple preparation process and high practicability.
Owner:ZHEJIANG UNIV OF TECH

Magnetic carbon nanomaterial hydrogel, preparation method thereof and seawater desalination application

The application discloses a magnetic carbon nanomaterial hydrogel, a preparation method thereof and seawater desalination application. The magnetic carbon nanomaterial hydrogel comprises a hydrogel, carbon nanomaterial and magnetic nanoparticles distributed in the hydrogel. The preparation method comprises the following steps: 1) mixing the hydrogel, the carbon nanomaterial and the magnetic nanoparticles to obtain a mixed solution; 2) freezing the mixed solution obtained in the step 1) to obtain a frozen product; 3) thawing the frozen product obtained in the step 2); 4) repeating the freezing in the step 2) and the thawing in the step 3) to obtain the magnetic carbon nanomaterial hydrogel. The magnetic carbon nanomaterial hydrogel prepared by the application can realize dynamic compression self-drainage through geometric deformation of an elastic magnetic evaporation body under the action of a magnetic field, and can improve the water evaporation rate of a photothermal interface water evaporation body.
Owner:XIAMEN UNIV +1

Production process of diuron

The invention discloses a production process of diuron, and belongs to the technical field of synthesis of diuron. The preparation method comprises the following specific steps: adding 3, 4-dichlorophenyl isocyanate, toluene and a catalyst into a reaction kettle, mixing, heating to 22-24 DEG C, adding a dimethylamine aqueous solution, heating to 40-50 DEG C, reacting, cooling to room temperature, preserving heat for 0.5-1 hour, centrifuging, washing and drying to obtain diuron, the catalyst is a cobalt selenium oxide loaded by a nitrogen-doped magnetic carbon nanotube, and the cobalt selenium oxide is expressed as Co3O4-SeO2 / N-MCNTs. The catalyst can improve the yield and purity of diuron due to abundant active sites, good chemical stability and effective avoidance of side reactions; the catalyst not only has high catalytic efficiency and mild reaction conditions, but also can be magnetically separated and is easy to recycle, so that the production cost is reduced.
Owner:ANHUI GUANGXIN AGROCHEM

An immobilized biocatalyst, a preparation method thereof, and a method for synthesizing astaxanthin monoester

The present invention belongs to the field of astaxanthin synthesis, and particularly relates to an immobilized biocatalyst, a preparation method thereof, and a method for synthesizing astaxanthin monoester. The preparation method of the immobilized biocatalyst includes derivatizing a magnetic carbon support and immobilizing a biocatalyst solution on the derivatized magnetic carbon support. The immobilized biocatalyst obtained by the method provided by the present invention can efficiently catalyze the synthesis of astaxanthin monoester from free astaxanthin, and has a high yield of astaxanthin monoester. At the same time, it can effectively avoid magnetic loss caused by being removed from the material, solves the problem of difficult separation in the application of biocatalysts, and the obtained immobilized enzyme can be recycled.
Owner:INNER MONGOLIA KINGDOMWAY PHARMA LTD +2

Magnetic carbon tube modified TiN0.9 / NC electromagnetic wave absorbent and preparation method thereof

The invention relates to a magnetic carbon tube modified TiN0.9 / NC electromagnetic wave absorbent and a preparation method thereof. According to the technical scheme, the preparation method comprises the following steps: carrying out solvothermal reaction on titanate and 2-aminoterephthalic acid to synthesize an NH2-MIL-125 template; adding the NH2-MIL-125 template into an aqueous solution of metal salt and dopamine, and tightly wrapping a continuous metal ion hybridized polydopamine layer on the surface of the disc-shaped template through an oxidative polymerization effect between metal ions and a dopamine monomer; through dicyandiamide-assisted high-temperature carbon thermal reduction treatment, the surface of a product is coated with a large number of multi-walled carbon nanotubes generated through catalysis of magnetic metal nanoparticles, and the magnetic carbon tube modified TiN0.9 / NC electromagnetic wave absorbent is prepared. The preparation method is simple to operate and controllable in morphology and operation process, and the prepared magnetic carbon tube modified TiN0.9 / NC electromagnetic wave absorbent can effectively absorb electromagnetic waves and is high in reflection loss and large in effective absorption bandwidth.
Owner:WUHAN UNIV OF SCI & TECH +1

Solid-state luminous magnetic carbon dot fluorescent material as well as preparation method and application thereof

PendingCN120966469ANanoopticsSensorsCross linkerBASIC FUCHSIN
The invention provides a solid-state luminous magnetic carbon dot fluorescent material as well as a preparation method and application thereof. Ammonium ferric citrate is taken as an iron source, basic fuchsin is taken as a carbon source, polyethyleneimine is taken as a cross-linking agent, and magnetic Fe3O4 is formed through reaction of polyethyleneimine and ammonium ferric citrate; magnetic Fe3O4 and carbon dots formed by a carbon source are connected through dehydration condensation of amino of polyethyleneimine and carboxyl on the surface of basic fuchsin, the solid-state light-emitting magnetic carbon dot fluorescent material in which the carbon dots and the magnetic Fe3O4 are dispersed and are not in contact is obtained, AIQ does not occur in the aggregate, solid-state light emitting of the magnetic carbon dot fluorescent material can be achieved, and the magnetic carbon dot fluorescent material has good application prospects. The magnetic carbon dot fluorescent material can be applied to fingerprint extraction.
Owner:WENZHOU MEDICAL UNIV

Magnetic carrier composite biological agent and preparation method thereof

The invention discloses a magnetic carrier composite biological agent and a preparation method thereof. The preparation method comprises the following steps: preparing a nano magnetic carbon base; preparing a functional bacterium colony stock solution; preparing a nano magnetic carbon base / functional bacterium compound bacterium solution through the nano magnetic carbon base and the functional bacterium colony; preparing emulsified vegetable oil; preparing a magnetic carrier composite biological agent from the emulsified vegetable oil and the nano magnetic carbon-based / functional bacteria composite bacterial liquid; according to the prepared composite biological agent, the problems of insufficient tolerance under high concentration, low efficiency under low concentration, long repair period and the like of a biological method are solved at the same time, and finally efficient, long-acting and small-disturbance repair for halogenated hydrocarbon in a wide concentration range is achieved.
Owner:江苏省环保集团南通有限公司

Magnetic carbon aerogel with infrared-radar dual stealth function and preparation method thereof

The application discloses a magnetic carbon aerogel with infrared-radar dual stealth function and a preparation method thereof. First, nickel chloride hexahydrate, sodium hydroxide and cetyltrimethylammonium bromide are dissolved in ethylene glycol, hydrazine hydrate is added, and then the mixture is reacted under heating and magnetic field to prepare a nickel chain; then a silanol solution after hydrolysis and condensation is blended with a bacterial cellulose gel to prepare a BC precursor solution, the BC precursor solution is uniformly mixed with the nickel chain and a carbon material dispersion liquid, and then directional freezing and freeze drying are performed to prepare the magnetic carbon aerogel. The method effectively solves the technical problems that in the prior art, it is difficult for infrared-radar dual stealth materials to maintain low infrared emissivity and light weight while realizing wide-frequency, strong and stable radar wave absorption performance, especially after the introduction of a magnetic component, oxidation is easily caused, dispersion is uneven, and the infrared characteristics are deteriorated.
Owner:SHAANXI UNIV OF SCI & TECH

Method for preparing light magnetic carbon composite electromagnetic compatibility material by inducing chelate salt through carbon nitride

The invention belongs to the technical field of electromagnetic compatibility, and discloses a method for preparing a light magnetic carbon composite electromagnetic compatibility material by inducing chelate salt through carbon nitride, which comprises the following steps: 1, fully dispersing metal chelate salt and graphitized carbon nitride to form a uniform mixture; and 2, carrying out temperature programming calcination treatment on the uniform mixture to obtain the target magnetic carbon composite material. According to the present invention, the construction of the rich porous structure is achieved, the preparation process is simple and environmentally friendly, the template method adopted for the conventional porous structure inevitably comprises the introduction and the removal of the template agent in the whole production process, the use of the acid, the alkali or the oxidizing agent is involved, and the harm and the pollution are serious; the adopted carbon nitride template can be decomposed in the high-temperature pore-forming process for preparing the wave-absorbing agent, so that the problem of subsequent template removal is avoided.
Owner:SOUTH WEST INST OF TECHN PHYSICS

An efficient magnetic carbon-based adsorbent, its preparation method and application

The present invention discloses an efficient magnetic carbon-based adsorbent, its preparation method and application, belonging to the technical field of solid waste resource utilization. The preparation method includes: mixing the screened pyrometallurgical gold extraction waste residue with hydrochloric acid, performing a primary microwave reaction, then carrying out solid-liquid separation and washing to obtain a ferric-rich acid leaching solution; ball-milling blast furnace injection ash to obtain fine slag, mixing the fine slag with the ferric-rich acid leaching solution, performing a secondary microwave reaction, adjusting the pH to alkaline to obtain a mixed solution of iron hydroxide and carbon, filtering by suction to obtain an iron-carbon mixed filter residue, washing with water to neutrality, drying, and performing high-temperature pyrolysis under nitrogen to obtain the efficient magnetic carbon-based adsorbent. The present invention can improve the recycling rate of pyrometallurgical gold extraction waste residue while efficiently adsorbing and desorbing acidic copper chloride etching waste liquid.
Owner:SHAANXI LANJI NEW MATERIAL TECHNOLOGY CO LTD

Nitrogen-doped carbon nanotube array loaded magnetic carbon aerogel and preparation method thereof

The invention discloses nitrogen-doped carbon nanotube array loaded magnetic carbon aerogel and a preparation method thereof.The method comprises the steps that cobalt salt and nickel salt are evenly dissolved in a biomass precursor aqueous solution, and a homogeneous solution is formed; adding a cross-linking aid to construct a three-dimensional network, and wrapping metal ions; performing freeze drying after directional freezing to form a directional porous structure; carrying out heat preservation and carbonization, converting the biomass into a porous carbon matrix, and reducing the cobalt / nickel salt into a uniformly embedded CoNi alloy; through two-stage heat treatment, the nitrogen-rich organic matter is decomposed to release a nitrogen source, and the vertical carbon nanotube array grows in situ. The material integrates CoNi alloy magnetic loss, carbon matrix dielectric loss and multistage structure scattering effect, realizes dielectric-electromagnetic cooperation, optimizes impedance matching, avoids strong surface reflection caused by high conductivity of a single carbon material, introduces polarization loss, widens an absorption frequency band, has excellent broadband efficient electromagnetic wave absorption performance, and is suitable for a complex electromagnetic environment.
Owner:SHAANXI UNIV OF SCI & TECH

A tannin micro-environment confined bimetallic carbon-based catalyst, and a preparation method and application thereof

PendingCN122644121APtru catalystMagnetic carbon
The present application relates to a kind of tannin microenvironment limited bimetallic carbon-based catalyst and its preparation method and application.The zero-valent zinc-containing magnetic carbon nanotube (ZFC) prepared by iron ion modification and zinc powder sintering is solid-phase ground with waxberry tannin foam (TF), the tannin limited microenvironment is constructed in situ on the surface of catalyst, and finally the composite material (ZCF-TF) is prepared.The present application utilizes the high nucleophilic characteristics of polyphenol hydroxyl group of tannin, not only can in-situ capture leached free metal ions in the reaction system to realize "interface reconstruction", solve the problem of secondary pollution of heavy metal;More through the unique surface microenvironment, the local electronic structure of catalyst is changed, the traditional non-selective radical dilemma is successfully avoided, and the Fenton-like catalysis is changed into electron transfer (ETP) and singlet oxygen dominated non-radical path.The catalyst shows precise and efficient degradation ability to antibiotics in water body, and has strong anti-water quality background interference ability.
Owner:SICHUAN UNIV

Powder control structure of discontinuous interface

The utility model discloses a powder control structure of a discontinuous interface, which comprises a magnetic roller and a powder control sheet, and is characterized in that the powder control sheet comprises a cutter blade I and a cutter blade II, the top surface of the cutter blade I is contacted and rubbed with the magnetic roller, and the top surface of the cutter blade II is lower than the top surface of the cutter blade I, so that a step surface is formed on the side surface of the cutter blade I; and the magnetic carbon powder adsorbed by the magnetic roller from the powder bin can collide with the step surface to be rubbed. Therefore, the carbon powder is collided and rubbed with the step surface when passing through the position, so that the carbon powder is charged due to additional friction force, the upper layer and the lower layer of the magnetic carbon powder on the surface of the magnetic roller are easier to exchange, and the printing blackness and the carbon powder transfer printing rate are improved.
Owner:ZHUHAI BENMA PRINTMAX IMAGINE

A method for preparing a magnetic carbon-based functional material by using algal residue, the magnetic carbon-based functional material and application

The application discloses a kind of methods for preparing magnetic carbon-based functional materials using algal residue, magnetic carbon-based functional materials and applications, belong to new material technical field and energy saving and environmental protection technical field.The algal residue is impregnated with sodium hydroxide in the method, and then treated by metal salt impregnation, high-temperature anaerobic activation, washing and drying to obtain the magnetic carbon-based functional materials.The method has the characteristics of simple production process, easy-to-obtain raw materials and high product solid-liquid efficiency.The method realizes the resource utilization of algal residue, and the prepared new material can be widely applied to the field of environmental protection, especially the field of water treatment and tetracycline degradation technology, and has good economic and social benefits.
Owner:ANHUI SCI & TECH UNIV

Preparation method and production equipment of heteroatom-doped magnetic carbon material

The invention discloses a preparation method and production equipment of a heteroatom-doped magnetic carbon material, and the method comprises the following steps: 1, uniformly mixing a raw material with a metallocene catalyst to obtain a mixture, and uniformly dispersing the mixture in a closed reaction kettle; 2, after the closed reaction kettle is completely sealed, inert protective gas is introduced; and 3, carrying out heat treatment, naturally cooling to room temperature, and taking out a product, namely the heteroatom-doped magnetic carbon material. The production equipment comprises a closed reaction kettle and a heteroatom addition tank, the closed reaction kettle comprises a reaction kettle body and an equipment box body; a thermal insulation system is mounted on the outer wall of the reaction kettle body, and a temperature control system is mounted on the equipment box body; and the heteroatom addition tank is communicated with the inner cavity of the reaction kettle body through a pipeline. Graphene can be conveniently and rapidly modified, the purpose of stable modification is achieved, and the prepared magnetic carbon material has the advantages of being low in product cost, simple in process, easy to operate, good in repeatability and high in quality.
Owner:SHANXI ROAD & BRIDGE CONSTR GROUP +2

CoNi alloy loaded nitrogen-doped magnetic carbon aerogel as well as preparation method and application thereof

The invention discloses CoNi alloy loaded nitrogen-doped magnetic carbon aerogel as well as a preparation method and application thereof, according to the method, a directional freezing method, a pyrolysis method and a solvothermal method are adopted to load CoNi on biomass derived carbon aerogel in situ, and a honeycomb-like magnetic nitrogen-doped carbon aerogel composite wave-absorbing material loaded with CoNi and a preparation method of the CoNi-loaded honeycomb-like magnetic nitrogen-doped carbon aerogel composite wave-absorbing material are constructed. Through the dielectric loss of the carbon aerogel, the CoNi alloy particles in the carbon aerogel provide magnetic loss, and the dielectric-electromagnetic synergistic effect is beneficial to optimization of impedance matching of the wave-absorbing material. Meanwhile, the multiple reflection and scattering of the electromagnetic waves in the directional honeycomb structure also help the dissipation of the electromagnetic waves.
Owner:SHAANXI UNIV OF SCI & TECH

Method and device for removing multiple pollutants in flue gas by using cross electro-acoustic modified magnetic carbon

The invention provides a method and a device for removing multiple pollutants in flue gas by using cross electro-acoustic modified magnetic carbon, and belongs to the field of atmospheric pollutant control. The method comprises the following steps: in a cross electro-acoustic modification device, utilizing an electro-acoustic synergistic effect to jointly activate a multi-element reagent to induce active free radical modified magnetic carbon, and then utilizing the modified magnetic carbon to induce oxidizing substances to oxidize and absorb various pollutants such as Hg0, As2O3, H2S, PH3 and CO in industrial airflow in a light-bubble micro-jet reaction kettle. The method has the outstanding technical advantages of simple technical device, high synergistic removal efficiency of multiple pollutants, high mixing and mass transfer efficiency of reaction media, energy conservation, low carbon, green and environment-friendly modification process and the like, and has a good industrial development prospect.
Owner:JIANGSU UNIV

A demulsifier for tar ammonia water and a preparation method thereof

The application discloses a demulsifier for tar ammonia water and a preparation method thereof. The preparation method of the demulsifier for tar ammonia water comprises the following steps: step (1), FeCl3.6H2O and FeCl2.4H2O are added into a solvent, modified carbon black is added after stirring, ultrasonic treatment is conducted, ammonia water is added to adjust pH under stirring, separation, washing, and finally drying to constant weight to obtain magnetic carbon black; step (2), modified magnetic carbon black is prepared; step (3), carboxylated cyclodextrin, modified magnetic carbon black and a catalyst are added into water, stirring and reaction are conducted, separation, washing, and then drying to constant weight are conducted, and the demulsifier for tar ammonia water is obtained. The demulsifier with magnetism is prepared through modified carbon black, the demulsification capacity of the demulsifier is improved through synergistic effect of multiple groups, the prepared magnetic demulsifier can be reused, and has a good application prospect.
Owner:神美科技有限公司

Breathable, hydrophobic and low-reflection electromagnetic shielding fabric and preparation method thereof

The invention discloses a breathable, hydrophobic and low-reflection electromagnetic shielding fabric and a preparation method thereof, and the preparation method comprises the following steps: coating a coupling agent modified cotton fabric substrate with a magnetic carbon nanomaterial, then taking the coupling agent modified cotton fabric substrate as a receiving electrode, and taking a double-sided electrostatic spinning hydrophobic polyurethane microfiber film as an isolation protection layer. The magnetic carbon nanomaterial has good impedance matching and abundant loss mechanism, so that the fabric shows efficient electromagnetic shielding performance mainly based on absorption. Due to good conductivity, the shielding coating can be used as a receiving electrode for electrostatic spinning, electrostatic force attracts a spinning solution into gaps of the fabric, so that the isolating layer is tightly coated on the fabric, the use fastness of the shielding coating is further improved, and the shielding coating has a hydrophobic function. In addition, the electromagnetic shielding fabric also has excellent air permeability and comfortable hand feeling.
Owner:QINGDAO UNIV +1

Method for enhancing electricity generation of microbial fuel cell by interface modification of free magnetic-rich carbon three-dimensional anode and bacteria

The application provides a method for enhancing electricity generation of a microbial fuel cell by modifying the interface between a free magnetic carbon three-dimensional biological anode and bacteria, and the method adopts a solvothermal method to prepare a hydrophilic magnetic nano Fe3O4@ formed porous carbon composite material which has strong electromagnetic performance, a large specific surface area and high biocompatibility, can be used as a three-dimensional biological anode in a microbial fuel cell (MFC), is beneficial to the adhesion of microorganisms and maximizes the colonization space of the microorganisms, can promote the extracellular electron transfer efficiency of bacteria and enhance interspecies electron transfer between bacteria and archaea as an excellent electron medium, improves the conversion rate of a biological anode and the output of electrons, and enhances electricity generation of the MFC.
Owner:HAINAN UNIV