The invention belongs to the field of
analytical chemistry, and relates to a detection method of
chlorinated phenols in a
textile through hollow
fiber liquid-phase microextraction. The detection method comprises the steps of extracting a sample by using
acetone, after concentrating an extracting solution to nearly dry, dissolving by using normal
hexane to obtain a
solvent, then taking a porous hollow
fiber tube as a carrier of microextraction
solvent, and transferring all extracted
solvent into a high performance liquid chromatograph for subsequent
assay determination. The detection method provided by the invention has the advantages that a hollow
fiber tube liquid-phase microextraction method is adopted, namely, the hollow fiber tube is taken as the carrier of the microextraction solvent, the extraction, gathering, separation and purification are integrated into a whole, the extraction efficiency is high, the
organic solvent consumption is less, the extraction is fast and sensitive, and the like; according to experiment results, the
recovery rate and precision of the method both satisfy the demands, and the method can be used for the detection of chlorinated
phenol mildew preventives in the
textile, and has wide application prospect.