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1961 results about "Photocatalytic degradation" patented technology

High-capacity intermittent industrial wastewater microwave photocatalytic degradation device

The invention relates to a high-capacity intermittent industrial wastewater microwave photocatalytic degradation device, belonging to the technical field of wastewater treatment. The existing microwave photocatalytic degradation technology for the organic pollutant-containing industrial wastewater has the problems that microwave energy is wasted and practical single-jar wastewater treatment quantity is relatively small, and has the problem of scaling since an electrodeless ultraviolet lamp screen protector in the device is soaked in wastewater liquid by the outer side face of a quartz tube for a long term. The invention intends to solve the problems globally.In order to solve the problems, an electrodeless ultraviolet lamp is arranged in a silk screen cage-shaped nonopaque microwave restraining device made from metal material, the microwave is guided into the microwave restraining device to be restrained, the useless dissipation of the microwave can be stopped, and the designed volume of an expander can be allowed to be greatly enlarged on the basis of the structure, so that the single-jar wastewater treatment quantity of a reactor can be greatly improved. An ultrasonic transducer is attached to the outer side face of the side wall of the reactor, so that the scale can be timely removed after the high-frequency ultrasonic wave reaches up to the scale.
Owner:NINGBO UNIV

Bi/BiOCl (bismuth oxychloride) composite photocatalyst as well as in-situ reduction preparation method and application thereof

The invention relates to the technical field of nanometer materials and photocatalytic degradation of organic pollutants, and in particular relates to a Bi/BiOCl (bismuth oxychloride) composite photocatalyst as well as an in-situ reduction preparation method and application thereof. Bi nano-particles with particle sizes of 5-20nm are uniformly distributed on a BiOCl nanosheet with 100-600nm or a the surface of a BiOCl microsphere being 1-3 microns to obtain the Bi/BiOCl composite photocatalyst; the Bi/BiOCl composite photocatalyst is prepared by gaseous-phase in-situ reduction or liquid-phase in-situ reduction; as Bi nano-particles are formed on a BiOCl substrate in an in-situ manner, the lattice matching degree of interfaces between the Bi and the BiOCl is high and the charge migration is facilitated; the Bi nano-particles have the good dispersibility, are difficult to cause agglomeration, and have the good size and distribution controllability; the Bi nano-particles can be well combined with the BiOCl and are difficult to drop off, the photo catalytic capability of the BiOCl under the existence of ultraviolet light can be improved, the spectral response range is expanded, and the visible photo catalytic capability can be acquired, and the Bi/BiOCl composite photocatalyst can be effectively applied to photocatalytic degradation of organic pollutants in a water body.
Owner:HEFEI UNIV OF TECH

Composite material with anti-bacterial and purifying functions and preparation method of composite material

The invention relates to a composite material with anti-bacterial and purifying functions and a preparation method of the composite material, and belongs to the technical field of environmental-friendly materials. The composite material with the anti-bacterial and purifying functions comprises raw materials in parts by weight as follows: 70-95 parts of a mineral composite adsorption material, 3-25 parts of a photocatalytic degradation material, 2-15 parts of a rare earth inorganic anti-bacterial material and 1-10 parts of an additive, wherein the mineral composite adsorption material is prepared from sepiolite, diatomite, medical stone and attapulgite; the photocatalytic degradation material is prepared from titanium oxide, tourmaline and far infrared ceramic powder; the rare earth inorganic anti-bacterial material is prepared from zinc oxide, cerium oxide and silver oxide; the additive is a mixture of activated carbon, carboxymethylcellulose and pumice powder. The composite material with anti-bacterial and purifying functions has high adsorption and decomposition rate, can be resistant to water and damp and has excellent anti-bacterial effect. Meanwhile, the invention provides the preparation method. According to the preparation method, the cost is low, the amount of produced wastewater is low, and powder is simple and convenient to apply.
Owner:淄博木齐新材料科技有限公司

Omnidirectional antibacterial intelligent type air purifier for vehicle

The invention relates to an omnidirectional antibacterial intelligent type air purifier for a vehicle, which comprises a shell, an air purification component, a fan power component, an energy component, an induction sensor component, a negative-ion generator and a display intelligent control component. The omnidirectional antibacterial intelligent type air purifier for the vehicle uses a nano silver modified titanium dioxide as a photocatalyst, thereby increasing photocatalysis effect and sterilization antibacterial performance. The omnidirectional antibacterial intelligent type air purifier for the vehicle uses an ultraviolet light emitting diode as a ultraviolet light source, thereby guaranteeing the photocatalyst to be capable of playing the role of degrading pollutants efficiently. The inner surface and the outer surface of an enclosure all have antibacterial performance, thereby guaranteeing bacteria not to live on the surface of an airframe of the omnidirectional antibacterial intelligent type air purifier for the vehicle, and guaranteeing personal safety. The omnidirectional antibacterial intelligent type air purifier for the vehicle can automatically induct air conditions, adjusts purification power in real time, and has intelligent control function.
Owner:SHANGHAI NAT ENG RES CENT FORNANOTECH

Method for preparing concavo-convex rod soil/zinc oxide nanometer composite material

The invention discloses a method for preparing concavo-convex rod soil/zinc oxide nanometer composite materials, which comprises the following steps: purifying and dispersing the concavo-convex rod soil in water to prepare concavo-convex rod soil dispersion liquid; then adjusting the temperature of the concavo-convex rod soil dispersion liquid to 30 to 100 DEG C; agitating the concavo-convex rod soil dispersion liquid dispersion liquid and while adding zinc salt aqueous solution with the concentration of 0.3 to 3 mol.L<-1> and carbonate aqueous solution with the concentration of 0.3 to 2 mol.L<-1> to the concavo-convex rod soil dispersion liquid dispersion liquid; and keeping the pH value of mixed liquid within the range of 6.0 to 8.0. The prepared mixed serous fluid comprising the prepared nanometer concavo-convex rod soil and basic zinc carbonate is filtered; and a filter cake is washed by deionized water; when the electrical conductivity of filtrate is less than 300 MuS.cm<-1>, the washing is finished; and the filter bake obtained is dried at the temperature of below 100 DEG C, then baked for 1 to 10 hours at the temperature of 300 to 600 DEG C, and finally crushed. The invention is simple and has the advantages of low energy consumption and high safety; the load of the adsorbing material prepared is uniform and has good dispersibility, strong adsorbability and remarkable photo-catalyzed degradation property.
Owner:JIANGSU POLYTECHNIC UNIVERSITY +1

Silver-modified carbon nitride composite photocatalytic material and preparation method thereof

The invention relates to a silver-modified carbon nitride composite photocatalytic material and a preparation method thereof. The preparation method comprises: dissolving dicyanodiamide or melamine in deionized water or dimethyl sulfoxide and performing ultrasonic dispersing, so as to obtain a dicyanodiamide or melamine dispersion liquid; dissolving silver nitrate in deionized water and stirring uniformly, so as to obtain a silver nitrate solution; slowly dropwise adding the silver nitrate solution into the above dicyanodiamide or melamine dispersion liquid under the condition of magnetic stirring, and continuing stirring the solution, so as to obtain a mixed precursor solution; using anhydrous ethanol and deionized water repeatedly wash the obtained mixed precursor solution for multiple times, and performing vacuum drying; and putting the obtained product in a proper crucible and covering, putting in a high-temperature furnace, and sintering for a period under the condition of nitrogen protection, so as to obtain a powdery sample. The advantages comprise that the raw material source is wide, the preparation technology is simple and practicable, and the cost is relatively low; and the prepared composite photocatalytic material has relatively good photocatalytic degradation effect on organic dye rhodamine B under irradiation of visible light.
Owner:JIANGSU UNIV

Preparation and application of hierarchical pore metal-organic framework loaded heteropolyacid catalyst

The invention discloses a preparation method and application of a hierarchical pore metal-organic framework loaded heteropolyacid catalyst. The catalyst adopts hydrothermal-extraction method for preparation. The method includes: dissolving an organic ligand, a template agent, a metal salt and Keggin type heteropolyacid in a solvent, conducting hydrothermal synthesis of a crystal product, and thenperforming Soxhlet extraction to obtain a catalyst. The obtained catalyst has a meso-micro hierarchical porous structure, realizes high dispersion of the active component heteropolyacid and ultra-highloading capacity, and at the same time solves the problems of large mass transfer resistance, long diffusion path and small reaction place in microporous materials. The catalyst provided by the invention shows excellent catalytic performance in both photocatalytic degradation of dye wastewater and catalysis of oxidation-extraction desulfurization reaction, the catalysis reaction uses visible light and hydrogen peroxide respectively, the process is clean, environment-friendly and green, and after repeated use, the catalyst still maintains high activity, and has high industrial application value.
Owner:CHINA UNIV OF PETROLEUM (EAST CHINA)

Preparation method of visible-light activated cuprous oxide/titanium dioxide nano-composite photocatalyst and applications thereof

The invention discloses a preparation method of a visible-light activated cuprous oxide/titanium dioxide nano-composite photocatalyst and applications thereof, belonging to the technical field of environmental pollution control. The preparation of the catalyst comprises the following steps of: 1) carrying out electrochemical oxidation reaction under the action of hydrofluoric acid with the concentration of 0.2 percent by weight for preparing a titanium dioxide nanotube electrode, wherein the tube diameter of a nanotube is about 80nm, and the tube length is 550nm; and 2) adopting a photoreduction chemical method to prepare the cuprous oxide/titanium dioxide nano-composite photocatalyst. The prepared composite photocatalyst has the advantages of simple synthesis, stable performance, the synthesis process belonging to the field of green chemistry and the like. The composition of cuprous oxide can not only reduce the defect of high composite probability of photoproduced electron-hole pairs, but also expand the light response range of the titanium dioxide nanotube electrode and further improve the photocatalytic degradation efficiency thereof to organic pollutants in the visible light range, thereby having very high practical value and application prospect.
Owner:DALIAN UNIV OF TECH

Multifunctional photocatalysis composite ceramic separation membrane as well as preparation method and use thereof

The invention belongs to the technical field of membrane and relates to a photocatalytic composite ceramic separation membrane using porous ceramic membrane as a carrier, a method for preparing the same and application of the separation membrane. The method is characterized in that a porous ceramic membrane substrate is used as the carrier to prepare hydroxyapatite sol and argent-titania composite sol through sol-gel technology; and a carrier membrane is subjected to secondary sol-gel dipping, drying and roasting sequentially to obtain the argent-carried titania/hydroxyapatite photocatalytic composite ceramic separation membrane with aperture of between 100 and 1,900 nm and porosity of between 20 and 55 percent. The photocatalytic composite ceramic separation membrane has biological adsorption and high photocatalytic activity and membrane permeability, improves separation of the composite membrane, photocatalytic degradation and sterilization, has remarkable effects of decontamination and sterilization, reduces the loss of porosity in the process of membrane preparation, has a simple preparation and application process, is easy for large-scale industrial production, integrates three units of membrane separation, photocatalytic degradation and sterilization and reduces investment and occupied area.
Owner:DALIAN UNIV OF TECH

Titanium dioxide nano tube electrode and its preparation process and application

The invention relates to a titanium dioxide nanometer tube electrode in the technology field of fathering the environmental pollution and its preparation method as well as its application. Its features lie in: choose the pure titanium or titanium alloy as the substrate, carry out the electrochemical oxidation in the condition of hydrofluoric acid with its density between 0.01wt% and 0.5wt%, form a titanium dioxide nanometer tube with its diameter between 40nm and 100nm and its length between 20nm and 50nm on the substrate vertically and get the integrative titanium dioxide nanometer tube electrode. The preparation features lie in: choose the substrate as the anode after grinding, etching and drying and the platinum sheet as the cathode, control the distance between the two electrodes between 10mm and 50mm, put them into the reactor, power on the stabilized voltage power supply with it voltage between 15V and 25V, after 1-to-30-minute reaction calcine them at the temperature of 400deg.C to 600deg.C for 40nin to 80min, cool it in natural condition and get the titanium dioxide nanometer tube electrode. The titanium dioxide nanometer tube electrode can be applied to the photocatalysed degradation and photoelectroncatalysed degradation to the organic pollutants. It has larger surface area and simple preparation method.
Owner:DALIAN UNIV OF TECH

Wastewater-degradation microwave photocatalytic device beneficial to inhibiting energy unnecessary dissipation

InactiveCN102826698ANo need to worry about temperature rise effectIncrease throughputMultistage water/sewage treatmentLiquid mediumUltraviolet
The invention relates to a wastewater-degradation microwave photocatalytic device beneficial to inhibiting energy unnecessary dissipation, belonging to the technical field of wastewater treatment. The invention aims to totally solve the problem of energy unnecessary dissipation since the wastewater body absorbs abundant microwave energy, and the problem of scaling on the outer side surface of the quartz tube for an electrodeless ultraviolet lamp shield in the existing microwave photocatalytic degradation technique of industrial wastewater containing organic pollutants. The electrodeless ultraviolet lamp is arranged in a metallic wire-cage-shaped transparent microwave restrictor, microwaves are introduced into the microwave restrictor, so that the microwave restrictor can inhibit the microwave from unnecessary dissipation. On the basis of the structure, the design volume of the reactor is allowed to be greatly expanded, thereby greatly enhancing the single-tank wastewater treatment capacity of the reactor; and an ultrasonic transducer is arranged on the inner side surface of the side wall of the microwave photocatalytic reactor, thereby instantly clearing the scales under the action of high-frequency ultrasonic by using the ultrasonic transmission of the liquid medium.
Owner:NINGBO UNIV

Method for preparing sulfur and nitrogen co-doped titanium dioxide with visible light catalytic activity

The invention provides a method for preparing sulfur and nitrogen co-doped titanium dioxide with visible light catalytic activity, which adopts a sol-gel method and comprises the following steps: hydrolyzing titanium ester and introducing sulfur and nitrogen sources to obtain a titanium dioxide sol, wherein the sulfur and nitrogen sources are from thiourea solution; in a sol system, dropwise adding 1 to 5 percent saturated aqueous solution of thiourea to perform the hydrolysis reaction to obtain the sol; then performing aging and volatilizing a diluent to obtain a titanium dioxide gel; drying the titanium dioxide gel and grinding into powders; performing heat treatment on the solid powder; and calcinating to obtain sulfur and nitrogen co-doped titanium dioxide nano powder. In the method, the thiourea is used as the raw materials of the nitrogen and sulfur sources, the sulfur and the nitrogen are simultaneously introduced in the process of the hydrolysis reaction of the sol to achieve synergistic effect and improve the reaction efficiency, raw material consumption is less, the process is simplified, the absorption range of visible light is effectively improved, the wavelength of the visible light is expanded to about 650nm, and the sulfur and nitrogen co-doped titanium dioxide has obvious visible light activity in the photocatalytic degradation reaction of organic pollutant molecules.
Owner:BEIJING UNIV OF CHEM TECH
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