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373results about How to "Improve surface topography" patented technology

Welding wire sending and pulverized solder sending laser cladding forming method and device

InactiveCN101733550AIncrease peripheral light intensityOvercoming the deficiency of undermeltingLiquid spraying apparatusWelding/cutting media/materialsLight beamLaser beams
The invention discloses a welding wire sending and pulverized solder sending laser cladding forming method. The method is characterized in that a conscope is used to change a solid laser beam transmitted by a laser to an annular light beam through light path transformation, then an annular focus lens is used to focus the annular light beam to an annular conical light beam, a hollow conical aphotic zone is formed in the annular conical light beam, a welding wire sending and pulverized solder sending protective gas composite nozzle is arranged in the aphotic zone and has the same axis of the annular conical light beam, a welding wire sending hole is arranged in the center, parallel pulverized solder sending holes are around the welding wire sending hole, collimating protective gas holes are parallel to and around the pulverized solder sending holes, wire is sent to a molten pool through the welding wire sending hole along the axial direction of the light beam and vertically to a machining face, airborne pulverized solder is sent to the molten pool through the pulverized solder sending holes at the same time, and collimating protective gas surrounds the welding wire and pulverized solder and is blown to the molten pool. The invention adopts the welding wire sending and pulverized solder sending protective gas composite nozzle to realize welding wire, pulverized solder and protective gas composite cladding and solve the defects of the prior art.
Owner:SUZHOU UNIV

Graphene/titanate nanometer composite visible-light activated photocatalyst and preparation method thereof

The invention discloses a graphene/titanate nanometer composite visible-light activated photocatalyst and a preparation method thereof, and belongs to the fields of nanometer composite materials and photocatalysis technology. The composite photocatalyst is prepared by compounding titanate and graphene, and the preparation method comprises the following steps: reacting tetrabutyl titanate with ammonia water to obtain a titanium hydroxyl compound; performing ultrasonic dispersion of graphene oxide in water, adding nitrate, stirring, mixing with the titanium hydroxyl compound and a potassium hydroxide aqueous solution, stirring, finally transferring the mixed solution into a reaction vessel to perform a hydrothermal reaction, after the reaction, performing centrifugation, filtration, washing, and vacuum drying of the product to obtain the composite photocatalyst. Photocatalytic degradation experiments show that the graphene/titanate composite photocatalyst prepared by the method has good photocatalytic degradation effect on rhodamine B under visible light irradiation. The photocatalyst of the invention has the advantages of relatively simple operation process, controllable morphology, no requirements for other reducing agents, and good visible-light activated photocatalysis performance.
Owner:JIANGSU UNIV

Perovskite solar cell and preparation method thereof

The invention discloses a perovskite solar cell and a preparation method thereof. The perovskite solar cell comprises a transparent conductive substrate, a hole transport layer, a decoration layer, a perovskite layer, an electron transport layer, a barrier layer and a metal electrode. The surfaces of PEDOT: PSS, NiOx and the hole transport layer are decorated by ionic liquid based on imidazole, atomic force microscope graphs before and after the decoration are compared, and the decorated surface appearance is more smooth, which is conducive to inhibiting the compounding of dark current. The perovskite layer is a new perovskite material 3MAI: PbAc2.xH2O (x is not smaller than 0 and is not greater than 3), and is prepared by quickly preheating a substrate and heating a perovskite precursor solution, namely instant heating assisted spray coating technology (HASP) at a low temperature (lower than 100 DEG C), which is conducive to increasing the grain size of perovskite and reducing the defects between perovskite grains so as to greatly improve the efficiency of the perovskite battery. The photoelectric conversion efficiency of the final battery device is greater than 19%, the flexible device efficiency is 10.8%, no hysteresis effect is formed, and thus the preparation method has a broad application prospect.
Owner:CENT SOUTH UNIV

Laser-based inside-laser coaxial wire-feeding additive manufacturing system and forming method

The invention discloses a laser-based inside-laser coaxial wire-feeding additive manufacturing system and a forming method. The laser-based inside-laser coaxial wire-feeding additive manufacturing system is formed by a laser, a wire feeder mechanism, a movement actuating mechanism, a molten pool shape monitoring feedback module and a system control module. After a part model is cut into slices, aninitial path is planned, input parameters and technological parameters in a technology database are compared, the molten pool temperature corresponding to technological parameters and input technology parameters under different feature structures is optimized, printing parameters and a robot code under an optimal path are generated, a high-speed infrared camera acquires molten pool shape parameters during the printing process and transmits to the system control module, the system control module compares the acquired molten pool shape data and the technology data of the technology database module, meanwhile, the molten pool temperature change is monitored, and the molten pool temperature is corrected through feedback-adjusting laser power and is monitored and feedback-adjusted in real time, so that the molten pool shape is uniform and consistent and the printing process is stably controlled during the printing process.
Owner:NAT INST CORP OF ADDITIVE MFG XIAN

Static magnetic field-laser coaxial composite fusion covering method and device

The invention relates to a static magnetic field-laser coaxial composite fusion covering method and a device and belongs to the technical field of laser processing. A static magnetic field is provided by an electromagnet, and the coaxial compositing of the magnetic field and a laser beam is realized through a device. When in magnetic field-laser coaxial fusion covering, the magnetic field generation device moves coaxially and synchronously with the laser beam, the coupling of the magnetic field and a laser-induced molten pool flow field can be completed, the laser fusion covering process is completed through a preset or coaxial powder delivery way, the flowing of the laser-induced molten pool can be inhibited, so that a purpose for controlling the solidification structure, improving the surface shape of the fuse covering layer, optimizing the distribution of the stress and reducing the splashing phenomenon in the fuse covering process can be realized. The coaxial synchronous motion of the magnetic field and the laser can be realized. The static magnetic field-laser coaxial composite fusion covering method and device have the characteristics of good capacity for controlling the fuse covering layer, wide application range, simplicity in structure, convenience in popularization and the like.
Owner:HANGZHOU BOHUA LASER TECH

Method for reinforcing laser cladding layer on surface of titanium alloy

The invention discloses a method for reinforcing a laser cladding layer on a surface of a titanium alloy, which comprises the following steps that base powder is evenly mixed with mixed powder of C, TiB2 and Cu with a certain quantity proportion to form a paste shape by utilizing sodium silicate solution; the base powder is a Ti-Al intermetallic compound or Fe and Al mixed powder, the size of thebase powder is 20-30mum, and the size of the mixed powder of C, TiB2 and Cu is 20-30mum; the paste-shaped mixed powder is evenly coated on the surface of the titanium alloy, the thickness of a coating is 0.3-2mm, and the coating is naturally aired; laser beams are utilized to perform laser cladding on the surface of a titanium alloy sample pre-provided with the coating, and during the vertical scanning process of the laser beams, argon is laterally and coaxially blown to protect a molten pool and a lens barrel; and the process parameters are that laser power is 650-1500W, scanning speed is 2-11mm / s, light spot diameter is 2-9mm, and argon protection air pressure is 0.2-0.9MPa. The method for reinforcing the laser cladding layer on the surface of the titanium alloy can obtain a titanium alloy surface reinforcing coating layer with good abrasion resistance and a surface shape, and is convenient and simple in process, strong in adaptability and convenient to popularize and apply.
Owner:SHANDONG UNIV

Process for intensifying ultrasonic vibration assisted electric spark pulse discharging surface

The invention discloses a process for intensifying an ultrasonic vibration assisted electric spark pulse discharging surface, comprising the following steps of: selecting 65Mn steel subjected to medium temperature tempering treatment after quenching, as a workpiece electrode and a monocrystal Si as a tool electrode; additionally arranging an ultrasonic vibration device on the tool electrode to assist the electric spark surface intensification; and with coal oil as a working solution, carrying out positive electrode electric spark surface intensification on the 65Mn steel by utilizing an electric spark processing machine tool, wherein the intensifying electricity parameters are that the pulse width is more than or equal to 4.2 mu s and less than 7.5mu s, the pulse width intrapulse ratio is between 0.21 and 0.56, a peak value current is more than or equal to 3.2A and less than 14.2A, the intensifying time is between 15min and 25min, the tool electrode-assisted ultrasonic vibration amplitude range is between 1mu m and 2mu m, and the frequency range is between 15 kHz and 60kHz. The invention improves the surface topography of an intensified layer so that the thickness distribution of the intensified layer is more uniform and more compact, increases the quantity of an intensifying phase and improves microhardness, abrasive resistance and surface Si content of the intensified layer.
Owner:SHANDONG UNIV

Production method of polysilicon rod

The invention discloses a production method of a polysilicon rod, comprising the following steps: when the surface temperature of a silicon core is 1100-1250 DEG C, leading in hydrogen to react with trichlorosilane for 30-45 hours; when the silicon core grows to have the diameter of 50mm, stopping current, and adding hydrogen flow rate to continuously react for 3-10 hours; when the surface temperature of the polysilicon rod is reduced to1000-1050 DEG C, applying the current, reducing the hydrogen flow rate, raising the surface temperature of the polysilicon rod to about 1080-1100 DEG C and keeping the surface temperature of the polysilicon rod for 30 hours; stopping the current, and increasing the hydrogen flow rate again to react for 2-6 hours; when the surface temperature of the polysilicon rod is reduced to 970-1020 DEG C, reducing the hydrogen flow rate again, applying the current, raising the surface temperature of the polysilicon rod to 1050-1080 DEG C, and then keeping the surface temperature of the polysilicon rod till a reduction reactor is stopped. The production method of the polysilicon rod can obviously improve the surface appearance of solar polysilicon in the production process, and the surface bump area of the polysilicon can be controlled within 8 percent.
Owner:JIANGSU ZHONGNENG POLYSILICON TECH DEV
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