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161results about How to "Improve deposition quality" patented technology

Solution composition and method for electroless deposition of coatings free of alkali metals

An electroless deposition solution of the invention for forming an alkali-metal-free coating on a substrate comprises a first-metal ion source for producing first-metal ions, a pH adjuster in the form of a hydroxide for adjusting the pH of the solution, a reducing agent, which reduces the first-metal ions into the first metal on the substrate, a complexing agent for keeping the first-metal ions in the solution, and a source of ions of a second element for generation of second-metal ions that improve the corrosion resistance of the aforementioned coating. The method of the invention consists of the following steps: preparing hydroxides of a metal such as Ni and Co by means of a complexing reaction, in which solutions of hydroxides of Ni and Co are obtained by displacing hydroxyl ions OH beyond the external boundary of ligands of mono- or polydental complexants; preparing a complex composition based on a tungsten oxide WO3 or a phosphorous tungstic acid, such as H3[P(W3O10)4], as well as on the use of tungsten compounds for improving anti-corrosive properties of the deposited films; mixing the aforementioned solutions of salts of Co, Ni, or W and maintaining under a temperatures within the range of 20° C. to 100° C.; and carrying out deposition from the obtained mixed solution.
Owner:LAM RES CORP

Laser-based inside-laser coaxial wire-feeding additive manufacturing system and forming method

The invention discloses a laser-based inside-laser coaxial wire-feeding additive manufacturing system and a forming method. The laser-based inside-laser coaxial wire-feeding additive manufacturing system is formed by a laser, a wire feeder mechanism, a movement actuating mechanism, a molten pool shape monitoring feedback module and a system control module. After a part model is cut into slices, aninitial path is planned, input parameters and technological parameters in a technology database are compared, the molten pool temperature corresponding to technological parameters and input technology parameters under different feature structures is optimized, printing parameters and a robot code under an optimal path are generated, a high-speed infrared camera acquires molten pool shape parameters during the printing process and transmits to the system control module, the system control module compares the acquired molten pool shape data and the technology data of the technology database module, meanwhile, the molten pool temperature change is monitored, and the molten pool temperature is corrected through feedback-adjusting laser power and is monitored and feedback-adjusted in real time, so that the molten pool shape is uniform and consistent and the printing process is stably controlled during the printing process.
Owner:NAT INST CORP OF ADDITIVE MFG XIAN

Magnetron sputtering device and magnetron sputtering method

ActiveCN105543792AReasonable device configurationVersatileVacuum evaporation coatingSputtering coatingPhysicsThin membrane
The invention discloses a magnetron sputtering device and a magnetron sputtering method. The magnetron sputtering device comprises a substrate table for placing a substrate, a target opposite to the substrate table and used for sputtering the substrate, and a reaction cavity for accommodating the substrate table and the target. The magnetron sputtering device further comprises an angle adjusting device corresponding to the target and used for adjusting an angle of the corresponding target to the substrate table. The magnetron sputtering method comprises the following steps: (1) the reaction cavity and the substrate are cleaned; and the target is mounted; (2) the angle of the target corresponding to the substrate and the distance between the target and the substrate are adjusted; (3) the reaction cavity is vacuumized; (4) the presputtering is performed; and meanwhile, the rotating and swinging functions of the substrate table are started; and (5) the magnetron sputtering is performed. The device can be applied to deposition of large-area films with high uniformity and excellent repeatability, and can realize continuous magnetron sputtering of multiple layers of films; and the method can save the film plating time and improve the film plating efficiency.
Owner:48TH RES INST OF CHINA ELECTRONICS TECH GROUP CORP

Preparation method of carbon nano tube

The invention relates to a preparation method of a carbon nano tube. A direct current plasma injection chemical vapour deposition system is adopted for preparing the carbon nano tube. The preparation method comprises the following steps: by taking a mixed solution of nickel nitrite and magnesium nitrite as a catalyst precursor, dropping the mixed solution on a substrate such as molybdenum, zirconium or the like; airing and then placing the substrates on a deposition platform in a cavity of direct current plasma injection chemical vapour deposition equipment; discharging a direct-current arc so that argon and hydrogen form high temperature plasma; decomposing and reducing the catalyst solution by the high temperature plasma, so as to generate a Ni/MgO catalyst; and after hydrocarbon gas isintroduced, cracking the hydrocarbon gas by using the high temperature plasma, and then injecting the cracked hydrocarbon gas on the substrate so that the carbon nano tube is formed in the presence of the catalyst. The preparation method provided by the invention has the advantages that: the catalyst is obtained while the carbon nano tube directly grows, preparation process is simple, deposition speed is fast, and deposition quality is good; and meanwhile, the bamboo-joint-like carbon nano tube is generated, and the prepared carbon nano tube has larger diameter, good crystallinity, no windingand good dispersibility.
Owner:TIANJIN UNIVERSITY OF TECHNOLOGY

Fin-type field effect transistor forming method

The invention discloses a fin-type field effect transistor forming method. The forming method comprises steps: a semiconductor substrate is provided, wherein the semiconductor substrate is provided with an NMOS region and a PMOS region, a first fin part is formed on the PMOS region, and a second fin part is formed on the NMOS region; a first dielectric layer is formed on the semiconductor substrate; a gate structure crossing the first fin part and the second fin part is formed on the surface of the first dielectric layer; a mobile chemical vapor deposition process is adopted to form a second dielectric layer on the first dielectric layer; a part of the second dielectric layer at the top part of the first fin part at two sides of the gate structure is removed to enable the top surface of the first fin part to be exposed; a first semiconductor layer is formed on the surface of the first fin part; an oxide layer is formed on the surface of the second semiconductor layer; a part of the second dielectric layer at the top part of the second fin part at two sides of the gate structure is removed to enable the top surface of the second fin part to be exposed; and a second semiconductor layer is formed on the surface of the second fin part.
Owner:SEMICON MFG INT (SHANGHAI) CORP

Machine tool for depositing optical fiber preform rods by outside chemical vapor deposition method

The invention relates to a machine tool for depositing optical fiber preform rods by an outside chemical vapor deposition method. The machine tool comprises a tool body; a reciprocating seat and blow lamps are respectively arranged on the tool body; rotary chucks are arranged on the reciprocating seat. The machine tool is characterized in that the blow lamps correspond to the rotary chucks, and are mounted below the axis of rotation; the blow lamps are connected with a feeding mechanism; the feeding direction of the feeding mechanism is perpendicular to the axis of rotation. The blow lamps can be subjected to dynamic regulation and control with the change of the deposition diameters of the optical fiber preform rods, so that the distances between the blow lamps and the deposition surfaces of the optical fiber preform rods are kept to be relatively constant, the blow lamps are always kept to be at optimal jet distance during the deposition process, so that not only can the uniformity of the jet dust granularity be maintained, but also the deposition precision and the deposition quality of the preform rods can be effectively improved, which effectively improves the deposition processing efficiency; the rotary chucks and the blow lamps are adopted, so that the processing efficiency of the optical fiber preform rods can be improved greatly.
Owner:YANGTZE OPTICAL FIBRE & CABLE CO LTD

Magnetic field for plating on inner wall of long pipe and field-enhanced arc ion plating device

The invention, belonging to the field of surface modification on materials, relates to a magnetic field for plating on inner wall of long pipe and a field-enhanced arc ion plating device, characterized in that: the magnetic field is used to restrain and control the plasma beam motion trail in the arc ion plating process, two sets of magnetic field generators are arranged in an arc ion plating deposition device, one set is arranged on the plasma transmission channel outside a vacuum chamber for using the magnetic field to focus the plasma beam and restrain the diameter of cross section and transmission efficiency when transmitting the plasma beam, and the other set is arranged on the outside of a tubular workpiece in the vacuum chamber for guiding the plasma beam to diffuse along with the central axial direction of the tubular workpiece; field enhancement is used in arc ion plating for using the magnetic field to realize accelerated directional flow of plasma, a pulsed electric field is arranged in the workpiece; the magnetic field and electric field are used to restrain and control the plasma beam, so as to realize the coating deposition of the plasma on the inner wall of the tube. The invention is suitable for depositing coatings on the inner wall of tubular workpiece which is used as the service surface.
Owner:INST OF METAL RESEARCH - CHINESE ACAD OF SCI

Cladding device for water-cooling wall of circulating fluidized bed boiler

The invention relates to a cladding device for a water-cooling wall of a circulating fluidized bed boiler, aiming at solving the problems that the existing circulating fluidized bed boiler produces a great deal of material during combustion, and the heating surface of a hearth is scoured by the material, so that the water-cooling wall of the boiler is seriously corroded, and the safe running of the boiler is influenced; and when being used for cladding the water-cooling wall of the circulating fluidized bed boiler, the traditional cladding technology has the problem that the cladding efficiency is low, the quality of the clad surface is poor, the labor intensity of workers is high, the work environment is poor and radiation to the human body is high. A melting gun swing device is arranged at one side of the upper end of a connecting plate, and a driving motor is arranged at the other side of the connecting plate; the driving motor is connected with the melting gun swing device in a transmission way; the front end of the melting gun swing device is provided with a melting gun; and the driving motor is connected with a computer by a control circuit. The cladding device is used for cladding the water-cooling wall of the circulating fluidized bed boiler.
Owner:HARBIN KENENG CLADDING TECH

Paraxial powder-feeding working head for laser powder processing

The invention relates to a paraxial powder-feeding working head for laser powder processing. The paraxial powder-feeding working head comprises a powder-gas separator, a powder-gas input chamber, a fast-plug connector, a powder collecting chamber, a first powder conveying tube, a processing gas input chamber, a processing gas collecting piece, a processing gas input joint, a fixed frame, a second powder conveying tube, a third powder conveying tube and a powder spray nozzle, wherein the processing gas collecting piece is a gradual-contraction funnel shaped component; a throttle valve is used for outputting a powder-carrying gas input by a powder feeder; a stainless steel wire net is arranged at the front end of the throttle valve. According to the paraxial powder-feeding working head disclosed by the invention, separation of metal powder and conveyed powder-carrying gas is realized, so that on one hand, outflow rate of the metal powder from the spray nozzle is lowered to ensure stability of powder conveying amount, and therefore, stable powder output amount requirements in laser powder processing processes of laser cladding, and the like are satisfied; on the other hand, a gas different from the powder-carrying gas is input from the processing gas input joint to achieve a purpose of protecting a processing piece; meanwhile, powder spraying speed of the powder feeding spray nozzle can be adjusted in an assisted manner, so that processing effect is controlled better.
Owner:INST OF SEMICONDUCTORS - CHINESE ACAD OF SCI

HFCVD batch preparation method of complex-shaped diamond-coated cutter

The invention discloses an HFCVD batch preparation method of a complex-shaped diamond film coated cutter. A handle of the complex-shaped cutter after being pretreated is inserted into a cutter coolingbase to be placed on the water-cooled workbench of HFCVD equipment. The cutter cooling base is formed by optimally matching a molybdenum sheet layer, a graphitic layer, a red copper layer or a stainless steel layer, and a drill hole matched with the handle in diameter and length is formed in the cutter cooling base. The HFCVD equipment adopts a single-layer hot filament. In the cutter mounting and film growing processes, the HFCVD equipment can realize free lifting of the cutter cooling base by controlling the lifting of the water-cooled workbench. Hydrogen, a carbon source and a doped sourceenter into the surface of the complex-shaped cutter to deposit a single-layer or composite diamond film. The HFCVD batch preparation method can conveniently and effectively control the temperature value of the blade area of the cutter, ensures the uniform distribution of a temperature field and a density field of a reactive group, ensures the uniform deposition of the diamond film, and avoids ofdepositing carbon impurities on the handle position to cause the phenomenon of a black bar.
Owner:SHANGHAI JIAO TONG UNIV

Supercritical-fluid-based 3D electrodeposition machining device and method

The invention provides a supercritical-fluid-based 3D electrodeposition machining device and method. The device comprises a carbon dioxide gas bottle, a high-pressure pump, a digital controller, a reactor, a moving anode assembly, a moving cathode assembly, a direct-current power supply and a cathode matrix serving as a machined part, wherein the reactor is internally provided with a mechanical stirrer; the moving anode assembly comprises a Z-directional linear motor, a driving lead screw, an anode connecting rod and a moving anode; the moving cathode assembly comprises an X-directional linear motor, a Y-directional linear motor, a guide rail, a moving block and a fixture; and when the supercritical-fluid-based 3D electrodeposition machining device is used, the moving anode and the cathode matrix are respectively and electrically connected with the anode and cathode of the direct-current power supply. The machining method mainly comprises the steps of carrying out chemical plating treatment on the cathode matrix in advance; mounting the cathode matrix; preparing a supercritical fluid; carrying out electrodeposition machining and after-treatment and the like. By using the supercritical-fluid-based 3D electrodeposition machining device and method, the electrodeposition speed can be effectively increased, the deposition quality can be improved, a complex and precise metal part can be prepared through electrodeposition in a three-dimensional space, and the application field of an electrodeposition technology is widened.
Owner:JIANGSU UNIV OF TECH

Method for forming semiconductor structure

The invention provides a method for forming a semiconductor structure. The method comprises the steps of providing a semiconductor substrate comprising a first region and a second region, forming a first grid dielectric layer on the first region and a first grid on the surface of the first grid dielectric layer, forming a second grid dielectric layer on the second region and a second grid on the surface of the second grid dielectric layer, forming a first dielectric layer that covers the semiconductor substrate, the first grid dielectric layer, the first grid, the second grid dielectric layer and the second grid, forming a protective layer on the surface of the first dielectric layer, forming a mask layer on the second region, removing the protective layer on the first region with the mask layer as a mask, removing the first dielectric layer on the first region after the removal of the mask layer, forming a second dielectric layer on the first region and the second region after the removal of the first dielectric layer from the first region, and etching the second dielectric layer till reaching the surface of the semiconductor substrate so as to form a first side wall and a second side wall. Based on the above method, side walls of different thicknesses are formed on different transistors, so that the performances of the transistors are adjusted.
Owner:SEMICON MFG INT (SHANGHAI) CORP
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